CN111166922A - Efficient antibacterial incense - Google Patents
Efficient antibacterial incense Download PDFInfo
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- CN111166922A CN111166922A CN202010065506.6A CN202010065506A CN111166922A CN 111166922 A CN111166922 A CN 111166922A CN 202010065506 A CN202010065506 A CN 202010065506A CN 111166922 A CN111166922 A CN 111166922A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61L—METHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
- A61L9/00—Disinfection, sterilisation or deodorisation of air
- A61L9/01—Deodorant compositions
- A61L9/013—Deodorant compositions containing animal or plant extracts, or vegetable material
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
- A01N65/06—Coniferophyta [gymnosperms], e.g. cypress
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
- A01N65/08—Magnoliopsida [dicotyledons]
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
- A01N65/08—Magnoliopsida [dicotyledons]
- A01N65/20—Fabaceae or Leguminosae [Pea or Legume family], e.g. pea, lentil, soybean, clover, acacia, honey locust, derris or millettia
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/13—Coniferophyta (gymnosperms)
- A61K36/14—Cupressaceae (Cypress family), e.g. juniper or cypress
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/35—Caprifoliaceae (Honeysuckle family)
- A61K36/355—Lonicera (honeysuckle)
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/48—Fabaceae or Leguminosae (Pea or Legume family); Caesalpiniaceae; Mimosaceae; Papilionaceae
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61P—SPECIFIC THERAPEUTIC ACTIVITY OF CHEMICAL COMPOUNDS OR MEDICINAL PREPARATIONS
- A61P31/00—Antiinfectives, i.e. antibiotics, antiseptics, chemotherapeutics
- A61P31/04—Antibacterial agents
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61L—METHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
- A61L2209/00—Aspects relating to disinfection, sterilisation or deodorisation of air
- A61L2209/20—Method-related aspects
- A61L2209/21—Use of chemical compounds for treating air or the like
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- Agronomy & Crop Science (AREA)
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Abstract
The invention discloses an efficient antibacterial incense. The incense comprises effective components and an adhesive, wherein the effective components comprise the following components in parts by weight: 30-40 parts of sappan wood, 15-25 parts of cacumen biotae and 8-12 parts of honeysuckle. The incense is prepared by extracting sappan wood, cacumen biotae and honeysuckle, concentrating to obtain clear paste, mixing the clear paste with an adhesive, forming and drying. The obtained incense has the effects of high-efficiency antibiosis and air freshening. The preparation method has the advantages of simple operation, convenient material acquisition and suitability for large-scale production.
Description
Technical Field
The invention belongs to the field of incense, and particularly relates to efficient antibacterial incense.
Background
The aromatherapy is a natural therapy for stimulating the respiratory system and skin of a human body by natural volatilization or combustion of plants. Has a long history around the world and is widely used. Especially in China, under the influence of traditional Chinese medicines, the traditional Chinese medicine incense therapy is invented very early in ancient times in China and is applied to clinic for preventing and treating various diseases. Therefore, a large number of incense formulas are summarized in the traditional Chinese medical history, and most of the incense formulas are used for preventing and treating various common infectious diseases.
Clinically, the existing traditional Chinese medicine formula for resisting bacteria has a few incense and better and fewer antibacterial effects, so that the incense which is convenient to obtain materials, free of side effect and efficient in antibiosis is very necessary.
Disclosure of Invention
The invention aims to provide an efficient antibacterial incense. The incense has strong antibacterial effect, and has effects of refreshing air, and preventing and treating infectious diseases.
The purpose of the invention is realized by the following technical scheme:
the efficient antibacterial incense comprises effective components and an adhesive, wherein the effective components comprise the following components in parts by weight: 30-40 parts of sappan wood, 15-25 parts of cacumen biotae and 8-12 parts of honeysuckle.
Further, the effective components comprise the following components in parts by weight: 33-37 parts of sappan wood, 13-17 parts of cacumen biotae and 9-11 parts of honeysuckle.
Furthermore, the effective components comprise the following components in parts by weight: 35 parts of sappan wood, 15 parts of cacumen biotae and 10 parts of honeysuckle.
Further, the adhesive is Indonesia nanmu sticky powder or elm bark powder.
The traditional Chinese medicine used in the invention:
sappan wood: sappan wood, also known as mahogany, Su balk and Su yang, is the dry heartwood of sappan wood of leguminosae, and it is sweet, salty, pungent and cool in nature and enters heart, liver and spleen meridians. Has effects of promoting blood circulation, removing blood stasis, relieving swelling and pain, and can be used for treating amenorrhea, dysmenorrhea, blood stasis, heart and abdominal pain, and traumatic swelling and pain. The pharmacological actions of the sapanwood mainly include the pharmacological actions of resisting inflammation, immunosuppression, resisting tumor, protecting blood vessels, resisting rejection reaction of heart transplantation, resisting oxidation and the like.
Honeysuckle flower: is flower bud of Lonicera japonica Thunb, Lonicera confusa Thunb, Lonicera japonica Thunb, and Lonicera fulvidraco of Caprifoliaceae, has effects of clearing heat and detoxicating, and dispelling pathogenic wind heat, and is centrally distributed in Henan, Shandong, Guangdong, etc. The honeysuckle flower mainly comprises organic acids, flavonoids, iridoid glycosides, triterpenoid saponins, volatile oil and other various components. The pharmacological actions of honeysuckle flower are mainly anti-inflammatory, antipyretic, anti-tumor, antibacterial, antiviral, anti-aging, anti-oxidation, blood sugar reduction, liver protection, lung protection, neuroprotection, organism immunity enhancement, platelet aggregation resistance and the like.
Cacumen biotae: is the branch tip and leaf of Platycladus orientalis of Cupressaceae. Bitter, astringent and slightly cold in nature. Has effects in cooling blood, stopping bleeding, relieving cough, eliminating phlegm, dispelling pathogenic wind, removing dampness, and removing toxic materials. In many pharmaceutical works, the Chinese arborvitae twig has the medicinal value of treating hematemesis, blood loss, epistaxis, dysentery, metrorrhagia, metrostaxis, wind-arthralgia, pain, expelling wind, promoting urination, dissipating fatigue and the like. The pharmacological actions of the cacumen biotae mainly include multiple pharmacological actions such as antibiosis, anti-inflammation, anti-tumor, antioxidation, neuroprotection, antilipemic and the like.
A preparation method of high-efficiency antibacterial incense comprises the following steps:
(1) weighing sappan wood, cacumen biotae and honeysuckle according to the proportion, adding 8-10 times of distilled water, heating and extracting for 2-3 times, wherein the extraction time is 2-3 h each time, filtering after each extraction, combining filtrates, and concentrating to obtain a clear paste;
(2) and (2) adding the adhesive into the clear paste prepared in the step (1), mixing and stirring uniformly, shaping, and drying to obtain the incense.
Further, the relative density of the clear paste in the step (1) is 1.0-1.2.
Further, in the step (2), the weight ratio of the adhesive to the clear paste is 2-4: 1.
further, the weight ratio of the adhesive to the clear paste in the step (2) is 3: 1.
further, drying in the step (2) at the temperature of 60-80 ℃ for 12-24 hours.
Further, the water content of the incense is controlled below 9%.
The invention has the following positive effects:
the invention provides a traditional Chinese medicine composition incense with brand new antibacterial and disinfection effects, which is prepared by adopting water extracts of a composition of sappan wood, cacumen biotae and honeysuckle as antibacterial active ingredients, has better antibacterial effects than the use of a single traditional Chinese medicine of sappan wood, cacumen biotae and honeysuckle as incense, and shows that the three medicines can generate synergistic antibacterial effects after being mixed.
The incense prepared by the invention has strong antibacterial effect and no toxic or side effect, and the emitted light fragrance can refresh the air and make people joyful.
Detailed Description
The present invention is further described in the following examples, which should not be construed as limiting the scope of the invention, but rather as providing the following examples which are set forth to illustrate and not limit the scope of the invention.
Example 1
A preparation method of high-efficiency antibacterial incense comprises the following steps:
weighing 35g of sappan wood, 15g of cacumen biotae and 10g of honeysuckle, adding 10 times of distilled water, heating and extracting for 2 times, wherein the extraction time is 2 hours each time, filtering after each extraction, and combining the filtrates to obtain a medicinal material extracting solution. Concentrating the medicinal material extractive solution at 80 deg.C to relative density of 1.12 to obtain medicinal material concentrated solution; adding adhesive of 3 times the weight of the clear paste into the medicinal material concentrated solution, mixing and stirring uniformly, shaping, drying at 60 ℃ for 24 hours, and obtaining the product with 7% of water.
Example 2
A preparation method of high-efficiency antibacterial incense comprises the following steps:
weighing 35g of sappan wood, 15g of cacumen biotae and 10g of honeysuckle, adding 10 times of distilled water, heating and extracting for 2 times, wherein the extraction time is 2 hours each time, filtering after each extraction, and combining the filtrates to obtain a medicinal material extracting solution. Concentrating the medicinal material extractive solution at 80 deg.C to relative density of 1.04 to obtain medicinal material concentrated solution; adding adhesive of 3 times the weight of the clear paste into the concentrated medicinal material solution, mixing and stirring uniformly, and shaping, wherein the drying temperature is 50 ℃, the time is 20 hours, and the water content is 5 percent.
Example 3
A preparation method of high-efficiency antibacterial incense comprises the following steps:
weighing 35g of sappan wood, 15g of cacumen biotae and 10g of honeysuckle, adding 10 times of distilled water, heating and extracting for 2 times, wherein the extraction time is 2 hours each time, filtering after each extraction, and combining the filtrates to obtain a medicinal material extracting solution. Concentrating the medicinal material extractive solution at 80 deg.C to relative density of 1.18 to obtain medicinal material concentrated solution; adding adhesive of 3 times the weight of the clear paste into the concentrated medicinal material solution, mixing and stirring uniformly, and shaping, wherein the drying temperature is 60 ℃, the drying time is 20 hours, and the water content is 9 percent.
Comparative example 1
The preparation method of the sappan wood incense comprises the following steps:
weighing 60g of sappan wood, adding 10 times of distilled water, heating and extracting for 2 times, wherein the extraction time is 2h each time, filtering after each extraction, and combining the filtrates to obtain a medicinal material extract. Concentrating the medicinal material extractive solution at 80 deg.C to relative density of 1.15 to obtain medicinal material concentrated solution; adding adhesive of 3 times the weight of the clear paste into the concentrated medicinal material solution, mixing and stirring uniformly, shaping, drying at 60 ℃ for 20 hours, and obtaining the product with 7% of water.
Comparative example 2
The preparation method of the cacumen biotae incense comprises the following steps:
weighing 60g of cacumen biotae, adding 10 times of distilled water, heating and extracting for 2 times, wherein the extraction time is 2h each time, filtering after each extraction, and combining the filtrates to obtain a medicinal material extracting solution. Concentrating the medicinal material extractive solution at 80 deg.C to relative density of 1.14 to obtain medicinal material concentrated solution; adding adhesive of 3 times the weight of the clear paste into the concentrated medicinal material solution, mixing and stirring uniformly, shaping, drying at 60 ℃ for 20 hours, and obtaining the product with 7% of water.
Comparative example 3
The preparation method of the honeysuckle incense comprises the following steps:
weighing 60g of honeysuckle, adding distilled water with the volume 10 times of that of the honeysuckle, heating and extracting for 2 times, wherein the extraction time is 2 hours each time, filtering after each extraction, and combining the filtrates to obtain a medicinal material extracting solution. Concentrating the medicinal material extractive solution at 80 deg.C to relative density of 1.09 to obtain medicinal material concentrated solution; adding adhesive of 3 times the weight of the clear paste into the concentrated medicinal material solution, mixing and stirring uniformly, shaping, drying at 60 ℃ for 20 hours, and obtaining the product with 7% of water.
Example 4
In vitro bacteriostasis test
1. Test strains
Staphylococcus aureus, Escherichia coli, Streptococcus, Corynebacterium diphtheriae
2. Reagent
Test solution: taking 1g of incense prepared in examples 1-3 and comparative examples 1-3, igniting the incense, putting the incense into a large conical flask, pumping air to dissolve the smoke through a gas collecting bottle washing device until the smoke is completely combusted, combining the solutions of 3 gas collecting bottles, concentrating the solution into a solution with the incense crude drug concentration of 10g/mL in a 60 ℃ oven, absorbing and concentrating the solution with 75% ethanol to obtain an ethanol dissolved substance, drying the ethanol dissolved substance to remove the ethanol, re-dissolving the ethanol dissolved substance with DMSO to obtain an ethanol-DMSO dissolved substance, and filtering and sterilizing the ethanol-DMSO dissolved substance by 0.22 mu m to obtain the incense;
control group: gentamicin and penicillin
3. Method and results
The concentration of the test bacteria prepared by the conventional method is 106Taking the bacterial liquid with a small sterilized cotton swab, slightly drawing lines in parallel and in cross in four different directions to uniformly coat the bacterial liquid on an agar plate 1; respectively placing the test solution, gentamicin and penicillin prepared in the embodiments 1-3 and the comparative examples 1-3 of the invention on different areas of the surface of the agar plate 1 inoculated with the flora and marking; the plates were incubated at 37 ℃ for 24 hours, the conditions of the inhibition rings around the paper sheets were observed, and the diameters of the inhibition rings were measured as shown in table 1 below, and the inhibitory effects of the respective incense were compared.
TABLE 1 results of measurement of zone of inhibition (mm)
As can be seen from Table 1, the incense of the examples 1-3 and the incense of the comparative examples 1-3 of the invention can play a good role in inhibiting the test strains, and particularly, the examples 1-3 have better bacteriostatic effect, which is close to that of the existing antibiotics gentamicin and penicillin. The result shows that the incense prepared by the sappan wood, the cacumen biotae and the honeysuckle in the form of the traditional Chinese medicine composition generates a synergistic effect, and has better bacteriostatic effect than the incense prepared by single traditional Chinese medicine.
Example 5
Test of sterilizing Effect
1. Test strains
Staphylococcus aureus, Escherichia coli, Streptococcus, Corynebacterium diphtheriae
2. Reagent
Incense prepared in examples 1 to 3 and comparative examples 1 to 3
3. Method and results
The bacterial suspension (corresponding to 10) was suspended in LB medium at a concentration of 0.5 M.turbidimetric at a super clean bench6CFU/mL bacterial concentration) dilution 105Taking 100 mul of the bacterial liquid, and evenly spreading the bacterial liquid on a sterile M-H agar culture medium with the thickness of 100 mm. Igniting Chinese medicinal incense in a clean bench, covering the coated plate with a cover, covering the cover, and covering the plate with the smoke for 30min, culturing at 37 deg.C for 12 hr, repeating for 3 times, observing and recording the number of bacterial plaques in different time
Table 2 bacterial test plaque number results (CFU 10)5)
Table 3 bacterial test plaque number calculation results (%)
The results of the incense tests of the simulated on-site sterilization test are shown in tables 2 and 3, and after the incense is smoked for 30min, each incense group can play a good sterilization role on the test strains, wherein the effect on staphylococcus aureus is the best, and the sterilization rate reaches 96%. Secondly, examples 1 to 3 have a better bactericidal effect than comparative examples 1 to 3. The result shows that the incense prepared by the sappan wood, the cacumen biotae and the honeysuckle in the form of the traditional Chinese medicine composition generates a synergistic effect and has better sterilization effect than the incense prepared by single traditional Chinese medicine.
Claims (10)
1. The efficient antibacterial incense is characterized by comprising effective components and an adhesive, wherein the effective components comprise the following components in parts by weight: 30-40 parts of sappan wood, 15-25 parts of cacumen biotae and 8-12 parts of honeysuckle.
2. The incense of claim 1, wherein the effective components comprise the following components in parts by weight: 33-37 parts of sappan wood, 13-17 parts of cacumen biotae and 9-11 parts of honeysuckle.
3. The incense of claim 1, wherein the effective components comprise the following components in parts by weight: 35 parts of sappan wood, 15 parts of cacumen biotae and 10 parts of honeysuckle.
4. The incense of claim 1 wherein the adhesive is a Indonesia wood flour or elm bark flour.
5. The method for preparing incense as claimed in any of claims 1 to 4, comprising the steps of:
(1) weighing sappan wood, cacumen biotae and honeysuckle according to the proportion, adding 8-10 times of distilled water, heating and extracting for 2-3 times, wherein the extraction time is 2-3 h each time, filtering after each extraction, combining filtrates, and concentrating to obtain a clear paste;
(2) and (2) adding the adhesive into the clear paste prepared in the step (1), mixing and stirring uniformly, shaping, and drying to obtain the incense.
6. The preparation method according to claim 5, wherein the relative density of the fluid extract in the step (1) is 1.0-1.2.
7. The preparation method according to claim 5, wherein the weight ratio of the adhesive to the fluid extract in the step (2) is 2-4: 1.
8. the preparation method according to claim 5, wherein the weight ratio of the adhesive to the fluid extract in the step (2) is 3: 1.
9. the preparation method according to claim 5, wherein the drying in the step (2) is carried out at a temperature of 60 ℃ to 80 ℃ for 12 hours to 24 hours.
10. The method according to claim 5, wherein in the step (2), the moisture content of the incense is controlled to be 9% or less.
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202010065506.6A CN111166922A (en) | 2020-01-20 | 2020-01-20 | Efficient antibacterial incense |
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| CN202010065506.6A CN111166922A (en) | 2020-01-20 | 2020-01-20 | Efficient antibacterial incense |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN112913864A (en) * | 2021-02-04 | 2021-06-08 | 福建诚盛香业有限公司 | Insect-expelling and degerming sanitary incense and preparation method thereof |
| CN114651818A (en) * | 2022-03-30 | 2022-06-24 | 泉州永春达盛香业股份有限公司 | Antibacterial incense and manufacturing method thereof |
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| CN1685851A (en) * | 2005-05-04 | 2005-10-26 | 蓝子花 | Sappan wood epidemic prevention antibactericide product |
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2020
- 2020-01-20 CN CN202010065506.6A patent/CN111166922A/en active Pending
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| CN1685851A (en) * | 2005-05-04 | 2005-10-26 | 蓝子花 | Sappan wood epidemic prevention antibactericide product |
| CN101502273A (en) * | 2009-03-17 | 2009-08-12 | 刘玉强 | Chinese medicinal incense |
| CN102935245A (en) * | 2012-12-03 | 2013-02-20 | 晓健科技（大连）有限公司 | Wind-cold dispelling incense |
| CN110583754A (en) * | 2018-06-13 | 2019-12-20 | 邹晓劲 | Technology for preserving meat by using herbal medicine |
| CN110680018A (en) * | 2019-03-31 | 2020-01-14 | 株式会社东亚产业 | Support member for incense core and incense core having the same |
Non-Patent Citations (1)
| Title |
|---|
| 薛广波主编: "《现代消毒学》", 31 July 2002, 北京：人民军医出版社 * |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN112913864A (en) * | 2021-02-04 | 2021-06-08 | 福建诚盛香业有限公司 | Insect-expelling and degerming sanitary incense and preparation method thereof |
| CN114651818A (en) * | 2022-03-30 | 2022-06-24 | 泉州永春达盛香业股份有限公司 | Antibacterial incense and manufacturing method thereof |
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