CN107034014B - A kind of francolin tea compound essential oil and its preparation method and application - Google Patents
A kind of francolin tea compound essential oil and its preparation method and application Download PDFInfo
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- CN107034014B CN107034014B CN201611201465.9A CN201611201465A CN107034014B CN 107034014 B CN107034014 B CN 107034014B CN 201611201465 A CN201611201465 A CN 201611201465A CN 107034014 B CN107034014 B CN 107034014B
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/02—Recovery or refining of essential oils from raw materials
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/47—Euphorbiaceae (Spurge family), e.g. Ricinus (castorbean)
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/88—Liliopsida (monocotyledons)
- A61K36/899—Poaceae or Gramineae (Grass family), e.g. bamboo, corn or sugar cane
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/08—Anti-ageing preparations
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/0003—Compounds of unspecified constitution defined by the chemical reaction for their preparation
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/02—Recovery or refining of essential oils from raw materials
- C11B9/022—Refining
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/02—Recovery or refining of essential oils from raw materials
- C11B9/025—Recovery by solvent extraction
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/02—Recovery or refining of essential oils from raw materials
- C11B9/027—Recovery of volatiles by distillation or stripping
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Abstract
The invention provides a kind of francolin tea compound essential oil, it is made up of the raw material of following parts by weight：10 30 parts of francolin tea essential oil, thin 5 20 parts of handle grass plants essential oil, wherein, the francolin tea essential oil is essential oil obtained from extracting francolin tea using steam distillation, and the thin handle grass plants essential oil is essential oil obtained from extracting the inflorescence of thin handle grass using steam distillation.Above two essential oil is organically combined in the present invention, complement each other, it is safe and non-stimulating, have no toxic side effect, not only make it have extremely strong penetration, by increasing capacitance it is possible to increase blood circulation, activating cell, dehumidifying sterilization, sterilization are eased pain, proceeded blood cycle, be anti-oxidant, preventing skin aging, and smell is naturally charming, user can be made to be in a cheerful frame of mind, alleviate pressure, improve sleep.
Description
Technical field
The present invention relates to a kind of compound essential oil, more particularly to a kind of francolin tea compound essential oil and its preparation method and application.
Background technology
Insomnia is a kind of common disease, the normal spiritedness of insomniac is depressed, fatigue and weak, agitation, dizziness, cardio palmus,
With the passing of time body function declines, and can cause the generation of a variety of diseases, have a strong impact on health, work and the life of people.At present to losing
The treatment of dormancy disease, Western medicine is more using hypnotic sedative agent, anxiolytic, and long-term use is also easy to produce drug resistance and dependence, and poison is secondary
Act on larger；The traditional Chinese medical science is used for the medicine or health food for controlling insomnia, contains epiphysin in formula, research shows that epiphysin exists more
While improving sleep, the incidence increase of convulsions.On the other hand, increase with the age, the loss of moisture, causes in human body
The elasticated net fracture of skin, skin histology atrophy are supported, collapses, follow the string, when elasticity and the reduction of water conservation degree, the flesh of skin corium
Skin will show the aging phenomenons such as thick, the dim, color spot of dry, coarse, loose, wrinkle, pore, and having a sleepless night can accelerate human body to decline
Always.
Essential oil has the function that health care, existing extensive utilization to beautifying medical industry.Essential oil mostlys come from fragrant plant
The parts such as flower, leaf, root, skin, stem, branch, fruit, seed, the methods of taking distillation, squeezing, extraction, absorption, obtained have feature
The oily mater of fragrance.They are the mixtures of many compounds.Mainly there are terpene hydrocarbons, arene, alcohols, aldehydes, ketone
Class, ethers, esters and phenols etc..The species of essential oil is many in existing market, a feast for the eyes, but simultaneously have improvement sleep and
The essential oil of anti aging effect is but very rare.Essential oil, which needs to act on inside of human body, can just play its effect, and in existing market
Some essential oils penetration it is inadequate, therefore greatly reduce the performance of its effect.
Francolin tea [Mallotus peltatus (Geiseler) Muller Argoviensis] be also mountain herb mixtures tea, gross tea
It is Euphorbiaceae Mallotus plant with standing grain aunt's tea.Francolin tea is mainly distributed on Wenchang, Wanning and Lingshui in Hainan Island, also Sanya,
In happy east, white sand, Dingan County, east, fine jade, the ground such as Bao Ting and Chang River be distributed, wherein with Wenchang Bronze Drum Ridge and Wanning Dongshan Ridge
The francolin tea produced is the most famous.In addition, also there is open country in China Guangdong, Yunnan, Guangxi, and the middle print peninsula and Sumatra
Cloth estranged.The blade of francolin tea can start strong holy basil gas is formed from fermentation in the drying process, and it dissipates fragrant process and held
Long and penetration is strong.
Francolin tea has significant health-care effect and medicinal efficacy, is the important Chinese medicine among the people in Hainan, is swung using history
Long, rich in plurality of active ingredients such as tea polysaccharide, Tea Polyphenols, gallic acid and Polyphenols in its extract.Modern pharmacology research
Show, the active ingredient in francolin tea has scavenging activated oxygen, antiatherosclerosis, promotes choleresis, suppresses germ
Activity, improve sleep, antifatigue aging and sedation-analgesia and other effects.Therefore the effect of utilizing francolin tea, develops and is slept with improvement
Sleep and the preparation of anti aging effect has a good application prospect.
The content of the invention
It is an object of the invention to overcome deficiency of the prior art, there is provided a kind of francolin tea compound essential oil, have antibacterial,
The effect of the effect of anti aging effect, crease-resistant, anti-inflammatory, nti-freckle and improvement sleep.
The first aspect of the invention is to provide a kind of francolin tea compound essential oil, is made up of the raw material of following parts by weight：Zhe
Gu tea essential oil 10-30 parts, thin handle grass plants essential oil 5-20 parts, wherein, the francolin tea essential oil is to be extracted using steam distillation
Essential oil obtained from taking francolin tea, the thin handle grass plants essential oil are obtained to be extracted the inflorescence of thin handle grass using steam distillation
The essential oil arrived.
Preferably, the francolin tea compound essential oil is made up of the raw material of following parts by weight：Francolin tea essential oil 15-25 parts, carefully
Handle grass plants essential oil 10-15 parts.
It is further preferred that the francolin tea compound essential oil is made up of the raw material of following parts by weight：20 parts of francolin tea essential oil,
Thin 12 parts of handle grass plants essential oil.
The second aspect of the invention is to provide the preparation method of the present invention one side francolin tea compound essential oil：
Extracted respectively using steam distillation francolin tea and thin handle grass and obtain francolin tea essential oil and thin handle grass plants essential oil, according to than
Example mixes francolin tea essential oil and thin handle grass plants essential oil, produces.
The fourth aspect of the invention is to provide the present invention one side francolin tea compound essential oil and is preparing improvement
Application in sleep product.
The fifth aspect of the invention is to provide the present invention one side francolin tea compound essential oil to be prevented in preparation
Application in skin aging product.
Beneficial effects of the present invention are：
Above two essential oil is organically combined in the present invention, complemented each other, it is safe and non-stimulating, have no toxic side effect,
Not only make it have extremely strong penetration, by increasing capacitance it is possible to increase blood circulation, activating cell, dehumidifying sterilization, sterilization analgesia, logical muscle are lived
Network, it is anti-oxidant, prevent skin aging, and smell is naturally charming, user can be made to be in a cheerful frame of mind, and alleviates pressure, improves sleep.
Embodiment
Technical scheme is further described below by way of specific embodiment.But following examples not structure
Into limitation of the invention.
The application method of compound essential oil of the present invention mainly has three big modes：
1. champignon uses.By compound essential oil of the present invention, drip according to every 10 cubic metres of uses 2, expanded using heat source type
Fragrant device carries out aroma diffusing.
2. spraying uses.By compound essential oil of the present invention, 4-8 is added according to every 10 milliliters of pure water or distilled water
Drop, fully shakes up, carries out spraying diffusion.
3. massage uses.By compound essential oil of the present invention, added according to matrix such as every 10 milliliters of base oils or emulsions
4-8 drops, fully mix, carry out skin massaging.
Embodiment 1
The inflorescence that thin handle grass is fully deployed is gathered, is cleaned clean it up, by the main shaft of inflorescence and the rachis of branch
Remove, only retain small ear and rachilla, with normal pressure steam distillation, distillation time is 4-6 hours.And then enter after the completion of distillation
Row water-oil separating, for the essential oil isolated through anhydrous sodium sulfate drying, products therefrom is faint yellow mobile liquid essential oil, is thin
Handle grass plants essential oil.
Fresh francolin tea is gathered, clean it up is cleaned, dried in the shade naturally, with normal pressure steam distillation, distillation time is
4-6 hours.And then water-oil separating is carried out after the completion of distillation, the essential oil isolated is through anhydrous sodium sulfate drying, products therefrom
For francolin tea essential oil.
Then francolin tea essential oil 20g and thin handle grass plants essential oil 12g are taken, is put into stirring container, with agitator with identical
Direction normal temperature stirring at low speed, each raw material is set to be sufficiently mixed uniformly, packing, sealing,.
Embodiment 2
The present embodiment is that the proportioning of francolin tea essential oil and thin handle grass plants essential oil is different from the difference of embodiment 1,
In the present embodiment, francolin tea essential oil 15g and thin handle grass plants essential oil 15g are taken, is put into stirring container, with agitator with phase Tongfang
To normal temperature stirring at low speed, each raw material is set to be sufficiently mixed uniformly, packing, sealing,.
Embodiment 3
The present embodiment is that the proportioning of francolin tea essential oil and thin handle grass plants essential oil is different from the difference of embodiment 1,
In the present embodiment, francolin tea essential oil 25g and thin handle grass plants essential oil 10g are taken, is put into stirring container, with agitator with phase Tongfang
To normal temperature stirring at low speed, each raw material is set to be sufficiently mixed uniformly, packing, sealing,.
Embodiment 4
The present embodiment is that the proportioning of francolin tea essential oil and thin handle grass plants essential oil is different from the difference of embodiment 1,
In the present embodiment, francolin tea essential oil 10g and thin handle grass plants essential oil 20g are taken, is put into stirring container, with agitator with phase Tongfang
To normal temperature stirring at low speed, each raw material is set to be sufficiently mixed uniformly, packing, sealing,.
Embodiment 5
The present embodiment is that the proportioning of francolin tea essential oil and thin handle grass plants essential oil is different from the difference of embodiment 1,
In the present embodiment, francolin tea essential oil 30g and thin handle grass plants essential oil 5g are taken, is put into stirring container, with agitator with phase Tongfang
To normal temperature stirring at low speed, each raw material is set to be sufficiently mixed uniformly, packing, sealing,.
The present invention prevents the effect of skin aging, high penetration
Take SPF level female KM kind mouse, 3 monthly ages 20,12 monthly ages 120.By the mouse at 120 12 monthly ages
It is randomly divided into 4 groups：Respectively Normal group, A groups, B groups, C groups, D groups and E groups, every group 20.Separately by 20 3 monthly ages
For female KM kind mouse as young group of control, its weight is 25-27g.Mouse presses group sub-cage rearing.It is natural in identical
Under the conditions of, conventional feeding drinking-water, experiment is proceeded by after adaptability raising.Before experiment the omoplate of mouse back two is sloughed with shaver
Ask hair 2cm × 4cm on skin, A-E groups are applied outside with the compound essential oil prepared in embodiment 1-5 respectively, Normal group and year
Light control group is applied outside with deionized water, preservative film protection 2h.Smear once daily, smear 0.5g every time, it is continuous to smear 50 days.It is real
Mouse is put to death after the completion of testing, determines HYP, SOD, MDA and LF value at its experiment skin.
The preparation of 10% Skin Homogenate and SOD, MDA, LF measure：
Take back lose hair or feathers after skin histology block about 0.5g, pre-cooled 0.9% sodium chloride solution rinsing, remove subcutaneous fat and
Other connective tissues, filter paper wipes dry, weighed quality, after tissue block shreds in the homogenate tube of falling people, adds 9 times of quality of the tissue block
The sodium chloride solution of precooling 0.9%, 10% tissue is made with interior cut tissue refiner and is homogenized and (is carried out in frozen water), then repeatedly
Freeze thawing 3 times, make it completely broken, cellular content dissociates in the liquid phase completely.SOD activity, MDA contents, skin in Skin Homogenate
The index parameters such as skin LF, build up bio-engineering corporation's kit specification method with reference to Nanjing and be measured.
Mouse skin SOD, MDA, LF measurement result are shown：Under Normal group SOD activity is notable compared with young control group
Drop, and MDA, LF content dramatically increase.
The significantly raised natural aging mice skin SOD activity of compound essential oil prepared by embodiment 1-5 energy, makes its MDA, LF
Content be decreased obviously.This experimental result confirms that the compound essential oil of the present invention has significant function of anti-skin aging.
HYP and collagen measure：
By mouse back skin depilatory and after removing connective tissue, acetone: ether：1: 1 (V/V) degreasing, 80 DEG C of drying, essence
It is close to weigh 50mg, add 6mol/L hydrochloric acid solutions 2mL to mix, 36h is hydrolyzed in 80 DEG C of baking ovens；Hydrolyzate 0.4mL is taken with 6mol/L's
Sodium hydroxide solution adjusts its pH value between 6-7, adds water to be settled to 10.0mL；Take hydrolyzate 0.2mL to enter test tube, sequentially add
Buffer solution 1mL, ammonia amine T 1mL, perchloric acid 1mL, developer 1mL, mix, 60 DEG C of water-bath 15min, 550nm wavelength 1cm optical path ratios
Color, blank zeroing, while prepare standard curve pipe.The mass fraction of collagen is with HYP mass in collagen point in sample
Number is calculated for 13%.
The measurement result of mouse skin HYP and collagen content shows, in the mouse skin of A-E groups HYP content compared with
Normal group is significantly improved, and difference has pole conspicuousness.The compound essential oil of this explanation present invention can promote skin collagen
Synthesis, skin is tended to rejuvenation.
The present invention improves the effect of sleep
The present invention tries out through crowd, to 300 insomniacs use Follow-up observation of continuous 3 months, the results showed that
92.3% insomniac is slept and improved, and allergy and other adverse reactions are had no during use.Show the invention pair
It is notable to improve sleeper effect, has no toxic side effect.
The specific embodiment of the present invention is described in detail above, but it is intended only as example, it is of the invention and unlimited
It is formed on particular embodiments described above.To those skilled in the art, it is any to the equivalent modifications that carry out of the present invention and
Substitute also all among scope of the invention.Therefore, the impartial conversion made without departing from the spirit and scope of the invention and
Modification, all should be contained within the scope of the invention.
Claims (6)
1. a kind of francolin tea compound essential oil, it is characterised in that be made up of the raw material of following parts by weight：Francolin tea essential oil 10-30 parts,
Thin handle grass plants essential oil 5-20 parts, wherein, the francolin tea essential oil is using obtained from steam distillation extraction francolin tea
Essential oil, the thin handle grass plants essential oil are essential oil obtained from extracting the inflorescence of thin handle grass using steam distillation.
2. francolin tea compound essential oil according to claim 1, it is characterised in that be made up of the raw material of following parts by weight：Zhe
Gu tea essential oil 15-25 parts, thin handle grass plants essential oil 10-15 parts.
3. francolin tea compound essential oil according to claim 1, it is characterised in that be made up of the raw material of following parts by weight：Zhe
20 parts of Gu tea essential oils, thin 12 parts of handle grass plants essential oil.
4. the preparation method of francolin tea compound essential oil as described in any one in a kind of 1-3 such as claim, it is characterised in that use
Steam distillation extracts the inflorescence of francolin tea and thin handle grass and obtains francolin tea essential oil and thin handle grass plants essential oil respectively, according to
Ratio mixes francolin tea essential oil and thin handle grass plants essential oil, produces.
5. francolin tea compound essential oil is preparing the application in improving sleep product as described in any one in claim 1-3.
6. francolin tea compound essential oil the answering in preparation prevents skin aging product as described in any one in claim 1-3
With.
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| CN109806375A (en) * | 2019-01-30 | 2019-05-28 | 东莞市炫墨生物科技有限公司 | Herbal medicine ball with health care massaging function and preparation method thereof |
| CN113520946A (en) * | 2021-07-31 | 2021-10-22 | 海南黎草纪新生物科技有限公司 | Formula and preparation method of green herbal skin care product |
| CN113773910B (en) * | 2021-09-30 | 2022-11-08 | 梵申兰科技(上海)有限公司 | Artemisia annua essential oil and white tea essential oil for promoting skin cell regeneration and their composition |
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| CN103598583B (en) * | 2013-11-14 | 2015-07-29 | 陕西科技大学 | A kind of francolin tea buccal tablet and preparation method thereof |
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