CN104758971A - Preparation method of pure natural jasmine solid aromatic - Google Patents
Preparation method of pure natural jasmine solid aromatic Download PDFInfo
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- CN104758971A CN104758971A CN201510143385.1A CN201510143385A CN104758971A CN 104758971 A CN104758971 A CN 104758971A CN 201510143385 A CN201510143385 A CN 201510143385A CN 104758971 A CN104758971 A CN 104758971A
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- CN
- China
- Prior art keywords
- fragrance
- flower
- jasmini sambac
- solid aromatic
- flos jasmini
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Landscapes
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- Fats And Perfumes (AREA)
Abstract
The invention discloses a preparation method of a pure natural jasmine solid aromatic. The preparation method of the pure natural jasmine solid aromatic comprises the following steps: after fresh jasmine flowers grow and breathe fragrance to the air, absorbing the fragrance by adopting a high polymer adsorbent for later use; mixing modified starch, fatty acid ester and glycerine, heating to 50-100 DEG C, stirring, mixing and dissolving together, then cooling to 35-45 DEG C, then adding the adsorbent absorbed with the fragrance, uniformly mixing, cooling and crushing into paste flakes, and then sealing and packaging with a thin film, so that the solid aromatic with pure natural jasmine fragrance is obtained. The obtained solid aromatic can slowly release pure natural fragrance, the fragrance is lasting and is harmless to a human body, and the obtained solid aromatic has the effect of refreshing and is applicable to places such as a saloon car, a hotel, a bedroom and an advanced office.
Description
Technical field
The present invention relates to a kind of preparation method of solid aromatic, particularly by the method for jasmine solid aromatic being prepared into pure natural after adsorbent Flos Jasmini Sambac natural scents, be that a kind of flower of health is swung fragrant freshener, be adapted at that car, hotel, bedroom, senior office etc. are local to be used.
Background technology
Flos Jasmini Sambac, another name: jasmine, Latin literary fame:
jasminum sambac (L.) Ait, the upright or climbing shrub of Oleaceae, gelsemium, up to 3 meters.Sprig is cylindrical or slightly flatten shape, hollow sometimes, dredges by pubescence.Leaf to life, Dan Ye, blade papery, circular, oval, ovum shape is oval or obovate, two terminal circle or blunt, base portion is micro-heart sometimes, slightly recessed or recessed above, below protruding, thready pulse at two sides Chang Mingxian, microprotrusion, except below between arteries and veins axil except normal tool tuft, all the other are without hair; Sliver Long Circle is to subcircular, and tip is round or blunt.Fruit is spherical, in atropurpureus.The florescence 5-8 month, the fruit phase 7-9 month.The Hua Jixiang of jasmine is famous scented tea raw material and important flavor of raw material; Flower, leaf is medicinal controls conjunctival congestion and swelling pain, and has the effect of relieving cough and resolving phlegm.
Flos Jasmini Sambac originates in India, and existing extensively planting is planted in subtropical zone.Mainly be distributed in China, Iran, Egypt, Turkey, Morocco, Algeria, Tunisia, and the Mediterranean country such as Spain, France, Italy, Southeast Asian countries all has cultivation.The Flos Jasmini Sambac base of Largest In China is positioned at Heng County, Nanning, and whole county cultivated area reaches 100,000 mu, flower-grower 330,000 people, and produce flower 80,000 tons per year, jasmine flower production accounts for national total output more than 80%, accounts for world's total amount more than 60%.This county plantation Flos Jasmini Sambac is with a long history, has six or seven one-hundred-year histories according to legend, and the Heng County Flos Jasmini Sambac florescence early, the florescence is long, alabastrum is large, output is high, quality is good, thick flavor and famous.The State Administration of Forestry, Chinese flower association called after " township of Chinese jasmine ", State General Administration for Quality Supervision's approval implements geography symbol product protection to Heng County Flos Jasmini Sambac.Flos Jasmini Sambac industry in Heng County is mainly based on flower scenting tea, and also have the producer of a small amount of several production Flos Jasmini Sambac extractum and absolute oil, the industrial structure is comparatively simple.
The pistil of the jasmine flower picked also has vitality, Flos Jasmini Sambac after plucking daytime, evening is after growing flower, still constantly tell perfume (or spice), tell in fragrant process in whole evening, occur telling fragrant peak period for four to five times, the flower pistil picked is told in fragrant process and is given off a strong fragrance, natural pure and beautiful, the fragrance of a flower is absorbed by a kind of adsorbent equipment with polymeric sorbent, saturated enfleurage after adsorbent be all generally use supercritical carbon dioxide extraction jasmine fresh idea Oleum sesami again.
Jasmin quintessence oil: Flos Jasmini Sambac delicate fragrance overflows, can extract Jasmin oil, and be the raw material manufacturing essence, the personal value of Jasmin oil is very high, is equivalent to the price of gold.Flos Jasmini Sambac also can smoke tea making leaf, or steams taking juice, can replace Liquor Flos Rosae Distillata, is located in the ground such as the Suzhou in the south of the River, Nanjing, Hangzhou, Jinhua and all produces as smoked tea flavour for a long time.In all " fragrance of a flower " the inside, Flos Jasmini Sambac is most important beyond doubt---and almost do not comprise Flos Jasmini Sambac fragrance in neither one daily essence, each bottle of perfume, each block fancy soap, each box cosmetics can smell the fragrance smelling Flos Jasmini Sambac.Moreover, Flos Jasmini Sambac fragrance involutory one-tenth perfume industry also has a huge contribution: hundreds of fragrance of a flower spice be find from the fragrance component of Flos Jasmini Sambac or chemist to imitate the fragrance of Flos Jasmini Sambac produced---the fragrance of Flos Jasmini Sambac be in the fragrance of a flower " rich and varied ", wherein include the animal perfume, QINGXIANG, medicated incense, fruital etc. of " just right ".Much valuable new spice all finds the earliest inside Flos Jasmini Sambac oil.What Flos Jasmini Sambac had " Flos Caryophylli " " little Hua " divides, and " Flos Caryophylli " is more much smaller than " little Hua ".Due to the needs of perfumery, Spanish jasmin is also planted in some area, and starts to extract Jasminum grandiflorum concrete and jasminum grandiflorum absolute sale.Production with other flower extractum is the same, Flos Jasmini Sambac extractum also with one or several organic solvent soaking extraction jasmine flowers fragrance component after boil off solvent again and obtain.The extractum fragrance obtained by carbon dioxide supercritical extraction method is more outstanding, also closer to the fragrance of natural fresh flower, and now suitability for industrialized production.Jasminun sambae aif can be extracted again from Flos Jasmini Sambac extractum with pure ethanol, be more suitable for the preparation needs of daily essence because the waxiness inside Flos Jasmini Sambac extractum is insoluble to ethanol, can affect essence in a lot of fields in application.
About essence, pastil, document is also had to describe the preparation method of some this respects, as:
Chinese patent: " solid essence and method for making thereof ", application publication number: CN86108841, relates to a kind of solid essence for each odor type daily living article and method for making thereof.This solid essence contains liquid essence, adsorbent, Ludox, EVA thiacyclohexane.The manufacture method of this solid essence: be no more than the condition of 80% at room temperature, normal pressure and relative humidity under, first by abundant for adsorbent dried according to a conventional method adsorptive liquid essence, then with Ludox cladding, clads with EVA thiacyclohexane afterwards again.Compared with prior art, be characterized in that fragrance keeping period extends greatly, and water-tolerant, manufacture method is simple and reliable.
Chinese patent: " microcapsule aromatizing agent and preparation method thereof and purposes ", application publication number: CN1073711, the preparation method of a kind of microcapsule aromatizing agent product and this product and the purposes of product.This microcapsule aromatizing agent is a kind of slurry be made up of beta-schardinger dextrin-, essence, carboxymethyl cellulose and water.This product is under the room temperature condition of 5-30 DEG C, and the type discharge fragrant time is 3-4 months; This product serves many purposes, and can make fragrant silk flower, solid essence, fragrant artware, also can be used for the daily living article of food industry, feedstuff, detergent and each odor type.Product is nontoxic, free from extraneous odour, and preparation method is simple, and cost is low, environmentally safe, for the microencapsulation of essence explores new way.
Chinese patent: " preparation method of essence microcapsule ", application publication number: CN103736434A, a kind of preparation method of essence microcapsule, spice and wall material are mixed into emulsion be atomized by the effect of shower nozzle, drop spherically sprays in hot-air with trickle, when after moisture evaporation wherein, be dispersed in the solid in drop and dried and that formation is intimate spherical powder, essence is then wrapped in the space inside ball by wall material.Beneficial effect of the present invention is: spraying dry has just achieved the micro encapsulation of essence, is used for preventing the degraded of active component or oxidation and liquid essence being converted to solid essence.Technology is very ripe, and relative inexpensiveness, simple to operate.
Chinese patent: " a kind of Multifunctional controlled-release transparent solid aromatic and preparation method thereof ", application number: 201310191820.9, summary: a kind of Multifunctional controlled-release transparent solid aromatic, this aromatic is made up of the raw material of following percentage by weight: gelatin 1 ~ 5%; Carrageenan 0.5 ~ 2%; Algin 0.5 ~ 2%; Agar 0.5 ~ 2%; Fragrances 0.5 ~ 5%; Activating agent 4 ~ 10%; Antibacterial 0.01 ~ 1%; Ethanol 10 ~ 20%; Bamboo vinegar solution 0.01 ~ 10%; Bridging agent 1 ~ 10%; Surplus is pure water; Also disclose the preparation method of this aromatic.Not containing the composition be harmful to health, and there is goodish transparency and intensity, extend storage and service time well, this product highly transparent, environmental protection, fragrance is not pungent naturally, release perfume (or spice) slowly homogeneous, air can be made to keep pure and fresh for a long time, have good air purification function, can widely use in daily life.
Chinese patent: " a kind of preparation method of gel-type natural indoor aromatic "; application number: 201010563829.4; summary: the preparation method of gel-type natural indoor aromatic; the method comprises step prepared by the extraction of Flos Albiziae and product: be take chloroform as solvent; according to solid-liquid ratio (g: ml)=1: 5 ~ 10, room temperature is extracted, supersound extraction; extraction time 1 ~ 2h, extraction time 1 ~ 3 time; Extracting solution is concentrating under reduced pressure at 50 DEG C, obtains Flos Albiziae extract after removing Extraction solvent completely; Then with ethylene glycol mix homogeneously, polyvinyl alcohol, hydroexpansivity resin-oatmeal for carrier, add above-mentioned Flos Albiziae extract, inject mould after sufficiently mixing, cool and obtain described gel-type natural indoor aromatic.The technical scheme adopted, successfully obtains the fragrant composition of tax in Flos Albiziae.The obtained effective slow release of gel-type natural indoor aromatic goes out soft pure and fresh fragrance, and portable easy-to-use, lasting is lasting, fragrance is pure, can remove abnormal flavour in air, all right refreshment, make us mental state peace, happy, contribute to alleviating the disease such as irritability, melancholy insomnia.
Essence, the pastil of above document introduction are all prepared from the direct compatibility of essence and flavoring agent, essence and flavoring agent composition is all chemosynthesis, although be unlikely to form harmful particulate matter, but it is equally containing the harmful substance such as ethanol, essence, therefore will when people be involuntary, enter into air, be rapidly absorbed by a human.Chemically angle is seen, the complicated component of aromatic, and mostly containing volatile material, abuse then easily produces some chemical reactions being difficult to expect.It can produce ill effect to the respiratory tract of people, skin, and also can't neglect the side effect that nervous system produces, minority also can damage hemopoietic system, stimulates child to breathe mucosa.The aromatic of synthetic, odor type is delicate fragrance, and giving off a strong fragrance is all different with the natural fragrance of a flower.
The case that the pollution caused due to artificial aromatic in recent years causes happens occasionally, and somebody treats the preceding paragraph time in the environment spraying perfume, there will be the symptoms such as skin pruritus, dizziness and cough, the serious asthma that even can happen suddenly.
Somebody there will be pruritus dermatitis unbearably once the aromatic contacting certain odor type, even Nausea and vomiting.These, both relevant with the allergic constitution of individual, more relevant with the pollution of aromatic, especially suffer from the people of allergic asthma, dermatitis, respiratory system disease, perfume or aromatic should be contacted less as far as possible.
Current China is existing of a great variety for the product of air freshener aspect, is summed up and is divided into gas, liquid, solid three types, and the air freshener of gaseous state has ozone and anion two type; Liquid air freshener is mainly dissolved in organic solvent with various different spice to be made; Solid-state mainly contain two class such as scented incense and incense." air freshener " that market is sold, is become to be grouped into by ethanol, essence, deionized water etc., also containing propellants such as propane, butane, dimethyl ether in canned products, and fills with Compressed Gas such as a certain amount of nitrogen.During use by scentetd come covering smell, can not react with causing the gas of abnormal flavour such as ammonia, hydrogen sulfide etc., also just can not decompose or remove this kind of harmful gas, and the secondary pollution in room can be caused, thus avoid as far as possible use.
Summary of the invention
In order to solve the deficiencies in the prior art, the invention provides a kind of preparation method of jasmine solid aromatic of pure natural, utilize in Flos Jasmini Sambac adsorption process, polymeric sorbent after the saturated adsorption fragrance of a flower directly with the mixed raw material such as modified starch, fatty acid ester, glycerol for the solid aromatic becoming a kind of pure natural, it is slowly homogeneous that it releases perfume (or spice), human body is had no adverse effects, can extensive use in daily life.
Technical scheme of the present invention is:
A kind of preparation method of jasmine solid aromatic of pure natural, utilize Flos Jasmini Sambac to grow flower to tell fragrant principle, first Flos Jasmini Sambac is grown flower, open after telling perfume (or spice) and absorb the fragrance of a flower with polymeric sorbent, add again after modified starch, fatty acid ester, glycerol and the polymeric sorbent after enfleuraging are mixed homogeneously and be pressed into lamellar, then pack and obtain solid aromatic;
Described preparation method comprises the following steps:
(1) pluck fresh Flos Jasmini Sambac alabastrum, at the indoor flower-growing 1 ~ 2 hour of 28 ~ 38 DEG C, become Unguis Tigris sample to the flowers are in blossom, be namely put on the flower stand of fragrance of a flower adsorbent equipment of sealing;
(2) open the air exhauster of fragrance of a flower adsorbent equipment, Flos Jasmini Sambac is told fragrant fragrance and deliver to the adsorption tower that polymeric sorbent is housed, allow adsorbent saturated adsorption Flos Jasmini Sambac fragrance;
(3) parts by weight 30 ~ 80 modified starch, 20 ~ 40 fatty acid esters, 30 ~ 60 glycerol are mixed and heated to 50 ~ 100 DEG C to stir and become a kind of immiscible material;
(4), after immiscible material being cooled to 35 ~ 45 DEG C, adding the polymeric sorbent mix homogeneously that parts by weight 12 ~ 72 have adsorbed the fragrance of a flower, be then cooled to room temperature rapidly, be pressed into cream lamellar with tablet machine, be then packaged into scented tea with diaphragm seal;
(5) pack with the scented tea of automatic packaging machine by good seal, obtain jasmine solid aromatic.
Above-described Flos Jasmini Sambac can also be Flos Jasmini Sambac with have tell Xiang Gong can flower combine, comprise wherein any one or more the combination of Flos Jasmini Sambac and Flos Osmanthi Fragrantis, Magnolia denudata, white orchid, Caulis seu folium chloranthi spicati (Chloranthus spicatus(Thunb.) Mak.), turtle turtle, Fructus Citri grandis, Fructus Gardeniae, Milan and Flos Rosae Rugosae.
Different flowers, opening is told fragrant different.Some physiology only close to ripe, but reaches technical maturity, can harvest in advance, safeguards, still can reach physiological maturity, bloom and tell perfume (or spice) under certain environment condition.As Flos Jasmini Sambac, alabastrum is full to be transferred to pure white, and tube extends, and calyx leaves, and can gather afternoon, and evening is open.What have must treat physiology full maturity in the tree, just opens and tells perfume (or spice), just can gather.If harvest in advance, although safeguard through flower, still can not open and tell perfume (or spice), as Flos micheliae Albae, chu lan flower.When Flos Osmanthi Fragrantis is petal, do not have fragrance, treat that petal comes off, perfume (or spice) is told in children's flower and opening, and corolla limit is open tells perfume (or spice), and limit is stretched increase 5-7 and opened rear pollen maturation, tells perfume and just reaches peak, and the flower of blossom fall subsequently falls.
Described polymeric sorbent is hard active fruit shell carbon, modified starch, chitosan, modified lignin resin class or have the macromolecule resin of absorption property.
Hard active fruit shell carbon to be a kind ofly made with natural shuck classes such as Fructus Pruni shell, walnut shell, Semen Castaneae shells, has the active carbon of adsorption function.Generally our active carbon used is all utilize bamboo through carbonization, activation, overheated, and a series of technique such as steam catalytic is made, and the processing technology of active fruit shell carbon is identical with it, and the difference of existence is raw-material difference.
Normal activated carbon and active fruit shell carbon, except difference to some extent in raw-material use, also also exist other some differences between them.Normal activated carbon utilizes bamboo, a kind of material of most environmental protection at last, but active fruit shell carbon is than its more environmental protection.Because shell all abandon by we mankind, once remove the kernel of its inherence, shell is just without its existent value.And active fruit shell carbon technique is just so a kind of shell seemed without existent value, really just to become than its price is taller originally adsorbent.On the other hand, it is the same the abandoning of rubbish that shell is used as, and while bringing pollution, also reduces the land used resource of rubbish to the earth.And shell is become active carbon, allow it have second time life exactly, reduce global pollution.Here it is normal activated carbon and active fruit shell carbon in essence different.
Hard active fruit shell carbon has powerful adsorption function, can extensively be applied to water purification industry, municipal wastewater treatment field, pharmaceuticals industry etc.It also has the special function purified air.And common active carbon, its adsorption function is but far away less than active fruit shell carbon.Just only according to the effect purified air.Although common active carbon can have too and purifies air, the function of particle in the middle of absorbed air, but its adsorption effect is but less than active fruit shell carbon.The difference of both, makes the status of active fruit shell carbon approach normal activated carbon step by step.Because active fruit shell carbon and normal activated carbon are raw-material different, their price is caused also to be difference to some extent between the two.Because hard active fruit shell carbon raw material is easily available shell, this means, its cost of raw material is than normal activated carbon, and price is also just lower.
No matter be in raw material environmental-protecting performance, clean-up effect and in price, hard active fruit shell carbon is all better than normal activated carbon.Have the active fruit shell carbon of the unusual advantage with normal activated carbon, the market is now welcomed by the general public gradually, believes without long time, and the pouplarity of active fruit shell carbon will far away higher than common active carbon.
Preparation is adsorbed as feature, has the resin sorbent of porous three dimensional structure.It is a kind of porous resin that in field of polymer technology recent years, new development is got up, by the monomer such as styrene and divinylbenzene, under the organic solvents such as toluene exist, and the little ball of the fish roe sample obtained by suspension copolymerization method.Be widely used in wastewater treatment, medicament isolation andpurification, as the carrier of chemical reaction catalyst, the filler of gas chromatographic analysis and gel permeation chromatography molecular-weight gradation post.Be characterized in regenerating easily, can Reusability.As coordinated anion and cation exchange resin, high isolation of purified level can be reached.
Modified starch is ative starch after process someway, changes its original physics or chemical characteristic to some extent.On the basis of the inherent character had at native starch, for improve starch performance, expand its range of application, utilize physics, chemistry or enzymatic treatment, starch molecule is introduced new functional group or changes starch molecule size and starch granular property, thus change the natural characteristic (as: gelatinization point, thermoviscosity and stability thereof, freeze-thaw stability, gel force, film property, the transparency etc.) of starch, make it be more suitable for the requirement of certain application.The modified starch that the present invention uses comprises crosslinked starch, esterification starch, etherification starch, acetyl starch, phosphate ester starch, acidified starch, cationic starch, carboxymethyl starch etc.
Fatty acid ester is the saturated and unsaturated fatty acid with straight chain and branched structure obtained by natural animal-plant oils and fats and petrochemical feedstocks, obtain with monohydric alcohol or polyhydric alcohol, owing to having, physiologically active, nutrition also had to human safety, low irritant some ester, strengthen the functions such as metabolism, therefore now extensively expand in food, medical science, pesticide, cosmetics and comprise surfactant, synthetic resin, fiber oil, intermetallic composite coating and prolong pressure and the application of engine lubrication wet goods characterization work field.Different with the kind difference of the fatty acid in structure, can obtain white to yellow solid or thick liquid, odorless.The stearic acid of propylene glycol and palmitate majority are white solid.The product obtained with oleic acid, linoleic acid etc. unsaturated acids is for weak yellow liquid.In addition powdery, granular and wax-like is also had.The HLB value of propylene glycol monostearate is about 2 ~ 3, is lipophilic emulsifier, water insoluble, dissolves in ethanol, ethyl acetate, chloroform etc.
Glycerinated formal name used at school is glycerol, and without the sweet clear and bright thick liquid of color and taste, odorless, has warm sweet taste, can absorb moisture from air, also can absorbing hydrogen sulphide, Blausure (German) and sulfur dioxide; Glycerol is fatty alcohol, has the chemism of fatty alcohol; Be again polyhydric alcohol, be the simplest trihydroxylic alcohol simultaneously, and therefore, the chemical property of glycerol, except the general character of fatty alcohol, also has the character of polyhydric alcohol.
Chitosan (
chitosan) be extensively existed by nature chitin (
chitin) obtain through deacetylation, chemical name is Chitosan (1-4)-2-amino-B-D glucose, from 1859, after first Frenchman Rouget obtains chitosan, the premium properties such as the biological functionality of this natural polymer and the compatibility, blood compatibility, safety, microbic resolvability, by all trades and professions extensive concern, achieve major progress at the applied research of the numerous areas such as medicine, food, chemical industry, cosmetics, water treatment, METAL EXTRACTION and recovery, biochemistry and biomedical engineering.
Lignin is the complicated phenol polymer of one formed by four kinds of alcohol monomers (to tonquinol, 4-hydroxy-3-methoxycinnamic alcohol, 5-hydroxyl 4-hydroxy-3-methoxycinnamic alcohol, sinapinic alcohol).Lignin is unique a kind of reproducible aromatic compound, due to non-toxic inexpensive, and has potentiality and the value of exploitation.At present, this natural reproducible resource of lignin is not fully used, but discharges or burn, and this not only causes the wasting of resources to a certain extent, but also causes problem of environmental pollution.Lignin is in the chemical modification reactions such as sulfonating reaction, oxidation reaction, graft copolymerization, condensation reaction, Mannich reaction, alkylated reaction, hydroxyalkylation reaction, by changing the structure of lignin, the character of lignin can be improved, expand the range of application of lignin.Adsorbent of the present invention adopts modified lignin resin, is all significant for the utilization of natural resources, the protection of environment.
Solid aromatic of the present invention is that a kind of flower of health is swung fragrant freshener, during use, after taking the sealing film packaging of solid aromatic apart, be placed on the suitable place of car, hotel, bedroom, senior office or be directly placed in container or vessel.
Outstanding substantive distinguishing features of the present invention and significant progress are:
1, the aromatic that is prepared from of the preparation method of the jasmine solid aromatic of pure natural of the present invention, both can expire fragrance, polymeric sorbent also can reach by the abnormal flavour, stink etc. absorbed in air the effect purified air, fundamentally improve air quality, during use, can not environmental pollution be caused;
2, the present invention utilizes Flos Jasmini Sambac to grow flower and tells fragrant principle, the fragrance of a flower is absorbed with polymeric sorbent, lamellar is pressed into after mixing homogeneously with modified starch, fatty acid ester, glycerol and the polymeric sorbent after enfleuraging again, then pack and become a kind of solid aromatic, be a kind of fragrance of pure natural, fragrance slowly releases perfume (or spice), long-drawn-out fragrant lasting, to human body without harm, and there is the effect of refreshing oneself, be adapted at the local use such as car, hotel, bedroom, senior office;
3, the preparation method of the jasmine solid aromatic of pure natural of the present invention, its adsorbent is a kind of macromolecular material with absorption property, as hard active fruit shell carbon, preparation, no matter be in raw material environmental-protecting performance, clean-up effect and in price, all be better than common adsorbent, reduce preparation cost;
4, the aromatic that is prepared from of the preparation method of the jasmine solid aromatic of pure natural of the present invention, easy to use, after taking the sealing film packaging of solid aromatic apart, is placed on the place of ventilation or is directly placed in container or vessel.
accompanying drawing illustrates:
Fig. 1 is process chart of the present invention.
Detailed description of the invention
Embodiment 1:
A kind of preparation method of jasmine solid aromatic of pure natural, first the fragrance of a flower is absorbed with polymeric sorbent, be pressed into lamellar after mixing homogeneously with modified starch, fatty acid ester, glycerol and the polymeric sorbent after enfleuraging again, then pack and become a kind of solid aromatic;
Described preparation method comprises the following steps:
(1), after fresh Flos Jasmini Sambac purchase is returned, first spreading for cooling, at the indoor flower-growing 1 ~ 2 hour of 28 ~ 38 DEG C, grows flower to the flowers are in blossom and becomes Unguis Tigris sample, be namely put on the flower stand of fragrance of a flower adsorbent equipment of sealing;
(2) open the air exhauster of fragrance of a flower adsorbent equipment, Flos Jasmini Sambac is told fragrant fragrance and deliver to the adsorption tower that hard active fruit shell carbon or modified starch are housed, allow polymeric sorbent saturated adsorption Flos Jasmini Sambac fragrance;
(3) parts by weight 30 modified starch, 20 fatty acid esters, 30 glycerol are mixed and heated to 50 ~ 100 DEG C to stir and become a kind of immiscible material;
(4), after immiscible material being cooled to 35 ~ 45 DEG C, adding the polymeric sorbent mix homogeneously that parts by weight 12 have adsorbed the fragrance of a flower, be then cooled to room temperature rapidly, be pressed into cream lamellar with tablet machine, be then packaged into scented tea with diaphragm seal;
(5) wire up with the scented tea of automatic packaging machine by good seal, thus obtain jasmine solid aromatic.
Described Flos Jasmini Sambac be Flos Jasmini Sambac with have tell Xiang Gong can flower combine, as wherein any one or more the combination of Flos Jasmini Sambac and Flos Osmanthi Fragrantis, Magnolia denudata Desr., yesterday fragrant flower, white orchid, Caulis seu folium chloranthi spicati (Chloranthus spicatus(Thunb.) Mak.), turtle turtle, Fructus Citri grandis, Fructus Gardeniae, tree orchid, Flos Rosae Rugosae.
Described polymeric sorbent is hard active fruit shell carbon, modified starch, chitosan, modified lignin resin class or have the macromolecule resin of absorption property.
When described solid aromatic uses, after taking the sealing film packaging of solid aromatic apart, be placed on the place of ventilation or be directly placed in container or vessel.
Embodiment 2
A kind of preparation method of jasmine solid aromatic of pure natural, utilize Flos Jasmini Sambac to grow flower and tell fragrant principle, the fragrance of a flower is absorbed with polymeric sorbent, be pressed into lamellar after mixing homogeneously with modified starch, fatty acid ester, glycerol and the polymeric sorbent after enfleuraging again, then pack and become a kind of solid aromatic;
Described preparation method comprises the following steps:
(1), after fresh Flos Jasmini Sambac purchase is returned, first spreading for cooling, at the indoor flower-growing 1 ~ 2 hour of 28 ~ 38 DEG C, grows flower to the flowers are in blossom and becomes Unguis Tigris sample, be namely put on the flower stand of fragrance of a flower adsorbent equipment of sealing;
(2) open the air exhauster of fragrance of a flower adsorbent equipment, Flos Jasmini Sambac is told fragrant fragrance and deliver to the adsorption tower that chitosan or modified lignin resin family macromolecule adsorbent are housed, allow polymeric sorbent saturated adsorption Flos Jasmini Sambac fragrance;
(3) parts by weight 55 modified starch, 30 fatty acid esters, 45 glycerol are mixed and heated to 50 ~ 100 DEG C to stir and become a kind of immiscible material;
(4), after immiscible material being cooled to 35 ~ 45 DEG C, adding the adsorbent mix homogeneously that parts by weight 42 have adsorbed the fragrance of a flower, be then cooled to room temperature rapidly, be pressed into cream lamellar with tablet machine, be then packaged into scented tea with diaphragm seal;
(5) wire up with the scented tea of automatic packaging machine by good seal, thus obtain jasmine solid aromatic.
Described Flos Jasmini Sambac be Flos Jasmini Sambac with have tell Xiang Gong can flower combine, as wherein any one or more the combination of Flos Jasmini Sambac and Flos Osmanthi Fragrantis, Magnolia denudata Desr., yesterday fragrant flower, white orchid, Caulis seu folium chloranthi spicati (Chloranthus spicatus(Thunb.) Mak.), turtle turtle, Fructus Citri grandis, Fructus Gardeniae, tree orchid, Flos Rosae Rugosae.
Described polymeric sorbent is hard active fruit shell carbon, modified starch, chitosan, modified lignin resin class or have the macromolecule resin of absorption property.
When described solid aromatic uses, after taking the sealing film packaging of solid aromatic apart, be placed on the place of ventilation or be directly placed in container or vessel.
Embodiment 3
A kind of preparation method of jasmine solid aromatic of pure natural, utilize Flos Jasmini Sambac to grow flower and tell fragrant principle, the fragrance of a flower is absorbed with polymeric sorbent, be pressed into lamellar after mixing homogeneously with modified starch, fatty acid ester, glycerol and the polymeric sorbent after enfleuraging again, then pack and become a kind of solid aromatic;
Described preparation method comprises the following steps:
(1), after fresh Flos Jasmini Sambac purchase is returned, first spreading for cooling, at the indoor flower-growing 1 ~ 2 hour of 28 ~ 38 DEG C, grows flower to the flowers are in blossom and becomes Unguis Tigris sample, be namely put on the flower stand of fragrance of a flower adsorbent equipment of sealing;
(2) open the air exhauster of fragrance of a flower adsorbent equipment, Flos Jasmini Sambac is told fragrant fragrance and deliver to the adsorption tower that polymeric sorbent is housed, allow polymeric sorbent saturated adsorption Flos Jasmini Sambac fragrance;
(3) parts by weight 80 modified starch, 40 fatty acid esters, 60 glycerol are mixed and heated to 50 ~ 100 DEG C to stir and become a kind of immiscible material;
(4), after immiscible material being cooled to 35 ~ 45 DEG C, adding the polymeric sorbent mix homogeneously that parts by weight 72 have adsorbed the fragrance of a flower, be then cooled to room temperature rapidly, be pressed into cream lamellar with tablet machine, be then packaged into scented tea with diaphragm seal;
(5) wire up with the scented tea of automatic packaging machine by good seal, thus obtain jasmine solid aromatic.
Described Flos Jasmini Sambac be Flos Jasmini Sambac with have tell Xiang Gong can flower combine, as wherein any one or more the combination of Flos Jasmini Sambac and Flos Osmanthi Fragrantis, Magnolia denudata Desr., yesterday fragrant flower, white orchid, Caulis seu folium chloranthi spicati (Chloranthus spicatus(Thunb.) Mak.), turtle turtle, Fructus Citri grandis, Fructus Gardeniae, tree orchid, Flos Rosae Rugosae.
Described polymeric sorbent is hard active fruit shell carbon, modified starch, chitosan, modified lignin resin class or have the macromolecule resin of absorption property.
When described solid aromatic uses, after taking the sealing film packaging of solid aromatic apart, be placed on the place of ventilation or be directly placed in container or vessel.
Claims (3)
1. the preparation method of the jasmine solid aromatic of a pure natural, it is characterized in that, first Flos Jasmini Sambac is grown flower, open after telling perfume (or spice) and absorb the fragrance of a flower with polymeric sorbent, add again after modified starch, fatty acid ester, glycerol and the polymeric sorbent after enfleuraging are mixed homogeneously and be pressed into lamellar, then pack and obtain solid aromatic;
Described preparation method comprises the following steps:
(1) pluck fresh Flos Jasmini Sambac alabastrum, at the indoor flower-growing 1 ~ 2 hour of 28 ~ 38 DEG C, become Unguis Tigris sample to the flowers are in blossom, be namely put on the flower stand of fragrance of a flower adsorbent equipment of sealing;
(2) open the air exhauster of fragrance of a flower adsorbent equipment, Flos Jasmini Sambac is told fragrant fragrance and deliver to the adsorption tower that polymeric sorbent is housed, allow polymeric sorbent saturated adsorption Flos Jasmini Sambac fragrance;
(3) parts by weight 30 ~ 80 modified starch, 20 ~ 40 fatty acid esters, 30 ~ 60 glycerol are mixed and heated to 50 ~ 100 DEG C to stir and become a kind of immiscible material;
(4), after immiscible material being cooled to 35 ~ 45 DEG C, adding the polymeric sorbent mix homogeneously that parts by weight 12 ~ 72 have adsorbed the fragrance of a flower, be then cooled to room temperature rapidly, be pressed into cream lamellar with tablet machine, be then packaged into scented tea with diaphragm seal;
(5) pack with the scented tea of automatic packaging machine by good seal, obtain jasmine solid aromatic.
2. the preparation method of the jasmine solid aromatic of pure natural according to claim 1, it is characterized in that, described Flos Jasmini Sambac can also be Flos Jasmini Sambac with have tell Xiang Gong can flower combine, comprise wherein any one or more the combination of Flos Jasmini Sambac and Flos Osmanthi Fragrantis, Magnolia denudata, white orchid, Caulis seu folium chloranthi spicati (Chloranthus spicatus(Thunb.) Mak.), turtle turtle, Fructus Citri grandis, Fructus Gardeniae, Milan and Flos Rosae Rugosae.
3. the preparation method of the jasmine solid aromatic of pure natural according to claim 1, it is characterized in that, described polymeric sorbent is the activated carbon modified starch of xylocarp shell, chitosan, modified lignin resin class or the macromolecule resin with absorption property.
Priority Applications (1)
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN105567429A (en) * | 2015-12-22 | 2016-05-11 | 大闽食品（漳州）有限公司 | Method for extracting osmanthus fragrans fragrance substance in absent of solvent |
| CN107041446A (en) * | 2017-01-09 | 2017-08-15 | 南宁市化工研究设计院 | It is a kind of to improve the method that jasmine fresh flower tells fragrant amount |
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| CN102264352A (en) * | 2008-11-14 | 2011-11-30 | 阿彻丹尼尔斯米德兰德公司 | Organogel compositions and processes for producing |
| CN103251967A (en) * | 2013-05-28 | 2013-08-21 | 杭州透云制香有限公司 | Vehicle-mounted incense sheet and production method thereof |
| CN103525556A (en) * | 2013-09-25 | 2014-01-22 | 广西茉莉花开发投资有限公司 | Ecological flower planting method before extracting jasmine flower aroma substances |
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Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102264352A (en) * | 2008-11-14 | 2011-11-30 | 阿彻丹尼尔斯米德兰德公司 | Organogel compositions and processes for producing |
| CN103251967A (en) * | 2013-05-28 | 2013-08-21 | 杭州透云制香有限公司 | Vehicle-mounted incense sheet and production method thereof |
| CN103525556A (en) * | 2013-09-25 | 2014-01-22 | 广西茉莉花开发投资有限公司 | Ecological flower planting method before extracting jasmine flower aroma substances |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN105567429A (en) * | 2015-12-22 | 2016-05-11 | 大闽食品（漳州）有限公司 | Method for extracting osmanthus fragrans fragrance substance in absent of solvent |
| CN107041446A (en) * | 2017-01-09 | 2017-08-15 | 南宁市化工研究设计院 | It is a kind of to improve the method that jasmine fresh flower tells fragrant amount |
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