CN104758971B - A kind of preparation method of pure natural jasmine solid aromatic - Google Patents
A kind of preparation method of pure natural jasmine solid aromatic Download PDFInfo
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- CN104758971B CN104758971B CN201510143385.1A CN201510143385A CN104758971B CN 104758971 B CN104758971 B CN 104758971B CN 201510143385 A CN201510143385 A CN 201510143385A CN 104758971 B CN104758971 B CN 104758971B
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- jasmine
- flower
- fragrance
- starch
- solid aromatic
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Abstract
The present invention discloses a kind of preparation method of pure natural jasmine solid aromatic, and fresh Jasmine is after growing flower and telling perfume (or spice), and fragrance polymeric sorbent absorbs standby after the fragrance of a flower；50 ~ 100 DEG C are mixed and heated to converted starch, fatty acid ester, glycerine, stirring is miscible together, then 35 ~ 45 DEG C are cooled to, the adsorbent added after enfleuraging is well mixed, cooling is pressed into cream sheet, then packed with diaphragm seal, that is, obtain a kind of solid aromatic with pure natural jasmin.The solid aromatic that this method makes, is a kind of pure natural fragrance, fragrance slowly releases perfume (or spice), and it is fragrant lasting to swing, and to human body non-hazardous, and has effects that to refresh oneself, is adapted to use in places such as car, hotel, bedroom, senior offices.
Description
Technical field
The present invention relates to a kind of preparation method of solid aromatic, particularly adsorbed with adsorbent after Jasmine natural scents
The method of pure natural jasmine solid aromatic is prepared into, is a kind of long-drawn-out fragrant freshener of healthy fresh flower, is adapted in car, guest
The places such as shop, bedroom, senior office are used.
Background technology
Jasmine, alias：Jasmine, Latin literary fame：Jasminum sambac (L.) Ait, Oleaceae, gelsemium are upright
Or climbing shrub, up to 3 meters.Sprig cylinder or slightly flattening shape, it is sometimes hollow, dredge by pubescence.Leaf is to life, Dan Ye, blade paper
Matter, circular, ellipse, ovate-elliptic or obovate, two terminal circle or blunt, base portion micro-heart sometimes, above it is slightly concave enter or it is recessed
Rise, protruding below, thready pulse is in two sides Chang Mingxian, microprotrusion, except often in addition to tool tuft, remaining is hairless between following arteries and veins；Sliver is oval
Shape to subcircular, tip is justified or blunt.It is really spherical, in atropurpureus.The month at florescence 5-8, the fruiting period 7-9 months.The Hua Jixiang of jasmine, is famous
Jasmine tea raw material and important flavor of raw material；Flower, leaf is medicinal controls red eye, swell pain, and has relieving cough and reducing sputum effect.
Jasmine originates in India, now plants and is planted in subtropical zone extensively.It is mainly distributed on China, Iran, Egyptian, native ear
Its, Morocco, Algeria, Tunisia, and the Mediterranean country, Southeast Asian countries such as Spain, France, Italy
There is cultivation.The Jasmine base of Largest In China is located at Nanning Heng County, and whole county cultivated area is up to 100,000 mu, and flower-grower 330,000
People, produces 80000 tons of fresh flower per year, and jasmine flower production accounts for national total output more than 80%, accounts for world's total amount more than 60%.This county plants jasmine
Jasmine is with a long history, there is six or seven one-hundred-year histories according to legend, morning at Heng County Jasmine florescence, florescence length, bud is big, yield is high, quality good,
Thick flavor and it is famous.The State Administration of Forestry, Chinese flower association are named as in " township of Chinese jasmine ", and State General Administration for Quality Supervision ratifies to horizontal stroke
County Jasmine implements geography symbol product protection.Heng County Jasmine industry mainly with based on fresh flower scenting jasmine tea, also
There is the producer of a small amount of several production jasmine flower concretes and absolute oil, the industrial structure is relatively simple.
The pistil of the jasmine fresh flower picked also have vitality, daytime harvesting after Jasmine, evening after growing flower,
Still constantly tell perfume (or spice), whole evening tell perfume (or spice) during, occur telling fragrant peak period four to five times, the fresh flower pistil picked
Tell and give off a strong fragrance during perfume (or spice), it is natural pure and beautiful, the fragrance of a flower is absorbed by a kind of adsorbent equipment with polymeric sorbent, saturation
Adsorbent after enfleuraging is typically all to extract jasmine fresh idea sesame oil with supercritical carbon dioxide again.
Refined jasmine oil：Jasmine delicate fragrance overflows, and can extract jasmine oil, is the raw material for manufacturing essence, the personal value of jasmine oil
It is very high, equivalent to the price of gold.Jasmine can also smoke tea making leaf, or steam taking juice, can replace japanese rose distillate, be located in the Soviet Union in the south of the River
The ground such as state, Nanjing, Hangzhou, Jinhua are all produced as smoked tea flavour for a long time.Inside all " fragrance of a flower ", Jasmine
It is undoubtedly most important --- almost in neither one daily essence not comprising Jasmine fragrance, each bottle of perfume, each piece
Perfumed soap, each box cosmetics can smelling to Jasmine fragrance.Moreover, Jasmine fragrance pairing into perfume industry also
There is a huge contribution：Hundreds of fragrance of a flower spices be found in the fragrance component of Jasmine or chemist imitate
What the fragrance of Jasmine was manufactured --- the fragrance of Jasmine is in the fragrance of a flower most " rich and varied ", " just to be arrived wherein including
The animal perfume of benefit ", blue or green perfume, medicine perfume, fruity etc..Many valuable new spices are found inside jasmin oil earliest
's.Jasmine has point of " great Hua " " little Hua ", and " great Hua " is more much smaller than " little Hua ".The need for blending, some areas are also planted
Spanish jasmin is planted, and starts to extract Jasminum grandiflorum concrete and jasminum grandiflorum absolute sale.As production with other fresh flower medicinal extract,
Jasmine flower concrete is also with obtained from boiling off solvent after the fragrance component of one or several organic solvent soaking extraction jasmine fresh flower again.With
The medicinal extract fragrance that carbon dioxide supercritical extraction method is obtained is more outstanding, also closer to the fragrance of natural fresh flower, has industrialized
Production.Absolute of jasmine can be extracted in jasmine flower concrete again with pure alcohol, the preparation more suitable for daily essence is needed
Will, because the wax inside jasmine flower concrete does not dissolve in alcohol, application of the essence in many fields can be influenceed.
On essence, pastil, also there is document to describe the preparation method of some this respects, such as：
Chinese patent：《Solid essence and its preparation method》, application publication number：CN86108841, is related to a kind of for all kinds of perfume (or spice)
The solid essence and its preparation method of type daily living article.The solid essence contains liquid essence, adsorbent, Ludox, and EVA rings are
Alkane.The manufacture method of the solid essence：It is no more than in normal temperature, normal pressure and relative humidity under conditions of 80%, first will be routinely square
The abundant adsorptive liquid essence of the dried adsorbent of method, is then cladded with Ludox, is cladded again with EVA thiacyclohexanes afterwards.With
Prior art is compared, and is characterized in that fragrance keeping period is greatly prolonged, and water-tolerant, and manufacture method is simple and reliable.
Chinese patent：《Microcapsule aromatizing agent and preparation method thereof and purposes》, application publication number：CN1073711, Yi Zhongwei
The purposes of the preparation method and product of capsule odorant product and the product.This microcapsule aromatizing agent is one kind by beta-schardinger dextrin, perfume (or spice)
The slurry of essence, carboxymethyl cellulose and water composition.The product under 5-30 DEG C of room temperature condition, type discharge perfume the time be
3-4 months；The product serves many purposes, and can make fragrant silk flower, solid essence, fragrant handicraft, it may also be used for food work
Industry, feed, the daily living article of detergent and each odor type.Product is nontoxic, free from extraneous odour, and preparation method is simple, and cost is low, right
Environmental nonpollution, is that the microencapsulation of essence explores new way.
Chinese patent：《The preparation method of essence microcapsule》, application publication number：CN103736434A, a kind of micro- glue of essence
The preparation method of capsule, is mixed into emulsion by spices and wall material and is atomized by the effect of shower nozzle, and drop is with trickle spherical
Spray into hot-air, after moisture evaporation therein, the solid being dispersed in drop is dried and forms almost spherical powder
End, and essence is then wrapped in the space inside ball by wall material.Beneficial effects of the present invention are：Spray drying just has been realized in
The microencapsulation of essence, for preventing the degraded or oxidation of active component and liquid essence being converted to solid essence.Technology is
Through very ripe, and it is relative inexpensiveness, simple to operate.
Chinese patent：《A kind of Multifunctional controlled-release transparent solid aromatic and preparation method thereof》, application number：
201310191820.9, summary：A kind of Multifunctional controlled-release transparent solid aromatic, the aromatic is by following percentage by weight
Raw material be made：Gelatin 1 ~ 5%；Carragheen 0.5 ~ 2%；Algin 0.5 ~ 2%；Agar 0.5 ~ 2%；Fragrances 0.5 ~ 5%；Activity
Agent 4 ~ 10%；Bactericide 0.01 ~ 1%；Ethanol 10 ~ 20%；Bamboo vinegar 0.01 ~ 10%；Bridging agent 1 ~ 10%；Surplus is pure water；It is also disclosed
The preparation method of the aromatic.Without composition harmful to health, and with fairly good transparency and intensity, extend well
Storage and use time, this product highly transparent, environmental protection, fragrance are not pungent naturally, release fragrant slow homogeneous, can make air
Keep pure and fresh for a long time, there is good air purification function, can widely use in daily life.
Chinese patent：《A kind of preparation method of gel-type natural indoor aromatic》, application number：201010563829.4,
Summary：The preparation method of gel-type natural indoor aromatic, prepared by extraction and product of this method including Flos Albiziae the step of：It is
Using chloroform as solvent, according to solid-liquid ratio (g: ml)=1: 5~10, room temperature is extracted, ultrasonic extraction, 1~2h of extraction time, extracts secondary
Number 1~3 time;Extract solution is concentrated under reduced pressure at 50 DEG C, removes Flos Albiziae extract is obtained after Extraction solvent completely;Then with ethylene glycol
Well mixed, polyvinyl alcohol, hydroexpansivity resin-oatmeal are carrier, add above-mentioned Flos Albiziae extract, inject after sufficiently mixing
Mould, cooling produces the gel-type natural indoor aromatic.The technical scheme of use, has been successfully obtained the tax in Flos Albiziae
Fragrant composition.Obtained gel-type natural indoor aromatic is effectively sustained out soft pure and fresh fragrance, and portable easy-to-use, lasting is held
Long, fragrance is pure, can remove peculiar smell in air, can also refresh the mind, and makes us mental state peace, happy, helps to alleviate the mind
The diseases such as uneasy, melancholy insomnia.
Essence, the pastil of document above introduction are all prepared from the direct compatibility of essence and flavoring agent, essence and flavoring agent composition
All it is chemical synthesis, although be unlikely to form harmful particulate matter, but it equally contains the harmful substances such as ethanol, essence, because
This will people unconsciously when, enter in air, be rapidly absorbed by a human.Chemically angle is seen, the composition of aromatic is answered
It is miscellaneous, volatile materials is contained mostly, abuse then easily produces some chemical reactions for being difficult to expect.Its breathing of meeting to people
Road, skin produce ill-effect, and the side effect that nervous system is produced also can't neglect, and minority can also damage hemopoietic system, pierce
Swash child's breathing mucous membrane.Artificial synthesized aromatic, odor type is delicate fragrance, and giving off a strong fragrance is all different with the natural fragrance of a flower.
In recent years because the case that the pollution that artificial aromatic is caused triggers happens occasionally, somebody was spraying perfume
The preceding paragraph time is treated in environment, it may appear that the symptom such as pruitus, dizziness and cough, the serious asthma that can even happen suddenly.
The dermatitis of itch unbearably, or even Nausea and vomiting will occur in the aromatic that somebody one contacts certain odor type.This
A bit, it is both relevant with personal allergic constitution, more relevant with the pollution of aromatic, especially with allergic asthma, dermatitis, breathing system
The people for disease of uniting, should try one's best contact perfume or aromatic less.
The existing species for the product in terms of air freshener of current China is various, is summed up and is divided into gas,
Liquid, solid three types, gaseous air freshener has ozone and anion two types；The air freshener of liquid is main
It is dissolved in organic solvent and is made with various different spices；Solid-state mainly has a class of fragrant incense and stacte etc. two.It is on the market
" air freshener ", is made up of compositions such as ethanol, essence, deionized waters, and propane, butane, dimethyl ether are also contained in canned products
Deng propellant, and it is filled with the compressed gas such as a certain amount of nitrogen., can not be with leading by distributing fragrance come covering smell when using
Cause gas such as ammonia, hydrogen sulfide etc. of peculiar smell to react, be also impossible to decompose or remove this kind of pernicious gas, and can cause
The secondary pollution in room, so avoiding using as far as possible.
The content of the invention
In order to solve the deficiencies in the prior art, the present invention provides a kind of preparation side of pure natural jasmine solid aromatic
Method, using in Jasmine adsorption process, polymeric sorbent after the saturation absorption fragrance of a flower directly with converted starch, fatty acid ester,
The raw materials such as glycerine are prepared by mixing into a kind of pure natural solid aromatic, and it releases fragrant slow homogeneous, and human body is had no adverse effects, can
Extensive use in daily life.
The technical scheme is that：
A kind of preparation method of pure natural jasmine solid aromatic, is the principle grown flower using Jasmine and tell perfume, first
Jasmine is grown flower, open tell after perfume (or spice) absorbs the fragrance of a flower with polymeric sorbent, add converted starch, fatty acid ester, glycerine with
Polymeric sorbent after enfleuraging is pressed into sheet after being well mixed, and then packs and obtains solid aromatic；
Described preparation method comprises the following steps：
（1）The fresh Jasmine bud of harvesting, in 28~38 DEG C of indoor flower-growing 1~2 hour, to the flowers are in blossom into brave pawl sample,
On the flower stand for being put into sealed fragrance of a flower adsorbent equipment；
（2）The air exhauster of fragrance of a flower adsorbent equipment is opened, the fragrance that Jasmine is told into perfume is sent to equipped with polymeric sorbent
Adsorption tower, allows adsorbent saturation to adsorb Jasmine fragrance；
（3）The converted starch of parts by weight 30 ~ 80,20 ~ 40 fatty acid esters, 30 ~ 60 glycerine are mixed and heated to 50 ~ 100 DEG C
Stir as a kind of immiscible material；
（4）Immiscible material is cooled to after 35 ~ 45 DEG C, addition parts by weight 12 ~ 72 have adsorbed the polymeric sorbent of the fragrance of a flower
It is well mixed, normal temperature is then rapidly cooled to, cream sheet is pressed into tablet press machine, then scented tea is packaged into diaphragm seal；
（5）The scented tea of good seal is packed with automatic packaging machine, jasmine solid aromatic is obtained.
Above-described Jasmine can also be that Jasmine combines with the fresh flower for telling Xiang Gong energy, including Jasmine and osmanthus
Flower, yulan, white orchid, Zhulan tree, turtle turtle, shaddock, cape jasmine, Milan and rose any of which or a variety of combinations.
Different flowers, it is open to tell fragrant different.Some physiology has reached technical maturity only proximate to maturation, can carry
Preceding harvesting, safeguards under the conditions of certain environment, still can reach physiological maturity, bloom and tell perfume (or spice).Such as Jasmine, full turn of bud
To be pure white, tube elongation, calyx leaves, can harvested afternoon, and open in the evening.What is had must treat physiology full maturity in the tree,
Just open and tell perfume (or spice), could harvest.If harvest in advance, although safeguarded by fresh flower, but will not still open and tell perfume (or spice), such as white orchid, pearl
Orchid.When sweet osmanthus is in petal, without fragrance, treat that petal comes off, young flower is to open to tell perfume (or spice), corolla side, which is opened, tells perfume (or spice), side, which is stretched, to be increased
Big 5-7 opens rear pollen maturation, tells fragrant just up to peak, subsequent blossom fall flower falls.
Described polymeric sorbent is hard active fruit shell carbon, modified starch, chitosan, modified lignin resin class or with suction
The macromolecule resin of attached performance.
Hard active fruit shell carbon be it is a kind of be made with the natural shuck class such as apricot shell, walnut shell, chestnut shell, with suction
The activated carbon of attached function.Activated carbon typically used in us is all by charing, activation, overheat, steam catalytic etc. using bamboo
A series of technique is made, and the manufacture craft of active fruit shell carbon is same, and the difference existed is the difference of raw material
.
Normal activated carbon and active fruit shell carbon are also existed not except the difference in the use of raw material, between them
Some differences.Normal activated carbon is to utilize bamboo, at last a kind of most environmentally friendly material, however, active fruit shell carbon is than it more
Plus environmental protection.Because shell is all abandoned by our mankind, once remove in it kernel, shell just do not have
Its existent value.And active fruit shell carbon technique is just a kind of such shell seemed without existent value, really just
Positive becomes than its taller adsorbent of script price.On the other hand, shell is considered as that rubbish is the same to be lost
Abandon, can to earth zone to pollute while, also reduce the land used resource of rubbish.And shell is become activated carbon, exactly allow it
Have second of life, reduce global pollution.Here it is normal activated carbon and the difference of active fruit shell carbon substantially.
Hard active fruit shell carbon has powerful adsorption function, and water purification industry, municipal sewage treatment can be applied to extensively
Industry, pharmaceuticals industry etc..It also has the function of special purification air.And common activated carbon, its adsorption function is but
Much it is less than active fruit shell carbon.Just only according to the effect of purification air.Although, common activated carbon can similarly have net
Change the function of suspended particulate among air, absorption air, but its adsorption effect is but less than active fruit shell carbon.Both
Difference so that normal activated carbon is approached in the status of active fruit shell carbon step by step.Because both active fruit shell carbon and normal activated carbon
Between raw material difference, the price for causing them is also difference.Because hard active fruit shell carbon raw material are conveniently may be used
The shell obtained, it means that, its cost of raw material is than normal activated carbon, and price is also just lower.
Either in terms of raw material environmental-protecting performance, clean-up effect and in price, hard active fruit shell carbon is better than general
Logical activated carbon.With the active fruit shell carbon with the unusual advantage of normal activated carbon, the market now is gradually by masses
Welcome, it is believed that without long time, the pouplarity of active fruit shell carbon will be significantly larger than common activated carbon.
Preparation is the resin sorbent with porous three dimensional structure with the characteristics of absorption.It is several recently
A kind of porous resin that new development is got up in year field of polymer technology, by the monomer such as styrene and divinylbenzene, has in toluene etc.
In the presence of machine solvent, pass through the small ball of roe sample made from suspension copolymerization method.It is widely used in wastewater treatment, medicament separation and carries
It is pure, the carrier as chemical reaction catalyst, the filler of gas chromatographic analysis and gel permeation chromatography molecular-weight gradation post.It is special
Point is regenerating easily, can be with Reusability.Such as coordinate anion and cation exchange resin, high isolation of purified level can be reached.
Modified starch is that ative starch changes the physically or chemically special of its original after some way is handled, to some extent
Property.On the basis of the inherent characteristic that native starch has, to improve the performance of starch, expanding its application, thing is utilized
Reason, chemistry or enzymatic treatment, new functional group is introduced on starch molecule or changes starch molecule size and starch granular property,
So as to change the natural characteristic of starch（Such as：Gelatinization point, thermoviscosity and its stability, freeze-thaw stability, gel force, film forming,
Transparency etc.）, make it more suitable for the requirement necessarily applied.The converted starch that the present invention is used includes crosslinked starch, esterification and formed sediment
Powder, etherification starch, acetyl starch, phosphate ester starch, acidified starch, cationic starch, CMS etc..
Fatty acid ester is that have the full of straight chain and branched structure by what natural animal-plant grease and petrochemical feedstocks were obtained
With with unrighted acid, with monohydric alcohol or polyhydric alcohol and obtain, due to property safe to the human body, low irritant and some
Ester also has physiologically active, nutrition, the function such as enhancing metabolism, thus existing widely develop in food, medical science, agricultural chemicals, cosmetics and including
Surfactant, synthetic resin, fiber oil, intermetallic composite coating and prolong pressure and the characteristic chemical field application such as engine lubricating oil.With
The species of aliphatic acid in structure is different and different, can obtain white solid or thick liquid to yellow, odorless.Propane diols it is hard
Resin acid and palmitate are most for white solid.Using product made from oleic acid, linoleic acid etc. unsaturated acids as weak yellow liquid.
In addition with powdery, granular and wax-like.The HLB value of propylene glycol monostearate is about 2 ~ 3, is lipophilic emulsifier, does not dissolve in
Water, dissolves in ethanol, ethyl acetate, chloroform etc..
Glycerine chemical name is glycerine, and no clear and bright thick liquid of color and taste sweet tea, odorless has warm sweet taste, can be absorbed from air
Moisture, can also absorb hydrogen sulfide, hydrogen cyanide and sulfur dioxide；Glycerine is fatty alcohol, the chemism with fatty alcohol；Again simultaneously
It is polyalcohol, is simplest trihydroxylic alcohol, therefore, the chemical property of glycerine is in addition to the general character of fatty alcohol, also polyalcohol
Property.
Chitosan (chitosan) be widely present by nature chitin (chitin) obtained by deacetylation
, chemical name is Chitosan (1-4) -2- amino-B-D glucose, and from 1859, Frenchman Rouget obtained shell first
After glycan, the biological functionality and compatibility of this natural polymer, blood compatibility, security, microbic resolvability etc. are excellent
It is benign can by all trades and professions extensive concern, medicine, food, chemical industry, cosmetics, water process, METAL EXTRACTION and recovery, it is biochemical and
The application study of the numerous areas such as biomedical engineering achieves major progress.
Lignin is by four kinds of alcohol monomers（To tonquinol, coniferyl alcohol, 5- hydroxyls coniferyl alcohol, sinapinic alcohol）One kind of formation is answered
Miscellaneous phenol polymer.Lignin is a kind of unique reproducible aromatic compound, due to non-toxic inexpensive, and with exploitation
Potentiality and value.At present, this natural reproducible resource of lignin is not fully used, but discharge or burning
Fall, this not only causes the wasting of resources to a certain extent, and also results in problem of environmental pollution.Lignin is in sulfonating reaction, oxygen
Change the chemical modification reactions such as reaction, graft copolymerization, condensation reaction, Mannich reaction, alkylated reaction, hydroxyalkylation reaction
In, by changing the structure of lignin, the property of lignin can be improved, expand the application of lignin.The suction of the present invention
Attached dose uses modified lignin resin, and the protection of utilization, environment for natural resources is respectively provided with important meaning.
Solid aromatic of the present invention is a kind of long-drawn-out fragrant freshener of healthy fresh flower, in use, taking solid aromatic apart
After the sealing film packaging of agent, it is placed on the appropriate place of car, hotel, bedroom, senior office or is directly placed at appearance
In device or vessel.
Utstanding substantial characteristics and significant improvement of the present invention are：
1st, the aromatic that the preparation method of the pure natural jasmine solid aromatic of the present invention is prepared from, can both distribute virtue
Perfume (or spice), polymeric sorbent can also be reached the effect of purification air by the peculiar smell in absorption air, stink etc., fundamentally be improved
Air quality, will not cause environmental pollution when using；
2nd, the present invention using Jasmine grow flower tells perfume principle, with polymeric sorbent absorb the fragrance of a flower, then with converted starch,
Fatty acid ester, glycerine with enfleurage after polymeric sorbent be well mixed after be pressed into sheet, then pack as a kind of solid
Body aromatic, is a kind of pure natural fragrance, and fragrance slowly releases perfume (or spice), and it is fragrant lasting to swing, to human body non-hazardous, and with the work(refreshed oneself
Effect, is adapted to use in places such as car, hotel, bedroom, senior offices；
3rd, the preparation method of the pure natural jasmine solid aromatic of the present invention, its adsorbent is a kind of with absorption property
High polymer material, such as hard active fruit shell carbon, preparation, either in terms of raw material environmental-protecting performance, clean-up effect
And in price, better than common adsorbent reduces preparation cost；
4th, the aromatic that the preparation method of the pure natural jasmine solid aromatic of the present invention is prepared from, easy to use, tears open
After the sealing film packaging for opening solid aromatic, it is placed on the place of ventilation or is directly placed in container or vessel.
Brief description of the drawings：
Fig. 1 is the process chart of the present invention.
Embodiment
Embodiment 1：
A kind of preparation method of pure natural jasmine solid aromatic, absorbs the fragrance of a flower, then use with polymeric sorbent first
Converted starch, fatty acid ester, glycerine with enfleurage after polymeric sorbent be well mixed after be pressed into sheet, then pack into
For a kind of solid aromatic；
Described preparation method comprises the following steps：
（1）After fresh Jasmine purchase is returned, first spreading for cooling, in 28~38 DEG C of indoor flower-growing 1~2 hour, grow flower to
The flowers are in blossom into brave pawl sample, that is, on the flower stand for being put into sealed fragrance of a flower adsorbent equipment；
（2）Open the air exhauster of fragrance of a flower adsorbent equipment, the fragrance that Jasmine is told into perfume be sent to equipped with hard active fruit shell carbon or
The adsorption tower of modified starch, allows polymeric sorbent saturation to adsorb Jasmine fragrance；
（3）The converted starch of parts by weight 30,20 fatty acid esters, 30 glycerine are mixed and heated into 50 ~ 100 DEG C to be stirred into
For a kind of immiscible material；
（4）Immiscible material is cooled to after 35 ~ 45 DEG C, addition parts by weight 12 have adsorbed the polymeric sorbent mixing of the fragrance of a flower
Uniformly, normal temperature is then rapidly cooled to, cream sheet is pressed into tablet press machine, then scented tea is packaged into diaphragm seal；
（5）The scented tea of good seal is wired up with automatic packaging machine, so as to obtain jasmine solid aromatic.
Described Jasmine is that Jasmine combines with the fresh flower for telling Xiang Gong energy, such as Jasmine and sweet osmanthus, yulan magnolia, night
Come fragrant flower, white orchid, Zhulan tree, turtle turtle, shaddock, cape jasmine, tree orchid, rose any of which or a variety of combinations.
Described polymeric sorbent is hard active fruit shell carbon, modified starch, chitosan, modified lignin resin class or with suction
The macromolecule resin of attached performance.
Described solid aromatic is placed on the ground of ventilation in use, take apart after the sealing film packaging of solid aromatic
Side is directly placed in container or vessel.
Embodiment 2
A kind of preparation method of pure natural jasmine solid aromatic, is grown flower using Jasmine and tells the principle of perfume, use high score
Sub- adsorbent absorbs the fragrance of a flower, then pressure after being well mixed with converted starch, fatty acid ester, glycerine and the polymeric sorbent after enfleuraging
Slabbing, is then packed as a kind of solid aromatic；
Described preparation method comprises the following steps：
（1）After fresh Jasmine purchase is returned, first spreading for cooling, in 28~38 DEG C of indoor flower-growing 1~2 hour, grow flower to
The flowers are in blossom into brave pawl sample, that is, on the flower stand for being put into sealed fragrance of a flower adsorbent equipment；
（2）The air exhauster of fragrance of a flower adsorbent equipment is opened, the fragrance that Jasmine is told into perfume is sent to equipped with chitosan or innovation wood
The adsorption tower of quality family macromolecule adsorbent, allows polymeric sorbent saturation to adsorb Jasmine fragrance；
（3）The converted starch of parts by weight 55,30 fatty acid esters, 45 glycerine are mixed and heated into 50 ~ 100 DEG C to be stirred into
For a kind of immiscible material；
（4）Immiscible material is cooled to after 35 ~ 45 DEG C, the adsorbent that addition parts by weight 42 have adsorbed the fragrance of a flower is well mixed,
Then normal temperature is rapidly cooled to, cream sheet is pressed into tablet press machine, then scented tea is packaged into diaphragm seal；
（5）The scented tea of good seal is wired up with automatic packaging machine, so as to obtain jasmine solid aromatic.
Described Jasmine is that Jasmine combines with the fresh flower for telling Xiang Gong energy, such as Jasmine and sweet osmanthus, yulan magnolia, night
Come fragrant flower, white orchid, Zhulan tree, turtle turtle, shaddock, cape jasmine, tree orchid, rose any of which or a variety of combinations.
Described polymeric sorbent is hard active fruit shell carbon, modified starch, chitosan, modified lignin resin class or with suction
The macromolecule resin of attached performance.
Described solid aromatic is placed on the ground of ventilation in use, take apart after the sealing film packaging of solid aromatic
Side is directly placed in container or vessel.
Embodiment 3
A kind of preparation method of pure natural jasmine solid aromatic, is grown flower using Jasmine and tells the principle of perfume, use high score
Sub- adsorbent absorbs the fragrance of a flower, then pressure after being well mixed with converted starch, fatty acid ester, glycerine and the polymeric sorbent after enfleuraging
Slabbing, is then packed as a kind of solid aromatic；
Described preparation method comprises the following steps：
（1）After fresh Jasmine purchase is returned, first spreading for cooling, in 28~38 DEG C of indoor flower-growing 1~2 hour, grow flower to
The flowers are in blossom into brave pawl sample, that is, on the flower stand for being put into sealed fragrance of a flower adsorbent equipment；
（2）The air exhauster of fragrance of a flower adsorbent equipment is opened, the fragrance that Jasmine is told into perfume is sent to equipped with polymeric sorbent
Adsorption tower, allows polymeric sorbent saturation to adsorb Jasmine fragrance；
（3）The converted starch of parts by weight 80,40 fatty acid esters, 60 glycerine are mixed and heated into 50 ~ 100 DEG C to be stirred into
For a kind of immiscible material；
（4）Immiscible material is cooled to after 35 ~ 45 DEG C, addition parts by weight 72 have adsorbed the polymeric sorbent mixing of the fragrance of a flower
Uniformly, normal temperature is then rapidly cooled to, cream sheet is pressed into tablet press machine, then scented tea is packaged into diaphragm seal；
（5）The scented tea of good seal is wired up with automatic packaging machine, so as to obtain jasmine solid aromatic.
Described Jasmine is that Jasmine combines with the fresh flower for telling Xiang Gong energy, such as Jasmine and sweet osmanthus, yulan magnolia, night
Come fragrant flower, white orchid, Zhulan tree, turtle turtle, shaddock, cape jasmine, tree orchid, rose any of which or a variety of combinations.
Described polymeric sorbent is hard active fruit shell carbon, modified starch, chitosan, modified lignin resin class or with suction
The macromolecule resin of attached performance.
Described solid aromatic is placed on the ground of ventilation in use, take apart after the sealing film packaging of solid aromatic
Side is directly placed in container or vessel.
Claims (3)
1. a kind of preparation method of pure natural jasmine solid aromatic, it is characterised in that Jasmine is grown flower first, opening is told
The fragrance of a flower is absorbed with polymeric sorbent after perfume (or spice), the polymeric sorbent after adding converted starch, fatty acid ester, glycerine and enfleuraging
Sheet is pressed into after well mixed, then packs and obtains solid aromatic；
Described preparation method is comprised the steps of：
（1）The fresh Jasmine bud of harvesting, in 28~38 DEG C of indoor flower-growing 1~2 hour, to the flowers are in blossom into brave pawl sample, that is, puts
Onto the flower stand of sealed fragrance of a flower adsorbent equipment；
（2）The air exhauster of fragrance of a flower adsorbent equipment is opened, the fragrance that Jasmine is told into perfume is sent to the absorption equipped with polymeric sorbent
Tower, allows polymeric sorbent saturation to adsorb Jasmine fragrance；
（3）The converted starch of parts by weight 30~80,20~40 fatty acid esters, 30~60 glycerine are mixed and heated to 50~100 DEG C
Stir as a kind of immiscible material；
（4）Immiscible material is cooled to after 35~45 DEG C, the polymeric sorbent that addition parts by weight 12~72 have adsorbed the fragrance of a flower is mixed
Close uniform, be then rapidly cooled to normal temperature, cream sheet is pressed into tablet press machine, then scented tea is packaged into diaphragm seal；
（5）The scented tea of good seal is packed with automatic packaging machine, jasmine solid aromatic is obtained；
The converted starch be crosslinked starch, esterification starch, etherification starch, acetyl starch, phosphate ester starch, acidified starch,
It is one or more in cationic starch, CMS.
2. the preparation method of pure natural jasmine solid aromatic according to claim 1, it is characterised in that described jasmine
Flower can also be that Jasmine combines with the fresh flower for telling Xiang Gong energy, including Jasmine and sweet osmanthus, yulan, white orchid, Zhulan tree, turtle
Turtle, shaddock, cape jasmine, Milan and rose any of which or a variety of combinations.
3. the preparation method of pure natural jasmine solid aromatic according to claim 1, it is characterised in that described high score
Sub- adsorbent is the activated carbon modified starch of xylocarp shell, chitosan, modified lignin resin class or the macromolecule resin with absorption property.
Priority Applications (1)
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| CN107041446A (en) * | 2017-01-09 | 2017-08-15 | 南宁市化工研究设计院 | It is a kind of to improve the method that jasmine fresh flower tells fragrant amount |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN102264352A (en) * | 2008-11-14 | 2011-11-30 | 阿彻丹尼尔斯米德兰德公司 | Organogel compositions and processes for producing |
| CN103251967A (en) * | 2013-05-28 | 2013-08-21 | 杭州透云制香有限公司 | Vehicle-mounted incense sheet and production method thereof |
| CN103525556A (en) * | 2013-09-25 | 2014-01-22 | 广西茉莉花开发投资有限公司 | Ecological flower planting method before extracting jasmine flower aroma substances |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN102264352A (en) * | 2008-11-14 | 2011-11-30 | 阿彻丹尼尔斯米德兰德公司 | Organogel compositions and processes for producing |
| CN103251967A (en) * | 2013-05-28 | 2013-08-21 | 杭州透云制香有限公司 | Vehicle-mounted incense sheet and production method thereof |
| CN103525556A (en) * | 2013-09-25 | 2014-01-22 | 广西茉莉花开发投资有限公司 | Ecological flower planting method before extracting jasmine flower aroma substances |
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