CN111281828A - Edible attapulgite based lipstick and preparation method thereof - Google Patents
Edible attapulgite based lipstick and preparation method thereof Download PDFInfo
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- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
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- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
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- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
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- A61Q1/00—Make-up preparations; Body powders; Preparations for removing make-up
- A61Q1/02—Preparations containing skin colorants, e.g. pigments
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Abstract
The invention discloses an edible attapulgite based lipstick which is prepared from the following raw materials: modified attapulgite, edible toner, olive oil, rose essential oil, tea polyphenol, food-grade vaseline and pharmaceutical-grade hyaluronic acid; and provides a preparation method thereof. The invention has the beneficial effects that: the lipstick provided by the invention uses the modified attapulgite and the pharmaceutical grade hyaluronic acid as lipstick base materials, has the advantages of positive and smooth appearance color, good moistening degree, moisture retention, coloring capacity and higher melting point; the formula is simple, the raw materials are safe and nonirritating, the quality is stable, and the olive oil, the tea polyphenol, the hyaluronic acid and other components in the lip nourishing cream provide effective nourishing for lips; the attapulgite enables the air permeability of the lipstick on a lip coating to be good, and the peach bark extract enables the durability of the lipstick to be better; the attapulgite has good loading capacity and extremely large specific surface area, so that the consumption of natural toner is greatly reduced; after the peach bark extract is modified, the moisturizing capability of the attapulgite clay is greatly improved.
Description
Technical Field
The invention relates to the technical field of cosmetics, in particular to an edible attapulgite-based lipstick and a preparation method thereof.
Background
Lipstick is a common cosmetic, and the net sales of lipstick in 2019 are more than 1 hundred million. The types of lipsticks currently include matte lipsticks, metallic lipsticks, bright lipsticks, and the like. Its advantages and disadvantages are as follows:
(1) the matte lipstick contains more toner, is heavily colored, contains more volatile oil, has no luster and no reflection, can keep fastness for a long time, contains less moisturizing components, and is not suitable for consumers with more thin lips and lip marks; but has the advantages of low tone, sinkage and stability and is very popular with women.
(2) The metal lipstick contains a large amount of pearlescence and has metal luster, but the makeup has obvious granular feel, poor durability and serious lip crack.
(3) The bright lipstick contains more high-gloss oil, is bright in color and good in moistening degree, but can be sticky to skin, teeth and mouth when being used for makeup, and can cause cheilitis.
According to the related foreign data, 18.2% of the cancer patients of young women have the etiology related to the lipstick and the lipstick. Lipstick contains high amount of heavy metals such as lead and cadmium, lead has accumulation property, and chronic lead poisoning caused by long-term inhalation of lipstick can cause anemia, abdominal pain, acute renal failure and brain neuropathy. The lipstick with good quality is very strict in lead content control, and generally cannot cause any influence as long as the lipstick is not swallowed too much or is smeared all the time at ordinary times, but for poor lipstick, because a consumer cannot judge the lead content of the lipstick by naked eyes, the human body is extremely easily damaged, and therefore, the choice of large-brand lipstick is advocated in the market. However, both the big lipstick and the low lipstick contain a large amount of chemical components, and cause discomfort to the user if used for a long time.
Chinese patent CN 105326668A (application No. 201510777692.5) reports a transparent lipstick and a preparation method thereof, wherein 35-45 parts of a mixture of diisostearyl malate and a bis-dioctadecylamine dimer linoleic acid/ethylenediamine copolymer, 15-25 parts of diisostearyl malate, 8-20 parts of olive oil, 1-8 parts of grape seed oil, 6-15 parts of green tea seed oil, 5-10 parts of macadamia nut oil, 2-5 parts of vitamin E, 0.1-0.5 part of natural perfume, 0.005-0.05 part of natural pigment and 0.1-0.5 part of propyl hydroxybenzoate. The transparent lipstick is safe and non-irritant, has clear appearance, high transparency and good moistening degree, and lips are bright and bright in color after being used. However, the safety of the lipstick cannot be guaranteed due to the fact that a large amount of the bis-dioctadecylamine dimerized linoleic acid/ethylenediamine copolymer and diisostearic malate are used.
Chinese patent CN 107669518A (application No. 201710978184.2) reports a preparation method of lipstick, which comprises fiber, grease, preservative, and auxiliary additive, wherein the weight portion of the water is 62-69, the weight portion of the inorganic filler is 6-9, the weight portion of the pigment is 0.3-1, the weight portion of the thickener is 4.06-5.5, the weight portion of the grease is 2-3, the weight portion of the emulsifier is 1.5-4.5, the weight portion of the humectant is 8-13, the weight portion of the preservative is 0.68-0.85, and the weight portion of the auxiliary additive is 0.55-1. The lipstick has a large amount of water-based components, no wax formulation, light and thin texture, no sticky feeling, refreshing and cool property, bright and lasting color, and is not easy to separate due to sweat when meeting water, thereby greatly improving the use experience of users. The lipstick still uses chemicals in large quantities.
At present, the market urgently needs a high-end lipstick product which is safe, has no toxic or side effect, has a positive color and luster, can be kept for a long time, has good air permeability and good moisture retention, is not easy to separate after sweating when meeting water and has lasting fragrance. This requires that the lipstick formulation not contain any chemically synthesized substances, especially not heavy metal ions.
Long-term experiments in the national pharmacopoeia and the subject group prove that the high-purity attapulgite is a medical reagent, and the attapulgite is also listed in the latest catalogue of cosmetic raw materials (the catalogue is named as attapulgite in English and Chinese). The high-purity attapulgite has good promotion effect on repairing skin of human body, and is very safe to human body through intravenous injection experiments and oral administration experiments. However, pure inorganic attapulgite is very suitable for pigment, but the problems of drying crack, poor water retention property and the like can be caused when the pure inorganic attapulgite is directly used in lipstick, so when the attapulgite is used as a raw material of cosmetics, particularly lipstick, the attapulgite needs to be subjected to surface organic modification.
Disclosure of Invention
The invention aims to overcome the defects in the prior art and provides an edible attapulgite-based lipstick and a preparation method thereof.
The inventor finds that the mural in the Tujongkou has bright color and can keep thousands of years of color in long-term experiments and application, mainly the pigment contains a large amount of attapulgite which is a magic substance, and the inventor prepares the edible lipstick by using attapulgite clay as a main raw material in view of the inspiration of the phenomenon.
According to the conventional grafting medicines, such as a surfactant, a chemical organic substance and the like, the problem of the use safety of the attapulgite for cosmetics is caused. The attapulgite is mainly used for lipstick contacting with lips, so that the attapulgite is modified by creatively taking edible natural extracted organic matters as a modifier and is used for preparing the lipstick, so that the safety of raw materials is guaranteed. The method for modifying attapulgite by using the peach bark extract is not reported in documents.
In order to achieve the purpose, the technical scheme provided by the invention is as follows: the edible attapulgite-based lipstick is prepared from the following raw materials in parts by weight: 35-75 parts of modified attapulgite, 1-3 parts of edible toner, 10-25 parts of olive oil, 0.1-0.5 part of rose essential oil, 0.5-1 part of antioxidant preservative, 5-25 parts of food-grade vaseline and 5-30 parts of pharmaceutical-grade hyaluronic acid.
Further, the edible attapulgite-based lipstick is prepared from the following raw materials in parts by weight: 60 parts of modified attapulgite, 2.5 parts of edible toner, 20 parts of olive oil, 0.3 part of rose essential oil, 0.7 part of antioxidant preservative, 8.5 parts of food-grade vaseline and 8 parts of pharmaceutical-grade hyaluronic acid.
Further, the preparation method of the modified attapulgite based lipstick comprises the following steps: crushing attapulgite raw ore into 4.5-5.5 cm small particles, drying at 120 ℃ to constant weight, preparing 20% slurry by using distilled water, stirring at 3000r/min for 1 hour, sieving with a 1200-mesh sieve, performing pressure filtration at 0.159Mpa, wherein the aperture of the filter cloth is 2500 meshes, and drying at 120 ℃ until the water content is lower than 3%; crushing and sieving with a 300-mesh sieve to obtain crude pure attapulgite clay; cleaning peach bark, crushing into 0.25-0.35 cm particles, adding water, decocting, adding water in an amount which is 20 times of the mass of the peach bark, decocting at 80 ℃ for 2 hours, then filtering under 0.159Mpa to remove bark residues, filtering with filter cloth with the pore diameter of 600 meshes to obtain pure peach bark mucus, testing the viscosity of the peach bark mucus, and finally controlling the liquid viscosity to be 99-101cps, wherein the viscosity is controlled by adding or evaporating water proportion; preparing the coarsely purified attapulgite clay crushed by 300 meshes and peach bark mucilage into slurry, wherein the mass ratio of the coarsely purified attapulgite clay to the peach bark mucilage is 1:19, stirring at a high speed and ultrasonically dispersing for 1 hour, the stirring speed is 3000r/min, the stirring time is 1 hour, the ultrasonic power is 60kHz, standing is carried out for 24 hours, the upper layer mucilage is taken, evaporation, concentration and drying are carried out at the temperature of 80 ℃, the water content in the solid is lower than 1.5%, the solid is ground to 400 meshes by a ball mill and then ground to 2500 meshes by a jet mill, and the modified attapulgite is obtained.
Further, the above edible attapulgite based lipstick is a commercially available tea extract tea polyphenol antioxidant preservative.
The second purpose of the invention is to provide a preparation method of the edible attapulgite-based lipstick, which comprises the following steps: heating and melting food-grade vaseline according to the weight part ratio, then adding modified attapulgite, edible toner, olive oil, rose essential oil, medical-grade hyaluronic acid and tea polyphenol antioxidant preservative at one time, then ultrasonically stirring, wherein the ultrasonic power is 60kHz, the stirring speed is 400r/min, after primary mixing is uniform, placing the paste into an agate ball milling tank, grinding at a high speed for 10 minutes, the grinding speed is 2500r/min, taking out, injecting the mixed material into a mold, cooling to 2-8 ℃, demolding, shaping, and boxing to obtain the edible attapulgite based lipstick.
The invention has the beneficial effects that: compared with the prior art, the edible attapulgite based lipstick and the preparation method thereof provided by the invention have the advantages that:
(1) the novel edible mineral substance lipstick provided by the invention uses the modified attapulgite and the pharmaceutical grade hyaluronic acid as lipstick base materials, so that the product has the characteristics of positive and smooth appearance color, good moistening degree, good coloring capability and higher melting point;
(2) the edible lipstick disclosed by the invention is simple in formula, safe in raw materials, free of irritation and stable in quality, contains the components such as olive oil, tea polyphenol and hyaluronic acid, can provide effective nourishing for lips, and simultaneously uses natural spice and natural pigment, so that the product has light fragrance, and the lips are bright and bright in color after being used;
(3) the invention uses the attapulgite/peach bark extract, and has the advantages that firstly, the attapulgite ensures that the air permeability of the lipstick on the lip coating film is improved; secondly, the durability of the product is improved after the attapulgite is modified by the peach bark extract; thirdly, after the peach bark extract is modified, the moisturizing capability of the attapulgite clay is greatly improved; fourthly, the attapulgite has good loading capacity and great specific surface area, so that the consumption of natural toner is greatly reduced.
The preparation method provided by the invention has the advantages that:
firstly, the attapulgite is skillfully refined and purified by utilizing the viscosity of the peach bark gum solution to obtain the high-purity attapulgite;
secondly, the peach gum and the purified attapulgite are directly concentrated, dried and ball-milled, and the surface of the attapulgite is modified by utilizing natural organic matters, so that the attapulgite is more easily combined with skin, and the durability and the moisture retention are improved;
thirdly, the peach bark extract has the effects of resisting oxidation and beautifying, and is very suitable for being used in cosmetics;
fourthly, the peach bark extract has high nutritive value and is helpful to the health of human bodies after being eaten frequently;
fifthly, the peach gum can play a role in fixing makeup and shaping in the lipstick.
Detailed Description
The raw materials used in the invention are as follows:
edible toner: guangzhou water chestnut color cosmetics, Inc., U.S. Sun powder, C19-012;
rose essential oil: gansu Wei river source bioengineering limited company, Wei river source gift box with 10mL of Guimei human rose essential oil;
tea polyphenol: shanghai Michelin Biochemical technology, Inc., cat #: t821916-100 g;
food-grade vaseline: shandong Han Lin Jun International trade Co., Ltd, goods number: HLJ-50-FSL;
pharmaceutical grade hyaluronic acid: west ampere wanfang biotechnology limited, cat #: 2019-5-TMZS.
Example 1:
the edible attapulgite based lipstick is prepared from the following raw materials in parts by weight: 35g of modified attapulgite, 1g of edible toner, 10g of olive oil, 0.1g of rose essential oil, 0.5g of tea polyphenol antioxidant preservative, 5g of food-grade vaseline and 5g of pharmaceutical-grade hyaluronic acid.
The preparation method of the modified attapulgite comprises the following steps: crushing attapulgite raw ore into 5.5 cm small particles, drying at 120 ℃ to constant weight, preparing 20 mass percent slurry by using distilled water, stirring at 3000r/min for 1 hour, sieving by using a 1200-mesh sieve, performing pressure filtration at 0.159Mpa, wherein the aperture of a filter cloth is 2500 meshes, and drying at 120 ℃ until the water content is 2%; crushing and sieving with a 300-mesh sieve to obtain crude pure attapulgite clay; cleaning peach bark, crushing into 0.35 cm particles, adding water, decocting, adding water in an amount which is 20 times of the mass of the peach bark, decocting at 80 ℃ for 2 hours, filtering under 0.159Mpa to remove bark residues, filtering with filter cloth with the aperture of 600 meshes to obtain pure peach bark mucus, testing the viscosity of the peach bark mucus, and finally controlling the liquid viscosity to be 101cps, wherein the viscosity is controlled by adding or evaporating water proportion; preparing the coarsely purified attapulgite clay crushed by 300 meshes and peach bark mucilage into slurry, wherein the mass ratio of the coarsely purified attapulgite clay to the peach bark mucilage is 1:19, stirring at a high speed and ultrasonically dispersing for 1 hour, the stirring speed is 3000r/min, the stirring time is 1 hour, the ultrasonic power is 60kHz, standing is 24 hours, taking the upper layer mucilage, evaporating, concentrating and drying at the temperature of 80 ℃ to ensure that the water content in the solid is 1%, grinding the solid to 400 meshes by using a ball mill, and crushing the ground solid to 2500 meshes by using a jet mill to obtain the modified attapulgite.
The preparation method of the edible attapulgite based lipstick comprises the following steps: heating and melting food-grade vaseline according to the weight ratio, then adding modified attapulgite, edible toner, olive oil, rose essential oil, medical-grade hyaluronic acid and tea polyphenol antioxidant preservative at one time, then carrying out ultrasonic stirring, carrying out ultrasonic power of 60kHz and stirring rotation speed of 400r/min, after primary mixing uniformly, placing the paste in an agate ball milling tank, carrying out high-speed grinding for 10 minutes at the grinding speed of 2500r/min, taking out, injecting the mixed material into a mould, cooling to 8 ℃, demoulding, shaping and boxing to obtain the edible attapulgite based lipstick.
Example 2:
the edible attapulgite based lipstick is prepared from the following raw materials in parts by weight: 75g of modified attapulgite, 3g of edible toner, 25g of olive oil, 0.5g of rose essential oil, 1g of tea polyphenol antioxidant preservative, 25g of food-grade vaseline and 30g of pharmaceutical-grade hyaluronic acid.
The preparation method of the modified attapulgite comprises the following steps: crushing attapulgite raw ore into 4.5 cm small particles, drying at 120 ℃ to constant weight, preparing 20 mass percent slurry by using distilled water, stirring at 3000r/min for 1 hour, sieving by using a 1200-mesh sieve, performing pressure filtration at 0.159Mpa, wherein the aperture of a filter cloth is 2500 meshes, and drying at 120 ℃ until the water content is 1 percent; crushing and sieving with a 300-mesh sieve to obtain crude pure attapulgite clay; cleaning peach bark, crushing into 0.25 cm particles, adding water, decocting, adding water in an amount which is 20 times of the mass of the peach bark, decocting at 80 ℃ for 2 hours, filtering under 0.159Mpa to remove bark residues, filtering with filter cloth with the aperture of 600 meshes to obtain pure peach bark mucus, testing the viscosity of the peach bark mucus, and finally controlling the liquid viscosity to be 99cps, wherein the viscosity is controlled by adding or evaporating water proportion; preparing the coarsely purified attapulgite clay crushed by 300 meshes and peach bark mucilage into slurry, wherein the mass ratio of the coarsely purified attapulgite clay to the peach bark mucilage is 1:19, stirring at a high speed and ultrasonically dispersing for 1 hour, the stirring speed is 3000r/min, the stirring time is 1h, the ultrasonic power is 60kHz, standing is carried out for 24 hours, the upper layer mucilage is taken, evaporation, concentration and drying are carried out at the temperature of 80 ℃ until the water content in the solid is 1.2%, the solid is ground to 400 meshes by a ball mill, and then the ground material is ground to 2500 meshes by a jet mill, so that the modified attapulgite is obtained.
The preparation method of the edible attapulgite based lipstick comprises the following steps: heating and melting food-grade vaseline according to the weight ratio, then adding modified attapulgite, edible toner, olive oil, rose essential oil, medical-grade hyaluronic acid and tea polyphenol antioxidant preservative at one time, then carrying out ultrasonic stirring, carrying out ultrasonic power of 60kHz and stirring rotation speed of 400r/min, after primary mixing uniformly, placing the paste in an agate ball milling tank, carrying out high-speed grinding for 10 minutes at the grinding speed of 2500r/min, taking out, injecting the mixed material into a mould, cooling to 2 ℃, demoulding, shaping and boxing to obtain the edible attapulgite based lipstick.
Example 3:
the edible attapulgite based lipstick is prepared from the following raw materials in parts by weight: 60g of modified attapulgite, 2.5g of edible toner, 20g of olive oil, 0.3g of rose essential oil, 0.7g of tea polyphenol antioxidant preservative, 8.5g of food-grade vaseline and 8g of pharmaceutical-grade hyaluronic acid.
The preparation method of the modified attapulgite comprises the following steps: crushing attapulgite raw ore into 5 cm small particles, drying at 120 ℃ to constant weight, preparing 20 mass percent slurry by using distilled water, stirring at 3000r/min for 1 hour, then sieving by using a 1200-mesh sieve, carrying out pressure filtration at 0.159MPa, wherein the aperture of a filter cloth is 2500 meshes, and drying at 120 ℃ until the water content is 1.5%; crushing and sieving with a 300-mesh sieve to obtain crude pure attapulgite clay; cleaning peach bark, crushing into 0.3 cm particles, adding water, decocting, adding water in an amount which is 20 times of the mass of the peach bark, decocting at 80 ℃ for 2 hours, filtering under 0.159Mpa to remove bark residues, filtering with filter cloth with the aperture of 600 meshes to obtain pure peach bark mucus, testing the viscosity of the peach bark mucus, and finally controlling the liquid viscosity to be 100cps, wherein the viscosity is controlled by adding or evaporating water proportion; preparing the coarsely purified attapulgite clay crushed by 300 meshes and peach bark mucilage into slurry, wherein the mass ratio of the coarsely purified attapulgite clay to the peach bark mucilage is 1:19, stirring at a high speed and ultrasonically dispersing for 1 hour, the stirring speed is 3000r/min, the stirring time is 1h, the ultrasonic power is 60kHz, standing is carried out for 24 hours, the upper layer mucilage is taken, evaporation, concentration and drying are carried out at the temperature of 80 ℃ until the water content in the solid is 0.8%, the solid is ground to 400 meshes by a ball mill, and then the ground material is ground to 2500 meshes by a jet mill, so that the modified attapulgite is obtained.
The preparation method of the edible attapulgite based lipstick comprises the following steps: heating and melting food-grade vaseline according to the weight ratio, then adding modified attapulgite, edible toner, olive oil, rose essential oil, medical-grade hyaluronic acid and tea polyphenol antioxidant preservative at one time, then carrying out ultrasonic stirring, carrying out ultrasonic power of 60kHz and stirring rotation speed of 400r/min, after primary mixing uniformly, placing the paste in an agate ball milling tank, carrying out high-speed grinding for 10 minutes at the grinding speed of 2500r/min, taking out, injecting the mixed material into a mould, cooling to 4 ℃, demoulding, shaping and boxing to obtain the edible attapulgite based lipstick.
Example 4:
the edible attapulgite-based lipstick of the invention is compared with a comparative sample to evaluate the excellent effects:
the comparative samples were three commercially available large brands of lipstick, designated as comparative A, comparative B and comparative C.
The product of example 3 and comparative lipstick, a to C, were tested for melting point, breaking force, coloring ability, moisture, transparency and stability by the following methods.
(1) Melting point: adopting a VIC melting point determination method in the 2010 edition appendix of Chinese pharmacopoeia;
(2) breaking force: testing by using a lipstick fracture instrument. Under the normal condition, the breaking force of the lipstick with the diameter of 12.7mm is in the range of 400-800 g, so that the lipstick is not easy to break in the using process;
(3) coloring ability and moistening degree: by adopting the practical use sensory evaluation, the score 5 shows good, the score 4 shows good, the score 3 shows general, the score 2 shows poor, and the score 1 shows poor; recording data after evaluation of 50 users (20 students at school, 30 cosmetics sales), and taking an average value;
(4) stability: the test is carried out for 3 months under four conditions of circulation at 25 ℃, 18 ℃ below zero, 48 ℃, 18 ℃ below zero and 48 ℃, and the test is unchanged after the test is recovered to normal temperature and can be normally used as the evaluation standard.
The test results are shown in table 2:
TABLE 2
| Name of lipstick | Melting Point (. degree.C.) | Breaking force | Moistening degree | Coloring power | Stability of |
| Example 3 lipstick of the invention | 68 | 525 | 4.9 | 4.8 | Qualified |
| Comparison A | 65 | 419 | 4.9 | 4.8 | Qualified |
| Comparison B | 71 | 618 | 4.8 | 4.6 | Qualified |
| Comparison C | 79 | 596 | 4.5 | 4.5 | Qualified |
As shown in the table 2, the edible lipstick prepared by the invention has the advantages of excellent performance, moderate melting point, strong breaking force, good coloring effect and moistening degree, and good evaluation by a subject, and meanwhile, the edible lipstick has lasting coloring and good stability.
The lipstick of the invention entrusts Gansu province drug inspection research institute to carry out safety test, and the result is shown in Table 3:
TABLE 3
As can be seen from the above Table 3, the edible mineral substance lipstick of the invention is safe, non-irritant and non-toxic.
The air permeability test method comprises the following steps: the best formulation of example 3 of the present invention and commercially available popular lipstick were coated onto the same fabric using a GELLOWEN air permeability tester, both at a thickness of 0.2 mm. Under the same conditions, the measurement was repeated 20 times at different sites of the same sample. The air permeability of the obtained formula product is 75%, and the air permeability of commercially available popular lipstick is 38%.
And (3) durability test: the experimental subjects were (1) the best formulation of example 3 of the present invention; (2) the attapulgite is not modified by the peach bark extract, and other proportions of the attapulgite are the same as the formula of the product in the embodiment 3 of the invention; (3) the product is sold in market under a certain brand. The test method comprises the following steps: and after the lipstick is smeared for 10 minutes, the lipstick is sipped on a white porcelain cup, and the situation of marks remained on the edge of the cup is observed, and the lip lines are displayed by printing on oil absorption paper after the lipstick is smeared for 10 minutes, and then the residual quantity of the lip lines is observed. A total of 20 users were invited to participate in the test and averaged. The full score is 20 minutes. And (3) testing results: object (1)17 points; object (2)9.5 points; object (3) score 11.
And (4) moisture retention performance test: the experimental subjects were (1) the best formulation of example 3 of the present invention; (2) the attapulgite is not modified by the peach bark extract, and other proportions of the attapulgite are the same as the formula of the product in the embodiment 3 of the invention; (3) the product is sold in market under a certain brand. The test method comprises the following steps: the subjects were coated on the same fabric, respectively, to a thickness of 0.2 mm. Under the same conditions, 10 samples were applied to each subject. Each sample was dried at 40 ℃ for 5 hours, and the weight before and after drying was weighed using a one-ten-thousandth balance, and the moisture retention capacity was calculated. And (3) testing results: object (1) 81%; object (2) 45%; subject (3) 62%.
Finally, it should be noted that: although the present invention has been described in detail with reference to the foregoing embodiments, it will be apparent to those skilled in the art that changes may be made in the embodiments and/or equivalents thereof without departing from the spirit and scope of the invention. Any modification, equivalent replacement, or improvement made within the spirit and principle of the present invention should be included in the protection scope of the present invention.
Claims (5)
1. The edible attapulgite-based lipstick is characterized by being prepared from the following raw materials in parts by weight: 35-75 parts of modified attapulgite, 1-3 parts of edible toner, 10-25 parts of olive oil, 0.1-0.5 part of rose essential oil, 0.5-1 part of antioxidant preservative, 5-25 parts of food-grade vaseline and 5-30 parts of pharmaceutical-grade hyaluronic acid.
2. The edible attapulgite-based lipstick according to claim 1, characterized in that the edible attapulgite-based lipstick is prepared from the following raw materials in parts by weight: 60 parts of modified attapulgite, 2.5 parts of edible toner, 20 parts of olive oil, 0.3 part of rose essential oil, 0.7 part of antioxidant preservative, 8.5 parts of food-grade vaseline and 8 parts of pharmaceutical-grade hyaluronic acid.
3. The edible attapulgite-based lipstick according to claim 1 or 2, wherein the preparation method of the modified attapulgite comprises the following steps: crushing attapulgite raw ore into 4.5-5.5 cm small particles, drying at 120 ℃ to constant weight, preparing 20% slurry by using distilled water, stirring at 3000r/min for 1 hour, sieving with a 1200-mesh sieve, performing pressure filtration at 0.159Mpa, wherein the aperture of the filter cloth is 2500 meshes, and drying at 120 ℃ until the water content is lower than 3%; crushing and sieving with a 300-mesh sieve to obtain crude pure attapulgite clay; cleaning peach bark, crushing into 0.25-0.35 cm particles, adding water, decocting, adding water in an amount which is 20 times of the mass of the peach bark, decocting at 80 ℃ for 2 hours, then filtering under 0.159Mpa to remove bark residues, filtering with filter cloth with the pore diameter of 600 meshes to obtain pure peach bark mucus, testing the viscosity of the peach bark mucus, and finally controlling the liquid viscosity to be 99-101cps, wherein the viscosity is controlled by adding or evaporating water proportion; preparing the coarsely purified attapulgite clay crushed by 300 meshes and peach bark mucilage into slurry, wherein the mass ratio of the coarsely purified attapulgite clay to the peach bark mucilage is 1:19, stirring at a high speed and ultrasonically dispersing for 1 hour, the stirring speed is 3000r/min, the stirring time is 1 hour, the ultrasonic power is 60kHz, standing is carried out for 24 hours, the upper layer mucilage is taken, evaporation, concentration and drying are carried out at the temperature of 80 ℃, the water content in the solid is lower than 1.5%, the solid is ground to 400 meshes by a ball mill and then ground to 2500 meshes by a jet mill, and the modified attapulgite is obtained.
4. The edible attapulgite-based lipstick according to claim 3, wherein said antioxidant preservative is a commercially available tea extract tea polyphenol antioxidant preservative.
5. The method for preparing the edible attapulgite-based lipstick according to claim 4, characterized by comprising the following steps: heating and melting food-grade vaseline according to the weight part ratio, then adding modified attapulgite, edible toner, olive oil, rose essential oil, medical-grade hyaluronic acid and tea polyphenol antioxidant preservative at one time, then ultrasonically stirring, wherein the ultrasonic power is 60kHz, the stirring speed is 400r/min, after primary mixing is uniform, placing the paste into an agate ball milling tank, grinding at a high speed for 10 minutes, the grinding speed is 2500r/min, taking out, injecting the mixed material into a mold, cooling to 2-8 ℃, demolding, shaping, and boxing to obtain the edible attapulgite based lipstick.
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113208951A (en) * | 2021-05-17 | 2021-08-06 | 西北师范大学 | Butter modified attapulgite and application thereof in preparation of lipstick |
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| CN103330676A (en) * | 2013-07-23 | 2013-10-02 | 陆飞 | Manufacturing method of edible lipstick |
| CN103566903A (en) * | 2013-09-29 | 2014-02-12 | 安徽金叶炭素科技有限公司 | Attapulgite clay modified active carbon and preparation method thereof |
| FR3058888A1 (en) * | 2016-11-23 | 2018-05-25 | Lvmh Recherche | FILMOGENIC COMPOSITION BASED ON PULLULAN AND ITS USES IN COSMETIC COMPOSITIONS FOR MAKE-UP AND / OR CARE OF KERATINIC MATERIALS, SKIN AND LIP |
| CN108670882A (en) * | 2018-07-23 | 2018-10-19 | 长江师范学院 | A kind of edible lipstick and preparation method thereof |
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Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103330676A (en) * | 2013-07-23 | 2013-10-02 | 陆飞 | Manufacturing method of edible lipstick |
| CN103566903A (en) * | 2013-09-29 | 2014-02-12 | 安徽金叶炭素科技有限公司 | Attapulgite clay modified active carbon and preparation method thereof |
| FR3058888A1 (en) * | 2016-11-23 | 2018-05-25 | Lvmh Recherche | FILMOGENIC COMPOSITION BASED ON PULLULAN AND ITS USES IN COSMETIC COMPOSITIONS FOR MAKE-UP AND / OR CARE OF KERATINIC MATERIALS, SKIN AND LIP |
| CN108670882A (en) * | 2018-07-23 | 2018-10-19 | 长江师范学院 | A kind of edible lipstick and preparation method thereof |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113208951A (en) * | 2021-05-17 | 2021-08-06 | 西北师范大学 | Butter modified attapulgite and application thereof in preparation of lipstick |
| CN113208951B (en) * | 2021-05-17 | 2022-05-27 | 西北师范大学 | Butter modified attapulgite and application thereof in preparation of lipstick |
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| CN111281828B (en) | 2021-03-16 |
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