CN111407799A - Multifunctional essential oil and preparation method thereof - Google Patents
Multifunctional essential oil and preparation method thereof Download PDFInfo
- Publication number
- CN111407799A CN111407799A CN202010235893.3A CN202010235893A CN111407799A CN 111407799 A CN111407799 A CN 111407799A CN 202010235893 A CN202010235893 A CN 202010235893A CN 111407799 A CN111407799 A CN 111407799A
- Authority
- CN
- China
- Prior art keywords
- essential oil
- stirring
- multifunctional
- oil
- temperature
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
Images
Classifications
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/53—Lamiaceae or Labiatae (Mint family), e.g. thyme, rosemary or lavender
- A61K36/534—Mentha (mint)
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/53—Lamiaceae or Labiatae (Mint family), e.g. thyme, rosemary or lavender
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/53—Lamiaceae or Labiatae (Mint family), e.g. thyme, rosemary or lavender
- A61K36/532—Agastache, e.g. giant hyssop
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/61—Myrtaceae (Myrtle family), e.g. teatree or eucalyptus
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K9/00—Medicinal preparations characterised by special physical form
- A61K9/0012—Galenical forms characterised by the site of application
- A61K9/007—Pulmonary tract; Aromatherapy
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61P—SPECIFIC THERAPEUTIC ACTIVITY OF CHEMICAL COMPOUNDS OR MEDICINAL PREPARATIONS
- A61P11/00—Drugs for disorders of the respiratory system
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61P—SPECIFIC THERAPEUTIC ACTIVITY OF CHEMICAL COMPOUNDS OR MEDICINAL PREPARATIONS
- A61P17/00—Drugs for dermatological disorders
- A61P17/04—Antipruritics
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61P—SPECIFIC THERAPEUTIC ACTIVITY OF CHEMICAL COMPOUNDS OR MEDICINAL PREPARATIONS
- A61P25/00—Drugs for disorders of the nervous system
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61P—SPECIFIC THERAPEUTIC ACTIVITY OF CHEMICAL COMPOUNDS OR MEDICINAL PREPARATIONS
- A61P25/00—Drugs for disorders of the nervous system
- A61P25/20—Hypnotics; Sedatives
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61P—SPECIFIC THERAPEUTIC ACTIVITY OF CHEMICAL COMPOUNDS OR MEDICINAL PREPARATIONS
- A61P29/00—Non-central analgesic, antipyretic or antiinflammatory agents, e.g. antirheumatic agents; Non-steroidal antiinflammatory drugs [NSAID]
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61P—SPECIFIC THERAPEUTIC ACTIVITY OF CHEMICAL COMPOUNDS OR MEDICINAL PREPARATIONS
- A61P7/00—Drugs for disorders of the blood or the extracellular fluid
- A61P7/10—Antioedematous agents; Diuretics
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q13/00—Formulations or additives for perfume preparations
Abstract
The invention belongs to the technical field of compound essential oil, and discloses multifunctional essential oil and a preparation method thereof. The method comprises the following steps: sequentially mixing peppermint essential oil, eucalyptus essential oil, lavender essential oil, clove essential oil, balm essential oil, rosemary essential oil and patchouli essential oil, heating, cooling and standing to obtain the multifunctional essential oil. The multifunctional essential oil comprises the following components in percentage by weight: 20-40% of mint essential oil, 5-15% of eucalyptus essential oil, 15-25% of lavender essential oil, 5-15% of clove essential oil, 5-15% of melissa essential oil, 5-15% of rosemary essential oil and 5-15% of patchouli essential oil. The multifunctional essential oil has strong penetrating power and unique fragrance, and when the multifunctional essential oil is used, the fragrance of the essential oil has layering effect and is long in retention time; for relieving viscera; preventing common cold, relieving dizziness and headache, and relieving car and sea sickness; relieving swelling and itching; promoting blood circulation by removing blood stasis and having good effect on traumatic injury.
Description
Technical Field
The invention belongs to the technical field of compound essential oil, and particularly relates to multifunctional essential oil and a preparation method thereof.
Background
The essential oil is volatile aromatic substance extracted from flower, leaf, stem, root or fruit of plant by steam distillation, squeezing, cold soaking or solvent extraction, and has volatility, and can enter body via nasal cavity and respiratory tract, and then directly deliver it to brain to regulate emotion and improve skin. The existing essential oil has the single effects of stopping dizziness and headache, stopping carsickness, relieving itching, diminishing inflammation and the like in function, has certain limitations, and cannot meet more requirements of people.
The compound essential oil is prepared according to different characteristics of various plant essential oils, and the compound essential oil is prepared according to a certain proportion for use, so that the effect of the single essential oil can be exerted to the maximum. In the compounding process of the essential oil, not only the absorption effect of the essential oil but also the fragrance harmony and the compatibility of the essential oil are considered. However, the existing compound essential oil is only prepared by simply mixing single essential oil, which is not beneficial to preparing the compound essential oil with better effect and unique fragrance.
Disclosure of Invention
In order to overcome the defects and shortcomings of the prior art, the invention aims to provide the multifunctional essential oil and the preparation method thereof. The essential oil of the invention has the functions of relieving viscera; preventing dizziness and headache caused by cold, and stopping carsickness and seasickness; preventing mosquito bite and rapid metabolism after mosquito bite, relieving swelling and itching; promoting blood circulation for removing blood stasis, and can be used for treating traumatic injury. By the method, the prepared essential oil has the advantages that the components are mutually synergistic, the penetrating power is strong, and the effect is better compared with the existing essential oil; the essential oil of the present invention has a pleasant aromatic odor; when in use, the essential oil has layering fragrance and long retention time.
The purpose of the invention is realized by the following technical scheme:
the multifunctional essential oil comprises the following components in percentage by weight:
the multifunctional essential oil preferably comprises the following components in percentage by weight:
the multifunctional essential oil more preferably comprises the following components in percentage by weight:
the mint essential oil is peppermint essential oil; the clove essential oil is clove bud essential oil.
Preferably, the mint essential oil is peppermint essential oil, and the trade name is: the pure essential oil of Peppermint, Peppermint oilpitita, is produced in India.
The eucalyptus essential oil is eucalyptus ( collagen eucalyptus) essential oil, trade name: eucalyptus globulus Oil, origin India.
The clove essential oil is pure clove bud essential oil, and the trade name is as follows: clove Oil, origin: india.
The melissa officinalis essential oil is melissa officinalis leaf oil, and the trade name is as follows: melissa oil, origin: india.
The rosemary essential oil is rosemary leaf oil, and the trade name is as follows: rosemary oil, origin: india.
The product name of the patchouli essential oil is as follows: patchouli oil dark, origin: india.
The lavender essential oil has a trade name: lavender essential oil, origin: the united states.
The preparation method of the multifunctional essential oil comprises the following steps:
sequentially adding peppermint essential oil, eucalyptus essential oil, lavender essential oil, clove essential oil, melissa essential oil, rosemary essential oil and patchouli essential oil, and adding one of the essential oils and stirring uniformly to obtain mixed essential oil; and heating the mixed essential oil at the heating temperature of 30-48 ℃, preserving the heat for 30-60 min, cooling, and standing for more than 12h to obtain the multifunctional essential oil.
The heating treatment is preferably temperature programmed treatment, the temperature programmed treatment is carried out under the condition that the temperature is raised to 30-38 ℃, the heat preservation treatment is carried out for 15-25 min, the temperature is continuously raised to 40-48 ℃, and the heat preservation treatment is carried out for 25-35 min; preferably, slowly heating from room temperature to 32-36 ℃, carrying out heat preservation treatment for 15-25 min, continuously heating to 42-46 ℃, and carrying out heat preservation treatment for 25-35 min; more preferably, the temperature is slowly increased from room temperature to 35 ℃, the heat preservation treatment is carried out for 20min, the temperature is continuously increased to 45 ℃, and the heat preservation treatment is carried out for 30 min.
The standing time is 20-36 h, preferably 24 h.
The cooling means cooling to 30 ℃.
Further preferably, the preparation method of the multifunctional essential oil comprises the following steps:
stirring peppermint essential oil and eucalyptus essential oil at a high speed, and then stirring at a low speed; adding lavender essential oil, stirring at high speed, and stirring at low speed; adding the clove essential oil, stirring at a high speed, and then stirring at a low speed; adding Melissa officinalis, stirring at high speed, stirring at low speed, adding Rosemary, stirring at high speed, stirring at low speed, adding herba Agastaches, stirring at high speed, and stirring at low speed; and then slowly heating under the condition of stirring, cooling and standing to obtain the multifunctional essential oil.
The high-speed stirring speed is 2000-4000 r/min, preferably 3000 r/min; the rotating speed of the low-speed stirring is 40-60 r/min, and preferably 50 r/min.
The high-speed stirring time is 2-4 min, preferably 3 min; the low-speed stirring time is 4-10 min, preferably 5 min.
The raw materials used by the invention are 7 plant essential oils, and different plant essential oils contain different chemical components (compounds such as aliphatic, aromatic and terpenoid), when various plant essential oils are mixed one by one according to a specific sequence, plant molecules in the latter essential oil and plant molecules in the former essential oil can be fully fused, and the specific aromatic molecules in the latter essential oil interact to generate unique fragrance, and then heating treatment is carried out, so that the fully fused plant essential oil molecules react, and then static precipitation is carried out, so that the molecules are balanced, and the problem of repellence of different molecules is solved. The compound essential oil prepared by the invention has strong penetrating power and unique fragrance, and when the compound essential oil is used, the fragrance of the essential oil has layering sense and is long in retention time; meanwhile, the essential oil is clear and transparent liquid, has no layering and is not turbid.
The multifunctional essential oil provided by the invention is mainly prepared from mint essential oil, the strong penetrating power of the mint essential oil is used for promoting the eucalyptus essential oil, the lavender essential oil, the clove essential oil, the balm essential oil, the rosemary essential oil and the patchouli essential oil to be absorbed more easily, and the curative effect of the essential oil is enhanced through the mutual coordination and mutual synergistic effect of the mint essential oil, the eucalyptus essential oil, the clove essential oil, the balm essential oil, the rosemary essential oil and the patchouli essential oil. By the preparation method, the obtained multifunctional essential oil can relieve internal organs; preventing common cold, relieving dizziness and headache, and relieving car and sea sickness; relieving swelling and itching; has good efficacy of promoting blood circulation and removing blood stasis.
Compared with the prior art, the essential oil has the following advantages and beneficial effects:
1) the multifunctional essential oil has strong permeability and unique fragrance, enables people to be fresh, cool, pleasant and comfortable, and has layered fragrance when being used, and the fragrance retention time is more than 2 hours;
2) the multifunctional essential oil of the invention can relieve viscera; preventing common cold, relieving dizziness and headache, and relieving car and sea sickness; relieving swelling and itching; promoting blood circulation by removing blood stasis and having good effect on traumatic injury.
Drawings
FIG. 1 is a chromatogram of Indian peppermint essential oil;
FIG. 2 is a chromatogram of Eucalyptus essential oil;
FIG. 3 is a chromatogram of Melissa officinalis essential oil;
FIG. 4 is a chromatogram of rosemary essential oil;
FIG. 5 is a chromatogram of patchouli essential oil;
FIG. 6 is a chromatogram of lavender essential oil;
FIG. 7 is a chromatogram of clove essential oil.
Detailed Description
The present invention will be described in further detail with reference to specific examples, but the embodiments of the present invention are not limited thereto.
The mint essential oil is peppermint essential oil, and the trade name is as follows: the pure essential oil of Peppermint, Peppermint oilpitita, is produced in India. Odor type: a vanilla type; odor intensity: the volatility is high; description of the odor: cool and powerful penetrating power, and refreshing (the natural menthol extracted from the mint is levorotatory and has cool and pungent penetrating smell); the color of the essential oil is shown: a pale yellow to colorless flowing liquid.
The mint essential oil in the examples is peppermint essential oil (peppermint oil-K-9071-KE-2019) supplied by katyani exports from India, and its chromatogram is shown in FIG. 1, and its components and contents are shown in Table 1.
Table 1 shows the content and distribution of the components of the Indian peppermint essential oil
The Eucalyptus essential Oil is Eucalyptus Globulus Oil ( Eucalyptus Globulus Oil, Indian, produced by Katyani exporters, Eucalyptus Globulus Oil-KE-L ot No. K-2300-KE-2011), the specific gravity is 0.905-0.9250 @20 ℃, the refractive index is 1.457-1.467 @20 ℃, the chromatogram thereof is shown in FIG. 2, the components and the content thereof are shown in Table 2, and the rest components are contained in addition to the components contained in Table 2.
TABLE 2 ingredients and contents of Eucalyptus essential oils
The melissa leaf essential oil is melissa leaf oil, and the trade name is as follows: melissa oil, origin: india. Melissa officinalis essential Oil (Melissa Oil, product model KE-1920), Melissa Pure essential Oil, supplied by katyaniexports. Odor type: and (4) herbal type. Odor intensity: the volatilization is fast. Description of the odor: fresh, sweet and delicate honey fragrance and citral herbal flavor, unique, natural and comfortable fragrance and aroma, and can be prepared by non-artificial method. The color of the essential oil is shown: light yellow clear flowing liquid. The specific gravity is 0.869-0.896 @20 ℃. The refractive index is 1.483-1.489 @20 ℃. The chromatogram thereof is shown in FIG. 3, and the components and contents thereof are shown in Table 3.
TABLE 3 ingredients and contents of Melissa essential oil
The rosemary essential oil is rosemary leaf oil, and the trade name is as follows: rosemary oil, origin: india. Rosemary Oil (Rosemary Oil, product model KE-7761) supplied by katyaniexports. Odor type: a herbaceous plant type; odor intensity: fast volatilization, odor description: has strong camphor-like and cool eudesmol fragrance and penetrating power; the color of the essential oil is shown: a light yellow to colorless liquid; specific gravity: 0.895-0.905 @20 ℃. Refractive index: 1.465 to 1.467@20 ℃. The chromatogram thereof is shown in FIG. 4, and the components and contents thereof are shown in Table 4.
TABLE 4 Rosemary oil composition and content
The product name of the patchouli essential oil is as follows: patchouli oil dark, origin: india. Patchouli essential Oil in the examples Patchouli essential Oil supplied by katyani exports (Patchouli Oil Dark, Patchouli Oil, product model KE-5623). Odor type: dried grass type. Odor intensity: slow volatility (can fix fragrance). Description of the odor: the fragrance of smoke and local smell (special fragrance). Specific gravity: 0.95-0.975 @20 ℃. Refractive index: 1.499-1.515 @20 ℃. The chromatogram thereof is shown in FIG. 5, and the components and contents thereof are shown in Table 5.
TABLE 5 composition and content of patchouli essential oil
In the examples, the lavender essential oil is American lavender essential oil, L averder OI L.
The chromatogram of the lavender essential oil, which is available from I L Health and BeautyNatural Oils Co., Inc., of USA, is shown in FIG. 6, and the components and contents are shown in Table 6, except the components contained in Table 6, the balance being other components.
TABLE 6 Lavender essential oil composition and content
The Clove essential Oil is Clove bud essential Oil, the trade name of which is Clove Oil, the origin of which is Indian, Clove essential Oil provided by katyani exports (Clove Oil, Clove Oil-KE-L ot No. K-5703-KE-2011), the specific gravity of which is 1.027-1.065 @20 ℃, the refractive index of which is 1.527-1.538 @20 ℃, the smell type of which is spice piquancy, the smell intensity of which is moderate in volatilization, the smell of which is described as round, smooth and warm spicy, has unique, natural and comfortable fragrance and note, and can be prepared by non-manual work, the chromatogram is shown in FIG. 7, and the components and the contents are shown in Table 7.
TABLE 7 ingredients and contents of clove essential oil
Example 1
The multifunctional essential oil comprises the following components in percentage by weight:
30% of mint essential oil, 10% of eucalyptus essential oil, 20% of lavender essential oil, 10% of clove essential oil, 10% of melissa essential oil, 10% of rosemary essential oil and 10% of pogostemon cablin essential oil.
The preparation method of the multifunctional essential oil comprises the following steps:
stirring peppermint essential oil and Eucalyptus essential oil at 3000r/min for homogenizing for 3min, and stirring at 50r/min for 5 min; adding lavender essential oil, stirring at 3000r/min for homogenizing for 3min, and stirring at 50r/min for 5 min; adding flos Caryophylli essential oil, stirring at 3000r/min for homogenizing for 3min, and stirring at 50r/min for 5 min; adding Melissa officinalis essential oil, stirring at 3000r/min for homogenizing for 3min, and stirring at 50r/min for 5 min; adding rosemary essential oil, stirring and homogenizing at 3000r/min for 3min, and stirring at 50r/min for 5 min; finally adding patchouli essential oil, stirring and homogenizing at the rotating speed of 3000r/min for 3min, and then stirring at the rotating speed of 50r/min for 5 min; slowly heating to 35 deg.C under stirring, stirring for 20min, slowly heating to 45 deg.C, stirring for 30min, cooling to 30 deg.C with cooling water, filtering with 300 mesh filter cloth, standing for 24h, inspecting, and packaging to obtain multifunctional essential oil.
The compound essential oil prepared by the invention has strong penetrating power and unique fragrance, and when the compound essential oil is used, the fragrance of the essential oil has layering sense and is long in retention time; meanwhile, the essential oil is clear and transparent liquid, has no layering and is not turbid.
Comparative example 1 (different order of raw material addition)
The present embodiment is different from embodiment 1 in that:
the adding sequence of the raw materials is as follows: 1. lavender essential oil; 2. clove essential oil; 3. melissa officinalis essential oil; 4. eucalyptus essential oil; 5. patchouli essential oil; 6. rosemary essential oil; 7. and (4) mint essential oil.
Comparative example 2 (No heating process)
The present embodiment is different from embodiment 1 in that: no heat treatment was performed.
Comparative example 3 (ordinary heating)
The present embodiment is different from embodiment 1 in that: adding herba Agastaches essential oil, stirring, heating to 35 deg.C, keeping the temperature for 30min, cooling, filtering, and standing for 24 hr.
Example 2
The multifunctional essential oil comprises the following components in percentage by weight:
20% of mint essential oil, 10% of eucalyptus essential oil, 20% of lavender essential oil, 10% of clove essential oil, 15% of melissa essential oil, 15% of rosemary essential oil and 10% of pogostemon cablin essential oil.
The preparation method of the multifunctional essential oil comprises the following steps:
stirring peppermint essential oil and Eucalyptus essential oil at 3000r/min for homogenizing for 3min, and stirring at 50r/min for 5 min; adding lavender essential oil, stirring at 3000r/min for homogenizing for 3min, and stirring at 50r/min for 5 min; adding flos Caryophylli essential oil, stirring at 3000r/min for homogenizing for 3min, and stirring at 50r/min for 5 min; adding Melissa officinalis essential oil, stirring at 3000r/min for homogenizing for 3min, and stirring at 50r/min for 5 min; adding rosemary essential oil, stirring and homogenizing at 3000r/min for 3min, and stirring at 50r/min for 5 min; finally adding patchouli essential oil, stirring and homogenizing at the rotating speed of 3000r/min for 3min, and then stirring at the rotating speed of 50r/min for 5 min; slowly heating to 35 deg.C under stirring, stirring for 20min, slowly heating to 45 deg.C, stirring for 30min, cooling to 30 deg.C with cooling water, filtering with 300 mesh filter cloth, standing for 24h, inspecting, and packaging to obtain multifunctional essential oil.
Example 3
The multifunctional essential oil comprises the following components in percentage by weight:
40% of mint essential oil, 15% of eucalyptus essential oil, 20% of lavender essential oil, 5% of clove essential oil, 10% of melissa essential oil, 5% of rosemary essential oil and 5% of patchouli essential oil.
The preparation method of the multifunctional essential oil comprises the following steps:
stirring peppermint essential oil and Eucalyptus essential oil at 3000r/min for homogenizing for 3min, and stirring at 50r/min for 5 min; adding lavender essential oil, stirring at 3000r/min for homogenizing for 3min, and stirring at 50r/min for 5 min; adding flos Caryophylli essential oil, stirring at 3000r/min for homogenizing for 3min, and stirring at 50r/min for 5 min; adding Melissa officinalis essential oil, stirring at 3000r/min for homogenizing for 3min, and stirring at 50r/min for 5 min; adding rosemary essential oil, stirring and homogenizing at 3000r/min for 3min, and stirring at 50r/min for 5 min; finally adding patchouli essential oil, stirring and homogenizing at the rotating speed of 3000r/min for 3min, and then stirring at the rotating speed of 50r/min for 5 min; slowly heating to 35 deg.C under stirring, stirring for 20min, slowly heating to 45 deg.C, stirring for 30min, cooling to 30 deg.C with cooling water, filtering with 300 mesh filter cloth, standing for 24h, inspecting, and packaging to obtain multifunctional essential oil.
And (3) testing the effect:
first, penetrating power
The target is as follows: penetrability, human body test feedback, essential oil penetrating to the vertex, stomach and viscera in a short time.
Testing the population: volunteers 20-45 years old were divided into 6 groups of 20 persons each.
The using method comprises the following steps: the compound essential oil is smeared on the palm and smells fragrance.
Penetration force effect: and 5, dividing: the penetrating power is strong, and a large amount of essential oil can penetrate to the top of the head, the stomach and viscera in a short time; and 4, dividing: the penetrating power is strong; and 3, dividing: the penetrating power is normal; and 2, dividing: the penetrating power is weak; 0 minute: no penetrating power.
The penetration effect was scored as 100 points full. The effect feedback situation is shown in table 8.
Second, fragrance
(1) The target is as follows: fragrance, pleasant and pleasant in sense; feeling the mood, being happy and comfortable.
Testing the population: volunteers 20-45 years old were divided into 6 groups of 20 persons each.
The using method comprises the following steps: the compound essential oil is smeared on the palm and smells fragrance. Each person scored the fragrance according to the pleasure and pleasure degree, with a maximum of 10 points and a minimum of 0 points. The average score was calculated for each group. The test results are shown in table 8.
(2) Sense of layering
The test method comprises the following steps: the compound essential oil is smeared in the palm, and people can feel whether the fragrance has layering feeling and what layering feeling when smelling the fragrance and using the heart. Note: the fragrance of the compound essential oil is basically given out simultaneously, but the layering sense of the compound essential oil with different processes and formulas is different when the compound essential oil is used for a heart. The hierarchical perception is divided into the front tone, the middle tone and the rear tone; the first is the former key, the last is the latter key, and the middle is the middle key. The results of the layering test are shown in table 8.
(3) Durability
The test method comprises the following steps: the compound essential oil is dropped on the paper for smelling fragrance (2 drops), and the fragrance condition on the paper for smelling fragrance is checked (including smelling) at certain intervals. The results of the fragrance longevity test are shown in table 8.
Third, appearance
Appearance index: appearance of the essential oil liquid: clear, transparent, not turbid, not layered.
The appearance of the complex essential oils of examples 1 to 3 and comparative examples 1 to 3 is shown in table 9.
TABLE 8 test results of penetration and fragrance of composite essential oils
TABLE 9 composite essential oil Properties, odor, and like parameters
Fourthly, 20 people with carsickness history are selected for carsickness stopping, the trolley is adopted to drive 30 kilometers, a small roadblock (prompting to step on the brake for deceleration) is arranged every 5 kilometers, one group (10 people) is coated with compound essential oil, and one group (10 people) is not coated with the essential oil, so that carsickness conditions are observed:
TABLE 10 Compound essential oil carsickness prevention situation
Fifth, mosquito expelling
The test method comprises the following steps: the belly and the back of the small rabbit are unhaired by health, the part which is not unhaired below the belly and the back is protected by thick cloth, then the two legs of the small rabbit are fixed in the mosquito cage, and the part which is not unhaired above the belly and the back of the small rabbit is positioned outside the mosquito cage through the round hole at the upper part of the mosquito cage and the sleeve part connected with the round hole. 100 female mosquitoes which did not suck blood were placed in the mosquito cage.
To determine the mosquito repelling effect, 9 rabbits were selected and divided into nine groups, one group was used as a control group, and the other 8 groups were coated with the compound essential oils prepared in examples 1 to 2 and comparative examples 1 to 6 on the backs and the abdomens of the unhaired rabbits, respectively, and the number of bites of the rabbits by mosquitoes was observed for 1 hour, 2 hours, 4 hours, 6 hours, 8 hours, 10 hours, and 12 hours, and the protection rate of the essential oils (effective protection rate (%) (number of bites by mosquitoes in the control group-number of bites by mosquitoes in the experimental group)/number of bites by mosquitoes in the control group) was calculated as × 100%, and the test results are shown in table 11.
TABLE 11 mosquito repellent Condition of Compound essential oils
1 hour | 2 hours | 4 |
6 |
8 |
10 | |
Blank group | ||||||
0 | 0 | 0 | 0 | 0 | 0 | |
Example 1 | 100% | 100% | 100% | 100% | 97% | 90% |
Example 2 | 100% | 100% | 100% | 100% | 92% | 86% |
Example 3 | 100% | 100% | 100% | 96% | 90% | 85% |
Comparative example 1 | 100% | 95% | 90% | 86% | 81% | 75% |
Comparative example 2 | 100% | 96% | 89% | 85% | 78% | 72% |
Comparative example 3 | 100% | 100% | 100% | 100% | 94% | 85% |
The multifunctional essential oil has strong penetrating power and unique fragrance, and when the multifunctional essential oil is used, the fragrance of the essential oil has layering effect and is long in retention time; for relieving viscera; preventing common cold, relieving dizziness and headache, and relieving car and sea sickness; relieving swelling and itching; promoting blood circulation by removing blood stasis and having good effect on traumatic injury.
Claims (10)
1. The preparation method of the multifunctional essential oil is characterized by comprising the following steps: the method comprises the following steps:
sequentially adding peppermint essential oil, eucalyptus essential oil, lavender essential oil, clove essential oil, melissa essential oil, rosemary essential oil and patchouli essential oil, and adding one of the essential oils and stirring uniformly to obtain mixed essential oil; heating the mixed essential oil at the heating temperature of 30-48 ℃, preserving heat for 30-60 min, cooling, and standing for more than 12h to obtain multifunctional essential oil;
the multifunctional essential oil comprises the following components in percentage by weight:
20-40% of mint essential oil
Eucalyptus oil 5-15%
15-25% of lavender essential oil
5-15% of clove essential oil
5-15% of melissa officinalis essential oil
5-15% of rosemary essential oil
5-15% of patchouli essential oil.
2. The method for preparing multifunctional essential oil according to claim 1, characterized in that:
the heating treatment is temperature programmed treatment, wherein the temperature programmed treatment comprises the steps of slowly raising the temperature from room temperature to 30-38 ℃, carrying out heat preservation treatment for 15-25 min, continuously raising the temperature to 40-48 ℃, and carrying out heat preservation treatment for 25-35 min.
3. The method for preparing multifunctional essential oil according to claim 2, characterized in that: the temperature programming condition is that the temperature is slowly increased from room temperature to 32-36 ℃, the heat preservation treatment is carried out for 15-25 min, the temperature is continuously increased to 42-46 ℃, and the heat preservation treatment is carried out for 25-35 min.
4. The method for preparing multifunctional essential oil according to claim 3, characterized in that: the temperature programming condition is that the temperature is slowly increased from room temperature to 35 ℃, the heat preservation treatment is carried out for 20min, the temperature is continuously increased to 45 ℃, and the heat preservation treatment is carried out for 30 min.
5. The method for preparing multifunctional essential oil according to claim 1, characterized in that: the standing time is 20-36 h.
6. The method for preparing multifunctional essential oil according to claim 1, characterized in that: the method comprises the following steps: stirring peppermint essential oil and eucalyptus essential oil at a high speed, and then stirring at a low speed; adding lavender essential oil, stirring at high speed, and stirring at low speed; adding the clove essential oil, stirring at a high speed, and then stirring at a low speed; adding Melissa officinalis, stirring at high speed, stirring at low speed, adding Rosemary, stirring at high speed, stirring at low speed, adding herba Agastaches, stirring at high speed, and stirring at low speed; and then slowly heating under the condition of stirring, cooling and standing to obtain the multifunctional essential oil.
7. The method for preparing the multifunctional essential oil according to claim 6, which is characterized in that: the high-speed stirring speed is 2000-4000 r/min; the rotating speed of the low-speed stirring is 40-60 r/min;
the high-speed stirring time is 2-4 min; the low-speed stirring time is 4-10 min.
8. The method for preparing multifunctional essential oil according to claim 1, characterized in that:
the multifunctional essential oil comprises the following components in percentage by weight:
mint essential oil 30%
Eucalyptus oil 10%
20 percent of lavender essential oil
Clove essential oil 10%
Melissa officinalis essential oil 10%
Rosemary oil 10%
10% of patchouli essential oil.
9. The method for preparing multifunctional essential oil according to claim 1, characterized in that: the mint essential oil is peppermint essential oil; the clove essential oil is clove bud essential oil.
10. A multifunctional essential oil obtained by the preparation method according to any one of claims 1 to 9.
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN202010235893.3A CN111407799A (en) | 2020-03-30 | 2020-03-30 | Multifunctional essential oil and preparation method thereof |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN202010235893.3A CN111407799A (en) | 2020-03-30 | 2020-03-30 | Multifunctional essential oil and preparation method thereof |
Publications (1)
Publication Number | Publication Date |
---|---|
CN111407799A true CN111407799A (en) | 2020-07-14 |
Family
ID=71485840
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CN202010235893.3A Pending CN111407799A (en) | 2020-03-30 | 2020-03-30 | Multifunctional essential oil and preparation method thereof |
Country Status (1)
Country | Link |
---|---|
CN (1) | CN111407799A (en) |
Cited By (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN112791121A (en) * | 2021-01-15 | 2021-05-14 | 杭州医之选生物科技有限公司 | Multifunctional compound essential oil |
CN115227857A (en) * | 2022-07-11 | 2022-10-25 | 广州汽车集团股份有限公司 | Perfume and vehicle essential oil |
CN115404128A (en) * | 2022-11-02 | 2022-11-29 | 广东顺德芳香世家天然产品制造有限公司 | Multifunctional essential oil composition and preparation method and application thereof |
Citations (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN101199773A (en) * | 2007-12-21 | 2008-06-18 | 北京中科雍和医药技术有限公司 | Compound essential oil of refreshing thinker |
CN103316084A (en) * | 2013-05-20 | 2013-09-25 | 钟小强 | Compound essential oil used for relieving lower back pain |
CN104758350A (en) * | 2015-03-12 | 2015-07-08 | 施敬东 | Refreshing and cool patch and preparation method thereof |
-
2020
- 2020-03-30 CN CN202010235893.3A patent/CN111407799A/en active Pending
Patent Citations (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN101199773A (en) * | 2007-12-21 | 2008-06-18 | 北京中科雍和医药技术有限公司 | Compound essential oil of refreshing thinker |
CN103316084A (en) * | 2013-05-20 | 2013-09-25 | 钟小强 | Compound essential oil used for relieving lower back pain |
CN104758350A (en) * | 2015-03-12 | 2015-07-08 | 施敬东 | Refreshing and cool patch and preparation method thereof |
Cited By (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN112791121A (en) * | 2021-01-15 | 2021-05-14 | 杭州医之选生物科技有限公司 | Multifunctional compound essential oil |
CN115227857A (en) * | 2022-07-11 | 2022-10-25 | 广州汽车集团股份有限公司 | Perfume and vehicle essential oil |
CN115404128A (en) * | 2022-11-02 | 2022-11-29 | 广东顺德芳香世家天然产品制造有限公司 | Multifunctional essential oil composition and preparation method and application thereof |
Similar Documents
Publication | Publication Date | Title |
---|---|---|
CN111407799A (en) | Multifunctional essential oil and preparation method thereof | |
CN104173261B (en) | Soothing, anti-allergy and skin-regenerating emulsion and preparation method thereof | |
CN102397182B (en) | Compound essential oil for improving skin properties | |
CN105106655B (en) | A kind of prosthetic burn and scald ointment and preparation method thereof | |
CN104042523A (en) | Natural plant therapeutic massage essential oil | |
KR20110000216A (en) | Composition for aromatic containing extracts of pine needlesand, artemisia, green tea leaves and the manufacturing method thereof | |
CN104694353B (en) | Health care wine for lady and preparation method thereof | |
Edwards | The Aromatherapy Companion: Medicinal Uses/Ayurvedic Healing/Body-Care Blends/Perfumes & Scents/Emotional Health & Well-Being | |
CN108635441A (en) | Compound essential oil composition, its application and the product for improving sleep | |
CN110403869A (en) | A kind of plant is releived composite essential oil and preparation method thereof | |
CN103446247A (en) | High-seepage-force compound essential oil for preventing skins from being aged | |
CN110339331A (en) | A kind of plant is releived essential oil | |
CN107213061A (en) | One kind releive moisturizing flower water | |
CN104434697A (en) | Mosquito-repelling and itching-relieving and skin-protecting and nerve-smoothing solid floral water and preparation method thereof | |
CN108078814A (en) | A kind of plant fragrance fluid composition with mosquito repellent function and its application in cosmetics | |
CN108403589A (en) | Natural plants face cream | |
CN105267119B (en) | It is a kind of to nourish moisturizing and injury repair lip gloss and preparation method thereof | |
Jones | The Complete Guide to Creating Oils, Soaps, Creams, and Herbal Gels for Your Mind and Body: 101 Natural Body Care Recipes | |
CN105105316B (en) | A kind of agilawood essential oil atomized liquid and preparation method thereof | |
CN107034014B (en) | A kind of francolin tea compound essential oil and its preparation method and application | |
CN108379639A (en) | A kind of air freshener and preparation method thereof | |
CN112273957A (en) | Traditional Chinese medicine pillow beneficial to sleep and preparation method thereof | |
KR101084489B1 (en) | Method for protecting scalp and solution manufactured thereby | |
CN111040896A (en) | Antibacterial, anti-inflammatory and skin-beautifying handmade soap | |
KR20150141078A (en) | Composition for removing the odor from aged person |
Legal Events
Date | Code | Title | Description |
---|---|---|---|
PB01 | Publication | ||
PB01 | Publication | ||
SE01 | Entry into force of request for substantive examination | ||
SE01 | Entry into force of request for substantive examination | ||
RJ01 | Rejection of invention patent application after publication | ||
RJ01 | Rejection of invention patent application after publication |
Application publication date: 20200714 |