CN111517882A - Camellia oil meal multi-effect nutrient liquid fertilizer and preparation method thereof - Google Patents
Camellia oil meal multi-effect nutrient liquid fertilizer and preparation method thereof Download PDFInfo
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- CN111517882A CN111517882A CN202010582147.1A CN202010582147A CN111517882A CN 111517882 A CN111517882 A CN 111517882A CN 202010582147 A CN202010582147 A CN 202010582147A CN 111517882 A CN111517882 A CN 111517882A
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- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05G—MIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
- C05G3/00—Mixtures of one or more fertilisers with additives not having a specially fertilising activity
- C05G3/60—Biocides or preservatives, e.g. disinfectants, pesticides or herbicides; Pest repellants or attractants
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- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05B—PHOSPHATIC FERTILISERS
- C05B7/00—Fertilisers based essentially on alkali or ammonium orthophosphates
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- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05G—MIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
- C05G5/00—Fertilisers characterised by their form
- C05G5/20—Liquid fertilisers
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Abstract
The invention discloses a camellia oil meal multi-effect nutrient liquid fertilizer and a preparation method thereof, wherein the camellia oil meal multi-effect nutrient liquid fertilizer comprises concentrated solution extracted from camellia oil meal, chinaberry fruit, rhizoma polygonati, radix stemonae, fructus xanthil and saponin; the weight ratio of each component is as follows according to the parts by weight: 100-500 parts of camellia oil meal, 20-100 parts of chinaberry fruit, 20-100 parts of rhizoma polygonati, 30-150 parts of radix stemonae, 30-150 parts of cocklebur fruit and 40-200 parts of gleditsia sinensis lam extract concentrated solution. Potassium phosphate and medium trace elements are also included. The camellia oil meal multi-effect nutrient solution fertilizer disclosed by the invention contains amino acid components which can provide rich nutrition required by crops, can promote the crops to grow quickly, accumulate nutrition and promote blossoming and fruiting, and the tea saponin components have antibacterial and insecticidal effects, have good stomach toxicity and contact poisoning effects on pests, and can be widely applied to economic forests, agricultural planting and flowers for preventing and treating snails, field snails, rice planthoppers, weevils, aphids, red spiders, leaf mites, rust diseases, blight and anthracnose; the pollution of chemical pesticide to environment is reduced.
Description
Technical Field
The invention relates to a nutrient liquid fertilizer, in particular to a camellia oil meal multi-effect nutrient liquid fertilizer and a preparation method thereof.
Background
Camellia oil meal, also called tea seed cake, is solid residue left after oil extraction from the fruit of the camellia plant, the tea meal contains a large amount of available components such as tea saponin, polysaccharide, protein and the like, and the comprehensive value of the tea meal cannot be fully embodied by utilizing the fertilizer prepared from the tea meal, so that other products can be developed by utilizing the effects of the components in the tea meal, and good economic benefit can be obtained. The camellia oleifera seed cake mainly comprises the following components: more than or equal to 1.1 percent of total nitrogen, more than or equal to 0.28 percent of total phosphorus, more than or equal to 1.18 percent of potassium, more than or equal to 80 percent of organic matters, 12 to 18 percent of tea saponin, 12 to 16 percent of protein, 30 to 50 percent of starch and saccharide, 10 to 12 percent of fiber and 18 amino acids. The tea saponin is a good surfactant and foaming agent, has strong decontamination capability, and can be widely used in the industries of chemical industry, food, medicine and the like to produce biological pesticides, fertilizers, shampoo, detergents, food additives, foaming agents in purifiers and fire extinguishers, and the like. The total content of protein and saccharide in the tea seed cake is 40-50%, and the tea seed cake can be used for plant protein energy feed. The amino acid and the oil tea cake contain eighteen amino acids, wherein the content of the amino acid necessary for animals is higher, and the oil tea cake can be used for producing energy feed and amino acid fertilizers. The nitrogen, phosphorus and potassium and organic matters in the tea seed cake are high in nutrient, the nitrogen, phosphorus and potassium and rich in organic matters, and the tea seed cake can be used as an organic fertilizer. The derived products and high value-added end products developed from the tea oil to the oil meal cover products such as foods, biological pesticides, multi-effect water soluble fertilizers, multi-effect functional organic fertilizers, beauty and skin care, washing and care, tea drinks, energy feeds, health care and the like.
At present, a great amount of chemical pesticides are used, so that severe pollution to food is caused, meanwhile, the environment is damaged, ecological balance is influenced, pesticide residues of agricultural products are increased, and the physical health of people is further harmed.
Disclosure of Invention
To the deficiency of the prior art, the technical problem to be solved by the present patent application is: how to provide a camellia oil meal multi-effect nutrient liquid fertilizer which has the effects of resisting bacteria and killing insects, reduces the use of chemical pesticides and the pollution to the environment and a preparation method thereof.
In order to achieve the purpose, the invention adopts the following technical scheme:
a multi-effect nutritional liquid fertilizer containing camellia oil cake comprises concentrated extractive solution of camellia oil cake, fructus Toosendan, rhizoma Polygonati, radix Stemonae, fructus Xanthii, and fructus Gleditsiae Abnormalis; the weight ratio of each component is as follows according to the parts by weight:
further, potassium phosphate and medium trace elements are also included.
Further, the medium trace elements are boron, iron, calcium and magnesium.
A preparation method of a camellia oil meal multi-effect nutrient liquid fertilizer comprises the following steps:
s1: preparing camellia oil meal, chinaberry fruit, rhizoma polygonati, radix stemonae, siberian cocklebur fruit, saponin, potassium phosphate, boron, iron, calcium and magnesium;
s2: pulverizing folium Camelliae sinensis oil cake, fructus Toosendan, rhizoma Polygonati, radix Stemonae, and fructus Xanthii, soaking and grinding fructus Gleditsiae Abnormalis to obtain viscous liquid, and concentrating to obtain concentrated solution of fructus Gleditsiae Abnormalis extract; wherein, the camellia oil meal is 100 to 500 parts, the chinaberry fruit is 20 to 100 parts, the sealwort is 20 to 100 parts, the stemona root is 30 to 150 parts, the cocklebur fruit is 30 to 150 parts, and the gleditsia sinensis lam extract is 40 to 200 parts;
s3: mixing the pulverized camellia oil meal, chinaberry fruit, rhizoma polygonati, radix stemonae, fructus xanthil and the extracted concentrated solution of the Chinese honeylocust fruit, mixing with distilled water according to the proportion of 2:5, initially heating and stirring, then initially soaking and filtering to obtain initial filtrate and filter residue;
s4: mixing the filter residue with distilled water according to the proportion of 4:5, heating and stirring again, soaking again, and filtering to obtain secondary filtrate;
s5: mixing the initial filtrate and the secondary filtrate to obtain a crude filtrate, adding ethanol into the crude filtrate, stirring uniformly, standing, and filtering to obtain a fine filtrate;
s6: concentrating the fine filtrate in vacuum to one third of the volume of the fine filtrate to obtain a concentrated solution;
s7: adding potassium phosphate, boron, iron, calcium and magnesium into the concentrated solution; obtaining the nutrient liquid fertilizer.
Further, in step S3, the temperature during the initial heating is 60 to 90 ℃, the heating time is 1.5 to 2 hours, and the initial soaking time is 20 to 40 minutes.
Further, in step S4, the temperature is heated again to 60-90 ℃, the heating time is 1.5-2 hours, and the initial soaking time is 20-40 minutes.
Further, in step S5, the ethanol is 95% ethanol; the ratio of the crude filtrate to the ethanol is 1: 0.5; the standing time is 2-3 hours.
Further, in step S6, the concentration temperature is 50-60 ℃.
Further, potassium phosphate, boron, iron, calcium and magnesium respectively account for 5%, 1%, 2%, 0.5% and 1% of the concentrated solution.
In conclusion, the camellia oil meal multi-effect nutrient liquid fertilizer disclosed by the invention contains amino acid components which can provide rich nutrition required by crops, promote the crops to grow quickly, accumulate nutrition and promote blossoming and fruiting, and the tea saponin components have antibacterial and insecticidal effects, have good stomach toxicity and contact killing effects on pests, and can be widely applied to economic forests, agricultural planting and flowers for preventing and treating snails, field snails, rice planthoppers, weevils, aphids, red spiders, leaf mites, rust diseases, blight and anthracnose; the pollution of chemical pesticide to environment is reduced. The preparation method disclosed by the invention is simple and easy to realize, and can better improve the production efficiency.
Detailed Description
In order to make the objects, technical solutions and advantages of the embodiments of the present invention clearer, the following will clearly and completely describe the technical solutions in the embodiments of the present invention, and it is obvious that the described embodiments are some embodiments of the present invention, but not all embodiments. All other embodiments, which can be derived by a person skilled in the art from the embodiments of the present invention without inventive step, are within the scope of the present invention.
The first embodiment is as follows:
a multi-effect nutritional liquid fertilizer containing camellia oil cake comprises concentrated extractive solution of camellia oil cake, fructus Toosendan, rhizoma Polygonati, radix Stemonae, fructus Xanthii, and fructus Gleditsiae Abnormalis; the weight ratio of each component is as follows according to the parts by weight: 100 parts of camellia oil meal, 20 parts of chinaberry fruit, 20 parts of rhizoma polygonati, 30 parts of radix stemonae, 30 parts of cocklebur fruit, 40 parts of saponin extraction concentrated solution, and potassium phosphate, boron, iron, calcium and magnesium.
A preparation method of a camellia oil meal multi-effect nutrient liquid fertilizer comprises the following steps:
s1: preparing camellia oil meal, chinaberry fruit, rhizoma polygonati, radix stemonae, siberian cocklebur fruit, saponin, potassium phosphate, boron, iron, calcium and magnesium;
s2: pulverizing folium Camelliae sinensis oil cake, fructus Toosendan, rhizoma Polygonati, radix Stemonae, and fructus Xanthii, soaking and grinding fructus Gleditsiae Abnormalis to obtain viscous liquid, and concentrating to obtain concentrated solution of fructus Gleditsiae Abnormalis extract; wherein, camellia oil meal 100 parts, chinaberry fruit 20 parts, Siberian solomonseal rhizome 20 parts, stemona root 30 parts, siberian cocklebur fruit 30 parts and gleditsia sinensis lam extract concentrated solution 40 parts;
s3: mixing the pulverized camellia oil meal, chinaberry fruit, rhizoma polygonati, radix stemonae, fructus xanthil and the extracted concentrated solution of the Chinese honeylocust fruit, mixing with distilled water according to the proportion of 2:5, initially heating and stirring, then initially soaking and filtering to obtain initial filtrate and filter residue; the temperature during the initial heating is 60 ℃, the heating time is 1.5 hours, and the initial soaking time is 20 minutes;
s4: mixing the filter residue with distilled water according to the proportion of 4:5, heating and stirring again, soaking again, and filtering to obtain secondary filtrate; the reheating temperature is 60 ℃, the heating time is 1.5 hours, and the initial soaking time is 20 minutes;
s5: mixing the initial filtrate and the secondary filtrate to obtain a crude filtrate, adding ethanol into the crude filtrate, stirring uniformly, standing, and filtering to obtain a fine filtrate; the ethanol is 95% ethanol; the ratio of the crude filtrate to the ethanol is 1: 0.5; the standing time is 2 hours;
s6: concentrating the fine filtrate in vacuum to one third of the volume of the fine filtrate to obtain a concentrated solution; the concentration temperature is 50 ℃;
s7: adding potassium phosphate, boron, iron, calcium and magnesium into the concentrated solution; the potassium phosphate, the boron, the iron, the calcium and the magnesium respectively account for 5%, 1%, 2%, 0.5% and 1% of the concentrated solution; obtaining the nutrient liquid fertilizer.
Example two:
a multi-effect nutritional liquid fertilizer containing camellia oil cake comprises concentrated extractive solution of camellia oil cake, fructus Toosendan, rhizoma Polygonati, radix Stemonae, fructus Xanthii, and fructus Gleditsiae Abnormalis; the weight ratio of each component is as follows according to the parts by weight: 300 parts of camellia oil meal, 60 parts of chinaberry fruit, 60 parts of rhizoma polygonati, 80 parts of radix stemonae, 80 parts of cocklebur fruit, 140 parts of gleditsia sinensis lam extract concentrated solution, and potassium phosphate, boron, iron, calcium and magnesium.
A preparation method of a camellia oil meal multi-effect nutrient liquid fertilizer comprises the following steps:
s1: preparing camellia oil meal, chinaberry fruit, rhizoma polygonati, radix stemonae, siberian cocklebur fruit, saponin, potassium phosphate, boron, iron, calcium and magnesium;
s2: pulverizing folium Camelliae sinensis oil cake, fructus Toosendan, rhizoma Polygonati, radix Stemonae, and fructus Xanthii, soaking and grinding fructus Gleditsiae Abnormalis to obtain viscous liquid, and concentrating to obtain concentrated solution of fructus Gleditsiae Abnormalis extract; wherein, 300 parts of camellia oil meal, 60 parts of chinaberry fruit, 60 parts of rhizoma polygonati, 80 parts of radix stemonae, 80 parts of cocklebur fruit and 140 parts of gleditsia sinensis lam extract concentrated solution;
s3: mixing the pulverized camellia oil meal, chinaberry fruit, rhizoma polygonati, radix stemonae, fructus xanthil and the extracted concentrated solution of the Chinese honeylocust fruit, mixing with distilled water according to the proportion of 2:5, initially heating and stirring, then initially soaking and filtering to obtain initial filtrate and filter residue; the temperature during the initial heating is 70 ℃, the heating time is 1.8 hours, and the initial soaking time is 30 minutes;
s4: mixing the filter residue with distilled water according to the proportion of 4:5, heating and stirring again, soaking again, and filtering to obtain secondary filtrate; the reheating temperature is 70 ℃, the heating time is 1.8 hours, and the initial soaking time is 30 minutes;
s5: mixing the initial filtrate and the secondary filtrate to obtain a crude filtrate, adding ethanol into the crude filtrate, stirring uniformly, standing, and filtering to obtain a fine filtrate; the ethanol is 95% ethanol; the ratio of the crude filtrate to the ethanol is 1: 0.5; the standing time is 2.5 hours;
s6: concentrating the fine filtrate in vacuum to one third of the volume of the fine filtrate to obtain a concentrated solution; the concentration temperature is 55 ℃;
s7: adding potassium phosphate, boron, iron, calcium and magnesium into the concentrated solution; the potassium phosphate, the boron, the iron, the calcium and the magnesium respectively account for 5%, 1%, 2%, 0.5% and 1% of the concentrated solution; obtaining the nutrient liquid fertilizer.
Example three:
a multi-effect nutritional liquid fertilizer containing camellia oil cake comprises concentrated extractive solution of camellia oil cake, fructus Toosendan, rhizoma Polygonati, radix Stemonae, fructus Xanthii, and fructus Gleditsiae Abnormalis; the weight ratio of each component is as follows according to the parts by weight: 500 parts of camellia oil meal, 100 parts of chinaberry fruit, 100 parts of rhizoma polygonati, 150 parts of radix stemonae, 150 parts of cocklebur fruit, 200 parts of gleditsia sinensis lam extract concentrated solution, and potassium phosphate, boron, iron, calcium and magnesium.
A preparation method of a camellia oil meal multi-effect nutrient liquid fertilizer comprises the following steps:
s1: preparing camellia oil meal, chinaberry fruit, rhizoma polygonati, radix stemonae, siberian cocklebur fruit, saponin, potassium phosphate, boron, iron, calcium and magnesium;
s2: pulverizing folium Camelliae sinensis oil cake, fructus Toosendan, rhizoma Polygonati, radix Stemonae, and fructus Xanthii, soaking and grinding fructus Gleditsiae Abnormalis to obtain viscous liquid, and concentrating to obtain concentrated solution of fructus Gleditsiae Abnormalis extract; wherein, the camellia oil meal is 500 parts, the chinaberry fruit is 100 parts, the sealwort is 100 parts, the sessile stemona root is 150 parts, the cocklebur fruit is 150 parts, and the gleditsia sinensis lam extract concentrated solution is 200 parts;
s3: mixing the pulverized camellia oil meal, chinaberry fruit, rhizoma polygonati, radix stemonae, fructus xanthil and the extracted concentrated solution of the Chinese honeylocust fruit, mixing with distilled water according to the proportion of 2:5, initially heating and stirring, then initially soaking and filtering to obtain initial filtrate and filter residue; the temperature during the initial heating is 90 ℃, the heating time is 1.5-2 hours, and the initial soaking time is 40 minutes;
s4: mixing the filter residue with distilled water according to the proportion of 4:5, heating and stirring again, soaking again, and filtering to obtain secondary filtrate; the reheating temperature is 90 ℃, the heating time is 2 hours, and the initial soaking time is 40 minutes;
s5: mixing the initial filtrate and the secondary filtrate to obtain a crude filtrate, adding ethanol into the crude filtrate, stirring uniformly, standing, and filtering to obtain a fine filtrate; the ethanol is 95% ethanol; the ratio of the crude filtrate to the ethanol is 1: 0.5; the standing time is 3 hours;
s6: concentrating the fine filtrate in vacuum to one third of the volume of the fine filtrate to obtain a concentrated solution; the concentration temperature is 60 ℃;
s7: adding potassium phosphate, boron, iron, calcium and magnesium into the concentrated solution; the potassium phosphate, the boron, the iron, the calcium and the magnesium respectively account for 5%, 1%, 2%, 0.5% and 1% of the concentrated solution; obtaining the nutrient liquid fertilizer.
Example four:
the camellia oil meal multi-effect nutrient solution fertilizer disclosed by the patent application is compared with the existing common water-soluble fertilizer in effect, and is as follows in table 1:
table 1 shows that, for pepper trees, the camellia oil meal multi-effect nutrient solution fertilizer and the common water-soluble fertilizer disclosed in the present application are applied respectively, and after 15 days, the leaves using the camellia oil meal nutrient solution fertilizer disclosed in the present application have dark green and glossy color, thick leaves, strong flexibility, and common water-soluble fertilizer has light green leaves and more yellow leaves.
In addition, the camellia oil meal multi-effect nutrient liquid fertilizer disclosed by the invention also has the antibacterial and insecticidal effects. In the aspect of disease and insect pest resistance, the camellia oil meal multi-effect nutrient solution fertilizer disclosed by the invention has the advantages that plant leaf spots and yellow leaves are obviously few, the plant diseases and insect pests are few, the overall disease resistance is improved, and the common water-soluble fertilizer cannot prevent and control the plant diseases and insect pests.
The camellia oil meal multi-effect nutrient solution fertilizer disclosed by the invention contains amino acid components which can provide rich nutrition required by crops, can promote the crops to grow quickly, accumulate nutrition and promote blossoming and fruiting, and the tea saponin components have antibacterial and insecticidal effects, have good stomach toxicity and contact poisoning effects on pests, and can be widely applied to economic forests, agricultural planting and flowers for preventing and treating snails, field snails, rice planthoppers, weevils, aphids, red spiders, leaf mites, rust diseases, blight and anthracnose; the pollution of chemical pesticide to environment is reduced. The preparation method disclosed by the invention is simple and easy to realize, and can better improve the production efficiency.
The above description is only for the preferred embodiment of the present invention, but the scope of the present invention is not limited thereto, and any person skilled in the art should be considered to be within the technical scope of the present invention, and the technical solutions and the inventive concepts thereof according to the present invention should be equivalent or changed within the scope of the present invention.
Claims (9)
1. A camellia oil meal multi-effect nutrient liquid fertilizer is characterized by comprising concentrated solution extracted from camellia oil meal, chinaberry fruit, rhizoma polygonati, radix stemonae, fructus xanthil and saponin; the weight ratio of each component is as follows according to the parts by weight:
2. the camellia oil meal multi-effect nutrient solution fertilizer as claimed in claim 1, further comprising potassium phosphate and medium trace elements.
3. The camellia oil meal multi-effect nutrient solution fertilizer as claimed in claim 1, wherein the medium trace elements are boron, iron, calcium and magnesium.
4. A preparation method of a camellia oil meal multi-effect nutrient liquid fertilizer is characterized by comprising the following steps:
s1: preparing camellia oil meal, chinaberry fruit, rhizoma polygonati, radix stemonae, siberian cocklebur fruit, saponin, potassium phosphate, boron, iron, calcium and magnesium;
s2: pulverizing folium Camelliae sinensis oil cake, fructus Toosendan, rhizoma Polygonati, radix Stemonae, and fructus Xanthii, soaking and grinding fructus Gleditsiae Abnormalis to obtain viscous liquid, and concentrating to obtain concentrated solution of fructus Gleditsiae Abnormalis extract; wherein, the camellia oil meal is 100 to 500 parts, the chinaberry fruit is 20 to 100 parts, the sealwort is 20 to 100 parts, the stemona root is 30 to 150 parts, the cocklebur fruit is 30 to 150 parts, and the gleditsia sinensis lam extract is 40 to 200 parts;
s3: mixing the pulverized camellia oil meal, chinaberry fruit, rhizoma polygonati, radix stemonae, fructus xanthil and the extracted concentrated solution of the Chinese honeylocust fruit, mixing with distilled water according to the proportion of 2:5, initially heating and stirring, then initially soaking and filtering to obtain initial filtrate and filter residue;
s4: mixing the filter residue with distilled water according to the proportion of 4:5, heating and stirring again, soaking again, and filtering to obtain secondary filtrate;
s5: mixing the initial filtrate and the secondary filtrate to obtain a crude filtrate, adding ethanol into the crude filtrate, stirring uniformly, standing, and filtering to obtain a fine filtrate;
s6: concentrating the fine filtrate in vacuum to one third of the volume of the fine filtrate to obtain a concentrated solution;
s7: adding potassium phosphate, boron, iron, calcium and magnesium into the concentrated solution; obtaining the nutrient liquid fertilizer.
5. The method for preparing the camellia oil meal multi-effect nutrient liquid fertilizer as claimed in claim 4, wherein in step S3, the temperature during initial heating is 60-90 ℃, the heating time is 1.5-2 hours, and the initial soaking time is 20-40 minutes.
6. The method for preparing the camellia oil meal multi-effect nutrient liquid fertilizer as claimed in claim 5, wherein in step S4, the reheating temperature is 60-90 ℃, the heating time is 1.5-2 hours, and the initial soaking time is 20-40 minutes.
7. The method for preparing the camellia oil meal multi-effect nutrient liquid fertilizer as claimed in claim 5, wherein in step S5, the ethanol is 95% ethanol; the ratio of the crude filtrate to the ethanol is 1: 0.5; the standing time is 2-3 hours.
8. The method for preparing the camellia oil meal multi-effect nutrient liquid fertilizer as claimed in claim 5, wherein in the step S6, the concentration temperature is 50-60 ℃.
9. The method for preparing the camellia oil meal multi-effect nutrient solution fertilizer as claimed in claim 5, wherein the potassium phosphate, boron, iron, calcium and magnesium respectively account for 5%, 1%, 2%, 0.5% and 1% of the concentrated solution.
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