CN111117776A - Environment-friendly aromatherapy candle and preparation method thereof - Google Patents
Environment-friendly aromatherapy candle and preparation method thereof Download PDFInfo
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- CN111117776A CN111117776A CN201911415660.5A CN201911415660A CN111117776A CN 111117776 A CN111117776 A CN 111117776A CN 201911415660 A CN201911415660 A CN 201911415660A CN 111117776 A CN111117776 A CN 111117776A
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11C—FATTY ACIDS FROM FATS, OILS OR WAXES; CANDLES; FATS, OILS OR FATTY ACIDS BY CHEMICAL MODIFICATION OF FATS, OILS, OR FATTY ACIDS OBTAINED THEREFROM
- C11C5/00—Candles
- C11C5/002—Ingredients
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Abstract
The invention discloses an environment-friendly aromatherapy candle, which is prepared from 100 parts of main combustion agent and 5-15 parts of aromatherapy microcapsule, wherein the main combustion agent is hydrogenated high-methyl ethyl carbonate, and the aromatherapy microcapsule is prepared from a core material, a wall material, an emulsifier and deionized water. The invention effectively utilizes the nontoxicity, high formability and sufficient combustion of the hydrogenated high methyl ethyl carbonate, thereby being capable of preparing the environment-friendly scented candle which is easy to have good plasticity, good formability and no pollution stimulation. The adopted microcapsule matrix can form particles with good dispersibility of the oil-in-water phase, and the loss of aroma components in the storage and transportation process is effectively reduced.
Description
Technical Field
The invention relates to the technical field of daily chemicals, in particular to an environment-friendly aromatherapy candle and a preparation method thereof.
Background
The earliest considerable history of human use of natural fragrances in the four ancient civilizations dates to 3000 to 5000 years ago. From the existing data, the utilization of the perfume plants has already been started in the spring, autumn and warring countries. The wide popularity of incense in the noble group was in the early West Han, roughly traced back to Han Wudi, and incense burners specifically for incense were available at that time. After a long time of development, aromatherapy has been widely accepted and used, and many different aromatherapy products are emerging, with aromatherapy candles being one of the most common aromatherapy products.
The prior aromatherapy candle has two problems: firstly, petroleum wax and resin are added, so that carcinogenic benzene and toluene, toxic gas carbon monoxide and carbon-containing smoke are easily generated due to thermal decomposition or insufficient combustion during combustion, and indoor air is polluted; and secondly, essence and aromatic essential oil are doped, the chemical components are complex to match, and irritant gas is easily generated during combustion, so that the aromatherapy effect is influenced.
The natural plant essential oil is applied to the candle, so that the effects of 'cleaning the heart, tasting and beautifying, exciting Han Wen and harmonizing the body and mind' can be achieved. When the candle is burnt and melted, the candle emits pleasant fragrance during burning, has the effects of relieving nerves, purifying air and eliminating peculiar smell, and has special significance for modern people with continuously increased living and working pressure.
Disclosure of Invention
In order to overcome the disadvantages of the prior art, one of the objects of the present invention is to provide an environment-friendly candle which is free from petroleum source compounds and is not liable to generate harmful gases or fumes which are harmful to health.
The second purpose of the invention is to provide a preparation method of the environment-friendly smoked candle.
One of the purposes of the invention is realized by adopting the following technical scheme:
an environment-friendly aromatherapy candle is prepared from 100 parts of main burning agent and 5-15 parts of aromatherapy microcapsule, wherein the main burning agent is hydrogenated high-methyl ethyl carbonate, and the aromatherapy microcapsule is prepared from a core material, a wall material, an emulsifier and deionized water.
The application provides the hydrogenated high-methyl ethyl carbonate as the main burning agent of the environment-friendly aromatherapy candle, which has the advantages of better environmental protection, no toxicity, good formability and full combustion; meanwhile, the aromatherapy microcapsule is a water-emulsified water bubble oil phase, so that the volatilization loss of precious essential oil components in the storage and transportation process is effectively reduced, and the aromatherapy fragrance is volatilized only during combustion in the candle.
Specifically, the environment-friendly fragrance candle main combustion agent is prepared by the following method: the hydrogenated vegetable oil reacts with a methylation or ethylation reagent to extract the product of the methylation or ethylation vegetable oil, namely the hydrogenated high methyl ethyl carbonate.
Specifically, the aromatherapy microcapsule is prepared from 5-15 parts of core materials, 15-45 parts of wall materials, 5-15 parts of emulsifiers and 20-50 parts of deionized water.
The wall material is more than two of maltodextrin, β -cyclodextrin, fiber ester, starch or modified starch, the core material can be coated by the gelatinization and adsorption molding effect of the wall material to form the microcapsule with better moldability, wherein the starch is one or more of wheat starch, corn starch, sweet potato starch and cassava starch.
Further, the emulsifier is one or more of sucrose ester, soybean phospholipid, sorbitol ester, rosin glyceride, lauric glyceride, caprylic/capric glyceride, sorbitan laurate, sorbitan oleate, sorbitan palmitate, sorbitan stearate, sucrose fatty acid ester and xylitol stearate. The above emulsifier is plant essential oil particles for forming oil-in-water phase.
Further, the core material comprises plant essential oil and modified plant oil. The plant essential oil is used as an effective component of the aromatherapy, and the modified plant oil or the plant oil is used as a carrier and a dispersing agent of the aromatherapy component, so that the slow-release of the aromatherapy component can be effectively ensured. In the core material, the proportion of the plant essential oil is 25-35 wt%.
Further, the plant essential oil is flower fragrance including rose essential oil, jasmine essential oil, lavender essential oil and peony essential oil, the fruit fragrance includes orange peel essential oil, lemon essential oil, grapefruit essential oil and pomegranate essential oil, and the wood fragrance includes one or more than two of sandalwood essential oil, cedar essential oil, rosewood essential oil, agilawood essential oil and camphor essential oil.
Further, the modified vegetable oil is one or more of esterified vegetable oil, fatty acid ester, methyl ethyl vegetable oil fatty acid ester, epoxidized vegetable oil and epoxidized vegetable oil fatty acid ester.
Further, the vegetable oil in the modified vegetable oil is one or more of coconut oil, olive oil, castor oil, soybean oil, corn oil, palm oil, rapeseed oil, cottonseed oil, peanut oil and sunflower seed oil.
The second purpose of the invention is realized by adopting the following technical scheme:
the preparation method of the environment-friendly aromatherapy candle comprises the following steps:
1) homogenizing the plant essential oil and the modified plant oil at the speed of 12000r/min of 8000-; homogenizing deionized water, emulsifier and wall material at 8000-;
2) slowly adding the oil phase into the water phase, and stirring to obtain an emulsion;
3) carrying out spray drying treatment on the emulsion, and carrying out curing, hardening and drying to obtain microcapsules;
4) and (3) uniformly mixing the main burning agent and the microcapsule, and forming to obtain the environment-friendly aromatherapy candle.
The preferred condition parameters for spray drying are: the feeding flow is 150-.
Compared with the prior art, the invention has the beneficial effects that:
the environment-friendly aromatherapy candle provided by the invention takes the hydrogenated high methyl ethyl carbonate as a main fuel, has high melting point and easy plasticity, can customize different shapes according to requirements, is used as a natural plant source fuel, and is completely combusted, clean and environment-friendly; the plant essential oil is prepared into the aromatherapy microcapsule, so that the release of aromatherapy components in the storage and transportation process can be effectively reduced, and the aromatherapy microcapsule is resistant to oxygen and sunlight and high in storage stability; the fragrance efficiency of the fragrance candle is improved; fragrance, air purification, nerve relief, and tranquilizing;
the environment-friendly scented candle provided by the invention adopts pure natural raw materials, can be biodegraded, and has a wide application range; does not contain various harmful chemical components such as aromatic organic matters and the like, has no irritation and good safety, is beneficial to the health of human bodies, and meets the national requirements on environmental protection.
The preparation method of the environment-friendly scented candle provided by the invention can form the environment-friendly scented candle with high storage and transportation resistance.
Detailed Description
The present invention is further described below with reference to specific embodiments, and it should be noted that, without conflict, any combination between the embodiments or technical features described below may form a new embodiment.
The following are specific examples of the present invention, and raw materials, equipments and the like used in the following examples can be obtained by purchasing them unless otherwise specified.
The invention provides an environment-friendly aromatherapy candle, which is prepared from 100 parts of main combustion agent and 5-15 parts of aromatherapy microcapsule, wherein the main combustion agent is hydrogenated high-methyl ethyl carbonate, and the aromatherapy microcapsule is prepared from a core material, a wall material, an emulsifier and deionized water.
The invention provides a preparation method of the environment-friendly aromatherapy candle, which comprises the following steps:
1) homogenizing the plant essential oil and the modified plant oil at the speed of 12000r/min of 8000-; homogenizing deionized water, emulsifier and wall material at 8000-;
2) slowly adding the oil phase into the water phase, and stirring to obtain an emulsion;
3) carrying out spray drying treatment on the emulsion, and carrying out curing, hardening and drying to obtain microcapsules;
4) and (3) uniformly mixing the main burning agent and the microcapsule, and forming to obtain the environment-friendly aromatherapy candle.
In the following embodiment, the main combustion agent is hydrogenated high methyl ethyl carbonate, that is, methylated or ethylated vegetable oil product extracted after methylation or ethylation of vegetable oil.
Example 1:
an environment-friendly functional aromatherapy candle is prepared from 90 wt% of main burning agent and 10 wt% of aromatherapy microcapsule; the aromatherapy microcapsule is prepared from the following components in parts by weight: 14 parts of core material, 8 parts of emulsifier, 30 parts of wall material and 48 parts of deionized water; specifically, the core material comprises 2 parts of rose essential oil, 2 parts of lavender essential oil, 5 parts of castor oil methyl ester and 5 parts of epoxidized soybean oil; the emulsifier comprises 5 parts of sucrose ester and 3 parts of soybean lecithin; the wall material comprises 10 parts of modified corn starch and 20 parts of maltodextrin.
The preparation method of the environment-friendly functional aromatherapy candle comprises the following steps:
1) pretreatment: homogenizing rose essential oil, lavender essential oil, methyl ricinoleate and epoxidized soybean oil at 10000r/min for 5min to obtain oil phase; homogenizing deionized water, sucrose ester, soybean phospholipid, modified corn starch and maltodextrin at 10000r/min for 5min to obtain water phase;
2) emulsification: slowly adding the oil phase into the water phase, and homogenizing at 1500r/min for 25min to obtain emulsion;
3) and (3) forming a capsule: carrying out spray drying treatment on the emulsion obtained in the step 2) at the feeding flow of 180kg/h, the hot air temperature of 90 ℃, the supplementary air temperature of 70 ℃ and the fluidized bed drying temperature of 60 ℃, and curing, hardening and drying to obtain microcapsules;
4) mixing the main combustion agent and the microcapsule according to the proportion of 9: 1, and performing filling, forming, cooling and demolding to obtain the environment-friendly functional aromatherapy candle.
Example 2:
an environment-friendly functional aromatherapy candle is prepared from 92 wt% of main combustion agent and 8 wt% of aromatherapy microcapsules, wherein the aromatherapy microcapsules are prepared from 14 parts by weight of core materials, 8 parts by weight of emulsifier, 33 parts by weight of wall materials and 45 parts by weight of deionized water, more specifically, the core materials comprise 3 parts by weight of sandalwood essential oil, 2 parts by weight of rosewood essential oil and 9 parts by weight of epoxy palm oil methyl ester, the emulsifier comprises 4 parts by weight of sorbitol ester and 4 parts by weight of caprylic capric glyceride, and the wall materials comprise 11 parts by weight of β -cyclodextrin and 22 parts by weight of modified sweet potato starch.
The preparation method of the environment-friendly functional aromatherapy candle comprises the following steps:
1) homogenizing sandalwood essential oil, rosewood essential oil and epoxy palm oil methyl ester oil at 8000r/min for 5min to obtain oil phase, and homogenizing deionized water, sorbitol ester, caprylic capric glyceride, β -cyclodextrin and modified sweet potato starch at 8000r/min for 5min to obtain water phase;
2) emulsification: slowly adding the oil phase into the water phase, and homogenizing at 1200r/min for 25min to obtain emulsion;
3) and (3) forming a capsule: carrying out spray drying treatment on the emulsion obtained in the step 2) at a feeding flow of 200kg/h, a hot air temperature of 100 ℃, a supplementary air temperature of 80 ℃ and a fluidized bed drying temperature of 70 ℃, and curing, hardening and drying to obtain microcapsules;
4) mixing the main combustion agent and the microcapsule according to a proportion of 92: 8, and performing filling, forming, cooling and demolding to obtain the environment-friendly functional aromatherapy candle.
Example 3:
an environment-friendly functional aromatherapy candle is prepared from 88 wt% of main burning agent and 12 wt% of aromatherapy microcapsule; the aromatherapy microcapsule is prepared from the following components in parts by weight: 14 parts of core material, 11 parts of emulsifier, 25 parts of wall material and 50 parts of deionized water; more specifically, the core material comprises 1 part of jasmine essential oil, 3 parts of grapefruit essential oil, 4 parts of sunflower seed oil methyl ester and 6 parts of epoxy corn oil; the emulsifier comprises 4 parts of sorbitan oleate and 7 parts of glycerol laurate; the wall material comprises 10 parts of fiber ester and 15 parts of maltodextrin.
The preparation method of the environment-friendly functional aromatherapy candle comprises the following steps:
1) pretreatment: homogenizing jasmine essential oil, grapefruit essential oil, sunflower seed oil methyl ester and epoxy corn oil at 12000r/min for 5min to obtain oil phase; homogenizing deionized water, sorbitan oleate, glyceryl laurate, cellulose ester and maltodextrin at 12000r/min for 5min to obtain a water phase;
2) emulsification: slowly adding the oil phase into the water phase, and homogenizing at 1200r/min for 25min to obtain emulsion;
3) and (3) forming a capsule: carrying out spray drying treatment on the emulsion obtained in the step 2) at a feeding flow of 150kg/h, a hot air temperature of 80 ℃, a supplementary air temperature of 60 ℃ and a fluidized bed drying temperature of 50 ℃, and carrying out curing, hardening and drying to obtain microcapsules;
4) mixing the main combustion agent and the microcapsule according to the proportion of 88: 12, and performing filling, forming, cooling and demolding to obtain the environment-friendly functional aromatherapy candle.
Example 4:
an environment-friendly functional aromatherapy candle is prepared from 85 wt% of main burning agent and 15 wt% of aromatherapy microcapsule, wherein the aromatherapy microcapsule is prepared from 15 parts of core materials, 8 parts of emulsifying agent, 35 parts of wall materials and 42 parts of deionized water in parts by weight, more specifically, the core materials comprise 2 parts of lavender essential oil, 3 parts of orange peel essential oil and 10 parts of olive oil methyl ester, the emulsifying agent comprises 5 parts of sorbitan palmitate and 3 parts of sucrose fatty acid ester, and the wall materials comprise 15 parts of β -cyclodextrin and 20 parts of modified corn starch.
The preparation method of the environment-friendly functional aromatherapy candle comprises the following steps:
1) homogenizing lavender essential oil, pericarpium Citri Junoris essential oil, and methyl ester of oleum Olivarum at 11000r/min for 5min to obtain oil phase, and homogenizing deionized water, sorbitan palmitate, sucrose fatty acid ester, β -cyclodextrin, and modified corn starch at 11000r/min for 5min to obtain water phase;
2) emulsification: slowly adding the oil phase into the water phase, and homogenizing at 1800r/min for 25min to obtain emulsion;
3) and (3) forming a capsule: carrying out spray drying treatment on the emulsion obtained in the step 2) at a feeding flow rate of 170kg/h, a hot air temperature of 85 ℃, a supplementary air temperature of 65 ℃ and a fluidized bed drying temperature of 55 ℃, and carrying out curing, hardening and drying to obtain microcapsules;
4) mixing the main combustion agent and the microcapsule according to the proportion of 85: 15, and carrying out filling, forming, cooling and demolding to obtain the environment-friendly functional aromatherapy candle.
Example 5:
an environment-friendly functional aromatherapy candle is prepared from 95 wt% of a main burning agent and 5 wt% of aromatherapy microcapsules, wherein the aromatherapy microcapsules are prepared from 15 parts of a core material, 5 parts of an emulsifier, 30 parts of a wall material and 50 parts of deionized water in parts by weight, the core material comprises 5 parts of camphor essential oil, 5 parts of castor oil methyl ester and 5 parts of olive oil methyl ester, the emulsifier comprises 4 parts of rosin glyceride and 1 part of soybean phospholipid, and the wall material comprises 15 parts of fiber ester and 15 parts of β -cyclodextrin.
The preparation method of the environment-friendly functional aromatherapy candle comprises the following steps:
1) homogenizing camphor essential oil, castor oil methyl ester and olive oil methyl ester at 13000r/min for 5min to obtain oil phase, and homogenizing deionized water, rosin glyceride, soybean phospholipid, fiber ester and β -cyclodextrin at 13000r/min for 5min to obtain water phase;
2) emulsification: slowly adding the oil phase into the water phase, and homogenizing at 1700r/min for 25min to obtain emulsion;
3) and (3) forming a capsule: carrying out spray drying treatment on the emulsion obtained in the step 2) at a feeding flow of 190kg/h, a hot air temperature of 95 ℃, a supplementary air temperature of 75 ℃ and a fluidized bed drying temperature of 65 ℃, and curing, hardening and drying to obtain microcapsules;
4) mixing the main combustion agent and the microcapsule according to the proportion of 95: 5, and performing filling, forming, cooling and demolding to obtain the environment-friendly functional aromatherapy candle.
Example 6:
an environment-friendly functional aromatherapy candle is prepared from 90 wt% of main burning agent and 10 wt% of aromatherapy microcapsule; the aromatherapy microcapsule is prepared from the following components in parts by weight: 14 parts of core material, 8 parts of emulsifier, 30 parts of wall material and 47 parts of deionized water; more specifically, the core material comprises 2 parts of cedar wood essential oil, 2 parts of rosewood essential oil, 5 parts of corn oil methyl ester and 5 parts of epoxy coconut oil; the emulsifier comprises 4 parts of lauric glyceride and 4 parts of xylitol anhydride stearate; the wall material comprises 10 parts of modified wheat starch and 20 parts of maltodextrin.
The preparation method of the environment-friendly functional aromatherapy candle comprises the following steps:
1) pretreatment: homogenizing cedar essential oil, rosewood essential oil, corn oil methyl ester and epoxy coconut oil at 14000r/min for 5min to obtain oil phase; homogenizing deionized water, lauric glyceride, xylitol anhydride stearate, modified wheat starch and maltodextrin at 13000r/min for 5min to obtain a water phase;
2) emulsification: slowly adding the oil phase into the water phase, and homogenizing at 1700r/min for 25min to obtain emulsion;
3) and (3) forming a capsule: carrying out spray drying treatment on the emulsion obtained in the step 2) at the feeding flow of 180kg/h, the hot air temperature of 90 ℃, the supplementary air temperature of 75 ℃ and the fluidized bed drying temperature of 65 ℃, and curing, hardening and drying to obtain microcapsules;
4) mixing the main combustion agent and the microcapsule according to the proportion of 90: 10, and performing filling, forming, cooling and demolding to obtain the environment-friendly functional aromatherapy candle.
Example 7:
an environment-friendly functional aromatherapy candle is prepared from 93 wt% of main combustion agent and 7 wt% of aromatherapy microcapsule, wherein the aromatherapy microcapsule is prepared from 15 parts of core material, 8 parts of emulsifier, 32 parts of wall material and 45 parts of deionized water in parts by weight, more specifically, the core material comprises 3 parts of rose essential oil, 2 parts of agilawood essential oil, 5 parts of epoxy palm oil methyl ester and 5 parts of olive oil methyl ester, the emulsifier comprises 4 parts of rosin glyceride and 4 parts of soybean phospholipid, and the wall material comprises 10 parts of fiber ester, 11 parts of β -cyclodextrin and 11 parts of maltodextrin.
The preparation method of the environment-friendly functional aromatherapy candle comprises the following steps:
1) pre-treating, namely homogenizing rose essential oil, agilawood essential oil, epoxy palm oil methyl ester and olive oil methyl ester at 13000r/min for 5min to obtain an oil phase, and homogenizing deionized water, rosin glyceride, soybean phospholipid, fiber ester, β -cyclodextrin and maltodextrin at 13000r/min for 5min to obtain a water phase;
2) emulsification: slowly adding the oil phase into the water phase, and homogenizing at 1700r/min for 25min to obtain emulsion;
3) and (3) forming a capsule: carrying out spray drying treatment on the emulsion obtained in the step 2) at a feeding flow of 190kg/h, a hot air temperature of 95 ℃, a supplementary air temperature of 75 ℃ and a fluidized bed drying temperature of 65 ℃, and curing, hardening and drying to obtain microcapsules;
4) mixing the main combustion agent and the microcapsule according to the weight ratio of 93: 7, and performing filling, forming, cooling and demolding to obtain the environment-friendly functional aromatherapy candle.
The above embodiments are only preferred embodiments of the present invention, and the protection scope of the present invention is not limited thereby, and any insubstantial changes and substitutions made by those skilled in the art based on the present invention are within the protection scope of the present invention.
Claims (10)
1. The environment-friendly aromatherapy candle is characterized by being prepared from 100 parts of main burning agent and 5-15 parts of aromatherapy microcapsule, wherein the main burning agent is hydrogenated high-methyl ethyl carbonate, and the aromatherapy microcapsule is prepared from a core material, a wall material, an emulsifier and deionized water.
2. The environment-friendly aromatherapy candle of claim 1, wherein the main burning agent is prepared by the following method: the hydrogenated vegetable oil reacts with a methylation or ethylation reagent to extract the product of the methylation or ethylation vegetable oil, namely the hydrogenated high methyl ethyl carbonate.
3. The environment-friendly aromatherapy candle according to claim 1, wherein the aromatherapy microcapsule is made of 5 to 15 parts of core material, 15 to 45 parts of wall material, 5 to 15 parts of emulsifier and 20 to 50 parts of deionized water.
4. The environment-friendly aromatherapy candle of claim 3, wherein the wall material is one or more of maltodextrin, β -cyclodextrin, cellulose ester, starch, or modified starch.
5. The environment-friendly aromatic candle according to claim 3, wherein the emulsifier is one or more of sucrose ester, soybean lecithin, sorbitol ester, rosin glyceride, lauric glyceride, caprylic/capric glyceride, sorbitan laurate, sorbitan oleate, sorbitan palmitate, sorbitan stearate, sucrose fatty acid ester, and xylitol stearate.
6. The environmentally friendly candle of claim 3, wherein the core material comprises plant essential oils and modified plant oils.
7. The environment-friendly aromatherapy candle according to claim 6, wherein the plant essential oil is one or more of floral fragrances including rose essential oil, jasmine essential oil, lavender essential oil and peony essential oil, fruit fragrances including orange peel essential oil, lemon essential oil, grapefruit essential oil and pomegranate essential oil, and woody fragrances including sandalwood essential oil, cedar essential oil, rosewood essential oil, agilawood essential oil and camphor essential oil.
8. The environment-friendly aromatherapy candle according to claim 6, wherein the modified vegetable oil is one or more of esterified vegetable oil, fatty acid ester, methyl ethyl vegetable oil fatty acid ester, epoxidized vegetable oil, and epoxidized vegetable oil fatty acid ester.
9. The environment-friendly aromatherapy candle according to claim 6, wherein the vegetable oil of the modified vegetable oil is one or more of coconut oil, olive oil, castor oil, soybean oil, corn oil, palm oil, rapeseed oil, cottonseed oil, peanut oil, and sunflower seed oil.
10. The method for preparing the environment-friendly aromatherapy candle according to any one of claims 1 to 9, comprising the steps of:
1) homogenizing the plant essential oil and the modified plant oil at the speed of 12000r/min of 8000-; homogenizing deionized water, emulsifier and wall material at 8000-;
2) slowly adding the oil phase into the water phase, and stirring to obtain an emulsion;
3) carrying out spray drying treatment on the emulsion, and carrying out curing, hardening and drying to obtain microcapsules;
4) and (3) uniformly mixing the main burning agent and the microcapsule, and forming to obtain the environment-friendly aromatherapy candle.
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| CN201911415660.5A CN111117776A (en) | 2019-12-31 | 2019-12-31 | Environment-friendly aromatherapy candle and preparation method thereof |
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| CN201911415660.5A CN111117776A (en) | 2019-12-31 | 2019-12-31 | Environment-friendly aromatherapy candle and preparation method thereof |
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| CN111117776A true CN111117776A (en) | 2020-05-08 |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN111558077A (en) * | 2020-06-30 | 2020-08-21 | 辽宁东科药业有限公司 | Traditional Chinese medicine nerve-soothing aromatherapy wax and preparation method thereof |
| CN113456745A (en) * | 2021-06-23 | 2021-10-01 | 陕西中医药大学 | Depression-relieving aromatherapy liquid and preparation method and application thereof |
| CN114191592A (en) * | 2021-12-25 | 2022-03-18 | 蔓莎(苏州)工艺制品有限公司 | Hot incense explosion incense |
| CN114570301A (en) * | 2022-03-11 | 2022-06-03 | 东莞市农业科学研究中心 | Camphor tree essential oil microcapsule and preparation method thereof |
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| CN109652214A (en) * | 2019-01-10 | 2019-04-19 | 蔓莎(苏州)工艺制品有限公司 | A kind of smokeless Scented candle and its manufacturing process |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN111558077A (en) * | 2020-06-30 | 2020-08-21 | 辽宁东科药业有限公司 | Traditional Chinese medicine nerve-soothing aromatherapy wax and preparation method thereof |
| CN113456745A (en) * | 2021-06-23 | 2021-10-01 | 陕西中医药大学 | Depression-relieving aromatherapy liquid and preparation method and application thereof |
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