KR102195975B1 - Mist for skin and fur of companion animal, and manufacturing method of the same - Google Patents

Abstract

The present invention relates to a mist for improving companion animal hair and a method for manufacturing the same. More specifically, the present invention relates to a mist for improving companion animal hair and which obtains active components of herbal materials through a traditional herbal medicine extraction method and a distillation method, and uses the same, and a method for manufacturing the same. In order to achieve the purpose, the present invention provides the mist for improving companion animal hair containing, based on 100 parts by weight of a herbal extract, 10 to 15 parts by weight of a Matricaria chamomilla extract, 1 to 3 parts by weight of DL-panthenol, and 1 to 3 parts by weight of 1,2-hexanediol.

Description

Mist for improving companion animal hair and its manufacturing method {MIST FOR SKIN AND FUR OF COMPANION ANIMAL, AND MANUFACTURING METHOD OF THE SAME}

The present invention relates to a mist for improving companion animal hair and a method for manufacturing the same, and more particularly, a mist for improving companion animal hair using the same after obtaining the active ingredient of the herbal material through a traditional herbal medicine extraction method and distillation method, and It is about the manufacturing method.

Moisturizing and nutrition of the skin, which is the first barrier to the external environment of the living body, is very important for the health of companion animals. However, conventional mists for companion animals contain various functional ingredients such as collagen and vitamins, but most of these ingredients contain chemical synthetic substances that are rather irritating to the skin or are not sufficiently penetrated and absorbed by the pet's coat. There was.

In recent years, among the natural herbal medicinal materials, products for hair management using ingredients that can stabilize sensitive and irritating hair have been developed, but due to the large particle size of natural ingredients, there is also a limit to absorption into the hair.

Therefore, in the present invention, in order to develop a mist for companion animal skin and a method for producing the same, which can soothe and nourish the skin while minimizing skin irritation using natural ingredients, and improve the absorption of moisture and active ingredients. Arrived.

Korean Patent Application Publication No. 10-2019-0042883 A

The present invention provides a mist for companion animal skin and a method of manufacturing the same, which can improve skin absorption of moisture and functional ingredients while minimizing skin irritation while providing soothing and nourishment to the skin. It is aimed at.

In order to achieve the above object, the present invention improves companion animal hair including 10 to 15 parts by weight of chamomile flower extract, 1 to 3 parts by weight of DL-panthenol and 1 to 3 parts by weight of 1,2-hexanediol per 100 parts by weight of herbal extract Provides a dragon mist.

At this time, the herbal extract, per 1 L of purified water, licorice 15-25g, aeyeop 10-15g, upper leaf 10-15g, pine needles 10-15g, jujube 10-15g, cnidium 3-8g and Angelicae 3-8g for 24 to 48 hours The step of supporting, extracting the active ingredient by heating the supporting solution containing the medicinal material in a hot water heater at 100 to 130°C for 2 to 3 hours, and diluting by adding 2 to 4 L of purified water per 1 L of the extract from which the active ingredient was extracted. , It is preferably prepared through the step of obtaining a distillate by heating in a still.

In addition, in order to improve stability and persistence, the mist of the present invention preferably further includes 10 to 20 parts by weight of chitin nanoparticles per 100 parts by weight of the herbal extract.

On the other hand, in order to achieve the above object, the present invention is 15 to 25 g of licorice per 1 L of purified water, 10 to 15 g of aeyeop, 10 to 15 g of upper leaves, 10 to 15 g of pine, 10 to 15 g of jujube, 3 to 8 g of cnidium and 3 to 8 g of angelica Supporting step of supporting for 24 to 48 hours, extraction step of extracting active ingredients by heating the supporting liquid loaded with medicinal materials at 100 to 130°C for 2 to 3 hours in a hot water heater, 2 to 2 purified water per 1L of extract from which the active ingredient is extracted After diluting by adding 4L, a distillation step of obtaining a herbal extract in the form of a distillate by heating in a still, and 10 to 15 parts by weight of chamomile flower extract per 100 parts by weight of the herbal extract, 1 to 3 parts by weight of DL-panthenol and 1,2 -It provides a method for producing a mist for improving companion animal hair, characterized in that it comprises a mixing step of mixing 1 to 3 parts by weight of hexanediol.

At this time, in the mixing step, 10 to 20 parts by weight of chitin nanoparticles per 100 parts by weight of the herbal extract may be further mixed.

The mist for improving companion animal hair manufactured according to the present invention, unlike conventional mist for companion animals, contains natural herbal ingredients instead of chemically synthesized substances and does not irritate the skin, and the active ingredients of the herbal ingredients are extracted from traditional herbal medicines. It is obtained through a method and a distillation method, so that it is efficiently permeated and absorbed into the coat of a companion animal.

1 is a conceptual diagram showing the manufacturing sequence of herbal extracts used in the mist for improving companion animal hair of the present invention.
Figure 2 is a flow chart of the production of chitin nanoparticles used in the mist for improving companion animal hair of the present invention.
3 is an electron micrograph of chitin nanoparticles used in the mist for improving companion animal hair of the present invention.
4 is an FT-IR photograph of chitin nanoparticles used in the mist for improving companion animal hair of the present invention.

Hereinafter, the present invention will be described in detail with reference to embodiments of the present invention. These examples are only illustratively presented to illustrate the present invention in more detail, and it will be apparent to those of ordinary skill in the art that the scope of the present invention is not limited by these examples. .

In addition, unless otherwise defined, all technical and scientific terms used in the present specification have the same meaning as commonly understood by one of ordinary skill in the art to which the present invention belongs, and in case of conflict, the present specification including definitions The description of will take precedence.

The mist for improving companion animal hair of the present invention includes 10 to 15 parts by weight of chamomile flower extract, 1 to 3 parts by weight of DL-panthenol, and 1 to 3 parts by weight of 1,2-hexanediol per 100 parts by weight of herbal extract.

At this time, the herbal extract, as shown in Figure 1, per 1 L of purified water licorice 15-25g, aeyeop 10-15g, upper leaf 10-15g, pine needles 10-15g, jujube 10-15g, cnidium 3-8g and angelica 3~ Supporting 8g for 24 to 48 hours, extracting the active ingredient by heating the supporting solution loaded with the medicinal material at 100 to 130°C for 2 to 3 hours in a kettle, and purified water 2 per 1L of the extract from which the active ingredient is extracted After diluting by adding ~4L, it is characterized in that it is prepared through the step of obtaining a distillate by heating in a still, and each step will be described in detail below.

The herbal extract of the present invention is characterized by using licorice, aeyeop, upper leaf, pine, jujube, cheonggung and angelica as main ingredients.

The artemisia argyi Lev. et Vant.), mugwort (A. princeps Pamp. var. orientlis Hara) or wild mugwort (A. montana Pamp.) leaves and young stems of the Asteraceae family are dried. It has the effect of opening pores due to its warming properties.

In addition, the upper leaf is a medicinal material dried leaves of a Morus alba L. or a plant related to the genus, and the pine leaf is a leaf of a pine tree, a pine tree (Pinus densiflora Sieb. et Zucc.), and both the upper leaf and the pine leaf are It has a soothing effect on the skin.

On the other hand, the cnidium is a perennial plant of the parsley family, the umbelwort of the dicotyledonous plant Ipanhwa group, and the angelica gigas refers to the dried roots of Angelica gigas Nakai or Angelica sinensis (Oliv.) Diels. The jujube refers to the ripe fruit of the jujube tree (Zizyphus jujuba Miller var. inermis Rehder) or the boeun jujube tree (Zizyphus jujuba Miller var. hoonensis TB Lee), and the licorice is a perennial plant of the dicotyledonous plant rosewood legume, the All of the medicines have the effect of adding radiance by nourishing the skin.

As for the herbal ingredients, per 1 L of purified water, 15 to 25 g of licorice, 10 to 15 g of aeyeop, 10 to 15 g of upper leaves, 10 to 15 g of pine, 10 to 15 g of jujube, 3 to 8 g of cnidium and 3 to 8 g of angelica are preferred. If the content of these is less than this, it is difficult to sufficiently exhibit each functional effect, and if it is more than this, the functional synergistic effect compared to cost increase is insufficient.

It is preferable that the herbal ingredients are immersed in purified water for 24 to 48 hours before starting the full extraction process. While the herbal ingredients are supported, sufficient moisture penetrates into the ingredients, so that the active ingredients may be more efficiently eluted in the heat extraction process.

The supporting solution, which has undergone the supporting process, is put into a hot water heater used in the manufacture of general herbal medicine, and heated at 100-130° C. for 2 to 3 hours to extract the active ingredient. Thereafter, the extract from which the active ingredient is extracted is not used as it is, but undergoes a separate distillation process to collect components of small molecular size that are easily absorbed into the coat of the companion animal. In detail, it is preferable that it is prepared by adding 2 to 4 L of purified water per 1 L of the extract from which the active ingredient is extracted, diluting it, and then heating it in a still to obtain a distillate. In detail, the distiller is first heated to 350~450℃, and when the distillate starts to drop drop by drop in the heated distiller, the temperature is lowered to 250℃ and the distillation process continues for 8~12 hours, and finally 2~4L distillation. Get the liquid

At this time, based on 1 L of the distillate thus obtained, 10 to 100 g of calcium oxide is added and stirred, and then allowed to stand at 5 to 15° C. for 12 to 24 hours to further undergo a step of filtering the supernatant. Such calcium oxide treatment is effective in improving the antibacterial activity of the distillate and removing odors.

The herbal extract obtained by the above-described distillation process is finally 10 to 15 parts by weight of chamomile flower extract, 1 to 3 parts by weight of DL-panthenol, and 1 to 3 parts by weight of 1,2-hexanediol per 100 parts by weight of the herbal extract. After mixing, it is finally put in a spray container and used.

The chamomile flower extract has excellent anti-inflammatory, antibacterial, and soothing effects, and is effective against skin troubles or inflammatory reactions. As for the chamomile flower extract, various extracts obtained by a general extraction method can be used, but preferably, the chamomile flower is heated and extracted using a natural solvent, fermented alcohol solution, and the extract obtained through the heating extraction process is distilled. It is preferable to use the one prepared through the step of obtaining an aqueous solution component.

The fermented alcoholic solution is a fluid liquid containing the main component of ethanol obtained by fermenting an aqueous solution containing starch or sugar, and the concentration of ethanol in the alcoholic solution is preferably 40 to 80%. Dried chamomile flowers and alcohol solution are mixed in a weight ratio of 1:10 to 1:100, and the active ingredient is extracted for 10 to 20 hours at a relatively low temperature of 50 to 70°C to minimize destruction of the active ingredient. It is desirable to do.

At this time, it is preferable to use alkaline ionized water as the aqueous solution so that the active ingredient can be extracted well even at a relatively low temperature. Alkaline ionized water has a smaller cluster of molecules than water, so it has good penetrating power, high heat conduction and high dissolving power, so that not only the elution of components is efficiently performed at a relatively low temperature, but also excellent absorption power.

The extract obtained using the fermented alcoholic solution is finally subjected to a distillation process to separate and use the aqueous solution component. The content of the chamomile flower extract prepared in this way is preferably 10 to 15 parts by weight per 100 parts by weight of the herbal extract, and if it is less than this, it is difficult to exert a sufficient functional effect, and if it is more than this, the content of other ingredients is lowered and the overall effect of the mist is reduced. Can be.

The DL-panthenol and 1,2-hexanediol each have a moisturizing effect and a preservative effect, and the content is preferably 1 to 3 parts by weight, respectively.

On the other hand, the purified water used to extract the oriental medicine materials of the present invention may be used as general purified water, preferably, purified water treated with water by supporting ceramic balls for 12 to 24 hours may be used. The purified water treated with the ceramic ball may not only contain an effective mineral component in the purified water, but may also have a sterilization effect through activation of water molecules.

As for the ceramic ball, various commercially available ceramic balls may be used, but preferably 30-50 wt% of illite pulverized with 300-400 mesh, 20-30 wt% of loess, and 10-30 wt% germanium are added to the purified water and mixed. Then, drying to a moisture content of 10 to 20%, adding 10 to 20 wt% of nano-crushed zeolite and 10 to 20 wt% of an oyster shell to the mixture through the drying step, and pulverizing the nano-crushed particles into the 300 to 400 mesh It is preferable to use the one prepared through the step of evenly mixing between the particles, and the step of molding the mixture to which the zeolite and the oyster shell are added into a spherical shape, and then firing the mixture at 800 to 1000° C. for 48 to 72 hours.

The ceramic ball is wet-mixed with illite, loess and germanium, which have a function of purifying water and activating water molecules, and dried so that the moisture content of the mixture becomes 10-20%, and then nano-crushed zeolite and oyster It is characterized by dry mixing by mixing the skin.

Wet mixing has the advantage of being well agglomerated, so that the difficulty of mixing can be solved, but a crack phenomenon occurs as the moisture dries in the subsequent drying process, and due to this crack, a minute crack occurs inside in the subsequent firing step. The ceramic ball used in the present invention is a mixture by first evenly mixing the pulverized material through wet mixing, and then adjusting the moisture content to 10-20% through the drying process, and then dry mixing the nano-ground zeolite and oyster shells thereto. Fine gaps between them can be evenly fused.

In the ceramic ball manufactured as described above, each component is evenly mixed and uniform pores are formed therein, so that contaminants in water are effectively decomposed and adsorbed to perform effective water treatment.

On the other hand, the mist of the present invention described above may further include 10 to 20 parts by weight of chitin nanoparticles per 100 parts by weight of the herbal extract.

Chitin is a polymer polysaccharide in which N-acetylglucosamine is bonded in the form of a long chain as shown in Formula 1 below, and is an important constituent of the hard epidermis of arthropods, the shell of mollusks, and the cell wall of fungi. Chitin is a white amorphous powder. It has poor reactivity and is less soluble in water and is more stable than cellulose, so it can withstand the decomposition of microorganisms.

Accordingly, it is actively used in the development of surgical 　 sutures, artificial skin 　, drugs 　 carriers, antihypertensive drugs, anti-hypertensive drugs 　, and medicines 　 and agricultural fields such as plant growth regulators, bio fertilizers and animal feeds. In addition, it can be used in the development of 　 products 　 such as food, health functional food, anticancer drugs, cosmetics, etc.

The mist of the present invention may further contain chitin nanoparticles having an anion on the surface, so that the chitin nanoparticles can be complexed through ionic bonding with cationic mineral components present in the mist.

By combining a cationic mineral component and anionic chitin nanoparticles on the surface, stability is improved when sprayed onto the skin than when the mineral component is independently present, and the effect can be maintained for a long time.

The chitin nanoparticles may be nanoparticles prepared by various methods, but in the present invention, as shown in FIG. 2, i) 0.5 to 1.5 g of chitin per 100 mL of distilled water, TEMPO (2,2,6,6-tetramethyl -1-piperidine oxoammonium) 0.01 ~ 0.1g, sodium bromide 0.1 ~ 1g added to the first mixing for 1 ~ 3 hours at 200 ~ 300rpm; ii) adding 5 mmol of sodium hypochlorite and then secondary mixing at 200 to 300 rpm for 1 to 3 hours; iii) adding sodium hydroxide to maintain the pH at 10-11; iv) neutralizing to pH 7 by adding hydrogen chloride; And v) centrifuging at 6500 to 7500 rpm for 20 to 30 minutes and then freeze drying for 3 to 5 days; can be prepared through.

Looking closely, first, for chitin oxidation, 0.5 to 1.5 g of chitin per 100 mL of distilled water, 0.01 to 0.1 g of TEMPO (2,2,6,6-tetramethyl-1-piperidine oxoammonium), and 0.1 to 1 g of sodium bromide are added. , Mix for 1 to 3 hours at 200 to 300 rpm. After adding 5 mmol of sodium hypochlorite again, the mixture is secondarily mixed at 200 to 300 rpm for 1 to 3 hours. 0.5M sodium hydroxide is added to maintain the pH at 10 to 11, preferably at pH 10.21, and then 0.5M hydrogen chloride is added again to neutralize the pH to 7. The neutralized chitin particles are centrifuged for 20 to 30 minutes at 6500 to 7500 rpm, preferably at 7000 rpm. At this time, after washing the centrifuged nanoparticles with water, the process of centrifuging may be repeated 2 to 3 more times. The centrifuged nanoparticles are freeze-dried for 3 to 5 days to finally obtain chitin nanoparticles.

3 is an electron micrograph of the chitin nanoparticles of the present invention, it can be seen that the size of the chitin particles prepared according to the present invention is formed at about 100 ~ 130 nm. 4 is an FT-IR photograph of the chitin nanoparticles of the present invention, showing that the degree of N-acetylation can be changed according to the second mixing time (1.5hr, 3hr).

Hereinafter, the configuration of the present invention and effects thereof will be described in more detail through specific manufacturing examples and examples. However, the present examples are for explaining the present invention more specifically, and the scope of the present invention is not limited to these examples.

[Examples and Comparative Examples]

Example 1

After sorting and weighing each 25g of aeyeop, upper leaf, pine, jujube, 10g each of cheonggung, angelica and 40g of licorice, the measured medicinal material was immersed in 2L of purified water for a day. Thereafter, 2080cc of the drug was extracted for 2 hours and 30 minutes with a hot water heater.

After adding 6020 cc of purified water to 2080 cc of the extracted drug, it was heated to 400° C. in a still. When the distillate began to drop drop by drop in the heated distiller, the temperature was lowered to 250° C., and the distillation was continued for 10 hours to obtain a transparent herbal extract of 6020 cc.

Then, the obtained herbal extract and the remaining ingredients were mixed in the content ratio shown in Table 1 to prepare a mist for improving companion animal hair.

Example 2

After obtaining the herbal extract in the same manner as in Example 1, the obtained herbal extract and the remaining ingredients were mixed in the content ratio shown in Table 1 to prepare a mist for improving companion animal hair.

Comparative Example 1

After sorting and weighing each 25g of aeyeop, upper leaf, pine, jujube, 10g each of cheonggung, angelica and 40g of licorice, the measured medicinal material was immersed in 2L of purified water for a day. Then, 2080cc of the drug was extracted for 2 hours and 30 minutes by using a bath electric kettle.

The obtained herbal extract was mixed in the content ratio of Table 1 to prepare a mist for improving companion animal hair.

ingredient Example 1 (w%) Example 2 (w%) Comparative Example 1 (w%) Herbal extract Extraction + Distillation 88 80 - Extract only - - 88 Chamomile flower extract 10 10 10 DL-panthenol One 1.5 One 1,2-hexanediol One 1.5 One Chitin nanoparticles - 12 -

[Experimental example: sensory test]

30 pet dogs were used for each of Examples 1 to 2 and Comparative Example 1 for a week (a total of 3 weeks), and then the improvement of the pet's coat was evaluated, and the results are shown in Table 2 below.

The evaluation was calculated using the general 5-point rating method, and the scores were divided into [5 points (very excellent), 4 points (excellent), 3 points (normal), 2 points (insufficient), 1 point (very insufficient)]. Example 2 received the best evaluation.

Example 1 Example 2 Comparative Example 1 Color 4.5 4.3 2.0 smell 4.2 4.0 2.2 burnish 4.2 4.5 2.5 Persistence 4.0 4.8 3.5

As mentioned above, the present invention has been described in connection with a preferred embodiment, but the technical idea of the invention is not limited thereto or is not limited thereto, and may be modified and variously implemented by those skilled in the art.

Claims (5)

delete delete delete A supporting step of supporting 15 to 25 g of licorice, 10 to 15 g of aeyeop, 10 to 15 g of upper leaves, 10 to 15 g of pine leaves, 10 to 15 g of jujube, 3 to 8 g of cnidium, and 3 to 8 g of angelica for 24 to 48 hours per 1 L of purified water;
An extraction step of extracting the active ingredient by heating the supporting liquid on which the medicinal material is supported at 100 to 130° C. for 2 to 3 hours in a hot water heater;
A distillation step of diluting by adding 2 to 4 L of purified water per 1 L of the extract from which the active ingredient is extracted, and then heating in a still to obtain a herbal extract in the form of a distillate;
After stirring by adding 10 to 100 g of calcium oxide based on 1 L of the herbal extract, filtering the supernatant by allowing it to stand at 5 to 15° C. for 12 to 24 hours; And
Mixing 10 to 15 parts by weight of chamomile flower extract, 1 to 3 parts by weight of DL-panthenol, 1 to 3 parts by weight of 1,2-hexanediol and 10 to 20 parts by weight of chitin nanoparticles per 100 parts by weight of the filtered herbal extract Including; mixing step;
The chamomile extract,
Heating and extracting the dried chamomile flowers using a fermented alcohol solution obtained by fermenting an aqueous solution containing starch or sugar; And distilling the extract obtained through the heat extraction step to obtain an aqueous solution component,
In the heating extraction step, the concentration of ethanol in the fermented alcohol solution is 40 to 80%, the dried chamomile flowers and the fermented alcohol solution are mixed at a weight ratio of 1:10 to 1:100, and the heat extraction is performed at 50 to 70°C. A method for producing a mist for improving companion animal hair, characterized in that made at a temperature for 10 to 20 hours. delete

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