CN111132985B - 用于制造甲基氯氢单硅烷的集成工艺 - Google Patents

用于制造甲基氯氢单硅烷的集成工艺 Download PDF

Info

Publication number
CN111132985B
CN111132985B CN201880061250.2A CN201880061250A CN111132985B CN 111132985 B CN111132985 B CN 111132985B CN 201880061250 A CN201880061250 A CN 201880061250A CN 111132985 B CN111132985 B CN 111132985B
Authority
CN
China
Prior art keywords
sime
reaction
mesi
process according
redistribution
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Active
Application number
CN201880061250.2A
Other languages
English (en)
Chinese (zh)
Other versions
CN111132985A (zh
Inventor
N.奥纳
T.桑托夫斯基
A.G.斯图姆
T.费尔德
K.刘易斯
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Momentive Performance Materials Inc
Original Assignee
Momentive Performance Materials Inc
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Momentive Performance Materials Inc filed Critical Momentive Performance Materials Inc
Publication of CN111132985A publication Critical patent/CN111132985A/zh
Application granted granted Critical
Publication of CN111132985B publication Critical patent/CN111132985B/zh
Active legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07FACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F7/00Compounds containing elements of Groups 4 or 14 of the Periodic Table
    • C07F7/02Silicon compounds
    • C07F7/08Compounds having one or more C—Si linkages
    • C07F7/12Organo silicon halides
    • C07F7/14Preparation thereof from optionally substituted halogenated silanes and hydrocarbons hydrosilylation reactions
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07FACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F7/00Compounds containing elements of Groups 4 or 14 of the Periodic Table
    • C07F7/02Silicon compounds
    • C07F7/08Compounds having one or more C—Si linkages
    • C07F7/12Organo silicon halides
    • C07F7/121Preparation or treatment not provided for in C07F7/14, C07F7/16 or C07F7/20
    • C07F7/126Preparation or treatment not provided for in C07F7/14, C07F7/16 or C07F7/20 by reactions involving the formation of Si-Y linkages, where Y is not a carbon or halogen atom
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02PCLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00Technologies relating to chemical industry
    • Y02P20/10Process efficiency

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Catalysts (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
CN201880061250.2A 2017-09-20 2018-09-20 用于制造甲基氯氢单硅烷的集成工艺 Active CN111132985B (zh)

Applications Claiming Priority (5)

Application Number Priority Date Filing Date Title
US201762560855P 2017-09-20 2017-09-20
US62/560,855 2017-09-20
EP18177918 2018-06-15
EP18177918.2 2018-06-15
PCT/US2018/051861 WO2019060487A1 (en) 2017-09-20 2018-09-20 INTEGRATED PROCESS FOR PRODUCING METHYLCHLOROHYDRIDOMONOSILANES

Publications (2)

Publication Number Publication Date
CN111132985A CN111132985A (zh) 2020-05-08
CN111132985B true CN111132985B (zh) 2024-01-02

Family

ID=64755695

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201880061250.2A Active CN111132985B (zh) 2017-09-20 2018-09-20 用于制造甲基氯氢单硅烷的集成工艺

Country Status (5)

Country Link
US (1) US11518773B2 (enExample)
EP (1) EP3684778B1 (enExample)
JP (1) JP2020534323A (enExample)
CN (1) CN111132985B (enExample)
WO (1) WO2019060487A1 (enExample)

Families Citing this family (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2019060485A1 (en) * 2017-09-20 2019-03-28 Momentive Performance Materials Inc. PROCESS FOR PRODUCING ORGANOHYDRIDOCHLOROSILANES
EP4069706A1 (en) * 2019-12-03 2022-10-12 Dow Silicones Corporation Branched oxydisilane/siloxane oligomers and methods for their preparation and use as heat transfer fluids
EP3915995B1 (en) * 2020-05-29 2025-11-26 Momentive Performance Materials Inc. Process for the stepwise synthesis of silahydrocarbons
CN113651844B (zh) * 2021-08-20 2023-09-12 唐山偶联硅业有限公司 连续法制备二甲基氢氯硅烷的工艺
CN114181243B (zh) * 2021-12-01 2024-04-02 浙江皇马科技股份有限公司 一种甲基二甲氧基氢硅烷的制备方法
KR20250120303A (ko) 2022-11-22 2025-08-08 모멘티브 퍼포먼스 머티리얼즈 게엠베하 하이드리도실란 제조 방법

Citations (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB851013A (en) * 1955-12-19 1960-10-12 Gen Electric Reduction of silicon compounds
US4115426A (en) * 1977-02-02 1978-09-19 Kawaken Fine Chemicals Co., Ltd. Method for the preparation of dialkylchlorosilanes
US4629801A (en) * 1985-02-04 1986-12-16 Rhone-Poulenc Specialites Chimiques Preparation of hydrogenosilanes
EP0380837A1 (en) * 1985-11-27 1990-08-08 E.I. Du Pont De Nemours And Company Process for reducing silicon, germanium and tin halides
JPH0324091A (ja) * 1989-06-21 1991-02-01 Tonen Chem Corp ジアルキルモノクロロシランの製造方法
US5252768A (en) * 1992-03-13 1993-10-12 Wacker-Chemie Gmbh Process for preparing a dimethylchlorosilane
CN1854145A (zh) * 2005-04-26 2006-11-01 瓦克化学股份公司 有机基氢硅烷的制造方法
CN104144934A (zh) * 2011-12-30 2014-11-12 莫门蒂夫性能材料股份有限公司 由常规非可裂化的直接法残留物合成有机基卤代硅烷单体

Family Cites Families (37)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US1501756A (en) * 1922-08-18 1924-07-15 Roessler & Hasslacher Chemical Electrolytic process and cell
US2458703A (en) * 1947-06-11 1949-01-11 Libbey Owens Ford Glass Co Reduction of compounds of silicon and halogen
US3099671A (en) * 1955-12-19 1963-07-30 Gen Electric Preparation of organosilanes
US3496206A (en) * 1967-06-01 1970-02-17 Gen Electric Method for making silicon hydrides
US3535092A (en) * 1968-06-14 1970-10-20 Gen Electric Reduction of halogen-containing silicon compounds
BE758312A (fr) 1969-11-03 1971-04-30 Dow Corning Procede a haute temperature pour la preparation de composes contenant des liaisons silicium-hydrogene
US3872220A (en) * 1974-01-24 1975-03-18 Foote Mineral Co Process for the production of lithium chloride
US4007257A (en) * 1975-03-27 1977-02-08 Atomic Energy Of Canada Limited Alkali metal hydride formation
JPS52151130A (en) * 1976-06-07 1977-12-15 Toshiba Silicone Preparation of dimethylchlorosilane
ES462575A1 (es) * 1976-09-24 1978-07-16 Union Carbide Corp Un procedimiento para la obtencion de silano.
DE2722221A1 (de) * 1977-05-17 1978-11-23 Studiengesellschaft Kohle Mbh Alkalimetallkomplexverbindungen, verfahren zu ihrer herstellung und ihre verwendung zur hydrierung und nitridierung von alkalimetallen
US4139428A (en) * 1977-10-31 1979-02-13 E. I. Du Pont De Nemours And Company Preparation of alkali metals
US4274834A (en) * 1979-04-11 1981-06-23 Foote Mineral Company Process for purification of lithium chloride
US4295986A (en) * 1979-05-14 1981-10-20 Gordon Roy G Low temperature catalytic reduction
US4291167A (en) * 1980-07-28 1981-09-22 Nalco Chemical Company Preparation of tetramethyldisilane from 1,2-tetramethyldichlorodisilane
FR2504109A1 (fr) * 1981-04-17 1982-10-22 Rhone Poulenc Spec Chim Procede de preparation de silane en milieu sels fondus
FR2532290A1 (fr) * 1982-08-31 1984-03-02 Rhone Poulenc Spec Chim Procede et dispositif d'hydrogenation en continu du lithium dans un melange de sels fondus
JPH0753574B2 (ja) * 1985-06-11 1995-06-07 三井東圧化学株式会社 シラン類の不均化方法
JPS6348289A (ja) * 1986-08-18 1988-02-29 Mitsui Toatsu Chem Inc アルキルクロロシラン類の製造方法
DE3637273C1 (de) * 1986-11-03 1988-04-07 Goldschmidt Ag Th Verfahren zur Herstellung von SiH-Gruppen enthaltenden Organopolysiloxanen
US4814155A (en) 1987-07-27 1989-03-21 Dow Corning Corporation Method of selective reduction of polyhalosilanes with alkyltin hydrides
US4973725A (en) 1988-06-28 1990-11-27 Union Carbide Chemicals And Plastics Company Inc. Direct synthesis process for organohalohydrosilanes
JPH0635466B2 (ja) * 1988-09-28 1994-05-11 信越化学工業株式会社 ジオルガノハロゲノシランの製造方法
US4980136A (en) * 1989-07-14 1990-12-25 Cyprus Foote Mineral Company Production of lithium metal grade lithium chloride from lithium-containing brine
US4966986A (en) 1989-08-03 1990-10-30 Dow Corning Corporation Method for preparing organohalosilanes
US4965388A (en) 1990-01-02 1990-10-23 Dow Corning Corporation Method for preparing organohalosilanes
US5300614A (en) * 1990-08-27 1994-04-05 E. I. Du Pont De Nemours And Company Silicon carbide precursors
US5136070A (en) 1991-12-23 1992-08-04 Dow Corning Corporation Sodium borohydride catalyzed disproportionation of cycloorganosilanes
DE19520737C2 (de) 1995-06-07 2003-04-24 Degussa Verfahren zur Herstellung von Alkylhydrogenchlorsilanen
US5856548A (en) 1997-05-17 1999-01-05 Th. Goldschmidt Ag Process for preparing dimethylmonochlorosilane
JP4458295B2 (ja) * 2007-02-21 2010-04-28 信越化学工業株式会社 ジメチルクロロシランの製造方法
RU2436788C1 (ru) 2010-05-18 2011-12-20 Общество с ограниченной ответственностью "Пермская химическая компания" Способ получения алкилсиланов
CN104892659A (zh) 2015-06-15 2015-09-09 常熟三爱富中昊化工新材料有限公司 一种二烷基一氯硅烷的合成方法
WO2019060485A1 (en) * 2017-09-20 2019-03-28 Momentive Performance Materials Inc. PROCESS FOR PRODUCING ORGANOHYDRIDOCHLOROSILANES
RU2020113716A (ru) * 2017-09-20 2021-10-20 Моментив Перформанс Матириалз Инк. Способ получения органогидрохлорсиланов
CN108129510B (zh) * 2018-01-17 2019-06-11 中国科学院化学研究所 一种氯烷基氢硅烷的制备方法
CN108530477B (zh) * 2018-06-08 2019-06-07 中国科学院化学研究所 一种氢化锂选择性还原氯烷基氯硅烷的方法

Patent Citations (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB851013A (en) * 1955-12-19 1960-10-12 Gen Electric Reduction of silicon compounds
US4115426A (en) * 1977-02-02 1978-09-19 Kawaken Fine Chemicals Co., Ltd. Method for the preparation of dialkylchlorosilanes
US4629801A (en) * 1985-02-04 1986-12-16 Rhone-Poulenc Specialites Chimiques Preparation of hydrogenosilanes
EP0380837A1 (en) * 1985-11-27 1990-08-08 E.I. Du Pont De Nemours And Company Process for reducing silicon, germanium and tin halides
JPH0324091A (ja) * 1989-06-21 1991-02-01 Tonen Chem Corp ジアルキルモノクロロシランの製造方法
US5252768A (en) * 1992-03-13 1993-10-12 Wacker-Chemie Gmbh Process for preparing a dimethylchlorosilane
CN1854145A (zh) * 2005-04-26 2006-11-01 瓦克化学股份公司 有机基氢硅烷的制造方法
CN104144934A (zh) * 2011-12-30 2014-11-12 莫门蒂夫性能材料股份有限公司 由常规非可裂化的直接法残留物合成有机基卤代硅烷单体

Non-Patent Citations (3)

* Cited by examiner, † Cited by third party
Title
Reduction of Alkylchlorosilanes by Sodium Hydride and Hydrogen-Chlorine Interchange in Chlorosilanes;ALFRED R. GILBERT 等;《Industrial and Engineering Chemistry》;19591231;第51卷(第5期);第665-668页 *
Selective Reduction of Dichlorodimethylsilane to chlorodimethylsilane;N. P. Sluchevskaya 等;《Journal of General Chemistry USSR》;19891231;第1647-1650页 *
Thermochemistry of Silicon-containing Compounds;ROBIN WALSH;《J. Chem. SOC.》;19831231;第79卷;第2233-2248页 *

Also Published As

Publication number Publication date
CN111132985A (zh) 2020-05-08
US11518773B2 (en) 2022-12-06
EP3684778B1 (en) 2023-08-02
RU2020113710A3 (enExample) 2022-04-29
RU2020113710A (ru) 2021-10-20
JP2020534323A (ja) 2020-11-26
WO2019060487A1 (en) 2019-03-28
EP3684778A1 (en) 2020-07-29
US20200262851A1 (en) 2020-08-20

Similar Documents

Publication Publication Date Title
CN111132985B (zh) 用于制造甲基氯氢单硅烷的集成工艺
WANNAGAT N-metallated silicon-nitrogen derivatives: preparation, structure and reactions
US11008349B2 (en) Process for the production of organohydridochlorosilanes
CN112839904B (zh) 由四氯硅烷和氢硅烷合成三氯硅烷
EP0798302B1 (en) Method for preparation of allylsilanes
EP0405560B1 (en) Preparation of tertiary-hydrocarbylsilyl compounds
EP3684777B1 (en) Process for the production of organohydridochlorosilanes
WO2019060475A2 (en) SYNTHESIS OF ORGANO-CHLOROSILANES FROM ORGANOSILANES
RU2785123C2 (ru) Интегрированный способ получения метилхлоргидридмоносиланов
EP3915995B1 (en) Process for the stepwise synthesis of silahydrocarbons
WO2019060486A1 (en) PROCESS FOR PRODUCING ORGANOHYDRIDOCHLOROSILANES FROM HYDRUROSILANES
WO2019060480A1 (en) CLEANING OF METHYLILISILANES, CARBODISILANES AND METHYLOLIGOSILANES WITH SALTS OF ALKALI AND ALKALINE-EARTH METALS
WO2019060481A1 (en) CLEAVING DISILANE, CARBODISILANE AND OLIGOSILANE WITH CLEAVING COMPOUND AS CATALYST AND HYDROGENATION SOURCE
KR20250120303A (ko) 하이드리도실란 제조 방법
Griess et al. Hydrosilanes. From Laboratory Curiosity to Semiconductors
WO2020001955A1 (en) Partially hydrogenated chlorosilanes and methods for preparing same by selective hydrogenation
CN114206815B (zh) 卤化四甲硅烷基硼酸盐
WO2019060479A1 (en) CLEAVAGE OF METHYLDISILANES IN METHYLMONOSILANES

Legal Events

Date Code Title Description
PB01 Publication
PB01 Publication
SE01 Entry into force of request for substantive examination
SE01 Entry into force of request for substantive examination
GR01 Patent grant
GR01 Patent grant