CN111067847A - Reverse-aging spray preparation with skin brightening and anti-wrinkle effects and preparation method thereof - Google Patents

Abstract

The invention discloses a reverse spray preparation with skin brightening and anti-wrinkle effects and a preparation method thereof, and the reverse spray preparation comprises the following raw materials in parts by weight: the skin care product comprises acetyl hexapeptide-8, tocopherol acetate, fullerene, trehalose, sodium hyaluronate, anise extract, glycyrrhiza glabra extract, hydrolyzed collagen, rutin extract, natural plant essence extract, butanediol, glycerol, a film forming agent, a humectant, an antioxidant and deionized water. The retro spray preparation with the skin brightening and anti-wrinkle effects and the preparation method thereof can immediately weaken wrinkles by inhibiting the contraction of expression muscles, achieve the purpose of filling up the loss of skin collagen by supplementing collagen, improve dry lines and fine lines of skin caused by water shortage, delay skin aging, greatly enhance the effects of anti-wrinkle skin brightening skin care products, improve skin oil secretion and regulate skin water-oil balance.

Description

Reverse-aging spray preparation with skin brightening and anti-wrinkle effects and preparation method thereof

Technical Field

The invention relates to the technical field of skin care products, in particular to a reversible spray preparation with skin brightening and anti-wrinkle effects and a preparation method thereof.

Background

The skin wrinkles are formed by reducing elastic fibers for maintaining normal tension of the skin, weakening secretion of sebaceous glands and reducing subcutaneous fat, so that the skin and deep tissues thereof are excessively relaxed and folded, facial wrinkles are particularly common, metabolism of the body is weakened along with the increase of age, aging wrinkles are gradually formed, the forehead generally appears earliest, then fishtail lines of eyes and smiling lines of cheeks, in addition, as muscles usually do the same reciprocating motion, marks are left on sunken parts between skin wrinkles, and extruded wrinkles can be formed for a long time, the wrinkles are divided into dynamic expression wrinkles and real wrinkles, and the dynamic expression wrinkles are wrinkles of surface skin caused by contraction and traction of expression muscles when the face has expressions, such as: eyebrow lines, head-up lines, fishtail lines, etc. The appearance of facial wrinkles in humans, besides the cause of natural aging, is more important to the excessive contraction of the expression muscles, and the true wrinkles are mainly due to the lack of collagen and elastin in the skin, and the collapse of the structure leads to the skin being loose, gradually drooping, and partially laminated, such as: upper eyelid sagging, lower eyelid lines, nasolabial folds, buccal wrinkles, neck wrinkles, and the like.

The existing anti-wrinkle skin-brightening skin care product has poor effect, cannot immediately fade wrinkles by inhibiting the contraction of expression muscles, cannot achieve the aim of filling up the loss of skin collagen by supplementing collagen, cannot improve dry lines and fine lines of skin caused by water shortage to delay skin aging, and thus brings great inconvenience to skin care of people.

Disclosure of Invention

Technical problem to be solved

Aiming at the defects of the prior art, the invention provides a retro spray preparation with skin brightening and anti-wrinkle effects and a preparation method thereof, and solves the problems that the anti-wrinkle skin brightening skin care product of the prior skin care product has poor effect, cannot immediately fade wrinkles by inhibiting the contraction of expression muscles, cannot fulfill the aim of filling up the loss of collagen of skin by supplementing collagen, cannot improve dry lines and fine lines of the skin caused by water shortage, and delay skin aging.

(II) technical scheme

In order to achieve the purpose, the invention is realized by the following technical scheme: a retro spray preparation with skin brightening and wrinkle resisting effects comprises the following raw materials in parts by weight: the anti-bacterial skin care lotion comprises, by weight, acetyl hexapeptide-83-5 parts, tocopherol acetate 3-5 parts, fullerene 3-5 parts, trehalose 3-5 parts, sodium hyaluronate 1-3 parts, anise extract 3-5 parts, glycyrrhiza glabra extract 3-5 parts, hydrolyzed collagen 3-5 parts, rutin extract 1-3 parts, natural plant extract 15-20 parts, butanediol 1-3 parts, glycerol 1-3 parts, a film forming agent 1-2 parts, a humectant 1-2 parts, an antioxidant 1-2 parts and the balance of deionized water.

Preferably, the humectant is composed of chlorella extract, urea, hydrolyzed rice extract, trehalose and phospholipids.

Preferably, the antioxidant is composed of raw umbellate, corn kernel extract, wild soybean protein, kelp extract and pea extract.

Preferably, the natural plant essence extract is composed of mango seed fat, date extract, cucumber fruit extract, wheat germ extract, phyllostachys pubescens extract and palm leaf tree extract.

Preferably, the film forming agent is composed of glycerol polymethacrylate, sodium polyacrylate grafted starch, polydimethylsiloxane and polysiloxane-11.

The invention also discloses a preparation method of the reverse-aged spray preparation with the skin brightening and anti-wrinkle effects, which specifically comprises the following steps:

s1, selecting and weighing raw materials: firstly, respectively measuring acetyl hexapeptide-8, tocopherol acetate, fullerene, trehalose, sodium hyaluronate, anise extract, glycyrrhiza glabra extract, hydrolyzed collagen, rutin extract, natural plant essence extract, butanediol, glycerol, a film forming agent, a humectant, an antioxidant and deionized water in required weight ratio by using weighing equipment;

s2, premixing of base materials: sequentially pouring acetyl hexapeptide-8, tocopherol acetate, fullerene, trehalose, sodium hyaluronate, a hypsizygus marmoreus extract, a glycyrrhiza glabra extract, hydrolyzed collagen, a rutin extract and a natural plant essence extract which are measured in the step S1 into mixing and stirring equipment, then adding deionized water in corresponding weight proportion, starting a stirring mechanism, and stirring for 30-40min at the rotation speed of 300-400r/min and the temperature of 26-33 ℃ to prepare a base material;

s3, preparation of an efficacy primary mixing agent: respectively pouring the butanediol, the glycerol, the humectant and the antioxidant weighed in the step S1 into the base material obtained in the step S2, and stirring at the rotating speed of 400-600r/min for 20-30min to fully mix the effective components of the humectant and the antioxidant with the base material, thereby obtaining an effective primary mixing agent;

s4, preparation of the retrogradation spray preparation: adding the film forming agent measured in the step S1 into the efficacy initial mixing agent prepared in the step S3, and stirring for 1-2 hours at the rotating speed of 700-900r/min to enable the mixed solution to be a viscous transparent liquid, thereby completing the preparation of the inverse aged spraying preparation;

s5, filling and packaging the preparation: and (4) filling the retrogradation spray preparation prepared in the step (S4) into spray container bottles by filling equipment, wherein each bottle can contain 5-6mL of the retrogradation spray preparation, then carrying out quality detection, and packaging for sale or warehousing for storage after the detection is qualified.

Acetyl hexapeptide-8 is hexapeptide, is a neurotransmitter inhibitory peptide, has high anti-wrinkle activity and small side effect, is one of the most effective components for inhibiting expression lines, can locally block nerve transmission muscle contraction information, influences skin sac nerve conduction, relaxes facial muscles, smoothes dynamic lines, static lines and fine lines, effectively reorganizes collagen elasticity, can increase the activity of elastin, relaxes facial lines, smoothes wrinkles and improves relaxation, and is a wrinkle inhibitory raw material in the world.

The fullerene has small molecular weight of only 0.7 nm, can be quickly absorbed and utilized by human skin tissues, and the fibroblast in the dermis layer of the skin has the function of synthesizing collagen.

The glycyrrhiza glabra extract has excellent effects of resisting inflammation, oxidation and melanin formation, preventing skin tissue roughness, resisting inflammation and resisting bacteria, is a whitening component with good curative effect and comprehensive functions at present, can repair the damage of free radicals and ultraviolet rays to skin, help the skin to restore pigment at night, prevent skin relaxation and make the skin tender, white! Clinical results show that the skin care product can effectively neutralize free radicals, improve skin lines and restore damaged skin, is compact and elastic, can inhibit the neuraminidase and restore melanin, can lighten formed spots and inhibit the formation of melanin.

The hydrolyzed collagen is obtained by hydrolyzing collagen with protease at a higher temperature, and under the double actions of temperature and enzyme, the hydrolyzed collagen has smaller relative molecular weight and molecular weight of 2KD, contains abundant amino acids and hydrophilic groups in molecules, can permeate into skin, quickly supplements lost collagen, accelerates the repair of skin, promotes the proliferation of dermal fibroblasts, improves the cell activity, provides raw materials for the fibroblasts to synthesize collagen, stimulates cells to synthesize more collagen, hyaluronic acid and the like, enables the damaged and aged skin to be filled, repaired and rebuilt a reticular structure, maintains the skin tension and keeps the skin elasticity.

The rutin can be used as an edible antioxidant, a nutrition enhancer and the like, has unique effects on skin aging caused by various factors, has good free radical resisting effect on the skin, is used as a natural sunscreen agent, is added with 10 percent of rutin, has obvious effect of eliminating active oxygen free radicals of cells when the absorption rate of ultraviolet reaches 98 percent, has vitamin P-like effect and anti-inflammatory effect, can reduce inflammation caused by mustard oil to eyes or skin, has antiviral effect, has the maximum inhibiting effect on vesicular stomatitis virus and strong antioxidant property when the concentration is 200 mu g/ml, can inhibit the formation of lipid peroxide by adding the rutin into lysosome-rich homogenate, can strongly absorb the ultraviolet ray at 280 nm, can be used in sunscreen whitening type cosmetic.

(III) advantageous effects

The invention provides a reverse-aged spray preparation with skin brightening and anti-wrinkle effects and a preparation method thereof. Compared with the prior art, the method has the following beneficial effects:

(1) the spray preparation has the effects of brightening skin and resisting wrinkles, can immediately fade wrinkles by inhibiting contraction of expression muscles, achieves the aim of filling up loss of collagen of skin by supplementing collagen, well improves dry lines and fine lines of skin caused by water shortage, delays skin aging, greatly enhances the effects of anti-wrinkle brightening skin care products, supplements skin collagen by adding hydrolyzed collagen and hexapeptide-8 into the skin care products, resists skin relaxation, enables the skin to be more elastic and compact, regulates the balance of a skin lipid membrane, enhances the immunity of the skin, relieves the skin sensitivity conditions of dryness, itching, redness and the like of the skin caused by seasonal weather dryness, improves abnormal cornification of a sebaceous orifice caused by skin tissue aging atrophy caused by water shortage, improves the secretion of skin oil, regulates the water and oil balance of the skin, thereby greatly facilitating the skin care of people.

(2) The prepared retrogradation spray preparation supplements moisture required by skin, maintains normal metabolism of the skin, improves pigments, color spots and the like of the skin due to water shortage, improves the skin dark yellow by polypeptide, lightens the skin, nourishes and softens cutin, improves dry and rough skin, optimizes an intercellular supporting structure, forms a layer of breathable hydrated viscoelastic membrane on the skin through macromolecular collagen, keeps the surface of the skin smooth, is rich in 3000 daltons of small molecular collagen, is suitable for the absorption limit of pores of the skin of a human body, and has high nutrition, high permeability and easy absorption.

Drawings

FIG. 1 is a flow chart of the preparation method of the present invention.

Detailed Description

The technical solutions in the embodiments of the present invention will be clearly and completely described below with reference to the drawings in the embodiments of the present invention, and it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all of the embodiments. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.

Referring to fig. 1, the embodiment of the present invention provides three technical solutions: a preparation method of a reversible spray preparation with skin brightening and anti-wrinkle effects specifically comprises the following steps:

example 1

S1, selecting and weighing raw materials: firstly, respectively measuring 4 parts of acetyl hexapeptide-8, 4 parts of tocopheryl acetate, 4 parts of fullerene, 4 parts of trehalose, 2 parts of sodium hyaluronate, 4 parts of anise extract, 4 parts of glycyrrhiza glabra extract, 4 parts of hydrolyzed collagen, 2 parts of rutin extract, 17 parts of natural plant essence extract, 2 parts of butanediol, 2 parts of glycerol, 1.5 parts of film forming agent, 1.5 parts of humectant, 1.5 parts of antioxidant and the balance of deionized water by using weighing equipment, wherein the humectant consists of chlorella extract, urea, hydrolyzed rice extract, trehalose and phospholipid, the antioxidant consists of raw ointment phenol acetate, corn kernel extract, wild soybean protein, kelp extract and pea extract, and the natural plant essence extract consists of mango butter, date extract, cucumber fruit extract, wheat germ extract, phyllostachys extract and palm leaf tree extract, the film forming agent consists of glycerol polymethacrylate, sodium polyacrylate grafted starch, polydimethylsiloxane and polysiloxane-11;

s2, premixing of base materials: sequentially pouring acetyl hexapeptide-8, tocopherol acetate, fullerene, trehalose, sodium hyaluronate, a hypsizygus marmoreus extract, a glycyrrhiza glabra extract, hydrolyzed collagen, a rutin extract and a natural plant essence extract which are measured in the step S1 into mixing and stirring equipment, adding deionized water in corresponding weight parts, starting a stirring mechanism, and stirring for 35min at the rotating speed of 350r/min and the temperature of 30 ℃ to prepare a base material;

s3, preparation of an efficacy primary mixing agent: respectively pouring the butanediol, the glycerol, the humectant and the antioxidant weighed in the step S1 into the base material obtained in the step S2, and stirring at the rotating speed of 500r/min for 25min to fully mix the effective components of the humectant and the antioxidant with the base material, thereby obtaining an effective primary mixing agent;

s4, preparation of the retrogradation spray preparation: adding the film forming agent measured in the step S1 into the efficacy initial mixing agent prepared in the step S3, and stirring at the rotating speed of 800r/min for 1.5 hours to enable the mixed solution to be a viscous transparent liquid, thereby completing the preparation of the inverse aged spraying preparation;

s5, filling and packaging the preparation: and (4) filling the retrogradation spray preparation prepared in the step (S4) into spray container bottles by filling equipment, wherein each bottle can contain 5.5mL of the retrogradation spray preparation, then carrying out quality detection, and packaging for sale or warehousing for storage after the detection is qualified.

Example 2

S1, selecting and weighing raw materials: firstly, respectively measuring 3 parts of acetyl hexapeptide-8, 3 parts of tocopheryl acetate, 3 parts of fullerene, 3 parts of trehalose, 1 part of sodium hyaluronate, 3 parts of anise extract, 3 parts of glycyrrhiza glabra extract, 3 parts of hydrolyzed collagen, 1 part of rutin extract, 15 parts of natural plant essence extract, 1 part of butanediol, 1 part of glycerol, 1 part of film forming agent, 1 part of humectant, 1 part of antioxidant and the balance of deionized water by a weighing device, wherein the humectant consists of chlorella extract, urea, hydrolyzed rice extract, trehalose and phospholipid, the antioxidant consists of raw ointment phenolic acetate, corn kernel extract, wild soybean protein, kelp extract and pea extract, the natural plant essence extract consists of mango seed fat, date extract, cucumber fruit extract, wheat germ extract, phyllostachys extract and palm leaf tree extract, the film forming agent consists of glycerol polymethacrylate, sodium polyacrylate grafted starch, polydimethylsiloxane and polysiloxane-11;

s2, premixing of base materials: sequentially pouring acetyl hexapeptide-8, tocopherol acetate, fullerene, trehalose, sodium hyaluronate, a hypsizygus marmoreus extract, a glycyrrhiza glabra extract, hydrolyzed collagen, a rutin extract and a natural plant essence extract which are measured in the step S1 into mixing and stirring equipment, adding deionized water in corresponding weight parts, starting a stirring mechanism, and stirring for 30min at the rotating speed of 300r/min and the temperature of 26 ℃ to prepare a base material;

s3, preparation of an efficacy primary mixing agent: respectively pouring the butanediol, the glycerol, the humectant and the antioxidant weighed in the step S1 into the base material obtained in the step S2, and stirring at the rotating speed of 400r/min for 20min to fully mix the effective components of the humectant and the antioxidant with the base material, thereby obtaining an effective primary mixing agent;

s4, preparation of the retrogradation spray preparation: adding the film forming agent measured in the step S1 into the efficacy initial mixing agent prepared in the step S3, and stirring at the rotating speed of 700r/min for 1h to enable the mixed solution to be a viscous transparent liquid, thereby completing the preparation of the inverse aged spraying preparation;

s5, filling and packaging the preparation: and (4) filling the retrogradation spray preparation prepared in the step (S4) into spray container bottles by filling equipment, wherein each bottle can contain 5mL of the retrogradation spray preparation, then carrying out quality detection, and packaging for sale or warehousing for storage after the detection is qualified.

Example 3

S1, selecting and weighing raw materials: firstly, respectively measuring 5 parts of acetyl hexapeptide-8, 5 parts of tocopherol acetate, 5 parts of fullerene, 5 parts of trehalose, 3 parts of sodium hyaluronate, 5 parts of anise extract, 5 parts of glycyrrhiza glabra extract, 5 parts of hydrolyzed collagen, 3 parts of rutin extract, 20 parts of natural plant essence extract, 3 parts of butanediol, 3 parts of glycerol, 2 parts of film forming agent, 2 parts of humectant, 2 parts of antioxidant and the balance of deionized water by a weighing device, wherein the humectant consists of chlorella extract, urea, hydrolyzed rice extract, trehalose and phospholipid, the antioxidant consists of gypsum phenol acetate, corn kernel extract, wild soybean protein, kelp extract and pea extract, the natural plant essence extract consists of mango seed fat, date extract, cucumber fruit extract, wheat germ extract, phyllanthus extract and phyllanthus extract, the film forming agent consists of glycerol polymethacrylate, sodium polyacrylate grafted starch, polydimethylsiloxane and polysiloxane-11;

s2, premixing of base materials: sequentially pouring acetyl hexapeptide-8, tocopherol acetate, fullerene, trehalose, sodium hyaluronate, a hypsizygus marmoreus extract, a glycyrrhiza glabra extract, hydrolyzed collagen, a rutin extract and a natural plant essence extract which are measured in the step S1 into mixing and stirring equipment, adding deionized water in corresponding weight parts, starting a stirring mechanism, and stirring for 40min at the rotation speed of 400r/min and the temperature of 33 ℃ to prepare a base material;

s3, preparation of an efficacy primary mixing agent: respectively pouring the butanediol, the glycerol, the humectant and the antioxidant weighed in the step S1 into the base material obtained in the step S2, and stirring at the rotating speed of 600r/min for 30min to fully mix the effective components of the humectant and the antioxidant with the base material, thereby obtaining an effective primary mixing agent;

s4, preparation of the retrogradation spray preparation: adding the film forming agent measured in the step S1 into the efficacy initial mixing agent prepared in the step S3, and stirring for 2 hours at the rotating speed of 900r/min to emulsify the mixed solution into a viscous transparent liquid, thereby completing the preparation of the inverse aged spraying preparation;

s5, filling and packaging the preparation: and (4) filling the retrogradation spray preparation prepared in the step (S4) into spray container bottles by filling equipment, wherein each bottle can contain 6mL of the retrogradation spray preparation, then carrying out quality detection, and packaging for sale or warehousing for storage after the detection is qualified.

Application case

After the reverse-age spray preparation prepared by the embodiment of the invention is used, the wrinkles are removed, and the skin returns to a compact state after being continuously used for 2-3 courses, so that the skin is plump, bright and glossy.

The wrinkles of 55 years old face and neck of the woman are obviously reduced, and the skin is restored to be compact after the spray preparation for the inverse age is continuously used for 4-5 courses, so that the skin is plump, bright and glossy.

Aged women, 37 years old, have expression muscle contraction after the eyes of face have fishtail line, after using the spray preparation of inverse age prepared in this invention embodiment, the wrinkle is obviously subsided, the skin resumes the tight state after using a course of treatment continuously, the skin is plump, bright and shiny, there is no wrinkle to appear.

To sum up the above

The invention can immediately fade wrinkles by inhibiting the contraction of expression muscles, achieves the aim of filling up the loss of skin collagen by supplementing collagen, well realizes the improvement of dry lines and fine lines of skin caused by water shortage, delays skin aging, greatly enhances the effects of anti-wrinkle skin-brightening skin care products, supplements skin collagen by adding hydrolyzed collagen and hexapeptide-8 into the skin care products, resists skin relaxation, enables the skin to be more elastic and compact, regulates the balance of a skin lipid membrane, enhances the immunity of the skin, relieves the seasonal weather dryness, causes the skin to be dry, itchy, reddish and other skin sensitive conditions, improves the abnormal cornification of the mouth of a sebaceous gland caused by the aging atrophy of skin tissues caused by water shortage of the skin, improves the secretion of skin oil, regulates the water and oil balance of the skin, greatly facilitates the skin care of people, and can supplement the water required by the skin, the skin moisturizing spray has the advantages that normal metabolism of the skin is maintained, pigments, color spots and the like of the skin due to water shortage are improved, the skin is dark yellow and bright, simultaneously, the skin is nourished and softened, dryness and roughness of the skin are improved, an intercellular support structure is optimized, a breathable hydrated viscoelastic film is formed on the skin through macromolecular collagen, the surface of the skin is kept smooth, the reverse-aged spray is rich in 3000 daltons of the micromolecular collagen, and the reverse-aged spray is suitable for the absorption limit of human skin pores, high in nutrition, high in permeability and easy to absorb.

It is noted that, herein, relational terms such as first and second, and the like may be used solely to distinguish one entity or action from another entity or action without necessarily requiring or implying any actual such relationship or order between such entities or actions. Also, the terms "comprises," "comprising," or any other variation thereof, are intended to cover a non-exclusive inclusion, such that a process, method, article, or apparatus that comprises a list of elements does not include only those elements but may include other elements not expressly listed or inherent to such process, method, article, or apparatus.

Although embodiments of the present invention have been shown and described, it will be appreciated by those skilled in the art that changes, modifications, substitutions and alterations can be made in these embodiments without departing from the principles and spirit of the invention, the scope of which is defined in the appended claims and their equivalents.

Claims (6)

1. The inverse aged spray with the effects of brightening skin and resisting wrinkles is characterized in that: the raw materials comprise the following components in parts by weight: the anti-bacterial skin care lotion comprises, by weight, acetyl hexapeptide-83-5 parts, tocopherol acetate 3-5 parts, fullerene 3-5 parts, trehalose 3-5 parts, sodium hyaluronate 1-3 parts, anise extract 3-5 parts, glycyrrhiza glabra extract 3-5 parts, hydrolyzed collagen 3-5 parts, rutin extract 1-3 parts, natural plant extract 15-20 parts, butanediol 1-3 parts, glycerol 1-3 parts, a film forming agent 1-2 parts, a humectant 1-2 parts, an antioxidant 1-2 parts and the balance of deionized water.

2. The inverse-aged spray formulation with skin-lightening and anti-wrinkle effects according to claim 1, characterized in that: the humectant consists of chlorella extract, urea, hydrolyzed rice extract, trehalose and phospholipids.

3. The inverse-aged spray formulation with skin-lightening and anti-wrinkle effects according to claim 1, characterized in that: the antioxidant comprises raw paste phenolic acetate, corn kernel extract, wild soybean protein, kelp extract and pea extract.

4. The inverse-aged spray formulation with skin-lightening and anti-wrinkle effects according to claim 1, characterized in that: the natural plant essence extract is composed of mango seed fat, date extract, cucumber extract, wheat germ extract, phyllostachys pubescens extract and palm leaf tree extract.

5. The inverse-aged spray formulation with skin-lightening and anti-wrinkle effects according to claim 1, characterized in that: the film forming agent is composed of glycerol polymethacrylate, sodium polyacrylate grafted starch, polydimethylsiloxane and polysiloxane-11.

6. A preparation method of a reversible spray preparation with skin brightening and anti-wrinkle effects is characterized in that: the method specifically comprises the following steps:

s1, selecting and weighing raw materials: firstly, respectively measuring acetyl hexapeptide-8, tocopherol acetate, fullerene, trehalose, sodium hyaluronate, anise extract, glycyrrhiza glabra extract, hydrolyzed collagen, rutin extract, natural plant essence extract, butanediol, glycerol, a film forming agent, a humectant, an antioxidant and deionized water in required weight ratio by using weighing equipment;

s2, premixing of base materials: sequentially pouring acetyl hexapeptide-8, tocopherol acetate, fullerene, trehalose, sodium hyaluronate, a hypsizygus marmoreus extract, a glycyrrhiza glabra extract, hydrolyzed collagen, a rutin extract and a natural plant essence extract which are measured in the step S1 into mixing and stirring equipment, then adding deionized water in corresponding weight proportion, starting a stirring mechanism, and stirring for 30-40min at the rotation speed of 300-400r/min and the temperature of 26-33 ℃ to prepare a base material;

s3, preparation of an efficacy primary mixing agent: respectively pouring the butanediol, the glycerol, the humectant and the antioxidant weighed in the step S1 into the base material obtained in the step S2, and stirring at the rotating speed of 400-600r/min for 20-30min to fully mix the effective components of the humectant and the antioxidant with the base material, thereby obtaining an effective primary mixing agent;

s4, preparation of the retrogradation spray preparation: adding the film forming agent measured in the step S1 into the efficacy initial mixing agent prepared in the step S3, and stirring for 1-2 hours at the rotating speed of 700-900r/min to enable the mixed solution to be a viscous transparent liquid, thereby completing the preparation of the inverse aged spraying preparation;

s5, filling and packaging the preparation: and (4) filling the retrogradation spray preparation prepared in the step (S4) into spray container bottles by filling equipment, wherein each bottle can contain 5-6mL of the retrogradation spray preparation, then carrying out quality detection, and packaging for sale or warehousing for storage after the detection is qualified.

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