CN111132985B - 用于制造甲基氯氢单硅烷的集成工艺 - Google Patents
用于制造甲基氯氢单硅烷的集成工艺 Download PDFInfo
- Publication number
- CN111132985B CN111132985B CN201880061250.2A CN201880061250A CN111132985B CN 111132985 B CN111132985 B CN 111132985B CN 201880061250 A CN201880061250 A CN 201880061250A CN 111132985 B CN111132985 B CN 111132985B
- Authority
- CN
- China
- Prior art keywords
- sime
- reaction
- mesi
- process according
- redistribution
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
- C07F7/00—Compounds containing elements of Groups 4 or 14 of the Periodic Table
- C07F7/02—Silicon compounds
- C07F7/08—Compounds having one or more C—Si linkages
- C07F7/12—Organo silicon halides
- C07F7/14—Preparation thereof from optionally substituted halogenated silanes and hydrocarbons hydrosilylation reactions
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
- C07F7/00—Compounds containing elements of Groups 4 or 14 of the Periodic Table
- C07F7/02—Silicon compounds
- C07F7/08—Compounds having one or more C—Si linkages
- C07F7/12—Organo silicon halides
- C07F7/121—Preparation or treatment not provided for in C07F7/14, C07F7/16 or C07F7/20
- C07F7/126—Preparation or treatment not provided for in C07F7/14, C07F7/16 or C07F7/20 by reactions involving the formation of Si-Y linkages, where Y is not a carbon or halogen atom
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P20/00—Technologies relating to chemical industry
- Y02P20/10—Process efficiency
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Catalysts (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
Applications Claiming Priority (5)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US201762560855P | 2017-09-20 | 2017-09-20 | |
| US62/560,855 | 2017-09-20 | ||
| EP18177918 | 2018-06-15 | ||
| EP18177918.2 | 2018-06-15 | ||
| PCT/US2018/051861 WO2019060487A1 (en) | 2017-09-20 | 2018-09-20 | INTEGRATED PROCESS FOR PRODUCING METHYLCHLOROHYDRIDOMONOSILANES |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN111132985A CN111132985A (zh) | 2020-05-08 |
| CN111132985B true CN111132985B (zh) | 2024-01-02 |
Family
ID=64755695
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201880061250.2A Active CN111132985B (zh) | 2017-09-20 | 2018-09-20 | 用于制造甲基氯氢单硅烷的集成工艺 |
Country Status (5)
| Country | Link |
|---|---|
| US (1) | US11518773B2 (enExample) |
| EP (1) | EP3684778B1 (enExample) |
| JP (1) | JP2020534323A (enExample) |
| CN (1) | CN111132985B (enExample) |
| WO (1) | WO2019060487A1 (enExample) |
Families Citing this family (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2019060485A1 (en) * | 2017-09-20 | 2019-03-28 | Momentive Performance Materials Inc. | PROCESS FOR PRODUCING ORGANOHYDRIDOCHLOROSILANES |
| EP4069706A1 (en) * | 2019-12-03 | 2022-10-12 | Dow Silicones Corporation | Branched oxydisilane/siloxane oligomers and methods for their preparation and use as heat transfer fluids |
| EP3915995B1 (en) * | 2020-05-29 | 2025-11-26 | Momentive Performance Materials Inc. | Process for the stepwise synthesis of silahydrocarbons |
| CN113651844B (zh) * | 2021-08-20 | 2023-09-12 | 唐山偶联硅业有限公司 | 连续法制备二甲基氢氯硅烷的工艺 |
| CN114181243B (zh) * | 2021-12-01 | 2024-04-02 | 浙江皇马科技股份有限公司 | 一种甲基二甲氧基氢硅烷的制备方法 |
| KR20250120303A (ko) | 2022-11-22 | 2025-08-08 | 모멘티브 퍼포먼스 머티리얼즈 게엠베하 | 하이드리도실란 제조 방법 |
Citations (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB851013A (en) * | 1955-12-19 | 1960-10-12 | Gen Electric | Reduction of silicon compounds |
| US4115426A (en) * | 1977-02-02 | 1978-09-19 | Kawaken Fine Chemicals Co., Ltd. | Method for the preparation of dialkylchlorosilanes |
| US4629801A (en) * | 1985-02-04 | 1986-12-16 | Rhone-Poulenc Specialites Chimiques | Preparation of hydrogenosilanes |
| EP0380837A1 (en) * | 1985-11-27 | 1990-08-08 | E.I. Du Pont De Nemours And Company | Process for reducing silicon, germanium and tin halides |
| JPH0324091A (ja) * | 1989-06-21 | 1991-02-01 | Tonen Chem Corp | ジアルキルモノクロロシランの製造方法 |
| US5252768A (en) * | 1992-03-13 | 1993-10-12 | Wacker-Chemie Gmbh | Process for preparing a dimethylchlorosilane |
| CN1854145A (zh) * | 2005-04-26 | 2006-11-01 | 瓦克化学股份公司 | 有机基氢硅烷的制造方法 |
| CN104144934A (zh) * | 2011-12-30 | 2014-11-12 | 莫门蒂夫性能材料股份有限公司 | 由常规非可裂化的直接法残留物合成有机基卤代硅烷单体 |
Family Cites Families (37)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US1501756A (en) * | 1922-08-18 | 1924-07-15 | Roessler & Hasslacher Chemical | Electrolytic process and cell |
| US2458703A (en) * | 1947-06-11 | 1949-01-11 | Libbey Owens Ford Glass Co | Reduction of compounds of silicon and halogen |
| US3099671A (en) * | 1955-12-19 | 1963-07-30 | Gen Electric | Preparation of organosilanes |
| US3496206A (en) * | 1967-06-01 | 1970-02-17 | Gen Electric | Method for making silicon hydrides |
| US3535092A (en) * | 1968-06-14 | 1970-10-20 | Gen Electric | Reduction of halogen-containing silicon compounds |
| BE758312A (fr) | 1969-11-03 | 1971-04-30 | Dow Corning | Procede a haute temperature pour la preparation de composes contenant des liaisons silicium-hydrogene |
| US3872220A (en) * | 1974-01-24 | 1975-03-18 | Foote Mineral Co | Process for the production of lithium chloride |
| US4007257A (en) * | 1975-03-27 | 1977-02-08 | Atomic Energy Of Canada Limited | Alkali metal hydride formation |
| JPS52151130A (en) * | 1976-06-07 | 1977-12-15 | Toshiba Silicone | Preparation of dimethylchlorosilane |
| ES462575A1 (es) * | 1976-09-24 | 1978-07-16 | Union Carbide Corp | Un procedimiento para la obtencion de silano. |
| DE2722221A1 (de) * | 1977-05-17 | 1978-11-23 | Studiengesellschaft Kohle Mbh | Alkalimetallkomplexverbindungen, verfahren zu ihrer herstellung und ihre verwendung zur hydrierung und nitridierung von alkalimetallen |
| US4139428A (en) * | 1977-10-31 | 1979-02-13 | E. I. Du Pont De Nemours And Company | Preparation of alkali metals |
| US4274834A (en) * | 1979-04-11 | 1981-06-23 | Foote Mineral Company | Process for purification of lithium chloride |
| US4295986A (en) * | 1979-05-14 | 1981-10-20 | Gordon Roy G | Low temperature catalytic reduction |
| US4291167A (en) * | 1980-07-28 | 1981-09-22 | Nalco Chemical Company | Preparation of tetramethyldisilane from 1,2-tetramethyldichlorodisilane |
| FR2504109A1 (fr) * | 1981-04-17 | 1982-10-22 | Rhone Poulenc Spec Chim | Procede de preparation de silane en milieu sels fondus |
| FR2532290A1 (fr) * | 1982-08-31 | 1984-03-02 | Rhone Poulenc Spec Chim | Procede et dispositif d'hydrogenation en continu du lithium dans un melange de sels fondus |
| JPH0753574B2 (ja) * | 1985-06-11 | 1995-06-07 | 三井東圧化学株式会社 | シラン類の不均化方法 |
| JPS6348289A (ja) * | 1986-08-18 | 1988-02-29 | Mitsui Toatsu Chem Inc | アルキルクロロシラン類の製造方法 |
| DE3637273C1 (de) * | 1986-11-03 | 1988-04-07 | Goldschmidt Ag Th | Verfahren zur Herstellung von SiH-Gruppen enthaltenden Organopolysiloxanen |
| US4814155A (en) | 1987-07-27 | 1989-03-21 | Dow Corning Corporation | Method of selective reduction of polyhalosilanes with alkyltin hydrides |
| US4973725A (en) | 1988-06-28 | 1990-11-27 | Union Carbide Chemicals And Plastics Company Inc. | Direct synthesis process for organohalohydrosilanes |
| JPH0635466B2 (ja) * | 1988-09-28 | 1994-05-11 | 信越化学工業株式会社 | ジオルガノハロゲノシランの製造方法 |
| US4980136A (en) * | 1989-07-14 | 1990-12-25 | Cyprus Foote Mineral Company | Production of lithium metal grade lithium chloride from lithium-containing brine |
| US4966986A (en) | 1989-08-03 | 1990-10-30 | Dow Corning Corporation | Method for preparing organohalosilanes |
| US4965388A (en) | 1990-01-02 | 1990-10-23 | Dow Corning Corporation | Method for preparing organohalosilanes |
| US5300614A (en) * | 1990-08-27 | 1994-04-05 | E. I. Du Pont De Nemours And Company | Silicon carbide precursors |
| US5136070A (en) | 1991-12-23 | 1992-08-04 | Dow Corning Corporation | Sodium borohydride catalyzed disproportionation of cycloorganosilanes |
| DE19520737C2 (de) | 1995-06-07 | 2003-04-24 | Degussa | Verfahren zur Herstellung von Alkylhydrogenchlorsilanen |
| US5856548A (en) | 1997-05-17 | 1999-01-05 | Th. Goldschmidt Ag | Process for preparing dimethylmonochlorosilane |
| JP4458295B2 (ja) * | 2007-02-21 | 2010-04-28 | 信越化学工業株式会社 | ジメチルクロロシランの製造方法 |
| RU2436788C1 (ru) | 2010-05-18 | 2011-12-20 | Общество с ограниченной ответственностью "Пермская химическая компания" | Способ получения алкилсиланов |
| CN104892659A (zh) | 2015-06-15 | 2015-09-09 | 常熟三爱富中昊化工新材料有限公司 | 一种二烷基一氯硅烷的合成方法 |
| WO2019060485A1 (en) * | 2017-09-20 | 2019-03-28 | Momentive Performance Materials Inc. | PROCESS FOR PRODUCING ORGANOHYDRIDOCHLOROSILANES |
| RU2020113716A (ru) * | 2017-09-20 | 2021-10-20 | Моментив Перформанс Матириалз Инк. | Способ получения органогидрохлорсиланов |
| CN108129510B (zh) * | 2018-01-17 | 2019-06-11 | 中国科学院化学研究所 | 一种氯烷基氢硅烷的制备方法 |
| CN108530477B (zh) * | 2018-06-08 | 2019-06-07 | 中国科学院化学研究所 | 一种氢化锂选择性还原氯烷基氯硅烷的方法 |
-
2018
- 2018-09-20 JP JP2020516627A patent/JP2020534323A/ja not_active Withdrawn
- 2018-09-20 CN CN201880061250.2A patent/CN111132985B/zh active Active
- 2018-09-20 US US16/647,573 patent/US11518773B2/en active Active
- 2018-09-20 EP EP18825807.3A patent/EP3684778B1/en active Active
- 2018-09-20 WO PCT/US2018/051861 patent/WO2019060487A1/en not_active Ceased
Patent Citations (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB851013A (en) * | 1955-12-19 | 1960-10-12 | Gen Electric | Reduction of silicon compounds |
| US4115426A (en) * | 1977-02-02 | 1978-09-19 | Kawaken Fine Chemicals Co., Ltd. | Method for the preparation of dialkylchlorosilanes |
| US4629801A (en) * | 1985-02-04 | 1986-12-16 | Rhone-Poulenc Specialites Chimiques | Preparation of hydrogenosilanes |
| EP0380837A1 (en) * | 1985-11-27 | 1990-08-08 | E.I. Du Pont De Nemours And Company | Process for reducing silicon, germanium and tin halides |
| JPH0324091A (ja) * | 1989-06-21 | 1991-02-01 | Tonen Chem Corp | ジアルキルモノクロロシランの製造方法 |
| US5252768A (en) * | 1992-03-13 | 1993-10-12 | Wacker-Chemie Gmbh | Process for preparing a dimethylchlorosilane |
| CN1854145A (zh) * | 2005-04-26 | 2006-11-01 | 瓦克化学股份公司 | 有机基氢硅烷的制造方法 |
| CN104144934A (zh) * | 2011-12-30 | 2014-11-12 | 莫门蒂夫性能材料股份有限公司 | 由常规非可裂化的直接法残留物合成有机基卤代硅烷单体 |
Non-Patent Citations (3)
| Title |
|---|
| Reduction of Alkylchlorosilanes by Sodium Hydride and Hydrogen-Chlorine Interchange in Chlorosilanes;ALFRED R. GILBERT 等;《Industrial and Engineering Chemistry》;19591231;第51卷(第5期);第665-668页 * |
| Selective Reduction of Dichlorodimethylsilane to chlorodimethylsilane;N. P. Sluchevskaya 等;《Journal of General Chemistry USSR》;19891231;第1647-1650页 * |
| Thermochemistry of Silicon-containing Compounds;ROBIN WALSH;《J. Chem. SOC.》;19831231;第79卷;第2233-2248页 * |
Also Published As
| Publication number | Publication date |
|---|---|
| CN111132985A (zh) | 2020-05-08 |
| US11518773B2 (en) | 2022-12-06 |
| EP3684778B1 (en) | 2023-08-02 |
| RU2020113710A3 (enExample) | 2022-04-29 |
| RU2020113710A (ru) | 2021-10-20 |
| JP2020534323A (ja) | 2020-11-26 |
| WO2019060487A1 (en) | 2019-03-28 |
| EP3684778A1 (en) | 2020-07-29 |
| US20200262851A1 (en) | 2020-08-20 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN111132985B (zh) | 用于制造甲基氯氢单硅烷的集成工艺 | |
| WANNAGAT | N-metallated silicon-nitrogen derivatives: preparation, structure and reactions | |
| US11008349B2 (en) | Process for the production of organohydridochlorosilanes | |
| CN112839904B (zh) | 由四氯硅烷和氢硅烷合成三氯硅烷 | |
| EP0798302B1 (en) | Method for preparation of allylsilanes | |
| EP0405560B1 (en) | Preparation of tertiary-hydrocarbylsilyl compounds | |
| EP3684777B1 (en) | Process for the production of organohydridochlorosilanes | |
| WO2019060475A2 (en) | SYNTHESIS OF ORGANO-CHLOROSILANES FROM ORGANOSILANES | |
| RU2785123C2 (ru) | Интегрированный способ получения метилхлоргидридмоносиланов | |
| EP3915995B1 (en) | Process for the stepwise synthesis of silahydrocarbons | |
| WO2019060486A1 (en) | PROCESS FOR PRODUCING ORGANOHYDRIDOCHLOROSILANES FROM HYDRUROSILANES | |
| WO2019060480A1 (en) | CLEANING OF METHYLILISILANES, CARBODISILANES AND METHYLOLIGOSILANES WITH SALTS OF ALKALI AND ALKALINE-EARTH METALS | |
| WO2019060481A1 (en) | CLEAVING DISILANE, CARBODISILANE AND OLIGOSILANE WITH CLEAVING COMPOUND AS CATALYST AND HYDROGENATION SOURCE | |
| KR20250120303A (ko) | 하이드리도실란 제조 방법 | |
| Griess et al. | Hydrosilanes. From Laboratory Curiosity to Semiconductors | |
| WO2020001955A1 (en) | Partially hydrogenated chlorosilanes and methods for preparing same by selective hydrogenation | |
| CN114206815B (zh) | 卤化四甲硅烷基硼酸盐 | |
| WO2019060479A1 (en) | CLEAVAGE OF METHYLDISILANES IN METHYLMONOSILANES |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| GR01 | Patent grant | ||
| GR01 | Patent grant |