CN111499197B - Multi-color cup for all-living things and preparation method thereof - Google Patents
Multi-color cup for all-living things and preparation method thereof Download PDFInfo
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- CN111499197B CN111499197B CN202010353518.9A CN202010353518A CN111499197B CN 111499197 B CN111499197 B CN 111499197B CN 202010353518 A CN202010353518 A CN 202010353518A CN 111499197 B CN111499197 B CN 111499197B
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- 238000002360 preparation method Methods 0.000 title claims description 7
- 238000010304 firing Methods 0.000 claims abstract description 34
- 239000002994 raw material Substances 0.000 claims abstract description 34
- 239000000919 ceramic Substances 0.000 claims abstract description 26
- 238000004321 preservation Methods 0.000 claims abstract description 12
- 238000000034 method Methods 0.000 claims abstract description 6
- 238000002156 mixing Methods 0.000 claims description 14
- 235000015895 biscuits Nutrition 0.000 claims description 13
- 239000002344 surface layer Substances 0.000 claims description 13
- 239000005995 Aluminium silicate Substances 0.000 claims description 12
- VTYYLEPIZMXCLO-UHFFFAOYSA-L Calcium carbonate Chemical compound [Ca+2].[O-]C([O-])=O VTYYLEPIZMXCLO-UHFFFAOYSA-L 0.000 claims description 12
- 235000012211 aluminium silicate Nutrition 0.000 claims description 12
- 238000000498 ball milling Methods 0.000 claims description 12
- 239000004927 clay Substances 0.000 claims description 12
- 238000001816 cooling Methods 0.000 claims description 12
- UQSXHKLRYXJYBZ-UHFFFAOYSA-N iron oxide Inorganic materials [Fe]=O UQSXHKLRYXJYBZ-UHFFFAOYSA-N 0.000 claims description 12
- NLYAJNPCOHFWQQ-UHFFFAOYSA-N kaolin Chemical compound O.O.O=[Al]O[Si](=O)O[Si](=O)O[Al]=O NLYAJNPCOHFWQQ-UHFFFAOYSA-N 0.000 claims description 12
- NDLPOXTZKUMGOV-UHFFFAOYSA-N oxo(oxoferriooxy)iron hydrate Chemical compound O.O=[Fe]O[Fe]=O NDLPOXTZKUMGOV-UHFFFAOYSA-N 0.000 claims description 12
- 239000010453 quartz Substances 0.000 claims description 12
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N silicon dioxide Inorganic materials O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims description 12
- DLYUQMMRRRQYAE-UHFFFAOYSA-N tetraphosphorus decaoxide Chemical compound O1P(O2)(=O)OP3(=O)OP1(=O)OP2(=O)O3 DLYUQMMRRRQYAE-UHFFFAOYSA-N 0.000 claims description 12
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 9
- 239000002002 slurry Substances 0.000 claims description 8
- PCHJSUWPFVWCPO-UHFFFAOYSA-N gold Chemical compound [Au] PCHJSUWPFVWCPO-UHFFFAOYSA-N 0.000 claims description 7
- 229910052737 gold Inorganic materials 0.000 claims description 7
- 239000010931 gold Substances 0.000 claims description 7
- QGZKDVFQNNGYKY-UHFFFAOYSA-O Ammonium Chemical compound [NH4+] QGZKDVFQNNGYKY-UHFFFAOYSA-O 0.000 claims description 6
- 235000019738 Limestone Nutrition 0.000 claims description 6
- DPXJVFZANSGRMM-UHFFFAOYSA-N acetic acid;2,3,4,5,6-pentahydroxyhexanal;sodium Chemical compound [Na].CC(O)=O.OCC(O)C(O)C(O)C(O)C=O DPXJVFZANSGRMM-UHFFFAOYSA-N 0.000 claims description 6
- DLHONNLASJQAHX-UHFFFAOYSA-N aluminum;potassium;oxygen(2-);silicon(4+) Chemical compound [O-2].[O-2].[O-2].[O-2].[O-2].[O-2].[O-2].[O-2].[Al+3].[Si+4].[Si+4].[Si+4].[K+] DLHONNLASJQAHX-UHFFFAOYSA-N 0.000 claims description 6
- 239000000440 bentonite Substances 0.000 claims description 6
- 229910000278 bentonite Inorganic materials 0.000 claims description 6
- SVPXDRXYRYOSEX-UHFFFAOYSA-N bentoquatam Chemical compound O.O=[Si]=O.O=[Al]O[Al]=O SVPXDRXYRYOSEX-UHFFFAOYSA-N 0.000 claims description 6
- 229910000019 calcium carbonate Inorganic materials 0.000 claims description 6
- 239000001768 carboxy methyl cellulose Substances 0.000 claims description 6
- 229940116318 copper carbonate Drugs 0.000 claims description 6
- GEZOTWYUIKXWOA-UHFFFAOYSA-L copper;carbonate Chemical compound [Cu+2].[O-]C([O-])=O GEZOTWYUIKXWOA-UHFFFAOYSA-L 0.000 claims description 6
- FPAFDBFIGPHWGO-UHFFFAOYSA-N dioxosilane;oxomagnesium;hydrate Chemical compound O.[Mg]=O.[Mg]=O.[Mg]=O.O=[Si]=O.O=[Si]=O.O=[Si]=O.O=[Si]=O FPAFDBFIGPHWGO-UHFFFAOYSA-N 0.000 claims description 6
- 239000010433 feldspar Substances 0.000 claims description 6
- 229910052900 illite Inorganic materials 0.000 claims description 6
- 239000006028 limestone Substances 0.000 claims description 6
- VGIBGUSAECPPNB-UHFFFAOYSA-L nonaaluminum;magnesium;tripotassium;1,3-dioxido-2,4,5-trioxa-1,3-disilabicyclo[1.1.1]pentane;iron(2+);oxygen(2-);fluoride;hydroxide Chemical compound [OH-].[O-2].[O-2].[O-2].[O-2].[O-2].[F-].[Mg+2].[Al+3].[Al+3].[Al+3].[Al+3].[Al+3].[Al+3].[Al+3].[Al+3].[Al+3].[K+].[K+].[K+].[Fe+2].O1[Si]2([O-])O[Si]1([O-])O2.O1[Si]2([O-])O[Si]1([O-])O2.O1[Si]2([O-])O[Si]1([O-])O2.O1[Si]2([O-])O[Si]1([O-])O2.O1[Si]2([O-])O[Si]1([O-])O2.O1[Si]2([O-])O[Si]1([O-])O2.O1[Si]2([O-])O[Si]1([O-])O2 VGIBGUSAECPPNB-UHFFFAOYSA-L 0.000 claims description 6
- 230000001590 oxidative effect Effects 0.000 claims description 6
- 239000000843 powder Substances 0.000 claims description 6
- 239000002893 slag Substances 0.000 claims description 6
- 235000019812 sodium carboxymethyl cellulose Nutrition 0.000 claims description 6
- 229920001027 sodium carboxymethylcellulose Polymers 0.000 claims description 6
- 235000019832 sodium triphosphate Nutrition 0.000 claims description 6
- 239000000375 suspending agent Substances 0.000 claims description 6
- 239000000454 talc Substances 0.000 claims description 6
- 235000012222 talc Nutrition 0.000 claims description 6
- 229910052623 talc Inorganic materials 0.000 claims description 6
- XOLBLPGZBRYERU-UHFFFAOYSA-N tin dioxide Chemical compound O=[Sn]=O XOLBLPGZBRYERU-UHFFFAOYSA-N 0.000 claims description 6
- 229910001887 tin oxide Inorganic materials 0.000 claims description 6
- VLCLHFYFMCKBRP-UHFFFAOYSA-N tricalcium;diborate Chemical compound [Ca+2].[Ca+2].[Ca+2].[O-]B([O-])[O-].[O-]B([O-])[O-] VLCLHFYFMCKBRP-UHFFFAOYSA-N 0.000 claims description 6
- UNXRWKVEANCORM-UHFFFAOYSA-I triphosphate(5-) Chemical compound [O-]P([O-])(=O)OP([O-])(=O)OP([O-])([O-])=O UNXRWKVEANCORM-UHFFFAOYSA-I 0.000 claims description 6
- WFKWXMTUELFFGS-UHFFFAOYSA-N tungsten Chemical compound [W] WFKWXMTUELFFGS-UHFFFAOYSA-N 0.000 claims description 6
- 229910052721 tungsten Inorganic materials 0.000 claims description 6
- 239000010937 tungsten Substances 0.000 claims description 6
- 239000000203 mixture Substances 0.000 claims description 3
- 238000005507 spraying Methods 0.000 claims description 3
- 235000005881 Calendula officinalis Nutrition 0.000 claims 1
- 240000000785 Tagetes erecta Species 0.000 claims 1
- 239000000463 material Substances 0.000 claims 1
- 230000000694 effects Effects 0.000 abstract description 9
- 241000283973 Oryctolagus cuniculus Species 0.000 abstract description 7
- 238000002425 crystallisation Methods 0.000 abstract description 5
- 230000008025 crystallization Effects 0.000 abstract description 5
- 239000000725 suspension Substances 0.000 abstract description 3
- 238000002844 melting Methods 0.000 abstract 1
- 230000008018 melting Effects 0.000 abstract 1
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 3
- 101001018064 Homo sapiens Lysosomal-trafficking regulator Proteins 0.000 description 2
- 102100033472 Lysosomal-trafficking regulator Human genes 0.000 description 2
- 235000010703 Modiola caroliniana Nutrition 0.000 description 2
- 244000038561 Modiola caroliniana Species 0.000 description 2
- 239000013078 crystal Substances 0.000 description 2
- 229910052742 iron Inorganic materials 0.000 description 2
- 239000002932 luster Substances 0.000 description 2
- 230000000630 rising effect Effects 0.000 description 2
- 239000003086 colorant Substances 0.000 description 1
- 238000010276 construction Methods 0.000 description 1
- 230000007547 defect Effects 0.000 description 1
- SZVJSHCCFOBDDC-UHFFFAOYSA-N ferrosoferric oxide Chemical compound O=[Fe]O[Fe]O[Fe]=O SZVJSHCCFOBDDC-UHFFFAOYSA-N 0.000 description 1
- 230000003760 hair shine Effects 0.000 description 1
- -1 iron ions Chemical class 0.000 description 1
- 239000009427 jiangzhi Substances 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- VIKNJXKGJWUCNN-XGXHKTLJSA-N norethisterone Chemical compound O=C1CC[C@@H]2[C@H]3CC[C@](C)([C@](CC4)(O)C#C)[C@@H]4[C@@H]3CCC2=C1 VIKNJXKGJWUCNN-XGXHKTLJSA-N 0.000 description 1
- 229910052573 porcelain Inorganic materials 0.000 description 1
- 238000011084 recovery Methods 0.000 description 1
- 238000006479 redox reaction Methods 0.000 description 1
- 238000004017 vitrification Methods 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C8/00—Enamels; Glazes; Fusion seal compositions being frit compositions having non-frit additions
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C8/00—Enamels; Glazes; Fusion seal compositions being frit compositions having non-frit additions
- C03C8/14—Glass frit mixtures having non-frit additions, e.g. opacifiers, colorants, mill-additions
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B33/00—Clay-wares
- C04B33/02—Preparing or treating the raw materials individually or as batches
- C04B33/13—Compounding ingredients
- C04B33/132—Waste materials; Refuse; Residues
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B41/00—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
- C04B41/009—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone characterised by the material treated
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B41/00—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
- C04B41/45—Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements
- C04B41/52—Multiple coating or impregnating multiple coating or impregnating with the same composition or with compositions only differing in the concentration of the constituents, is classified as single coating or impregnation
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B41/00—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
- C04B41/80—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone of only ceramics
- C04B41/81—Coating or impregnation
- C04B41/89—Coating or impregnation for obtaining at least two superposed coatings having different compositions
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/02—Composition of constituents of the starting material or of secondary phases of the final product
- C04B2235/30—Constituents and secondary phases not being of a fibrous nature
- C04B2235/32—Metal oxides, mixed metal oxides, or oxide-forming salts thereof, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
- C04B2235/327—Iron group oxides, their mixed metal oxides, or oxide-forming salts thereof
- C04B2235/3272—Iron oxides or oxide forming salts thereof, e.g. hematite, magnetite
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/02—Composition of constituents of the starting material or of secondary phases of the final product
- C04B2235/30—Constituents and secondary phases not being of a fibrous nature
- C04B2235/34—Non-metal oxides, non-metal mixed oxides, or salts thereof that form the non-metal oxides upon heating, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
- C04B2235/3427—Silicates other than clay, e.g. water glass
- C04B2235/3436—Alkaline earth metal silicates, e.g. barium silicate
- C04B2235/3445—Magnesium silicates, e.g. forsterite
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P40/00—Technologies relating to the processing of minerals
- Y02P40/60—Production of ceramic materials or ceramic elements, e.g. substitution of clay or shale by alternative raw materials, e.g. ashes
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Ceramic Engineering (AREA)
- Materials Engineering (AREA)
- Organic Chemistry (AREA)
- Structural Engineering (AREA)
- Geochemistry & Mineralogy (AREA)
- General Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Life Sciences & Earth Sciences (AREA)
- Environmental & Geological Engineering (AREA)
- Dispersion Chemistry (AREA)
- Compositions Of Oxide Ceramics (AREA)
Abstract
The invention relates to a colorful building cup, which comprises a ceramic blank, and a ground glaze and a surface glaze which are covered on the surface of the blank, wherein the ground glaze and the surface glaze can be combined with each other through fine proportioning and selection of raw materials; in the firing process, the multi-color green cup is required to be subjected to heat preservation twice, wherein the first heat preservation can obtain excellent glaze quality, the second heat preservation is performed at 1120-1130 ℃ and is performed in a crystallization area, the two glazes of the base glaze and the overglaze are combined in a melting way to form a flowing effect, the base glaze and the overglaze flow to form a golden rabbit hair and red rabbit hair alternate effect, and a hanging glaze tear is generated at the bottom suspension position of a green body, so that the multi-color green cup has rich color tone change and is colorful, and each piece of work can show a flower world different from a 'ware like a ten thousand iridescence' seen by naked eyes under a fifty-fold microscope, so that the multi-color green cup is named as a multi-color green cup.
Description
Technical Field
The invention relates to the technical field of ceramic manufacture, in particular to a multi-color cup for a living things and a preparation method thereof.
Background
The Jiangzhi is a bright pearl in the history of Chinese ceramics. The cup has beautiful appearance, changeable glaze, as the vast amount of universe, and is unique and beautiful compared with other porcelain, and is still fashionable over thousands of years. In recent decades, a great deal of recovery research work is carried out by experts and artists in the ceramic field to obtain a certain effect, but the situation that a good party is difficult to find and a fine product is difficult to obtain is not thoroughly changed, and the precious historical cultural heritage is almost lost. The traditional glaze construction of the cup mainly comprises rabbit milli cup and oil drop cup.
Along with the continuous improvement of the living standard of people, the pursuit of the surface effect of the traditional cup building is also continuously improved, as the colorful purple golden oil disclosed in the application number CN201810106372.0 is used for building the cup, the number of pinholes of the cup building glaze is small, crystallization is thorough, the three-dimensional sense of the crystal is strong, the oil drops are thick and colorful, and the cup building glaze takes purple gold as a basis, and shines out of colorful luster, thus having strong artistic aesthetic feeling; the black background mauve oil drop is provided with a cup as disclosed in the application number CN201810101131.7, the cup is good in vitrification effect, the glaze is black and bright, crystal spots with mauve luster are irregularly scattered on the glaze, the crystallization is natural, the spot density of the oil drop is good, and the three-dimensional feeling and layering sense of the spot are strong.
The existing build cup is characterized in that a green body and glaze with high iron content are used, iron ions in the green body and the glaze can be separated out at a high temperature stage and reduced into ferroferric oxide to be colored through oxidation-reduction reaction, so that the build cup with any color can be colored only at the firing temperature of more than 1250 ℃, the firing temperature is high, the colors are random, the relative precise control cannot be realized, and the yield is low.
Disclosure of Invention
In order to solve the defects in the prior art, the invention provides a preparation method of a multi-color cup for everything and a transparent glaze.
In order to achieve the above purpose, the technical scheme adopted by the invention is as follows: the colorful building cup comprises a ceramic green body, and a ground coat glaze and a surface layer glaze which are covered on the surface of the green body, wherein the thickness of the ground coat glaze is 2-3mm, and the thickness of the surface layer glaze is 0.5-1.5mm; the under-glaze comprises the following raw materials in percentage by weight: 40-45 parts of feldspar, 15-18 parts of quartz, 10-15 parts of limestone, 5-10 parts of calcium borate, 5-10 parts of talcum powder, 3-5 parts of kaolin, 1-2 parts of copper carbonate, 2-5 parts of tin oxide, 1-3 parts of sodium carboxymethylcellulose and 1-3 parts of phosphorus pentoxide; the surface glaze comprises the following raw materials in parts by weight: 45-50 parts of potassium feldspar, 15-20 parts of quartz, 10-15 parts of calcium carbonate, 5-10 parts of kaolin, 5-10 parts of red ferric oxide, 1-5 parts of ammonium tripolyphosphate and 0.3-1 part of suspending agent.
Further, the ceramic body comprises the following raw materials in percentage by weight: ji Zhou clay 30-40 parts, purple gold clay 10-15 parts, calcined talc 10-15 parts, illite 10-15 parts, tungsten tailing slag 10-15 parts, bentonite 5-10 parts and ferric oxide powder 1-5 parts.
Further, the ceramic body comprises the following raw materials in percentage by weight: ji Zhou clay 36 parts, gold clay 12 parts, calcined talc 14 parts, illite 13 parts, tungsten tailing slag 12 parts, bentonite 9 parts and ferric oxide powder 4 parts.
Further, the raw materials of the ground coat comprise the following components: 43 parts of feldspar, 16 parts of quartz, 11 parts of limestone, 8 parts of calcium borate, 9 parts of talcum powder, 4 parts of kaolin, 1.5 parts of copper carbonate, 3.2 parts of tin oxide, 2.3 parts of sodium carboxymethyl cellulose and 2 parts of phosphorus pentoxide.
Further, the surface glaze comprises the following raw materials in parts by weight: 49 parts of potassium feldspar, 18 parts of quartz, 14 parts of calcium carbonate, 6 parts of kaolin, 8 parts of red ferric oxide, 4 parts of ammonium tripolyphosphate and 1 part of suspending agent.
A preparation method of a colorful building cup for everything, which comprises the following specific steps:
step 1, preparing a ceramic blank according to raw material components of the ceramic blank;
step 2, preparing ground glaze slip and surface glaze slip according to the raw material groups of ground glaze and surface glaze respectively;
step 3, placing the ceramic blank prepared in the step 1 into a kiln for biscuit firing, wherein the temperature is less than 700-750 ℃, and a biscuit firing blank is obtained;
step 4, glazing a ground coat on the surface of the biscuit firing blank, wherein the glazing thickness of the ground coat is 2-3mm;
step 5, when the ground coat is dried to the water content of 10-20%, applying surface layer glaze slip on the surface of the ground coat;
and 6, after the surface layer glaze slip is dried, placing the biscuit firing blank body with the ground coat glaze and the surface layer glaze into a kiln again, and firing and forming under an oxidizing atmosphere, wherein the firing temperature is 1238-1330 ℃.
Further, the step of preparing the underglaze slip in the step 2 is as follows: mixing the raw material components of the underglaze according to the proportion, ball milling for 4-8 hours to obtain ceramic green body slurry, wherein the proportion of the raw material to the water to the balls is 2:1:1 during the ball milling, the fineness of the glaze is 150-200 meshes, the screen residue is 0.1-0.15%, and the relative density of the glaze slurry is 1.5-1.8.
Further, the step of preparing the underglaze slip in the step 2 is as follows: mixing the raw material components of the surface glaze according to the proportion, ball milling the mixture for 15 to 20 hours to obtain ceramic green body slurry, wherein the proportion of the mixture to the water to the balls is 1:2:1 during the ball milling, the fineness of the glaze is 250 to 300 meshes, the screen residue is 0.06 to 0.8 percent, and the relative density of the glaze slurry is 1.2 to 1.3.
Furthermore, the glaze release process of the overglaze in the step 5 adopts glaze spraying.
Further, in step 6, firing is controlled as follows:
in the temperature rising stage, the kiln is heated to 1150 ℃ in oxidizing atmosphere for 4-5 hours,
in the firing stage, the temperature reaches 1238-1330 ℃ after 1-2 hours in the kiln, reaches the firing temperature, and is kept at the firing temperature for 30-80 minutes;
in the cooling stage, cooling the interior of the kiln to 1120-1130 ℃ at a cooling speed of 10-15 ℃/min;
the second heat preservation stage, the kiln is kept at 1120-1130 ℃ for 90-120 minutes;
and in the cooling stage, the kiln is cooled to be naturally cooled after 3-5 hours.
According to the multi-color building cup, through fine proportioning and selection of the raw materials, the pulling coefficient between the two glazes is small, the two glazes can be combined with each other, and the combination degree of the base glaze and the surface glaze with a blank body is good; in the firing process, the multi-color green cup is required to be subjected to heat preservation twice, wherein the first heat preservation can obtain excellent glaze quality at the high temperature of 1238-1330 ℃, the second heat preservation is performed at the temperature of 1120-1130 ℃ and is performed in a crystallization area, the two glazes of the ground glaze and the surface glaze are fused and combined to form a flowing effect, the ground glaze and the surface glaze flow to form a golden rabbit hair and red rabbit hair alternate effect, and each hanging glaze tear is generated at the bottom suspension position of the green body, so that the multi-color green cup has rich color tone change, the speckle is colorful, and each work can show a different' ware image with the color of ten times as much as ten times as possible under a microscope, and the name of the multi-color green cup is called as a toy.
Detailed Description
The invention is further described below by means of specific embodiments.
The colorful building cup comprises a ceramic green body, and a ground coat glaze and a surface layer glaze which are covered on the surface of the green body, wherein the thickness of the ground coat glaze is 2-3mm, and the thickness of the surface layer glaze is 0.5-1.5mm;
the under-glaze comprises the following raw materials in percentage by weight: 40-45 parts of feldspar, 15-18 parts of quartz, 10-15 parts of limestone, 5-10 parts of calcium borate, 5-10 parts of talcum powder, 3-5 parts of kaolin, 1-2 parts of copper carbonate, 2-5 parts of tin oxide, 1-3 parts of sodium carboxymethylcellulose and 1-3 parts of phosphorus pentoxide;
the surface glaze comprises the following raw materials in parts by weight: 45-50 parts of potassium feldspar, 15-20 parts of quartz, 10-15 parts of calcium carbonate, 5-10 parts of kaolin, 5-10 parts of red ferric oxide, 1-5 parts of ammonium tripolyphosphate and 0.3-1 part of suspending agent.
The raw materials of the green body comprise the following components: ji Zhou clay 30-40 parts, purple gold clay 10-15 parts, calcined talc 10-15 parts, illite 10-15 parts, tungsten tailing slag 10-15 parts, bentonite 5-10 parts and ferric oxide powder 1-5 parts.
First embodiment:
the colorful building cup comprises a ceramic green body, and a ground coat glaze and a surface layer glaze which are covered on the surface of the green body, wherein the thickness of the ground coat glaze is 2-3mm, and the thickness of the surface layer glaze is 0.5-1.5mm;
the raw materials of the ceramic body comprise the following components: ji Zhou clay 36 parts, gold clay 12 parts, burned talcum 14 parts, illite 13 parts, tungsten tailing slag 12 parts, bentonite 9 parts and ferric oxide powder 4 parts;
the under-glaze comprises the following raw materials in percentage by weight: 43 parts of feldspar, 16 parts of quartz, 11 parts of limestone, 8 parts of calcium borate, 9 parts of talcum powder, 4 parts of kaolin, 1.5 parts of copper carbonate, 3.2 parts of tin oxide, 2.3 parts of sodium carboxymethylcellulose and 2 parts of phosphorus pentoxide;
the surface glaze comprises the following raw materials in parts by weight: 49 parts of potassium feldspar, 18 parts of quartz, 14 parts of calcium carbonate, 6 parts of kaolin, 8 parts of red ferric oxide, 4 parts of ammonium tripolyphosphate and 1 part of suspending agent.
A preparation method of a colorful building cup for everything, which comprises the following specific steps:
step 1, preparing a ceramic blank according to raw material components of the ceramic blank;
step 2, preparing ground glaze slip and surface glaze slip according to raw material groups of ground glaze and surface glaze respectively, mixing according to the proportion of raw material components of the ground glaze when preparing the ground glaze slip, mixing and ball milling for 4-8 hours to obtain ceramic body slip, wherein the proportion of water to balls is 2:1:1 during mixing and ball milling, the fineness of glaze is 150-200 meshes, the screen residue is 0.1-0.15%, the relative density of glaze slip is 1.5-1.8, mixing according to the proportion of raw material components of the surface glaze when preparing the surface glaze slip, mixing and ball milling for 15-20 hours to obtain ceramic body slip, the proportion of water to balls is 1:2:1 during mixing and ball milling, the fineness of glaze is 250-300 meshes, the screen residue is 0.06-0.8%, and the relative density of glaze slip is 1.2-1.3;
step 3, placing the ceramic blank prepared in the step 1 into a kiln for biscuit firing, wherein the temperature is less than 700-750 ℃, and a biscuit firing blank is obtained;
step 4, glazing a ground coat on the surface of the biscuit firing blank, wherein the glazing thickness of the ground coat is 2-3mm;
step 5, when the ground coat is dried to the water content of 10-20%, applying surface layer glaze slip on the surface of the ground coat by adopting a glaze spraying process;
step 6, after waiting for the surface glaze slip to be dried, putting the biscuit firing blank body with the ground glaze and the surface glaze into a kiln again, firing and forming under the oxidizing atmosphere, wherein the firing temperature is 1238-1330 ℃, the specific control is as follows,
in the temperature rising stage, the kiln is heated to 1150 ℃ in oxidizing atmosphere for 4-5 hours,
in the firing stage, the temperature reaches 1238-1330 ℃ after 1-2 hours in the kiln, reaches the firing temperature, and is kept at the firing temperature for 30-80 minutes;
in the cooling stage, cooling the interior of the kiln to 1120-1130 ℃ at a cooling speed of 10-15 ℃/min;
the second heat preservation stage, the kiln is kept at 1120-1130 ℃ for 90-120 minutes;
and in the cooling stage, the kiln is cooled to be naturally cooled after 3-5 hours.
According to the multi-color building cup, through fine proportioning and selection of the raw materials, the pulling coefficient between the two glazes is small, the two glazes can be combined with each other, and the combination degree of the base glaze and the surface glaze with a blank body is good; in the firing process, the multi-color green cup is required to be subjected to heat preservation twice, wherein the first heat preservation can obtain excellent glaze quality at the high temperature of 1238-1330 ℃, the second heat preservation is performed at the temperature of 1120-1130 ℃ and is performed in a crystallization area, the two glazes of the ground glaze and the surface glaze are fused and combined to form a flowing effect, the ground glaze and the surface glaze flow to form a golden rabbit hair and red rabbit hair alternate effect, and each hanging glaze tear is generated at the bottom suspension position of the green body, so that the multi-color green cup has rich color tone change, the speckle is colorful, and each work can show a different' ware image with the color of ten times as much as ten times as possible under a microscope, and the name of the multi-color green cup is called as a toy.
The foregoing is merely one specific embodiment of the present invention, but the design concept of the present invention is not limited thereto, and any insubstantial modification of the present invention by using the concept shall belong to the behavior of infringement of the protection scope of the present invention.
Claims (8)
1. The colorful building cup for the everything is characterized by comprising a ceramic green body, and a bottom glaze and a surface glaze which are covered on the surface of the green body, wherein the thickness of the bottom glaze is 2-3mm, and the thickness of the surface glaze is 0.5-1.5mm;
the raw material composition of the underglaze is as follows: 40-45 parts of feldspar, 15-18 parts of quartz, 10-15 parts of limestone, 5-10 parts of calcium borate, 5-10 parts of talcum powder, 3-5 parts of kaolin, 1-2 parts of copper carbonate, 2-5 parts of tin oxide, 1-3 parts of sodium carboxymethylcellulose and 1-3 parts of phosphorus pentoxide;
the surface glaze comprises the following raw materials in parts by weight: 45-50 parts of potassium feldspar, 15-20 parts of quartz, 10-15 parts of calcium carbonate, 5-10 parts of kaolin, 5-10 parts of red ferric oxide, 1-5 parts of ammonium tripolyphosphate and 0.3-1 part of suspending agent;
the preparation method of the universal biological multicolor building cup comprises the following specific steps:
step 1, preparing a ceramic blank according to raw material components of the ceramic blank;
step 2, preparing ground glaze slip and surface glaze slip according to raw material components of ground glaze and surface glaze respectively;
step 3, placing the ceramic blank prepared in the step 1 into a kiln for biscuit firing, wherein the biscuit firing temperature is 700-750 ℃, and obtaining a biscuit firing blank;
step 4, applying a ground coat on the surface of the biscuit firing blank, wherein the glazing thickness of the ground coat is 2-3mm;
step 5, when the ground coat is dried to the water content of 10-20%, applying surface layer glaze slip on the surface of the ground coat;
step 6, after waiting for the surface layer glaze slip to be dried, putting the biscuit firing blank body with the ground coat glaze and the surface layer glaze into a kiln again, and firing and forming under an oxidizing atmosphere, wherein the firing temperature is 1238-1330 ℃;
the specific control of the firing forming is as follows:
a temperature rise stage, in which the kiln is heated to 1150 ℃ for 4-5 hours under an oxidizing atmosphere, and a firing stage, in which the kiln is heated to 1238-1330 ℃ for 1-2 hours, and the kiln is kept at the firing temperature for 30-80 minutes;
in the cooling stage, cooling the interior of the kiln to 1120-1130 ℃ at a cooling speed of 10-15 ℃/min;
the second heat preservation stage, the kiln is kept at 1120-1130 ℃ for 90-120 minutes;
and in the cooling stage, the kiln is naturally cooled for 3-5 hours.
2. The universal multi-color architectural cup according to claim 1, wherein the raw materials of the ceramic body are as follows: ji Zhou clay 30-40 parts, purple gold clay 10-15 parts, calcined talc 10-15 parts, illite 10-15 parts, tungsten tailing slag 10-15 parts, bentonite 5-10 parts and ferric oxide powder 1-5 parts.
3. The universal multi-color architectural cup according to claim 2, wherein the raw materials of the ceramic body are as follows: ji Zhou clay 36 parts, gold clay 12 parts, calcined talc 14 parts, illite 13 parts, tungsten tailing slag 12 parts, bentonite 9 parts and ferric oxide powder 4 parts.
4. The base coat glaze according to claim 1 or 2, wherein the base coat glaze comprises the following raw materials: 43 parts of feldspar, 16 parts of quartz, 11 parts of limestone, 8 parts of calcium borate, 9 parts of talcum powder, 4 parts of kaolin, 1.5 parts of copper carbonate, 3.2 parts of tin oxide, 2.3 parts of sodium carboxymethyl cellulose and 2 parts of phosphorus pentoxide.
5. A multi-colour cup for a living things according to claim 3, wherein the surface glaze comprises the following raw materials: 49 parts of potassium feldspar, 18 parts of quartz, 14 parts of calcium carbonate, 6 parts of kaolin, 8 parts of red ferric oxide, 4 parts of ammonium tripolyphosphate and 1 part of suspending agent.
6. The base coat glaze system according to claim 1, wherein the step of preparing the base coat glaze slip in step 2 comprises the steps of: mixing according to the proportion of the raw material components of the underglaze, mixing and ball milling for 4-8 hours to obtain underglaze slurry, and mixing and ball milling: water: the ratio of the balls is 2:1:1, the fineness of the glaze is 150-200 meshes, the screen residue is 0.1-0.15%, and the relative density of the glaze slurry is 1.5-1.8.
7. The base station of claim 1, wherein the step of preparing the top coat glaze slip in step 2 comprises the steps of: mixing the raw material components of the surface glaze according to the proportion, mixing and ball milling for 15-20 hours to obtain surface glaze slurry, and mixing and ball milling the materials: water: the ratio of the balls is 1:2:1, the fineness of the glaze is 250-300 meshes, the screen residue is 0.06-0.8%, and the relative density of the glaze slurry is 1.2-1.3.
8. The multi-color marigold of claim 1, wherein: the glazing process of the overglaze in the step 5 adopts glaze spraying.
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Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2005082438A (en) * | 2003-09-08 | 2005-03-31 | Osamu Ohira | Yo-hen adorned pottery and its manufacturing method |
| CN101130463A (en) * | 2007-07-13 | 2008-02-27 | 邱林铿 | Production method of ceramic for generating gold crystallization dapple on glaze of ceramic and ceramic glaze used thereof |
| CN104987137A (en) * | 2015-07-30 | 2015-10-21 | 江苏省宜兴彩陶工艺厂 | Method for applying rabbit-hair-like glaze on ceramic body |
| CN108046604A (en) * | 2017-12-29 | 2018-05-18 | 平顶山市神前传奇唐钧瓷有限公司 | A kind of oil droplet Tang chun glaze and prepare the technique of pottery using it |
| CN108585771A (en) * | 2018-05-09 | 2018-09-28 | 南平市曜变陶瓷研究院 | Small cup and preparation process are built in a kind of change of sunlight |
| CN109942188A (en) * | 2019-04-16 | 2019-06-28 | 福建省德化问瓷阁陶瓷有限公司 | A kind of green temmoku glaze ceramics of matt and its manufacture craft |
-
2020
- 2020-04-29 CN CN202010353518.9A patent/CN111499197B/en active Active
Patent Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2005082438A (en) * | 2003-09-08 | 2005-03-31 | Osamu Ohira | Yo-hen adorned pottery and its manufacturing method |
| CN101130463A (en) * | 2007-07-13 | 2008-02-27 | 邱林铿 | Production method of ceramic for generating gold crystallization dapple on glaze of ceramic and ceramic glaze used thereof |
| CN104987137A (en) * | 2015-07-30 | 2015-10-21 | 江苏省宜兴彩陶工艺厂 | Method for applying rabbit-hair-like glaze on ceramic body |
| CN108046604A (en) * | 2017-12-29 | 2018-05-18 | 平顶山市神前传奇唐钧瓷有限公司 | A kind of oil droplet Tang chun glaze and prepare the technique of pottery using it |
| CN108585771A (en) * | 2018-05-09 | 2018-09-28 | 南平市曜变陶瓷研究院 | Small cup and preparation process are built in a kind of change of sunlight |
| CN109942188A (en) * | 2019-04-16 | 2019-06-28 | 福建省德化问瓷阁陶瓷有限公司 | A kind of green temmoku glaze ceramics of matt and its manufacture craft |
Non-Patent Citations (1)
| Title |
|---|
| 布莱恩•泰勒.陶瓷原料.《釉 釉料及陶瓷颜色配制手册》.上海科学出版社,2015,第29-33页. * |
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