JP6469471B2 - Fragrance-containing sheet and method for producing the same - Google Patents
Fragrance-containing sheet and method for producing the same Download PDFInfo
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- JP6469471B2 JP6469471B2 JP2015027260A JP2015027260A JP6469471B2 JP 6469471 B2 JP6469471 B2 JP 6469471B2 JP 2015027260 A JP2015027260 A JP 2015027260A JP 2015027260 A JP2015027260 A JP 2015027260A JP 6469471 B2 JP6469471 B2 JP 6469471B2
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- 239000003205 fragrance Substances 0.000 title claims description 47
- 238000004519 manufacturing process Methods 0.000 title claims description 17
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 36
- 239000007800 oxidant agent Substances 0.000 claims description 28
- FGIUAXJPYTZDNR-UHFFFAOYSA-N potassium nitrate Chemical compound [K+].[O-][N+]([O-])=O FGIUAXJPYTZDNR-UHFFFAOYSA-N 0.000 claims description 20
- 239000002304 perfume Substances 0.000 claims description 18
- 230000001590 oxidative effect Effects 0.000 claims description 13
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 11
- 239000000796 flavoring agent Substances 0.000 claims description 10
- 235000019634 flavors Nutrition 0.000 claims description 10
- 235000010333 potassium nitrate Nutrition 0.000 claims description 10
- 239000004323 potassium nitrate Substances 0.000 claims description 10
- 239000000463 material Substances 0.000 claims description 5
- 238000001035 drying Methods 0.000 claims description 4
- 239000000049 pigment Substances 0.000 claims description 4
- VLTRZXGMWDSKGL-UHFFFAOYSA-N perchloric acid Chemical compound OCl(=O)(=O)=O VLTRZXGMWDSKGL-UHFFFAOYSA-N 0.000 claims description 3
- 229910002651 NO3 Inorganic materials 0.000 claims description 2
- NHNBFGGVMKEFGY-UHFFFAOYSA-N Nitrate Chemical compound [O-][N+]([O-])=O NHNBFGGVMKEFGY-UHFFFAOYSA-N 0.000 claims description 2
- VLTRZXGMWDSKGL-UHFFFAOYSA-M perchlorate Inorganic materials [O-]Cl(=O)(=O)=O VLTRZXGMWDSKGL-UHFFFAOYSA-M 0.000 claims description 2
- 235000019441 ethanol Nutrition 0.000 description 22
- 239000000243 solution Substances 0.000 description 10
- ISAOCJYIOMOJEB-UHFFFAOYSA-N benzoin Chemical compound C=1C=CC=CC=1C(O)C(=O)C1=CC=CC=C1 ISAOCJYIOMOJEB-UHFFFAOYSA-N 0.000 description 6
- 239000007864 aqueous solution Substances 0.000 description 5
- 241000402754 Erythranthe moschata Species 0.000 description 4
- 239000008213 purified water Substances 0.000 description 4
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 description 3
- 244000028419 Styrax benzoin Species 0.000 description 3
- 235000000126 Styrax benzoin Nutrition 0.000 description 3
- 235000008411 Sumatra benzointree Nutrition 0.000 description 3
- 229960002130 benzoin Drugs 0.000 description 3
- 238000013329 compounding Methods 0.000 description 3
- 235000019382 gum benzoic Nutrition 0.000 description 3
- 238000000034 method Methods 0.000 description 3
- LRHPLDYGYMQRHN-UHFFFAOYSA-N N-Butanol Chemical compound CCCCO LRHPLDYGYMQRHN-UHFFFAOYSA-N 0.000 description 2
- 150000001298 alcohols Chemical class 0.000 description 2
- 238000002485 combustion reaction Methods 0.000 description 2
- 235000013373 food additive Nutrition 0.000 description 2
- 239000002778 food additive Substances 0.000 description 2
- BDERNNFJNOPAEC-UHFFFAOYSA-N propan-1-ol Chemical compound CCCO BDERNNFJNOPAEC-UHFFFAOYSA-N 0.000 description 2
- VWDWKYIASSYTQR-UHFFFAOYSA-N sodium nitrate Chemical compound [Na+].[O-][N+]([O-])=O VWDWKYIASSYTQR-UHFFFAOYSA-N 0.000 description 2
- 239000000758 substrate Substances 0.000 description 2
- 241000717739 Boswellia sacra Species 0.000 description 1
- 240000007311 Commiphora myrrha Species 0.000 description 1
- 235000006965 Commiphora myrrha Nutrition 0.000 description 1
- 239000004863 Frankincense Substances 0.000 description 1
- 235000007265 Myrrhis odorata Nutrition 0.000 description 1
- AMQJEAYHLZJPGS-UHFFFAOYSA-N N-Pentanol Chemical compound CCCCCO AMQJEAYHLZJPGS-UHFFFAOYSA-N 0.000 description 1
- GWEVSGVZZGPLCZ-UHFFFAOYSA-N Titan oxide Chemical compound O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 description 1
- 230000001476 alcoholic effect Effects 0.000 description 1
- 235000019568 aromas Nutrition 0.000 description 1
- 238000000222 aromatherapy Methods 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- 239000012153 distilled water Substances 0.000 description 1
- 239000004744 fabric Substances 0.000 description 1
- 230000035876 healing Effects 0.000 description 1
- 239000012535 impurity Substances 0.000 description 1
- 239000012046 mixed solvent Substances 0.000 description 1
- 238000002156 mixing Methods 0.000 description 1
- 150000002823 nitrates Chemical class 0.000 description 1
- 239000003960 organic solvent Substances 0.000 description 1
- 238000001556 precipitation Methods 0.000 description 1
- 235000010344 sodium nitrate Nutrition 0.000 description 1
- 239000004317 sodium nitrate Substances 0.000 description 1
- 239000007921 spray Substances 0.000 description 1
- 238000005507 spraying Methods 0.000 description 1
- 229910001220 stainless steel Inorganic materials 0.000 description 1
- 239000010935 stainless steel Substances 0.000 description 1
- 238000003756 stirring Methods 0.000 description 1
- 239000008399 tap water Substances 0.000 description 1
- 235000020679 tap water Nutrition 0.000 description 1
- OGIDPMRJRNCKJF-UHFFFAOYSA-N titanium oxide Inorganic materials [Ti]=O OGIDPMRJRNCKJF-UHFFFAOYSA-N 0.000 description 1
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Description
本発明は、薫香などの香りを楽しむことができる香料含有シート並びにその製造方法に関する。 The present invention relates to a fragrance-containing sheet capable of enjoying a scent such as musk and a method for producing the same.
従来より、ストレスに対する癒し効果を得る目的として、また、薫香など香りを楽しむために香料と酸化剤を紙などの基材シートに含浸させ、これを無炎燃焼させて発香させる香料含有シート（実用新案文献１）が知られている。 Conventionally, for the purpose of obtaining a healing effect against stress, and in order to enjoy a scent such as musk, a fragrance-containing sheet that impregnates a base sheet such as paper with a fragrance and an oxidant and burns it flamelessly ( Utility model literature 1) is known.
前記香料含有シートは、先ず硝酸カリウムなどの酸化剤水溶液に紙等のシート基材を浸積するか、或いは、酸化剤水溶液を基材に噴霧するなどして酸化剤含有シートを作成し、これを乾燥後、香料や香料アルコール溶液で賦香処理し、最後に再乾燥して作成していた。これは、酸化剤が水溶性で、アルコールには溶解せず、香料は有機溶媒に溶解しやすいために、別々の工程で基材に含浸して乾燥する必要があったためである。 The fragrance-containing sheet is prepared by first immersing a sheet base material such as paper in an aqueous oxidizing agent solution such as potassium nitrate, or by spraying an aqueous oxidizing agent solution onto the base material to prepare an oxidizing agent-containing sheet. After drying, the fragrance was treated with a fragrance or a fragrance alcohol solution, and finally re-dried. This is because the oxidizing agent is water-soluble, does not dissolve in alcohol, and the fragrance easily dissolves in an organic solvent, so that it is necessary to impregnate the substrate and dry it in a separate step.
そこで本発明は前記従来のような面倒な工程を要することなく作成できる香料含有シートとその製造方法を提供することを目的とする。 Then, this invention aims at providing the fragrance | flavor containing sheet | seat which can be produced without requiring the said troublesome process as the said conventional, and its manufacturing method.
本発明者は前記課題を解決するべく、鋭意研究の結果、前記酸化剤と香料を特定の混合溶媒に溶解させることで一度に酸化剤と香料を基材シートに含浸状態にできることを知見した。
本発明の香料含有シートの製造方法は、香料３〜１８質量部、酸化剤０．１〜１．５質量部、水１０〜３０質量部、アルコール６０〜８０質量部からなる香料酸化剤アルコール溶液を調製する工程と、前記香料酸化剤アルコール溶液を基材シートに含浸する工程と、前記香料酸化剤アルコール溶液を含浸させた基材シートを乾燥させる工程と、からなり、前記酸化剤は、硝酸塩または過塩素酸塩であることを特徴とする。
また、香料含有シートの製造方法は、前記製造方法において、前記酸化剤が硝酸カリウムで、前記アルコールがエタノールであることを特徴とする。
また、香料含有シートの製造方法は、前記製造方法において、前記基材シートが紙であることを特徴とする。
また、香料含有シートの製造方法は、前記製造方法において、前記基材シートの表面に顔料インキで意匠層を形成する工程を含むことを特徴とする。
As a result of earnest research, the present inventor has found that the base sheet can be impregnated with the oxidizing agent and the fragrance at once by dissolving the oxidizing agent and the fragrance in a specific mixed solvent . .
Method for producing a flavor-containing sheet of the present invention, Perfume 3-18 parts by weight, oxidizing agent 0.1 to 1.5 parts by weight of water 10 to 30 parts by weight, flavoring oxidant alcohols consisting of alcohols 60 to 80 parts by weight preparing a solution, a step of impregnating the perfume oxidant alcohol solution to the substrate sheet, and drying the base sheet impregnated with perfume oxidant alcoholic solution, Tona is, the oxidizing agent is characterized nitrate or perchlorate der Rukoto.
Also, the manufacturing method of the Perfume-containing sheet, before SL Manufacturing method, in the oxidizing agent is potassium nitrate, wherein the alcohol is ethanol.
Also, the manufacturing method of the Perfume-containing sheet, before SL Manufacturing method, the base sheet is characterized in that it is a paper.
Also, the manufacturing method of the Perfume-containing sheet, before SL Manufacturing method, characterized in that it comprises a step of forming a decorative layer with a pigment ink on the surface of the base sheet.
本発明の香料含有シート並びにその製造方法においては、基材シートに一液の香料酸化剤アルコール溶液を含浸させることができるので、複雑な工程を要することなく、乾燥時間も短く、極めて簡単な方法で香料含有シートを得ることができる。 In the perfume-containing sheet and the method for producing the perfume of the present invention, since the base sheet can be impregnated with one solution of the perfume oxidant alcohol solution, a complicated process is not required, the drying time is short and an extremely simple method. A fragrance-containing sheet can be obtained.
図１は本発明の香料含有シートの一実施の形態の説明断面図である。説明のため、模式的に示したものである。図１中の符号１は香料含有シートを示し、符号２で示される紙からなる基材シートに符号３で示されるレジノイドベンゾイン等からなる香料を５質量部、符号４で示される硝酸カリウムからなる酸化剤１質量部、図略の精製水からなる水２５質量部、同じく図略のエタノールからなるアルコール７０質量部からなる香料酸化剤アルコール溶液を含浸させたものである。
使用に際しては、前記香料含有シートをマッチ、火器等からの炎により無炎燃焼させて使用する。この燃焼熱により含浸された香料が発香する。
FIG. 1 is an explanatory cross-sectional view of one embodiment of a fragrance-containing sheet of the present invention. It is schematically shown for explanation.
In use, the fragrance-containing sheet is used after being flamelessly burned by a flame from a match, firearm or the like. The fragrance | flavor impregnated with this combustion heat aromas.
図１に示す香料含有シートは、次のようにして作成した。
先ず、レジノイドベンゾイン等からなる調合香料５ｇと純度９５％エタノールからなるアルコール７４ｇとの香料エタノール溶液と、食品添加物グレードの硝酸カリウムからなる酸化剤１ｇと精製水からなる水２５ｇとの硝酸カリウム水溶液の各々を調製し、更に香料エタノール溶液を弱く撹拌しながら徐々に硝酸カリウム水溶液を加え均一にした後、室温で２〜３時間静置して香料酸化剤アルコール水溶液を得た。この際、沈殿等が生じた場合は、ろ紙またはろ布等で濾過して使用する。
The fragrance-containing sheet shown in FIG. 1 was prepared as follows.
First, each of a potassium nitrate aqueous solution of 5 g of a blended fragrance made of resinoid benzoin and the like and 74 g of an alcohol made of 95% purity ethanol, 1 g of an oxidizer made of food additive grade potassium nitrate and 25 g of water made of purified water. Further, the aqueous solution of potassium nitrate was gradually added and homogenized while weakly stirring the fragrance ethanol solution, and then allowed to stand at room temperature for 2 to 3 hours to obtain a fragrance oxidant alcohol aqueous solution. At this time, if precipitation or the like occurs, it is filtered and used with filter paper or filter cloth.
次に、紙からなる基材シートをステンレス製トレイの中に設置したネット（網）の上に置き、トリガータイプのスプレーディスペンサーを用いて前記基材シート全体に均一に前記香料酸化剤アルコール水溶液を噴霧した。 Next, a base sheet made of paper is placed on a net installed in a stainless steel tray, and the fragrance oxidant alcohol aqueous solution is uniformly applied to the entire base sheet using a trigger type spray dispenser. Sprayed.
次いで、前記香料酸化剤アルコール水溶液を噴霧した基材シートをトレイの中のネット（網）の上で、２８〜３０℃で８〜１０時間風乾し、本発明の香料含有シートを得た。 Subsequently, the base material sheet sprayed with the fragrance oxidant alcohol aqueous solution was air-dried at 28 to 30 ° C. for 8 to 10 hours on a net in the tray to obtain a fragrance-containing sheet of the present invention.
図２は、本発明香料含有シートの他の実施の形態を示すもので、前記のようにして得られた香料含有シートに酸化チタンからなる顔料インキでアルファベット文字からなる意匠層５を形成したものを示す。図示したものは、無炎燃焼させてシートが黒化した後、その黒色面上に前記顔料インキで形成された意匠層５が白く浮き上がった状態になったところを示している。
FIG. 2 shows another embodiment of the fragrance-containing sheet of the present invention, in which the fragrance-containing sheet obtained as described above is formed with a
以上では本発明の香料含有シート並びにその製造方法の幾つかの実施の形態を示したが、本発明は前記図示した実施の形態に限定されるものではない。 Although several embodiments of the fragrance-containing sheet and the method for producing the same according to the present invention have been described above, the present invention is not limited to the illustrated embodiments.
本発明において使用される、前記香料としては、ベンゾイン、オリバナム、ミルラ等のレジノイド香料等が挙げられ、商品のコンセプトにより適宜選択使用できるが、例えばアロマテラピー等で使用する場合や香りの残存性を持たせる場合はコンクリート系やレジノイド系天然香料、固化結晶性天然香料、或いは、合成香料を用いるのが好ましい。
また、その配合量は香りの揮散性と保香残香性の観点から３〜１８質量部とする必要があるが、５〜８質量部の範囲が好ましい。
Examples of the fragrance used in the present invention include resinoid fragrances such as benzoin, olibanum, and myrrh, and can be appropriately selected and used depending on the concept of the product.For example, when used in aromatherapy, etc. In the case of having it, it is preferable to use a concrete or resinoid natural fragrance, a solidified crystalline natural fragrance, or a synthetic fragrance.
Moreover, although the compounding quantity needs to be 3-18 mass parts from a viewpoint of the volatility of a fragrance and an incense remaining fragrance, the range of 5-8 mass parts is preferable.
また、前記酸化剤としては硝酸カリウム、硝酸ナトリウム等の各種硝酸塩や過塩素酸塩等が挙げられるが、取り扱いの安全性の観点から食品添加剤としも認められている硝酸カリウムが好ましい。
また、その配合量は連続延焼と安全性の観点から０．１〜１．５質量部とする必要あるが、０．５〜１．２質量部の範囲が好ましい。
尚、酸化剤はアルコールには溶解しないのでアルコール水に過飽和の状態で溶解させておくのが好ましい。
Examples of the oxidizing agent include various nitrates such as potassium nitrate and sodium nitrate, and perchlorates, but potassium nitrate, which is also recognized as a food additive from the viewpoint of handling safety, is preferable.
Moreover, although the compounding quantity needs to be 0.1-1.5 mass parts from a viewpoint of continuous fire spread and safety, the range of 0.5-1.2 mass parts is preferable.
In addition, since an oxidizing agent does not melt | dissolve in alcohol, it is preferable to make it melt | dissolve in alcohol water in the supersaturated state.
また、前記水は蒸留水、精製水、水道水等が使用でき、香料に影響を及ぼす不純物、コストの観点からは精製水の使用が好ましい。
また、その配合量は硝酸カリウムの十分な溶解性の観点から１０〜３０質量部とする必要があるが、１５〜２５質量部の範囲が好ましい。
また、前記アルコールとしてはメチルアルコール、エチルアルコール、プロピルアルコール、ブチルアルコール、アミルアルコール挙げられ、製品の安全性と香料の溶解性の観点からエタノールが好ましい。
特に、香料の溶解性の観点から９５％以上の高濃度のアルコールの使用が好ましい。
また、その配合量は香料の種類により溶解度が異なるが生産性と作業性の観点から６０〜８０質量部とする必要があるが、６５〜７５質量部の範囲が好ましい。
Moreover, distilled water, purified water, tap water, etc. can be used for the said water, and use of purified water is preferable from a viewpoint of the impurity which affects a fragrance | flavor and cost.
Moreover, although the compounding quantity needs to be 10-30 mass parts from a sufficient solubility viewpoint of potassium nitrate, the range of 15-25 mass parts is preferable.
Examples of the alcohol include methyl alcohol, ethyl alcohol, propyl alcohol, butyl alcohol, and amyl alcohol. Ethanol is preferable from the viewpoint of product safety and perfume solubility.
In particular, it is preferable to use an alcohol having a high concentration of 95% or more from the viewpoint of the solubility of the fragrance.
The blending amount varies depending on the kind of the fragrance, but it is necessary to be 60 to 80 parts by mass from the viewpoint of productivity and workability, but the range of 65 to 75 parts by mass is preferable.
本発明の香料含有シートは薫香を目的として使用できることは言うまでもなく、室内のフレグランスオーナメントとして、テーブルの上に置いたり、壁に貼ってルームフレグランスとしても使用できる。 It goes without saying that the perfume-containing sheet of the present invention can be used for the purpose of musk, and can be used as a room fragrance as an indoor fragrance ornament on a table.
本発明によれば、簡単な製造方法で香料含有シートが得られ、得られた香料含有シートは薫香を目的として使用したり、室内のフレグランスオーナメントやルームフレグランスとしても使用できて産業上有用である。 According to the present invention, a perfume-containing sheet can be obtained by a simple production method, and the obtained perfume-containing sheet can be used for the purpose of musk, and can be used as an indoor fragrance ornament or room fragrance, which is industrially useful. .
１ 香料含有シート
２ 基材シート
３ 香料
４ 酸化剤
５ 意匠層
DESCRIPTION OF
Claims (4)
前記香料酸化剤アルコール溶液を基材シートに含浸する工程と、
前記香料酸化剤アルコール溶液を含浸させた基材シートを乾燥させる工程と、
からなり、
前記酸化剤は、硝酸塩または過塩素酸塩であることを特徴とする香料含有シートの製造方法。 A step of preparing a fragrance oxidant alcohol solution consisting of 3 to 18 parts by mass of fragrance, 0.1 to 1.5 parts by mass of oxidant, 10 to 30 parts by mass of water, and 60 to 80 parts by mass of alcohol;
Impregnating a base sheet with the perfume oxidant alcohol solution;
Drying the base sheet impregnated with the perfume oxidant alcohol solution;
Tona is,
The oxidizing agent, method for producing a flavor-containing sheet, wherein the nitrate or perchlorate der Rukoto.
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| KR102408396B1 (en) * | 2021-11-22 | 2022-06-10 | 설성문 | A manufacturing method of paper incense that emits fragrance when burned |
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| JP6750989B2 (en) * | 2016-09-16 | 2020-09-02 | 大王製紙株式会社 | Aroma sheet manufacturing method |
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| DE102006023413A1 (en) * | 2006-05-17 | 2007-11-22 | Bayer Cropscience Ag | Soaked with insecticidal paper |
| US20070298995A1 (en) * | 2006-06-21 | 2007-12-27 | Symrise Gmbh & Co. Kg | Fragrance-containing compositions comprising deliquescent substances |
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| KR102408396B1 (en) * | 2021-11-22 | 2022-06-10 | 설성문 | A manufacturing method of paper incense that emits fragrance when burned |
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