CN111188111A - 一种抑菌型棉纺织面料制备工艺 - Google Patents
一种抑菌型棉纺织面料制备工艺 Download PDFInfo
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- CN111188111A CN111188111A CN202010179019.2A CN202010179019A CN111188111A CN 111188111 A CN111188111 A CN 111188111A CN 202010179019 A CN202010179019 A CN 202010179019A CN 111188111 A CN111188111 A CN 111188111A
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- 229920000742 Cotton Polymers 0.000 title claims abstract description 31
- 239000004753 textile Substances 0.000 title claims abstract description 24
- 239000004744 fabric Substances 0.000 title claims abstract description 21
- 238000002360 preparation method Methods 0.000 title claims abstract description 16
- 230000000844 anti-bacterial effect Effects 0.000 title claims description 11
- 239000000835 fiber Substances 0.000 claims abstract description 87
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 claims abstract description 33
- 238000002791 soaking Methods 0.000 claims abstract description 29
- 229920001661 Chitosan Polymers 0.000 claims abstract description 22
- 229920000297 Rayon Polymers 0.000 claims abstract description 22
- FOIXSVOLVBLSDH-UHFFFAOYSA-N Silver ion Chemical compound [Ag+] FOIXSVOLVBLSDH-UHFFFAOYSA-N 0.000 claims abstract description 22
- XLOMVQKBTHCTTD-UHFFFAOYSA-N Zinc monoxide Chemical compound [Zn]=O XLOMVQKBTHCTTD-UHFFFAOYSA-N 0.000 claims abstract description 22
- 238000002156 mixing Methods 0.000 claims abstract description 19
- 239000002994 raw material Substances 0.000 claims abstract description 15
- IXPNQXFRVYWDDI-UHFFFAOYSA-N 1-methyl-2,4-dioxo-1,3-diazinane-5-carboximidamide Chemical compound CN1CC(C(N)=N)C(=O)NC1=O IXPNQXFRVYWDDI-UHFFFAOYSA-N 0.000 claims abstract description 11
- KWSLGOVYXMQPPX-UHFFFAOYSA-N 5-[3-(trifluoromethyl)phenyl]-2h-tetrazole Chemical compound FC(F)(F)C1=CC=CC(C2=NNN=N2)=C1 KWSLGOVYXMQPPX-UHFFFAOYSA-N 0.000 claims abstract description 11
- NIXOWILDQLNWCW-UHFFFAOYSA-M Acrylate Chemical compound [O-]C(=O)C=C NIXOWILDQLNWCW-UHFFFAOYSA-M 0.000 claims abstract description 11
- 229920001817 Agar Polymers 0.000 claims abstract description 11
- 235000017166 Bambusa arundinacea Nutrition 0.000 claims abstract description 11
- 235000017491 Bambusa tulda Nutrition 0.000 claims abstract description 11
- 235000004431 Linum usitatissimum Nutrition 0.000 claims abstract description 11
- 235000015334 Phyllostachys viridis Nutrition 0.000 claims abstract description 11
- 239000008272 agar Substances 0.000 claims abstract description 11
- 239000011425 bamboo Substances 0.000 claims abstract description 11
- 239000003610 charcoal Substances 0.000 claims abstract description 11
- XGZVUEUWXADBQD-UHFFFAOYSA-L lithium carbonate Chemical compound [Li+].[Li+].[O-]C([O-])=O XGZVUEUWXADBQD-UHFFFAOYSA-L 0.000 claims abstract description 11
- 229910052808 lithium carbonate Inorganic materials 0.000 claims abstract description 11
- 229920000728 polyester Polymers 0.000 claims abstract description 11
- 239000000661 sodium alginate Substances 0.000 claims abstract description 11
- 235000010413 sodium alginate Nutrition 0.000 claims abstract description 11
- 229940005550 sodium alginate Drugs 0.000 claims abstract description 11
- 229910001379 sodium hypophosphite Inorganic materials 0.000 claims abstract description 11
- 239000011787 zinc oxide Substances 0.000 claims abstract description 11
- 239000002562 thickening agent Substances 0.000 claims abstract description 9
- ILJSQTXMGCGYMG-UHFFFAOYSA-N triacetic acid Chemical compound CC(=O)CC(=O)CC(O)=O ILJSQTXMGCGYMG-UHFFFAOYSA-N 0.000 claims abstract description 4
- 230000003385 bacteriostatic effect Effects 0.000 claims abstract 9
- 238000001035 drying Methods 0.000 claims description 16
- 241001330002 Bambuseae Species 0.000 claims description 10
- 241000208202 Linaceae Species 0.000 claims description 10
- 238000003756 stirring Methods 0.000 claims description 10
- 229920002284 Cellulose triacetate Polymers 0.000 claims description 7
- NNLVGZFZQQXQNW-ADJNRHBOSA-N [(2r,3r,4s,5r,6s)-4,5-diacetyloxy-3-[(2s,3r,4s,5r,6r)-3,4,5-triacetyloxy-6-(acetyloxymethyl)oxan-2-yl]oxy-6-[(2r,3r,4s,5r,6s)-4,5,6-triacetyloxy-2-(acetyloxymethyl)oxan-3-yl]oxyoxan-2-yl]methyl acetate Chemical compound O([C@@H]1O[C@@H]([C@H]([C@H](OC(C)=O)[C@H]1OC(C)=O)O[C@H]1[C@@H]([C@@H](OC(C)=O)[C@H](OC(C)=O)[C@@H](COC(C)=O)O1)OC(C)=O)COC(=O)C)[C@@H]1[C@@H](COC(C)=O)O[C@@H](OC(C)=O)[C@H](OC(C)=O)[C@H]1OC(C)=O NNLVGZFZQQXQNW-ADJNRHBOSA-N 0.000 claims description 7
- 238000009941 weaving Methods 0.000 claims description 6
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- 238000005057 refrigeration Methods 0.000 claims description 2
- 238000004519 manufacturing process Methods 0.000 abstract description 4
- 239000000463 material Substances 0.000 abstract description 3
- 240000006240 Linum usitatissimum Species 0.000 abstract 1
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- 238000005516 engineering process Methods 0.000 description 4
- 238000000034 method Methods 0.000 description 3
- 238000012986 modification Methods 0.000 description 2
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- GNFTZDOKVXKIBK-UHFFFAOYSA-N 3-(2-methoxyethoxy)benzohydrazide Chemical compound COCCOC1=CC=CC(C(=O)NN)=C1 GNFTZDOKVXKIBK-UHFFFAOYSA-N 0.000 description 1
- FGUUSXIOTUKUDN-IBGZPJMESA-N C1(=CC=CC=C1)N1C2=C(NC([C@H](C1)NC=1OC(=NN=1)C1=CC=CC=C1)=O)C=CC=C2 Chemical compound C1(=CC=CC=C1)N1C2=C(NC([C@H](C1)NC=1OC(=NN=1)C1=CC=CC=C1)=O)C=CC=C2 FGUUSXIOTUKUDN-IBGZPJMESA-N 0.000 description 1
- 230000000712 assembly Effects 0.000 description 1
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- 150000001875 compounds Chemical class 0.000 description 1
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- 230000007547 defect Effects 0.000 description 1
- 238000009984 hand spinning Methods 0.000 description 1
- 239000004745 nonwoven fabric Substances 0.000 description 1
- 239000000047 product Substances 0.000 description 1
- 239000007858 starting material Substances 0.000 description 1
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Abstract
本发明公开了一种抑菌型棉纺织面料制备工艺,制作过程中涉及到三大部分材料,分别是混纺原料、浸泡溶液、增稠剂,其中混纺原料包括变性聚粘胶纤维、纳米银纤维、竹炭纤维、亚麻纤维、棉纤维、粘胶纤维、蚕丝纤维、聚酯纤维、壳聚糖纤维和三醋酸纤维,浸泡溶液包括氧化锌溶液、氢氧化钠溶液、银离子溶液、次磷酸钠溶液、丙烯酸酯溶液和碳酸锂溶液,增稠剂包括甲壳胺、琼脂和海藻酸钠,本发明制作出的棉纺织面料具有很强的抑菌性,使用过程中健康卫生,并且生产规模不大,生产成本低,提高了产品的性能。
Description
技术领域
本发明涉及棉纺织相关技术领域,具体为一种抑菌型棉纺织面料制备工艺。
背景技术
纺织原意是取自纺纱与织布的总称,但是随着纺织知识体系和学科体系的不断发展和完善,特别是非织造纺织材料和三维复合编织等技术产生后,已经不仅是传统的手工纺纱和织布,也包括无纺布技术,现代三维编织技术,现代静电纳米成网技术等生产的服装用、产业用、装饰用纺织品。所以,现代纺织是指一种纤维或纤维集合体的多尺度结构加工技术。
现有技术中的抗菌棉纺织面料,抗菌性能并不是很理想,存在一定的缺陷,并且现有的抗菌棉纺织面料的生产工艺比较复杂,需要花费大量的人力物力,并且经济成本也会非常的高。
发明内容
本发明的目的是针对现有的问题,提供一种抑菌型棉纺织面料制备工艺,使得制作出的棉纺织面料具有很强的抑菌性,使用过程中健康卫生,并且生产规模不大,生产成本低,提高了产品的性能。
本发明为实现上述技术目的所采用的技术方案为:一种抑菌型棉纺织面料制备工艺,原料成分包括三大部分,分别是混纺原料、浸泡溶液、增稠剂,其中混纺原料包括变性聚粘胶纤维、纳米银纤维、竹炭纤维、亚麻纤维、棉纤维、粘胶纤维、蚕丝纤维、聚酯纤维、壳聚糖纤维和三醋酸纤维,浸泡溶液包括氧化锌溶液、氢氧化钠溶液、银离子溶液、次磷酸钠溶液、丙烯酸酯溶液和碳酸锂溶液,增稠剂包括甲壳胺、琼脂和海藻酸钠,其中原料成分的具体含量为:变性聚粘胶纤维:10—15重量份,纳米银纤维:15—25重量份,竹炭纤维:20—30重量份,亚麻纤维:25—30重量份,棉纤维:25—40重量份,粘胶纤维:40—50重量份,蚕丝纤维:10—20重量份,聚酯纤维:35—60重量份,壳聚糖纤维:20—30重量份,三醋酸纤维:15—30重量份,氧化锌溶液:10—15重量份,氢氧化钠溶液:20—30重量份,银离子溶液:15—25重量份,次磷酸钠溶液:8—16重量份,丙烯酸酯溶液:12—26重量份,碳酸锂溶液:40-50重量份,甲壳胺:5—15重量份,琼脂:15—15重量份,海藻酸钠:15-25重量份。
进一步的,步骤1中将10-25重量份的变性聚粘胶纤维与15-25重量份的纳米银纤维混纺成的纱线放入10-15重量份的氧化锌溶液中进行浸泡的时间为30min-50min。
进一步的,步骤2中将20-30重量份的竹炭纤维与25-30重量份的亚麻纤维混纺成的纱线放入20-30重量份的氢氧化钠溶液中进行浸泡的时间为30min-50min。
进一步的,步骤3中的25-40重量份的棉纤维与40-50重量份的粘胶纤维混纺成的纱线放入15-25重量份的银离子溶液中进行浸泡的时间为1h-1.5h。
进一步的,步骤4中的10-20重量份的蚕丝纤维与35-60重量份的聚酯纤维混纺成的纱线放入8-16重量份的次磷酸钠溶液中进行浸泡的时间为40min-1h。
进一步的,步骤5中的20-30重量份的壳聚糖纤维与15-30重量份的三醋酸纤维混纺成的纱线放入12-26重量份的丙烯酸酯溶液中进行浸泡的时间为20min-40min。
进一步的,步骤6中对五种纱线进行烘干处理的方式为统一处理,统一放置在烘干房内进行烘干处理,烘干处理的温度为50℃-65℃。
进一步的,步骤7中将40-50重量份的碳酸锂溶液中放入5-15重量份的甲壳胺进行搅拌处理的时间为10min-15min,将10-15重量份的琼脂与15-25重量份的海藻酸钠放入静置溶液中搅拌处理的时间为7min-10min,搅拌后的液体进行冷藏处理的温度为-5℃-0℃。
进一步的,步骤8中将五种纱线一起放入步骤7中的溶液中进行浸泡的时间为1h-1.5h,并且步骤8中对于纱线烘干处理的温度为45℃-50℃。
具体实施方式
下面对本发明做进一步的阐述,以下步骤中所用的原料均为本领域常规的原料或者是从市面上能够购买得到。
一种抑菌型棉纺织面料制备工艺,原料成分包括三大部分,分别是混纺原料、浸泡溶液、增稠剂,其中混纺原料包括变性聚粘胶纤维、纳米银纤维、竹炭纤维、亚麻纤维、棉纤维、粘胶纤维、蚕丝纤维、聚酯纤维、壳聚糖纤维和三醋酸纤维,浸泡溶液包括氧化锌溶液、氢氧化钠溶液、银离子溶液、次磷酸钠溶液、丙烯酸酯溶液和碳酸锂溶液,增稠剂包括甲壳胺、琼脂和海藻酸钠,其中原料成分的具体含量为:变性聚粘胶纤维:10—15重量份,纳米银纤维:15—25重量份,竹炭纤维:20—30重量份,亚麻纤维:25—30重量份,棉纤维:25—40重量份,粘胶纤维:40—50重量份,蚕丝纤维:10—20重量份,聚酯纤维:35—60重量份,壳聚糖纤维:20—30重量份,三醋酸纤维:15—30重量份,氧化锌溶液:10—15重量份,氢氧化钠溶液:20—30重量份,银离子溶液:15—25重量份,次磷酸钠溶液:8—16重量份,丙烯酸酯溶液:12—26重量份,碳酸锂溶液:40-50重量份,甲壳胺:5—15重量份,琼脂:15—15重量份,海藻酸钠:15-25重量份。
具体步骤为:
a.将10-25重量份的变性聚粘胶纤维与15-25重量份的纳米银纤维混纺成纱线,将混纺成的纱线放入10-15重量份的氧化锌溶液中进行浸泡。
b.将20-30重量份的竹炭纤维与25-30重量份的亚麻纤维混纺成纱线,将混纺成的纱线放入20-30重量份的氢氧化钠溶液中进行浸泡。
c.将25-40重量份的棉纤维与40-50重量份的粘胶纤维混纺成纱线,将混纺成的纱线放入15-25重量份的银离子溶液中进行浸泡。
d.将10-20重量份的蚕丝纤维与35-60重量份的聚酯纤维混纺成纱线,将混纺成的纱线放入8-16重量份的次磷酸钠溶液中进行浸泡。
e.将20-30重量份的壳聚糖纤维与15-30重量份的三醋酸纤维混纺成纱线,将混纺成的纱线放入12-26重量份的丙烯酸酯溶液中进行浸泡。
f.将步骤a、步骤b、步骤c、步骤d、步骤e中浸泡后的纱线进行烘干处理,烘干处理完毕后进行静置。
g.在40-50重量份的碳酸锂溶液中放入5-15重量份的甲壳胺进行搅拌处理,搅拌结束后静置一段时间,待静置溶液中出现沉淀物后再将10-15重量份的琼脂与15-25重量份的海藻酸钠放入溶液中,再次进行搅拌处理,然后将将搅拌后的液体进行冷藏处理,一段时间后取出。
h.将步骤f中烘干处理后的五种纱线一起放入步骤g中的溶液中进行浸泡,一段时间后将其全部取出,然后进行烘干处理。
i.将步骤h中烘干后的纱线织成面料即可。
对于本领域的技术人员而言,可根据以上描述的技术方案以及构思做出其它各种相应的改变以及变形,而所有的这些改变以及变形都应该属于本发明权利要求的保护范围之内。
Claims (9)
1.一种抑菌型棉纺织面料制备工艺,其特征在于:原料成分包括三大部分,分别是混纺原料、浸泡溶液、增稠剂,其中混纺原料包括变性聚粘胶纤维、纳米银纤维、竹炭纤维、亚麻纤维、棉纤维、粘胶纤维、蚕丝纤维、聚酯纤维、壳聚糖纤维和三醋酸纤维,浸泡溶液包括氧化锌溶液、氢氧化钠溶液、银离子溶液、次磷酸钠溶液、丙烯酸酯溶液和碳酸锂溶液,增稠剂包括甲壳胺、琼脂和海藻酸钠。
其中原料成分的具体含量为:
混纺原料:
变性聚粘胶纤维:10—15重量份
纳米银纤维:15—25重量份
竹炭纤维:20—30重量份
亚麻纤维:25—30重量份
棉纤维:25—40重量份
粘胶纤维:40—50重量份
蚕丝纤维:10—20重量份
聚酯纤维:35—60重量份
壳聚糖纤维:20—30重量份
三醋酸纤维:15—30重量份
浸泡溶液:
氧化锌溶液:10—15重量份
氢氧化钠溶液:20—30重量份
银离子溶液:15—25重量份
次磷酸钠溶液:8—16重量份
丙烯酸酯溶液:12—26重量份
碳酸锂溶液:40-50重量份
增稠剂:
甲壳胺:5—15重量份
琼脂:15—15重量份
海藻酸钠:15-25重量份
步骤1:将10-25重量份的变性聚粘胶纤维与15-25重量份的纳米银纤维混纺成纱线,将混纺成的纱线放入10-15重量份的氧化锌溶液中进行浸泡。
步骤2:将20-30重量份的竹炭纤维与25-30重量份的亚麻纤维混纺成纱线,将混纺成的纱线放入20-30重量份的氢氧化钠溶液中进行浸泡。
步骤3:将25-40重量份的棉纤维与40-50重量份的粘胶纤维混纺成纱线,将混纺成的纱线放入15-25重量份的银离子溶液中进行浸泡。
步骤4:将10-20重量份的蚕丝纤维与35-60重量份的聚酯纤维混纺成纱线,将混纺成的纱线放入8-16重量份的次磷酸钠溶液中进行浸泡。
步骤5:将20-30重量份的壳聚糖纤维与15-30重量份的三醋酸纤维混纺成纱线,将混纺成的纱线放入12-26重量份的丙烯酸酯溶液中进行浸泡。
步骤6:将步骤1、步骤2、步骤3、步骤4、步骤5中浸泡后的纱线进行烘干处理,烘干处理完毕后进行静置。
步骤7:在40-50重量份的碳酸锂溶液中放入5-15重量份的甲壳胺进行搅拌处理,搅拌结束后静置一段时间,待静置溶液中出现沉淀物后再将10-15重量份的琼脂与15-25重量份的海藻酸钠放入溶液中,再次进行搅拌处理,然后将将搅拌后的液体进行冷藏处理,一段时间后取出。
步骤8:将步骤6中烘干处理后的五种纱线一起放入步骤7中的溶液中进行浸泡,一段时间后将其全部取出,然后进行烘干处理。
步骤9:将步骤8中烘干后的纱线织成面料即可。
2.根据权利要求1所述的一种抑菌型棉纺织面料制备工艺,其特征在于:所述步骤1中将10-25重量份的变性聚粘胶纤维与15-25重量份的纳米银纤维混纺成的纱线放入10-15重量份的氧化锌溶液中进行浸泡的时间为30min-50min。
3.根据权利要求1所述的一种抑菌型棉纺织面料制备工艺,其特征在于:所述步骤2中将20-30重量份的竹炭纤维与25-30重量份的亚麻纤维混纺成的纱线放入20-30重量份的氢氧化钠溶液中进行浸泡的时间为30min-50min。
4.根据权利要求1所述的一种抑菌型棉纺织面料制备工艺,其特征在于:所述步骤3中的25-40重量份的棉纤维与40-50重量份的粘胶纤维混纺成的纱线放入15-25重量份的银离子溶液中进行浸泡的时间为1h-1.5h。
5.根据权利要求1所述的一种抑菌型棉纺织面料制备工艺,其特征在于:所述步骤4中的10-20重量份的蚕丝纤维与35-60重量份的聚酯纤维混纺成的纱线放入8-16重量份的次磷酸钠溶液中进行浸泡的时间为40min-1h。
6.根据权利要求1所述的一种抑菌型棉纺织面料制备工艺,其特征在于:所述步骤5中的20-30重量份的壳聚糖纤维与15-30重量份的三醋酸纤维混纺成的纱线放入12-26重量份的丙烯酸酯溶液中进行浸泡的时间为20min-40min。
7.根据权利要求1所述的一种抑菌型棉纺织面料制备工艺,其特征在于:所述步骤6中对五种纱线进行烘干处理的方式为统一处理,统一放置在烘干房内进行烘干处理,烘干处理的温度为50℃-65℃。
8.根据权利要求1所述的一种抑菌型棉纺织面料制备工艺,其特征在于:所述步骤7中将40-50重量份的碳酸锂溶液中放入5-15重量份的甲壳胺进行搅拌处理的时间为10min-15min,将10-15重量份的琼脂与15-25重量份的海藻酸钠放入静置溶液中搅拌处理的时间为7min-10min,搅拌后的液体进行冷藏处理的温度为-5℃-0℃。
9.根据权利要求1所述的一种抑菌型棉纺织面料制备工艺,其特征在于:所述步骤8中将五种纱线一起放入步骤7中的溶液中进行浸泡的时间为1h-1.5h,并且步骤8中对于纱线烘干处理的温度为45℃-50℃。
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