CN111454793A - Skin-cleaning and mite-killing traditional Chinese medicine soap and preparation method thereof - Google Patents
Skin-cleaning and mite-killing traditional Chinese medicine soap and preparation method thereof Download PDFInfo
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D9/00—Compositions of detergents based essentially on soap
- C11D9/02—Compositions of detergents based essentially on soap on alkali or ammonium soaps
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/48—Medical, disinfecting agents, disinfecting, antibacterial, germicidal or antimicrobial compositions
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D9/00—Compositions of detergents based essentially on soap
- C11D9/04—Compositions of detergents based essentially on soap containing compounding ingredients other than soaps
- C11D9/06—Inorganic compounds
- C11D9/18—Water-insoluble compounds
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D9/00—Compositions of detergents based essentially on soap
- C11D9/04—Compositions of detergents based essentially on soap containing compounding ingredients other than soaps
- C11D9/22—Organic compounds, e.g. vitamins
- C11D9/26—Organic compounds, e.g. vitamins containing oxygen
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D9/00—Compositions of detergents based essentially on soap
- C11D9/04—Compositions of detergents based essentially on soap containing compounding ingredients other than soaps
- C11D9/22—Organic compounds, e.g. vitamins
- C11D9/26—Organic compounds, e.g. vitamins containing oxygen
- C11D9/262—Organic compounds, e.g. vitamins containing oxygen containing carbohydrates
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D9/00—Compositions of detergents based essentially on soap
- C11D9/04—Compositions of detergents based essentially on soap containing compounding ingredients other than soaps
- C11D9/22—Organic compounds, e.g. vitamins
- C11D9/26—Organic compounds, e.g. vitamins containing oxygen
- C11D9/265—Organic compounds, e.g. vitamins containing oxygen containing glycerol
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D9/00—Compositions of detergents based essentially on soap
- C11D9/04—Compositions of detergents based essentially on soap containing compounding ingredients other than soaps
- C11D9/22—Organic compounds, e.g. vitamins
- C11D9/26—Organic compounds, e.g. vitamins containing oxygen
- C11D9/267—Organic compounds, e.g. vitamins containing oxygen containing free fatty acids
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D9/00—Compositions of detergents based essentially on soap
- C11D9/04—Compositions of detergents based essentially on soap containing compounding ingredients other than soaps
- C11D9/22—Organic compounds, e.g. vitamins
- C11D9/38—Products in which the composition is not well defined
Abstract
The invention discloses a skin-cleaning mite-killing traditional Chinese medicine soap which comprises the following raw materials in parts by weight: 15-40 parts of water, 2-8 parts of glycerol, 1-6 parts of sorbitol, 1-6 parts of sucrose, 3-8 parts of propylene glycol, 2-10 parts of ferment stock solution, 2-10 parts of sulfur extract, 1-5 parts of palm oil, 1-5 parts of olive oil, 1-5 parts of grape seed oil, 1-5 parts of coconut oil, 1-5 parts of lauric acid, 1-5 parts of stearic acid, 30-45 parts of sodium fatty acid, 3-8 parts of honeysuckle extract, 3-8 parts of sophora flavescens extract, 0.2-2 parts of tea tree essential oil, 0.1-1.2 parts of ginseng and 1-4 parts of honeysuckle. According to the skin-cleaning mite-killing traditional Chinese medicine soap, natural Chinese herbal medicines of honeysuckle and sophora flavescens are extracted and put into the soap, so that the skin-cleaning mite-killing traditional Chinese medicine soap can effectively inhibit bacteria and kill mites, inhibit breeding of mites, and solve various skin problems such as excessive oil secretion.
Description
Technical Field
The invention relates to the technical field of soaps and preparation methods thereof, in particular to a traditional Chinese medicine soap for clearing skin and removing mites and a preparation method thereof.
Background
The skin is a natural coat covering the surface of a human body and is also the largest organ of the human body, and healthy skin can complete complex physiological functions, also can embody the aesthetic feeling of the human body and enables people to have a good health and vitality.
However, due to the invasion of mites and bacteria, the skin becomes dark yellow due to the blockage of pores by metabolic waste, and the skin becomes red, swollen and variola.
Facial cleansing is important for the prevention of mite-infected faces, but overly aggressive chemical products can disrupt the natural barrier of the skin and even lead to paradoxical cycles of more complete skin cleansing and more intense oil secretion.
The bactericidal and acaricidal drugs containing a plurality of western medicine components comprise salicylic acid, triclosan and the like, but the acid brushing effect is achieved by thinning the cuticle of the skin, so that the skin is greatly damaged.
The toilet soap has the functions of sterilizing and cleaning the skin, and is commonly used in the life of people, but most of the toilet soaps in the market at present do not have the efficacies of removing mites, relieving swelling and itching, and the people who use the toilet soap can not remove the mites parasitized on the skin, but only can realize the most basic effect of cleaning the skin.
Disclosure of Invention
Aiming at the technical defects, the invention aims to provide a traditional Chinese medicine soap for cleaning skin and removing mites and a preparation method thereof, so as to solve the problems in the background art.
In order to solve the technical problems, the invention adopts the following technical scheme:
the invention provides a skin-cleaning mite-removing traditional Chinese medicine soap which comprises the following raw materials in parts by weight:
15-40 parts of water, 2-8 parts of glycerol, 1-6 parts of sorbitol, 1-6 parts of sucrose, 3-8 parts of propylene glycol, 2-10 parts of ferment stock solution, 2-10 parts of sulfur extract, 1-5 parts of palm oil, 1-5 parts of olive oil, 1-5 parts of grape seed oil, 1-5 parts of coconut oil, 1-5 parts of lauric acid, 1-5 parts of stearic acid, 30-45 parts of sodium fatty acid, 3-8 parts of honeysuckle extract, 3-8 parts of sophora flavescens extract, 0.2-2 parts of tea tree essential oil, 0.1-1.2 parts of ginseng and 1-4 parts of honeysuckle.
The traditional Chinese medicine soap for cleaning skin and removing mites comprises the following raw materials in parts by weight:
15 parts of water, 2 parts of glycerol, 1 part of sorbitol, 1 part of sucrose, 3 parts of propylene glycol, 2 parts of an enzyme stock solution, 2 parts of a sulfur extract, 1 part of palm oil, 1 part of olive oil, 1 part of grape seed oil, 1 part of coconut oil, 1 part of lauric acid, 1 part of stearic acid, 30 parts of sodium fatty acid, 3 parts of a honeysuckle extract, 3 parts of a sophora flavescens extract, 0.2 part of tea tree essential oil, 0.1 part of ginseng and 1 part of honeysuckle.
The traditional Chinese medicine soap for cleaning skin and removing mites comprises the following raw materials in parts by weight:
40 parts of water, 8 parts of glycerol, 6 parts of sorbitol, 6 parts of sucrose, 8 parts of propylene glycol, 10 parts of an enzyme stock solution, 10 parts of a sulfur extract, 5 parts of palm oil, 5 parts of olive oil, 5 parts of grape seed oil, 5 parts of coconut oil, 5 parts of lauric acid, 5 parts of stearic acid, 45 parts of sodium fatty acid, 8 parts of a honeysuckle extract, 8 parts of a sophora flavescens extract, 2 parts of tea tree essential oil, 1.2 parts of ginseng and 4 parts of honeysuckle.
The traditional Chinese medicine soap for cleaning skin and removing mites comprises the following raw materials in parts by weight:
30 parts of water, 6 parts of glycerol, 4 parts of sorbitol, 4 parts of sucrose, 6 parts of propylene glycol, 8 parts of an enzyme stock solution, 8 parts of a sulfur extract, 4 parts of palm oil, 4 parts of olive oil, 4 parts of grape seed oil, 4 parts of coconut oil, 4.5 parts of lauric acid, 4.5 parts of stearin, 40 parts of sodium fatty acid, 6 parts of a honeysuckle extract, 6 parts of a sophora flavescens extract, 1.5 parts of tea tree essential oil, 0.5 part of ginseng and 3 parts of honeysuckle.
The traditional Chinese medicine soap for cleaning skin and removing mites comprises the following raw materials in parts by weight:
35 parts of water, 5 parts of glycerol, 4 parts of sorbitol, 4 parts of sucrose, 4.8 parts of propylene glycol, 6.5 parts of enzyme stock solution, 6.5 parts of sulfur extract, 3 parts of palm oil, 3 parts of olive oil, 3 parts of grape seed oil, 3 parts of coconut oil, 3.5 parts of lauric acid, 3 parts of stearin, 37 parts of sodium fatty acid, 4 parts of honeysuckle extract, 5.5 parts of sophora flavescens extract, 1.3 parts of tea tree essential oil, 0.8 part of ginseng and 2 parts of honeysuckle.
The traditional Chinese medicine soap for cleaning skin and removing mites comprises the following raw materials in parts by weight:
20 parts of water, 4 parts of glycerol, 2 parts of sorbitol, 2 parts of sucrose, 4 parts of propylene glycol, 5 parts of an enzyme stock solution, 5 parts of a sulfur extract, 2 parts of palm oil, 2 parts of olive oil, 2 parts of grape seed oil, 2 parts of coconut oil, 2 parts of lauric acid, 2 parts of stearic acid, 35 parts of sodium fatty acid, 5 parts of a honeysuckle extract, 5 parts of a sophora flavescens extract, 1 part of tea tree essential oil, 0.6 part of ginseng and 2.5 parts of honeysuckle.
Preferably, the sodium fatty acid is sodium cocoate.
Preferably, the preparation method of the honeysuckle extract comprises the following steps:
soaking flos Lonicerae in 10-15 times (v/w, ml/g) of water at 70 deg.C or 75 deg.C for 2 times, each for 1 hr, mixing extractive solutions, concentrating under reduced pressure at 65-70 deg.C to 1.5-3 times (v/w, ml/g) of flos Lonicerae weight, and drying under reduced pressure.
Preferably, the preparation method of the sophora flavescens extract comprises the following steps:
cleaning radix Sophorae Flavescentis, breaking cell wall in cell wall breaking machine for 8-12min, adding 6-10 times of 50% ethanol solution, and performing ultrasonic treatment for 25-35 min; extracting for 90-150min by water bath reflux after the ultrasound is finished, wherein the extraction temperature is 50-65 ℃, collecting the extracting solution, adding 50% of ethanol to immerse the medicine residues, extracting for 40-80min by water bath reflux for the second time, collecting the extracting solution, adding 50% of ethanol to immerse the medicine residues, extracting for 40-80min by water bath reflux for the third time, extracting for 3 times in total, combining the extracting solutions for 3 times, filtering by a 10-micron filter membrane, concentrating the filtrate under reduced pressure at-0.09 Mpa and 55 ℃ to obtain a thick paste with the relative density of 1.30 at 60 ℃, and drying the thick paste under reduced pressure at-0.09 Mpa and 55 ℃ to obtain the traditional Chinese medicine.
A preparation method of a traditional Chinese medicine soap for cleaning skin and removing mites comprises the following steps:
(1) respectively drying Ginseng radix and flos Lonicerae;
(2) heating palm oil, olive oil, grape seed oil, coconut oil, lauric acid, stearic acid and sodium fatty acid to melt, continuously stirring, cooling to 50-70 ℃ at 20-50 rpm, and keeping the temperature;
(3) heating glycerol, sorbitol, sucrose, propylene glycol, ferment stock solution, and sulfur extract to melt, stirring, cooling to 20-50 deg.C at 20-50 rpm, and keeping the temperature;
(4) adding the second liquid into the mixture obtained in step (2) slowly in small amount for several times while stirring, and adding flos Lonicerae extract, radix Sophorae Flavescentis extract, tea tree essential oil and dried Ginseng radix and flos Lonicerae obtained in step (1) when the temperature is reduced to below 40 deg.C;
(5) stirring, demoulding after two days at room temperature, saponifying after one week, and cutting into blocks.
Preferably, in the step (1), the drying of the honeysuckle comprises four stages:
the first stage is as follows: spreading flos Lonicerae into 1-3 cm thin layer, and oven drying at 30-35 deg.C for 1-2 hr;
and a second stage: raising the drying temperature to 38-41 ℃ and drying for 5-7 hours;
and a third stage: raising the drying temperature to 45-50 deg.C, maintaining for 6-8 hr to further dehydrate and dry flos Lonicerae;
and a final stage: the drying temperature is raised to 55-58 ℃ and the drying time is 1-2 hours.
The honeysuckle is dried at low temperature, the temperature is gradually increased, the highest temperature is not more than 60 ℃, and the deterioration of flavonoid and iridoid chemical components in the honeysuckle can be effectively prevented.
Preferably, in the step (1), the ginseng drying comprises four stages:
the first stage is as follows: spreading the ginseng with the length of 3-6 cm in a single layer, controlling the drying temperature at 30-38 ℃ and the drying time for 2 hours; not to be too dense to utilize ventilation to remove moisture.
And a second stage: raising the drying temperature to 45-50 ℃ and the drying time to 7-10 hours;
and a third stage: the drying temperature is reduced to 38-43 ℃, and the drying temperature is maintained for 6-8 hours;
and a final stage: the drying temperature is raised to 45-50 ℃ and the drying time is 3-6 hours.
In the whole drying process of the ginseng, the relative humidity is 58-61%, the temperature and the air flow in the whole drying room are uniform through the hot air circulating part, the conditions of constant temperature and constant humidity are realized in the whole drying process, and the drying quality of the ginseng is very ensured. The drying temperature is repeatedly carried out from low to high and then from high to low until the phase and the drying degree meet the requirements. The dried ginseng has good quality, good color and high product grade.
The invention has the beneficial effects that:
(1) according to the skin-cleaning mite-killing traditional Chinese medicine soap, natural Chinese herbal medicines of honeysuckle and sophora flavescens are extracted and put into the soap, so that bacteria and mites can be effectively inhibited, breeding of mites can be inhibited, and various skin problems such as excessive grease secretion can be improved. The soap body contains multiple natural oil extracts such as olive oil, grape seed oil and coconut oil, and tea tree essential oil and ferment stock solution are added, so that the skin barrier can be repaired, and the moisture and elasticity of the skin can be maintained.
(2) The invention has good cleaning effect by selecting proper grease, essential oil and traditional Chinese medicine, nourishes skin, dredges pores, enhances skin immunity, resists bacteria, clears skin and removes mites.
(3) The soap body contains the whole ginseng and the honeysuckle as traditional Chinese medicine ornaments, which can be clearly seen, the honeysuckle adopts a low-temperature drying method, the temperature is gradually increased, the highest temperature is not more than 60 ℃, and the deterioration of flavonoid and iridoid chemical components in the honeysuckle can be effectively prevented. In the whole drying process of the ginseng, the process from low to high and then from high to low is also carried out, the relative humidity is strictly controlled to be 58-61%, the temperature and airflow in the whole drying room are uniform through the hot air circulation component, the conditions of constant temperature and constant humidity are realized in the whole drying process, and the drying quality of the ginseng is very ensured. The drying temperature is repeatedly carried out from low to high and then from high to low until the phase and the drying degree meet the requirements. The dried ginseng has good quality, good color and high product grade.
(4) The preparation method of the traditional Chinese medicine soap for cleaning skin and removing mites is simple and easy to operate, and all indexes meet the requirements in QB/T2485-2008 (type II).
In order to facilitate the understanding of the present invention, the efficacy of the raw materials of the present invention will be further described below.
Kuh-seng, bitter in taste, cold in nature, has the functions of clearing heat and drying dampness, killing parasites and promoting urination. The clinical common treatment of eczema, skin itch and mange is that the external application can also treat gynecological inflammations such as trichomonas vaginitis and the like. Since ancient times, the insecticidal efficacy of kuh-seng was regarded by physicians of all ages. Famous medical doctors in south china beam can carry the kuh-seng energy: for those who suffer from scabies and who drink wine stain, they can kill parasites. The Chinese herbal medicine is prepared by recording kuh-seng: for heat-toxin wind, skin irritation and sore. Record the Sophora flavescens Ainan Bencao: cool blood, clear heat toxin, scabies and pus-nest sore toxin. Treating skin pruritus, tinea, skin ulcer, obstinate dander, intestinal wind and hematochezia. Dispel wind, remove swelling and toxicity, and remove phlegm-toxicity. Referring now to mite discoloration, mites do indeed exist in our skin and pores, and investigations have shown that: about 99% of adults have mites on their faces! However, kuh-seng is a natural pesticide given to us by nature.
Honeysuckle flower is sweet in taste, cold in nature, has the functions of clearing away heat and toxic materials and dispelling wind and heat, and is a commonly used medicine for treating skin diseases such as sores and ulcers in traditional Chinese medicine. Pharmacological studies show that the honeysuckle has an inhibitory effect on various bacteria (typhoid bacillus, paratyphoid bacillus, escherichia coli, proteus, pseudomonas aeruginosa, bordetella pertussis, vibrio cholerae, staphylococcus, streptococcus, pneumococcus and meningococcus) in vitro. The honeysuckle has very high medicinal value, is safe and nontoxic, and is one of medicinal and edible health-preserving food materials recommended by Weijian Wei Jian. The record of Yunnan herbal medicine, honeysuckle: clearing heat, relieving sores, abscess, deep-rooted carbuncle, ulcer on the back, erysipelas and scrofula. The raw herb medicinal material is thought to be honeysuckle: it can cure carbuncle, deep-rooted carbuncle, furunculosis, dysentery, malnutritional ulcer and skin heat. The honeysuckle is recorded in the 'herbal preparation': "nourish blood and quench thirst". It is indicated for scabies. "
Detailed Description
Example 1
The traditional Chinese medicine soap for cleaning skin and removing mites comprises the following raw materials in parts by weight:
15 parts of water, 2 parts of glycerol, 1 part of sorbitol, 1 part of sucrose, 3 parts of propylene glycol, 2 parts of an enzyme stock solution, 2 parts of a sulfur extract, 1 part of palm oil, 1 part of olive oil, 1 part of grape seed oil, 1 part of coconut oil, 1 part of lauric acid, 1 part of stearic acid, 30 parts of sodium fatty acid, 3 parts of a honeysuckle extract, 3 parts of a sophora flavescens extract, 0.2 part of tea tree essential oil, 0.1 part of ginseng and 1 part of honeysuckle.
The sodium fatty acid is sodium coconut oil fatty acid.
The preparation method of the honeysuckle extract comprises the following steps:
soaking flos Lonicerae in 10 times (v/w, ml/g) of water at 70 deg.C for 2 times, each for 1 hr, mixing extractive solutions, concentrating under reduced pressure at 65 deg.C to 1.5 times (v/w, ml/g) of flos Lonicerae weight, and drying under reduced pressure.
The preparation method of the sophora flavescens extract comprises the following steps:
cleaning radix Sophorae Flavescentis, breaking cell wall in cell wall breaking machine for 8min, adding 50% ethanol solution with mass ratio of 6 times, and performing ultrasonic treatment for 25 min; extracting for 90min by water bath reflux after the ultrasound is finished, wherein the extraction temperature is 50 ℃, collecting an extracting solution, adding 50% ethanol to immerse the medicine residues, extracting for 40min by water bath reflux for the second time, collecting an extracting solution, adding 50% ethanol to immerse the medicine residues, extracting for 40min by water bath reflux for the third time, extracting for 3 times in total, combining the extracting solutions of 3 times, filtering by a 10-micron filter membrane, concentrating the filtrate under reduced pressure at-0.09 Mpa and 55 ℃ to obtain a thick paste with the relative density of 1.30 at 60 ℃, and drying the thick paste under reduced pressure at-0.09 Mpa and 55 ℃ to obtain the traditional Chinese medicine.
A preparation method of a traditional Chinese medicine soap for cleaning skin and removing mites comprises the following steps:
(1) respectively drying Ginseng radix and flos Lonicerae;
(2) heating palm oil, olive oil, grape seed oil, coconut oil, lauric acid, stearic acid and sodium fatty acid to melt, continuously stirring, cooling to 50 ℃ at 20 r/min, and keeping the temperature;
(3) heating glycerol, sorbitol, sucrose, propylene glycol, ferment stock solution, and sulfur extract to melt, stirring, cooling to 20 deg.C/min, and keeping the temperature;
(4) adding the second liquid into the mixture obtained in step (2) slowly in small amount for several times while stirring, and adding flos Lonicerae extract, radix Sophorae Flavescentis extract, tea tree essential oil and dried Ginseng radix and flos Lonicerae obtained in step (1) when the temperature is reduced to below 40 deg.C;
(5) stirring, demoulding after two days at room temperature, saponifying after one week, and cutting into blocks.
In the step (1), the honeysuckle flower drying comprises four stages:
the first stage is as follows: spreading flos Lonicerae into 1-2 cm thin layer, and oven drying at 30 deg.C for 1 hr;
and a second stage: the drying temperature is increased to 38 ℃, and the drying time is 5 hours;
and a third stage: raising the drying temperature to 45 ℃, maintaining for 6 hours and further dehydrating and drying the honeysuckle;
and a final stage: the drying temperature is raised to 55 ℃, and the drying time is 1 hour.
The honeysuckle is dried at low temperature, the temperature is gradually increased, the highest temperature is not more than 60 ℃, and the deterioration of flavonoid and iridoid chemical components in the honeysuckle can be effectively prevented.
In the step (1), the ginseng drying comprises four stages:
the first stage is as follows: spreading the ginseng with the length of 3-3.5 cm in a single layer, controlling the drying temperature at 30 ℃ and the drying time for 2 hours; not to be too dense to utilize ventilation to remove moisture.
And a second stage: the drying temperature is increased to 45 ℃, and the drying time is 7 hours;
and a third stage: the drying temperature is reduced to 38 ℃, and the drying temperature is maintained for 6 hours;
and a final stage: the drying temperature is raised to 45 ℃ and the drying time is 3 hours.
In the whole drying process of the ginseng, the relative humidity is 58-61%, the temperature and the air flow in the whole drying room are uniform through the hot air circulating part, the conditions of constant temperature and constant humidity are realized in the whole drying process, and the drying quality of the ginseng is very ensured. The drying temperature is repeatedly carried out from low to high and then from high to low until the phase and the drying degree meet the requirements. The dried ginseng has good quality, good color and high product grade.
Example 2
The traditional Chinese medicine soap for cleaning skin and removing mites comprises the following raw materials in parts by weight:
40 parts of water, 8 parts of glycerol, 6 parts of sorbitol, 6 parts of sucrose, 8 parts of propylene glycol, 10 parts of an enzyme stock solution, 10 parts of a sulfur extract, 5 parts of palm oil, 5 parts of olive oil, 5 parts of grape seed oil, 5 parts of coconut oil, 5 parts of lauric acid, 5 parts of stearic acid, 45 parts of sodium fatty acid, 8 parts of a honeysuckle extract, 8 parts of a sophora flavescens extract, 2 parts of tea tree essential oil, 1.2 parts of ginseng and 4 parts of honeysuckle.
The sodium fatty acid is sodium coconut oil fatty acid.
The preparation method of the honeysuckle extract comprises the following steps:
soaking flos Lonicerae in 15 times (v/w, ml/g) of water at 75 deg.C for 2 times, each for 1 hr, mixing extractive solutions, concentrating under reduced pressure at 70 deg.C to 3 times (v/w, ml/g) of flos Lonicerae weight, and drying under reduced pressure.
The preparation method of the sophora flavescens extract comprises the following steps:
cleaning radix Sophorae Flavescentis, breaking cell wall in cell wall breaking machine for 12min, adding 10 times of 50% ethanol solution, and performing ultrasonic treatment for 35 min; extracting for 150min by water bath reflux after the ultrasound is finished, wherein the extraction temperature is 65 ℃, collecting an extracting solution, adding 50% ethanol to immerse the medicine residues, extracting for 80min by water bath reflux for the second time, collecting an extracting solution, adding 50% ethanol to immerse the medicine residues, extracting for 80min by water bath reflux for the third time, extracting for 3 times in total, combining the extracting solutions of 3 times, filtering by a 10-micron filter membrane, concentrating the filtrate under reduced pressure at-0.09 Mpa and 55 ℃ to obtain a thick paste with the relative density of 1.30 at 60 ℃, and drying the thick paste under reduced pressure at-0.09 Mpa and 55 ℃ to obtain the traditional Chinese medicine.
A preparation method of a traditional Chinese medicine soap for cleaning skin and removing mites comprises the following steps:
(1) respectively drying Ginseng radix and flos Lonicerae;
(2) heating palm oil, olive oil, grape seed oil, coconut oil, lauric acid, stearic acid and sodium fatty acid to melt, continuously stirring, cooling to 50-70 ℃ at 20-50 rpm, and keeping the temperature;
(3) heating glycerol, sorbitol, sucrose, propylene glycol, ferment stock solution, and sulfur extract to melt, stirring, cooling to 20-50 deg.C at 20-50 rpm, and keeping the temperature;
(4) adding the second liquid into the mixture obtained in step (2) slowly in small amount for several times while stirring, and adding flos Lonicerae extract, radix Sophorae Flavescentis extract, tea tree essential oil and dried Ginseng radix and flos Lonicerae obtained in step (1) when the temperature is reduced to below 40 deg.C;
(5) stirring, demoulding after two days at room temperature, saponifying after one week, and cutting into blocks.
In the step (1), the honeysuckle flower drying comprises four stages:
the first stage is as follows: spreading flos Lonicerae into 2-3 cm thin layer, and oven drying at 35 deg.C for 2 hr;
and a second stage: the drying temperature is increased to 41 ℃, and the drying time is 7 hours;
and a third stage: raising the drying temperature to 50 ℃, and maintaining for 8 hours to further dehydrate and dry the honeysuckle;
and a final stage: the drying temperature is raised to 58 ℃ and the drying time is 2 hours.
The honeysuckle is dried at low temperature, the temperature is gradually increased, the highest temperature is not more than 60 ℃, and the deterioration of flavonoid and iridoid chemical components in the honeysuckle can be effectively prevented.
In the step (1), the ginseng drying comprises four stages:
the first stage is as follows: spreading the ginseng with the length of 3-3.5 cm in a single layer, controlling the drying temperature at 38 ℃ and the drying time for 2 hours; not to be too dense to utilize ventilation to remove moisture.
And a second stage: the drying temperature is increased to 50 ℃, and the drying time is 10 hours;
and a third stage: the drying temperature is reduced to 43 ℃, and the drying temperature is maintained for 8 hours;
and a final stage: the drying temperature is raised to 50 ℃ and the drying time is 6 hours.
In the whole drying process of the ginseng, the relative humidity is 58-61%, the temperature and the air flow in the whole drying room are uniform through the hot air circulating part, the conditions of constant temperature and constant humidity are realized in the whole drying process, and the drying quality of the ginseng is very ensured. The drying temperature is repeatedly carried out from low to high and then from high to low until the phase and the drying degree meet the requirements. The dried ginseng has good quality, good color and high product grade.
Example 3
The traditional Chinese medicine soap for cleaning skin and removing mites comprises the following raw materials in parts by weight:
30 parts of water, 6 parts of glycerol, 4 parts of sorbitol, 4 parts of sucrose, 6 parts of propylene glycol, 8 parts of an enzyme stock solution, 8 parts of a sulfur extract, 4 parts of palm oil, 4 parts of olive oil, 4 parts of grape seed oil, 4 parts of coconut oil, 4.5 parts of lauric acid, 4.5 parts of stearin, 40 parts of sodium fatty acid, 6 parts of a honeysuckle extract, 6 parts of a sophora flavescens extract, 1.5 parts of tea tree essential oil, 1 part of ginseng and 3 parts of honeysuckle.
The sodium fatty acid is sodium coconut oil fatty acid.
The preparation method of the honeysuckle extract comprises the following steps:
soaking flos Lonicerae in 12 times (v/w, ml/g) of water at 70 deg.C for 2 times, each for 1 hr, mixing extractive solutions, concentrating under reduced pressure at 67 deg.C to 2 times (v/w, ml/g) of flos Lonicerae weight, and drying under reduced pressure.
The preparation method of the sophora flavescens extract comprises the following steps:
cleaning radix Sophorae Flavescentis, breaking cell wall in cell wall breaking machine for 9min, adding 7 times of 50% ethanol solution, and performing ultrasonic treatment for 28 min; extracting for 110min by water bath reflux after the ultrasound is finished, wherein the extraction temperature is 55 ℃, collecting an extracting solution, adding 50% ethanol to immerse the medicine residues, extracting for 50min by water bath reflux for the second time, collecting an extracting solution, adding 50% ethanol to immerse the medicine residues, extracting for 50min by water bath reflux for the third time, extracting for 3 times in total, combining the extracting solutions of 3 times, filtering by a 10-micron filter membrane, concentrating the filtrate under reduced pressure at-0.09 Mpa and 55 ℃ to obtain a thick paste with the relative density of 1.30 at 60 ℃, and drying the thick paste under reduced pressure at-0.09 Mpa and 55 ℃ to obtain the traditional Chinese medicine.
A preparation method of a traditional Chinese medicine soap for cleaning skin and removing mites comprises the following steps:
(1) respectively drying Ginseng radix and flos Lonicerae;
(2) heating palm oil, olive oil, grape seed oil, coconut oil, lauric acid, stearic acid and sodium fatty acid to melt, continuously stirring, cooling to 50-70 ℃ at 20-50 rpm, and keeping the temperature;
(3) heating glycerol, sorbitol, sucrose, propylene glycol, ferment stock solution, and sulfur extract to melt, stirring, cooling to 20-50 deg.C at 20-50 rpm, and keeping the temperature;
(4) adding the second liquid into the mixture obtained in step (2) slowly in small amount for several times while stirring, and adding flos Lonicerae extract, radix Sophorae Flavescentis extract, tea tree essential oil and dried Ginseng radix and flos Lonicerae obtained in step (1) when the temperature is reduced to below 40 deg.C;
(5) stirring, demoulding after two days at room temperature, saponifying after one week, and cutting into blocks.
In the step (1), the honeysuckle flower drying comprises four stages:
the first stage is as follows: spreading flos Lonicerae into 1-3 cm thin layer, and oven drying at 30-35 deg.C for 1-2 hr;
and a second stage: raising the drying temperature to 38-41 ℃ and drying for 5-7 hours;
and a third stage: raising the drying temperature to 45-50 deg.C, maintaining for 6-8 hr to further dehydrate and dry flos Lonicerae;
and a final stage: the drying temperature is raised to 55-58 ℃ and the drying time is 1-2 hours.
The honeysuckle is dried at low temperature, the temperature is gradually increased, the highest temperature is not more than 60 ℃, and the deterioration of flavonoid and iridoid chemical components in the honeysuckle can be effectively prevented.
In the step (1), the ginseng drying comprises four stages:
the first stage is as follows: spreading the ginseng with the length of 4-6 cm in a single layer, controlling the drying temperature at 35-38 ℃ and the drying time for 2 hours; not to be too dense to utilize ventilation to remove moisture.
And a second stage: raising the drying temperature to 45-50 ℃ and the drying time to 9-10 hours;
and a third stage: the drying temperature is reduced to 38-43 ℃, and the drying temperature is maintained for 6-8 hours;
and a final stage: the drying temperature is raised to 45-50 ℃ and the drying time is 3-6 hours.
In the whole drying process of the ginseng, the relative humidity is 58-61%, the temperature and the air flow in the whole drying room are uniform through the hot air circulating part, the conditions of constant temperature and constant humidity are realized in the whole drying process, and the drying quality of the ginseng is very ensured. The drying temperature is repeatedly carried out from low to high and then from high to low until the phase and the drying degree meet the requirements. The dried ginseng has good quality, good color and high product grade.
Example 4
The traditional Chinese medicine soap for cleaning skin and removing mites comprises the following raw materials in parts by weight:
35 parts of water, 5 parts of glycerol, 4 parts of sorbitol, 4 parts of sucrose, 4.8 parts of propylene glycol, 6.5 parts of enzyme stock solution, 6.5 parts of sulfur extract, 3 parts of palm oil, 3 parts of olive oil, 3 parts of grape seed oil, 3 parts of coconut oil, 3.5 parts of lauric acid, 3 parts of stearin, 37 parts of sodium fatty acid, 4 parts of honeysuckle extract, 5.5 parts of sophora flavescens extract, 1.3 parts of tea tree essential oil, 1 part of ginseng and 3 parts of honeysuckle.
The sodium fatty acid is sodium coconut oil fatty acid.
The preparation method of the honeysuckle extract comprises the following steps:
soaking flos Lonicerae in 13 times (v/w, ml/g) of water at 75 deg.C for 2 times, each for 1 hr, mixing extractive solutions, concentrating under reduced pressure at 69 deg.C to 1.8 times (v/w, ml/g) of flos Lonicerae weight, and drying under reduced pressure.
The preparation method of the sophora flavescens extract comprises the following steps:
cleaning radix Sophorae Flavescentis, breaking cell wall in cell wall breaking machine for 10min, adding 50% ethanol solution with mass ratio of 8 times, and performing ultrasonic treatment for 30 min; extracting for 120min by water bath reflux after the ultrasound is finished, wherein the extraction temperature is 60 ℃, collecting an extracting solution, adding 50% ethanol to immerse the medicine residues, extracting for 60min by water bath reflux for the second time, collecting an extracting solution, adding 50% ethanol to immerse the medicine residues, extracting for 60min by water bath reflux for the third time, extracting for 3 times in total, combining the extracting solutions of 3 times, filtering by a 10-micron filter membrane, concentrating the filtrate under reduced pressure at-0.09 Mpa and 55 ℃ to obtain a thick paste with the relative density of 1.30 at 60 ℃, and drying the thick paste under reduced pressure at-0.09 Mpa and 55 ℃ to obtain the traditional Chinese medicine.
A preparation method of a traditional Chinese medicine soap for cleaning skin and removing mites comprises the following steps:
(1) respectively drying Ginseng radix and flos Lonicerae;
(2) heating palm oil, olive oil, grape seed oil, coconut oil, lauric acid, stearic acid and sodium fatty acid to melt, continuously stirring, cooling to 55 ℃, and keeping the temperature;
(3) heating glycerol, sorbitol, sucrose, propylene glycol, ferment stock solution, and sulfur extract to melt, stirring, rotating at 28 rpm, cooling to 30 deg.C, and keeping the temperature;
(4) adding the second liquid into the mixture obtained in step (2) slowly in small amount for several times while stirring, and adding flos Lonicerae extract, radix Sophorae Flavescentis extract, tea tree essential oil and dried Ginseng radix and flos Lonicerae obtained in step (1) when the temperature is reduced to below 40 deg.C;
(5) stirring, demoulding after two days at room temperature, saponifying after one week, and cutting into blocks.
In the step (1), the honeysuckle flower drying comprises four stages:
the first stage is as follows: spreading flos Lonicerae into 1-3 cm thin layer, and oven drying at 32 deg.C for 70 min;
and a second stage: raising the drying temperature to 38-41 ℃ and drying for 5-7 hours;
and a third stage: raising the drying temperature to 45-47 ℃, and maintaining for 7 hours to further dehydrate and dry the honeysuckle;
and a final stage: the drying temperature is raised to 55-58 ℃ and the drying time is 1-2 hours.
The honeysuckle is dried at low temperature, the temperature is gradually increased, the highest temperature is not more than 60 ℃, and the deterioration of flavonoid and iridoid chemical components in the honeysuckle can be effectively prevented.
In the step (1), the ginseng drying comprises four stages:
the first stage is as follows: spreading the ginseng with the length of 3-6 cm in a single layer, controlling the drying temperature at 30-34 ℃ and the drying time for 2 hours; not to be too dense to utilize ventilation to remove moisture.
And a second stage: the drying temperature is increased to 45-48 ℃, and the drying time is 7-8 hours;
and a third stage: the drying temperature is reduced to 38-40 ℃, and the drying is maintained for 7-8 hours;
and a final stage: the drying temperature is raised to 45-47 ℃ and the drying time is 3-6 hours.
In the whole drying process of the ginseng, the relative humidity is 58-61%, the temperature and the air flow in the whole drying room are uniform through the hot air circulating part, the conditions of constant temperature and constant humidity are realized in the whole drying process, and the drying quality of the ginseng is very ensured. The drying temperature is repeatedly carried out from low to high and then from high to low until the phase and the drying degree meet the requirements. The dried ginseng has good quality, good color and high product grade.
Example 5
The traditional Chinese medicine soap for cleaning skin and removing mites comprises the following raw materials in parts by weight:
20 parts of water, 4 parts of glycerol, 2 parts of sorbitol, 2 parts of sucrose, 4 parts of propylene glycol, 5 parts of an enzyme stock solution, 5 parts of a sulfur extract, 2 parts of palm oil, 2 parts of olive oil, 2 parts of grape seed oil, 2 parts of coconut oil, 2 parts of lauric acid, 2 parts of stearic acid, 35 parts of sodium fatty acid, 5 parts of a honeysuckle extract, 5 parts of a sophora flavescens extract, 1 part of tea tree essential oil, 0.6 part of ginseng and 2.5 parts of honeysuckle.
The sodium fatty acid is sodium coconut oil fatty acid.
The preparation method of the honeysuckle extract comprises the following steps:
soaking flos Lonicerae in 13 times (v/w, ml/g) of water at 70 deg.C for 2 times, each for 1 hr, mixing extractive solutions, concentrating under reduced pressure at 68 deg.C to 2.3 times (v/w, ml/g) of flos Lonicerae weight, and drying under reduced pressure.
The preparation method of the sophora flavescens extract comprises the following steps:
cleaning radix Sophorae Flavescentis, breaking cell wall in cell wall breaking machine for 11min, adding 9 times of 50% ethanol solution, and performing ultrasonic treatment for 32 min; extracting for 135min by water bath reflux after the ultrasound is finished, wherein the extraction temperature is 62 ℃, collecting an extracting solution, adding 50% ethanol to immerse the medicine residues, extracting for 70min by water bath reflux for the second time, collecting an extracting solution, adding 50% ethanol to immerse the medicine residues, extracting for 70min by water bath reflux for the third time, extracting for 3 times in total, combining the extracting solutions of 3 times, filtering by a 10-micron filter membrane, concentrating the filtrate under reduced pressure at-0.09 Mpa and 55 ℃ to obtain a thick paste with the relative density of 1.30 at 60 ℃, and drying the thick paste under reduced pressure at-0.09 Mpa and 55 ℃ to obtain the traditional Chinese medicine.
A preparation method of a traditional Chinese medicine soap for cleaning skin and removing mites comprises the following steps:
(1) respectively drying Ginseng radix and flos Lonicerae;
(2) heating palm oil, olive oil, grape seed oil, coconut oil, lauric acid, stearic acid and sodium fatty acid to melt, continuously stirring, cooling to 60 ℃, and preserving heat, wherein the materials are stirred continuously at 30 r/min;
(3) heating glycerol, sorbitol, sucrose, propylene glycol, ferment stock solution, and sulfur extract to melt, stirring, cooling to 60 deg.C for 30 r/min, and keeping the temperature;
(4) adding the second liquid into the mixture obtained in step (2) slowly in small amount for several times while stirring, and adding flos Lonicerae extract, radix Sophorae Flavescentis extract, tea tree essential oil and dried Ginseng radix and flos Lonicerae obtained in step (1) when the temperature is reduced to below 40 deg.C;
(5) stirring, demoulding after two days at room temperature, saponifying after one week, and cutting into blocks.
In the step (1), the honeysuckle flower drying comprises four stages:
the first stage is as follows: spreading flos Lonicerae into 2-3 cm thin layer, and oven drying at 33-35 deg.C for 90-120 min;
and a second stage: the drying temperature is increased to 40-41 ℃, and the drying time is 6-7 hours;
and a third stage: raising the drying temperature to 48-50 deg.C, maintaining for 6-7 hr to further dehydrate and dry flos Lonicerae;
and a final stage: the drying temperature is raised to 55-56 ℃, and the drying time is 1-2 hours.
The honeysuckle is dried at low temperature, the temperature is gradually increased, the highest temperature is not more than 60 ℃, and the deterioration of flavonoid and iridoid chemical components in the honeysuckle can be effectively prevented.
In the step (1), the ginseng drying comprises four stages:
the first stage is as follows: spreading the ginseng with the length of 3-6 cm in a single layer, controlling the drying temperature at 36-38 ℃ and the drying time for 2 hours; not to be too dense to utilize ventilation to remove moisture.
And a second stage: the drying temperature is increased to 46-48 ℃, and the drying time is 8-9 hours;
and a third stage: the drying temperature is reduced to 39-41 ℃ and maintained for 6-8 hours;
and a final stage: the drying temperature is raised to 46-48 ℃ and the drying time is 4-5 hours.
In the whole drying process of the ginseng, the relative humidity is 58-61%, the temperature and the air flow in the whole drying room are uniform through the hot air circulating part, the conditions of constant temperature and constant humidity are realized in the whole drying process, and the drying quality of the ginseng is very ensured. The drying temperature is repeatedly carried out from low to high and then from high to low until the phase and the drying degree meet the requirements. The dried ginseng has good quality, good color and high product grade.
First, the conventional performance evaluation was performed on the skin-cleansing and mite-removing traditional Chinese medicine soaps prepared in examples 1 to 5.
The Chinese medicinal soaps obtained in examples 1 to 5 were examined for appearance, smell, total effective content, moisture and volatile matter, free caustic alkali, total free alkali, chloride, total phosphorus pentoxide, and transparency with reference to QB/T2485-2008 (type II), and the test standards are shown in Table 1, and the test results are shown in Table 2.
TABLE 1 test standards
The actual measurement result of the marked item with a is the result converted according to the requirement specified in QB/T2485-2008.
Table 2 examples 1-5 the results of the measurements obtained according to the test criteria of table 1
Second, evaluation of mite-removing effect of the skin-cleansing and mite-removing traditional Chinese medicine soap prepared in examples 1 to 5
1. Test object
The skin-cleaning and mite-killing traditional Chinese medicine soap prepared in examples 1-5 and the commercially available oil-controlling, acne-removing and mite-killing soap for ziyutang and pharmacy are used as comparative examples, the traditional Chinese medicine soap prepared in examples 1-5 and the mite-killing soap for comparative examples are respectively diluted and dissolved with physiological saline to prepare an aqueous solution with the mass fraction of 1.0%, and the aqueous solution is used as a test sample solution, and one physiological saline is used as a blank control sample solution.
2. Test method
Each test sample solution and blank control sample solution were tested separately according to the following procedure:
① 3 covered glass jars with a bottom of 400mmx400mm side length and a height of 100mm were prepared as petri dishes, and a piece of sponge 10mm thick and about 200mm side length was placed in each petri dish.
② test sample solution was poured into each dish (the solution level is just above the sponge) and 0.05g of mite feed was added to each dish;
③ placing 200 live mites into each dish;
④ covering the upper cover of the culture dish, placing the culture dish in a constant temperature and humidity incubator, wherein the temperature is (25+2) deg.C, and the humidity is (75 + -5)%;
⑤ 24h later, the number of live mites in the dish was observed and recorded with a dissecting mirror.
The killing rate Y represents the average value of the numbers of the live mites of three blank control samples, T represents the average value of the numbers of the live mites of three test samples, Y is (B-T)/B is 100%, more than or equal to 95% of the samples have strong mite prevention effect, more than or equal to 80% of the samples have strong mite prevention effect, and more than or equal to 60% of the samples have mite prevention effect.
3. Test results
The results of the mite kill rate test are shown in table 3.
TABLE 3 mite kill Rate test results
As is apparent from table 3, the mite removing rate of the traditional Chinese medicine soaps prepared in examples 1 to 5 is as high as 97% or more, and the mite removing rate of the traditional Chinese medicine soaps prepared in examples 4 and 5 is as high as 99%, which is far higher than that of the commercially available mite removing soaps.
Third, bacteriostasis experiment
1. Test object
The skin-cleaning and mite-killing traditional Chinese medicine soap prepared in examples 1-5 and the commercially available oil-controlling, acne-removing and mite-killing soap for ziyuntang and pharmacy are used as comparative examples, and the traditional Chinese medicine soap of examples 1-5 and the mite-killing soap of the comparative examples are diluted and dissolved with physiological saline to prepare an aqueous solution with the mass fraction of 1.0%, and the aqueous solution is used as a test sample solution.
2. Test method
The tested strains are bacteria such as Escherichia coli (Escherichia coli), Staphylococcus aureus (Staphylococcus aureus) and Pseudomonas aeruginosa, Aspergillus niger (Aspergillus niger) and Propionibacterium acnes (Propionibacterium acnes) which are cultured under the conditions that the bacteria are cultured for 36-48 hours at 30-37 ℃ by using lecithin Tween 80-nutrient agar medium, the bacteria are cultured for 120 hours at 20-25 ℃ by using Bengal red medium, the Propionibacterium acnes are cultured for 24-48 hours at 20-25 ℃ by using potato glucose agar medium at 20-25 ℃, the bacteria concentration is diluted to 1.0 × 109CFU/m L, and the Propionibacterium acnes concentration is diluted to 1.0 × 109CFU/m L, Aspergillus niger concentration diluted to 1.0 × 107CFU/m L, respectively transferring 0.1m L of the above strain diluent to a plate containing a corresponding solid culture medium, uniformly coating by using a coating rod, placing 7 Oxford cups in each plate at equal intervals, adding 0.1m L into 6 Oxford cups as a test sample solution, adding 0.1m L of sterilized normal saline into the other Oxford cup as a negative control, placing the plate of Aspergillus niger and Propionibacterium acnes at 25 ℃ for culturing for 72 hours, and culturing the bacteriaThe plate was incubated at 37 ℃ for 72 hours. The diameter of the zone was measured using a vernier caliper and the results are shown in table 4.
TABLE 4 results of bacteriostatic experiments
The bacteriostatic experiment results show that the skin-cleaning mite-removing traditional Chinese medicine soap prepared by the invention has an obvious inhibitory effect on tested strains, and the diameters of the inhibition zones of the skin-cleaning mite-removing traditional Chinese medicine soap prepared by the embodiments 1-5 of the invention are more than two times larger than those of ginseng oil-control acne-removing mite-removing soap compared with escherichia coli, staphylococcus aureus, pseudomonas aeruginosa, aspergillus niger and propionibacterium acnes.
It will be apparent to those skilled in the art that various changes and modifications may be made in the present invention without departing from the spirit and scope of the invention. Thus, if such modifications and variations of the present invention fall within the scope of the claims of the present invention and their equivalents, the present invention is also intended to include such modifications and variations.
Claims (10)
1. The traditional Chinese medicine soap for cleaning skin and removing mites is characterized by comprising the following raw materials in parts by weight:
15-40 parts of water, 2-8 parts of glycerol, 1-6 parts of sorbitol, 1-6 parts of sucrose, 3-8 parts of propylene glycol, 2-10 parts of ferment stock solution, 2-10 parts of sulfur extract, 1-5 parts of palm oil, 1-5 parts of olive oil, 1-5 parts of grape seed oil, 1-5 parts of coconut oil, 1-5 parts of lauric acid, 1-5 parts of stearic acid, 30-45 parts of sodium fatty acid, 3-8 parts of honeysuckle extract, 3-8 parts of sophora flavescens extract, 0.2-2 parts of tea tree essential oil, 0.1-1.2 parts of ginseng and 1-4 parts of honeysuckle.
2. The traditional Chinese medicine soap for cleaning skin and removing mites as claimed in claim 1, which comprises the following raw materials in parts by weight:
15 parts of water, 2 parts of glycerol, 1 part of sorbitol, 1 part of sucrose, 3 parts of propylene glycol, 2 parts of an enzyme stock solution, 2 parts of a sulfur extract, 1 part of palm oil, 1 part of olive oil, 1 part of grape seed oil, 1 part of coconut oil, 1 part of lauric acid, 1 part of stearic acid, 30 parts of sodium fatty acid, 3 parts of a honeysuckle extract, 3 parts of a sophora flavescens extract, 0.2 part of tea tree essential oil, 0.1 part of ginseng and 1 part of honeysuckle.
3. The traditional Chinese medicine soap for cleaning skin and removing mites as claimed in claim 1, which comprises the following raw materials in parts by weight:
40 parts of water, 8 parts of glycerol, 6 parts of sorbitol, 6 parts of sucrose, 8 parts of propylene glycol, 10 parts of an enzyme stock solution, 10 parts of a sulfur extract, 5 parts of palm oil, 5 parts of olive oil, 5 parts of grape seed oil, 5 parts of coconut oil, 5 parts of lauric acid, 5 parts of stearic acid, 45 parts of sodium fatty acid, 8 parts of a honeysuckle extract, 8 parts of a sophora flavescens extract, 2 parts of tea tree essential oil, 1.2 parts of ginseng and 4 parts of honeysuckle.
4. The traditional Chinese medicine soap for cleaning skin and removing mites as claimed in claim 1, which comprises the following raw materials in parts by weight:
35 parts of water, 5 parts of glycerol, 4 parts of sorbitol, 4 parts of sucrose, 4.8 parts of propylene glycol, 6.5 parts of enzyme stock solution, 6.5 parts of sulfur extract, 3 parts of palm oil, 3 parts of olive oil, 3 parts of grape seed oil, 3 parts of coconut oil, 3.5 parts of lauric acid, 3 parts of stearin, 37 parts of sodium fatty acid, 4 parts of honeysuckle extract, 5.5 parts of sophora flavescens extract, 1.3 parts of tea tree essential oil, 0.8 part of ginseng and 2 parts of honeysuckle.
5. The skin-cleaning mite-killing traditional Chinese medicine soap as claimed in claim 1, wherein the sodium fatty acid is sodium coconut oil fatty acid.
6. The skin-cleaning mite-killing traditional Chinese medicine soap as claimed in claim 1, wherein the preparation method of the honeysuckle extract comprises the following steps:
soaking flos Lonicerae in 10-15 times (v/w, ml/g) of water at 70 deg.C or 75 deg.C for 2 times, each for 1 hr, mixing extractive solutions, concentrating under reduced pressure at 65-70 deg.C to 1.5-3 times (v/w, ml/g) of flos Lonicerae weight, and drying under reduced pressure.
7. The traditional Chinese medicine soap for cleaning skin and removing mites as claimed in claim 1, wherein the preparation method of the sophora flavescens extract comprises the following steps:
cleaning radix Sophorae Flavescentis, breaking cell wall in cell wall breaking machine for 8-12min, adding 6-10 times of 50% ethanol solution, and performing ultrasonic treatment for 25-35 min; extracting for 90-150min by water bath reflux after the ultrasound is finished, wherein the extraction temperature is 50-65 ℃, collecting the extracting solution, adding 50% of ethanol to immerse the medicine residues, extracting for 40-80min by water bath reflux for the second time, collecting the extracting solution, adding 50% of ethanol to immerse the medicine residues, extracting for 40-80min by water bath reflux for the third time, extracting for 3 times in total, combining the extracting solutions for 3 times, filtering by a 10-micron filter membrane, concentrating the filtrate under reduced pressure at-0.09 Mpa and 55 ℃ to obtain a thick paste with the relative density of 1.30 at 60 ℃, and drying the thick paste under reduced pressure at-0.09 Mpa and 55 ℃ to obtain the traditional Chinese medicine.
8. A preparation method of a traditional Chinese medicine soap for cleaning skin and removing mites is characterized by comprising the following steps:
(1) respectively drying Ginseng radix and flos Lonicerae;
(2) heating palm oil, olive oil, grape seed oil, coconut oil, lauric acid, stearic acid and sodium fatty acid to melt, continuously stirring, cooling to 50-70 ℃ at 20-50 rpm, and keeping the temperature;
(3) heating glycerol, sorbitol, sucrose, propylene glycol, ferment stock solution, and sulfur extract to melt, stirring, cooling to 20-50 deg.C at 20-50 rpm, and keeping the temperature;
(4) adding the second liquid into the mixture obtained in step (2) slowly in small amount for several times while stirring, and adding flos Lonicerae extract, radix Sophorae Flavescentis extract, tea tree essential oil and dried Ginseng radix and flos Lonicerae obtained in step (1) when the temperature is reduced to below 40 deg.C;
(5) stirring, demoulding after two days at room temperature, saponifying after one week, and cutting into blocks.
9. The method for preparing the traditional Chinese medicine soap for cleaning skin and removing mites as claimed in claim 8, wherein in the step (1), the drying of the honeysuckle comprises four stages:
the first stage is as follows: spreading flos Lonicerae into 1-3 cm thin layer, and oven drying at 30-35 deg.C for 1-2 hr;
and a second stage: raising the drying temperature to 38-41 ℃ and drying for 5-7 hours;
and a third stage: raising the drying temperature to 45-50 deg.C, maintaining for 6-8 hr to further dehydrate and dry flos Lonicerae;
and a final stage: the drying temperature is raised to 55-58 ℃ and the drying time is 1-2 hours.
10. The method for preparing a traditional Chinese medicine soap for cleaning skin and removing mites as claimed in claim 1, wherein in the step (1), the drying of ginseng comprises four stages:
the first stage is as follows: spreading the ginseng with the length of 3-6 cm in a single layer, controlling the drying temperature at 30-38 ℃ and the drying time for 2 hours; not to be too dense, so as to utilize ventilation to eliminate moisture;
and a second stage: raising the drying temperature to 45-50 ℃ and the drying time to 7-10 hours;
and a third stage: the drying temperature is reduced to 38-43 ℃, and the drying temperature is maintained for 6-8 hours;
and a final stage: the drying temperature is raised to 45-50 ℃ and the drying time is 3-6 hours.
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Application publication date: 20200728 |