CN111040535A - Stone-imitated textured paint and preparation method thereof - Google Patents
Stone-imitated textured paint and preparation method thereof Download PDFInfo
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- CN111040535A CN111040535A CN201911210971.8A CN201911210971A CN111040535A CN 111040535 A CN111040535 A CN 111040535A CN 201911210971 A CN201911210971 A CN 201911210971A CN 111040535 A CN111040535 A CN 111040535A
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D133/00—Coating compositions based on homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides, or nitriles thereof; Coating compositions based on derivatives of such polymers
- C09D133/04—Homopolymers or copolymers of esters
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
- C09D5/28—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes for wrinkle, crackle, orange-peel, or similar decorative effects
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/60—Additives non-macromolecular
- C09D7/61—Additives non-macromolecular inorganic
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/60—Additives non-macromolecular
- C09D7/61—Additives non-macromolecular inorganic
- C09D7/62—Additives non-macromolecular inorganic modified by treatment with other compounds
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/60—Additives non-macromolecular
- C09D7/63—Additives non-macromolecular organic
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/65—Additives macromolecular
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K3/00—Use of inorganic substances as compounding ingredients
- C08K3/18—Oxygen-containing compounds, e.g. metal carbonyls
- C08K3/20—Oxides; Hydroxides
- C08K3/22—Oxides; Hydroxides of metals
- C08K2003/2237—Oxides; Hydroxides of metals of titanium
- C08K2003/2241—Titanium dioxide
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K3/00—Use of inorganic substances as compounding ingredients
- C08K3/18—Oxygen-containing compounds, e.g. metal carbonyls
- C08K3/24—Acids; Salts thereof
- C08K3/26—Carbonates; Bicarbonates
- C08K2003/265—Calcium, strontium or barium carbonate
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K3/00—Use of inorganic substances as compounding ingredients
- C08K3/30—Sulfur-, selenium- or tellurium-containing compounds
- C08K2003/3045—Sulfates
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/03—Polymer mixtures characterised by other features containing three or more polymers in a blend
- C08L2205/035—Polymer mixtures characterised by other features containing three or more polymers in a blend containing four or more polymers in a blend
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- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Paints Or Removers (AREA)
Abstract
The limestone-imitated texture paint comprises hydroxyethyl cellulose, bentonite, ethylene glycol, a wetting agent, a dispersing agent, a defoaming agent, 2-amino-2 methyl-1-propanol, titanium dioxide, heavy calcium carbonate, barium sulfate, calcined kaolin, pure acrylic emulsion, alcohol ester twelve, a surface control auxiliary agent, a water-based anti-scraping wear-resisting agent, a polysiloxane auxiliary agent, a bactericide and water. The limestone-imitated modeling texture paint has rich modeling texture effects; the pure acrylic emulsion with a small molecular structure is adopted as a main film forming substance, has the characteristics of small particle size and strong permeability, can be directly coated on the lower-layer coating, can be completely permeated and fused with the lower-layer coating, and has extremely excellent fusion property; meanwhile, the paint has excellent initial polishing performance, so that the surface of a coating film is flat and smooth, and the effect is natural and vivid; in addition, the construction method is simple, the construction tools are common spray guns, rollers or natural alginate wool and the like, the operation is simple, and the construction is convenient.
Description
Technical Field
The invention relates to the technical field of building coatings, in particular to an imitative limestone modeling texture paint and a preparation method thereof.
Background
Limestone is a natural stone and plays a very important role in building materials, at present, people adopt limestone for decoration and have exquisite appearance and receive more and more attention of people when decorating buildings, however, limestone is directly used for outer wall decoration, the manufacturing cost is extremely high, and the hidden trouble of falling off for a long time exists. Currently, although there is an aqueous coating of limestone imitation which replaces limestone, the texture effect coating applied on the limestone imitation has the problems of difficult construction polishing, abrupt color points, difficult infiltration and fusion with the lower layer coating, poor fusion, uneven surface, and only spot spraying texture, single effect. Therefore, the research and development of the limestone-imitated texture paint which is easy to construct and polish, has rich texture effect and can be completely permeated and fused with the lower layer coating has very important significance.
Disclosure of Invention
Aiming at the defects of the prior art, the invention aims to provide a stone-imitated modeling texture paint and a preparation method thereof. The limestone-imitated texture paint has rich texture effect, has different texture effects such as wire drawing, dot spraying, color wiping and the like, and overcomes the defect that the prior texture layer paint only has the dot spraying effect; the coating has extremely strong permeability, can be directly coated on the lower layer coating, can be permeated and fused with the lower layer coating, and has extremely excellent fusion; meanwhile, the paint has excellent initial polishing performance, so that the surface of a paint film is flat and smooth, and the effect is natural and vivid. In addition, the construction method is simple, the construction tools are common spray guns, rollers or natural alginate wool and the like, the operation is simple, and the construction is convenient.
The invention is realized by the following technical scheme:
an imitative limestone modeling texture paint comprises the following components in parts by mass:
further, the additive comprises the following components in parts by mass:
further, the organic modified bentonite is sodium bentonite with a sheet structure.
Further, the wetting agent is selected from one or more than one of anionic surfactant, nonionic surfactant or polyether modified polysiloxane compound.
Further, the dispersant is selected from anionic dispersants or nonionic dispersants.
Further, the pure acrylic emulsion is a copolymer of acrylic ester and methacrylic ester, and the solid content is 45-51%.
The acrylic emulsion used in the invention is a copolymer of acrylic ester and methacrylic ester, can form a more compact paint film, has excellent water resistance and weather resistance, has the emulsion particle size of 50-100nm, small particle size and excellent penetrability, improves the penetrability of the modeling texture paint, and is convenient for the penetration and fusion of texture color and lower layer paint.
Further, the surface control auxiliary agent is polyacrylate.
The surface control auxiliary agent used in the invention has excellent compatibility and initial sanding property, not only can improve the excellent smooth touch of the coating, but also has excellent leveling property and defoaming property, and can generate synergistic effect with a water-based scratch-resistant wear-resistant agent in a formula, so that the hardness and smooth hand feeling of the coating are further improved, and the coating is smooth, hard and flat.
Further, the aqueous scratch and abrasion resistant agent is a silicone polymer solution.
The water-based scratch-resistant wear-resistant agent used in the invention can generate further crosslinking reaction with film-forming substances in the formula along with the increase of the curing time, so that the hardness of the coating can be enhanced, and the permanent silky hand feeling of the coating can be provided.
Furthermore, the polysiloxane auxiliary agent can generate good synergistic effect with the surface control auxiliary agent, so that the auxiliary agent can be enriched on the surface of a coating film, the coating film can form a compact lubricating layer, dynamic lubrication between color points and the surface of a base layer is facilitated, the surface hand feeling of the coating layer is improved, and a flat and smooth paint film surface is facilitated to be obtained.
Further, the bactericide is selected from one or more of isothiazolinone, formaldehyde releasing agent and benzimidazole.
Further, the defoaming agent is selected from one or two of a mineral oil defoaming agent and a silicone defoaming agent.
The invention has the beneficial effects that: the limestone-imitated modeling texture paint has rich modeling texture effects, has various texture effects such as wire drawing, dot spraying, color wiping and the like, and overcomes the defect that the prior texture layer paint can only have the dot spraying effect; the pure acrylic emulsion with a small molecular structure is adopted as a main film forming substance, has the characteristics of small particle size and strong permeability, can be directly coated on the lower-layer coating, can be completely permeated and fused with the lower-layer coating, and has extremely excellent fusion property; meanwhile, the paint has excellent initial polishing performance, so that the surface of a coating film is flat and smooth, and the effect is natural and vivid; in addition, the construction method is simple, the construction tools are common spray guns, rollers or natural alginate wool and the like, the operation is simple, and the construction is convenient.
Detailed Description
The present invention will be described in detail with reference to specific examples.
Example 1
An imitative limestone modeling texture paint comprises the following components in parts by mass:
the preparation method of the limestone-imitated modeling texture paint comprises the following steps:
(1) adding hydroxyethyl cellulose and sodium bentonite into water, then sequentially and slowly adding ethylene glycol, 2-amino-2-methyl-1-propanol, a mineral oil defoaming agent, a wetting agent sodium alkyl succinate and a dispersant sodium tripolyphosphate, and stirring at 500r/min for uniform dispersion;
(2) then, slowly adding titanium dioxide, heavy calcium carbonate, barium sulfate and calcined kaolin in sequence, and stirring and dispersing uniformly at 1500 r/min;
(3) slowly adding a pure acrylic emulsion acrylate-methacrylate copolymer, stirring at 900r/min for uniform dispersion, sequentially adding alcohol ester dodeca, surface control additive polyacrylate, water-based anti-scraping wear-resistant agent silicone polymer solution, bactericide formaldehyde, polysiloxane additive and organic silicon defoamer, and stirring at 900r/min for uniform dispersion.
Example 2
An imitative limestone modeling texture paint comprises the following components in parts by mass:
the preparation method of the limestone-imitated modeling texture paint comprises the following steps:
(1) adding hydroxyethyl cellulose and sodium bentonite into water, then sequentially and slowly adding ethylene glycol, 2-amino-2 methyl-1-propanol, a mineral oil defoaming agent, a wetting agent polyether modified dimethyl siloxane and a dispersing agent sodium hexametaphosphate, and stirring and dispersing uniformly at 800 r/min;
(2) then, slowly adding titanium dioxide, heavy calcium carbonate, barium sulfate and calcined kaolin in sequence, and uniformly stirring and dispersing at 2000 r/min;
(3) slowly adding a pure acrylic emulsion acrylate-methacrylate copolymer, sequentially adding alcohol ester dodeca, a surface control additive polyacrylate, a water-based anti-scraping wear-resistant agent silicone polymer solution, a bactericide 2-methyl-4-isothiazoline-3-one, a polysiloxane additive and an organic silicon defoamer, and uniformly stirring at 1200r/min to obtain the acrylic ester/methacrylate copolymer.
Example 3
An imitative limestone modeling texture paint comprises the following components in parts by mass:
the preparation method of the limestone-imitated modeling texture paint comprises the following steps:
(1) adding hydroxyethyl cellulose and sodium bentonite into water, then sequentially and slowly adding ethylene glycol, 2-amino-2 methyl-1-propanol, a mineral oil defoaming agent, a wetting agent polyethoxy nonyl phenol and a dispersant polyacrylic acid ammonium salt, and stirring and uniformly dispersing at 300 r/min;
(2) then, slowly adding titanium dioxide, heavy calcium carbonate, barium sulfate and calcined kaolin in sequence, and stirring and dispersing uniformly at 1000 r/min;
(3) slowly adding a pure acrylic emulsion acrylate-methacrylate copolymer, sequentially adding alcohol ester dodeca, a surface control additive polyacrylate, a water-based anti-scraping wear-resistant agent silicone polymer solution, a bactericide 2-methyl-4-isothiazoline-3-one, a polysiloxane additive and an organic silicon defoamer, and uniformly stirring at 600r/min to obtain the acrylic ester/methacrylate copolymer.
The products of examples 1-3 were tested according to the GB/T9755-2014 synthetic resin emulsion exterior wall coating specifications, wherein the bond strength was tested according to the GB/T9779-2015 specifications, and the data are given in Table 1 below.
The formula of the existing product is used as a control sample, and the water-in-water multicolor paint is composed of 100 parts of basic paint, 90 parts of mixed auxiliary material and 95 parts of blending auxiliary material in parts by mass; the base coating comprises the following raw materials, by mass, 40 parts of deionized water, 1.5 parts of hydroxyethyl cellulose, 0.33 part of paraffin-based mineral oil, 0.14 part of ammonia water, 0.14 part of polyethoxy nonyl phenol, 0.41 part of polyacrylic acid sodium salt, 3 parts of titanium dioxide, 2 parts of alcohol ester, 0.93 part of propylene glycol, 45 parts of styrene-acrylic emulsion, 0.3 part of formaldehyde and 7.06 parts of magnesium aluminum silicate solution; the mixed auxiliary material comprises 96.63 parts of deionized water, 0.27 part of hydroxyethyl cellulose, 2.4 parts of magnesium aluminum silicate, 0.3 part of formaldehyde, 0.3 part of sodium polyacrylate and 0.1 part of ammonia water by mass; the blending auxiliary material comprises 89 parts of styrene-acrylic emulsion, 3.5 parts of alcohol ester, 1.42 parts of propylene glycol, 0.15 part of polyurethane polymer, 0.15 part of formaldehyde, 0.22 part of ammonia water and 5.56 parts of deionized water in parts by mass.
TABLE 1 technical indices of the products of examples 1-3 and the existing products
As can be seen from the above table 1, the limestone-imitated texture paint has rich texture effects, has texture effects of wire drawing, dot spraying and color wiping, and also has excellent application property and initial polishing property; meanwhile, the paint film can be completely permeated and fused with the lower-layer paint, so that the paint film has smooth, flat and hard hand feeling, excellent compatibility with the lower-layer paint, excellent bonding strength and far better comprehensive performance than the existing commercial products.
Claims (10)
1. The limestone-imitated modeling texture paint is characterized by comprising the following components in parts by mass:
2. the apatite-imitated texture paint as claimed in claim 1, wherein the additive comprises the following components in parts by mass:
3. the apatite-imitated texture paint as claimed in claim 1, wherein the bentonite is sodium bentonite.
4. The paint of claim 1, wherein the wetting agent is selected from one or more of anionic surfactant, nonionic surfactant, and polyether-modified polysiloxane.
5. The apatite-imitated texture paint as claimed in claim 1, wherein the dispersant is selected from anionic dispersant or nonionic dispersant.
6. The apatite-imitated texture paint as claimed in claim 1, wherein the acrylic emulsion is a copolymer of acrylate and methacrylate, and the solid content is 45-51%.
7. The apatite-imitated texture paint as claimed in claim 1, wherein the surface control assistant is polyacrylate.
8. The apatite-modeled texture paint of claim 1, wherein the aqueous scratch and wear resistant agent is a silicone polymer solution.
9. The apatite-imitated texture paint as claimed in claim 2, wherein the bactericide is selected from one or more of isothiazolinone, formaldehyde releasing agent, benzimidazole.
10. The apatite-imitated texture paint as claimed in claim 2, wherein the defoamer is selected from one or two of a mineral oil defoamer and a silicone defoamer.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201911210971.8A CN111040535A (en) | 2019-12-02 | 2019-12-02 | Stone-imitated textured paint and preparation method thereof |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201911210971.8A CN111040535A (en) | 2019-12-02 | 2019-12-02 | Stone-imitated textured paint and preparation method thereof |
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| CN111040535A true CN111040535A (en) | 2020-04-21 |
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| CN201911210971.8A Pending CN111040535A (en) | 2019-12-02 | 2019-12-02 | Stone-imitated textured paint and preparation method thereof |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111484781A (en) * | 2020-04-28 | 2020-08-04 | 天津德普威涂料有限公司 | Limestone-imitated multicolor paint and construction method thereof |
| CN113831810A (en) * | 2021-11-09 | 2021-12-24 | 浙江志强涂料有限公司 | As-cast finish concrete imitation coating and preparation method thereof |
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| CN108285711A (en) * | 2018-02-10 | 2018-07-17 | 浙江德尔福涂料有限公司 | A kind of imitative lime fluorspar coating and preparation method thereof |
| CN108641499A (en) * | 2018-03-30 | 2018-10-12 | 浙江长兴凯士涂料有限公司 | A kind of imitative lime stone cobweb coating |
| CN109266145A (en) * | 2018-09-06 | 2019-01-25 | 江苏久诺建材科技股份有限公司 | A kind of lacquer of color inhibition |
| WO2019101799A1 (en) * | 2017-11-21 | 2019-05-31 | Brillux Gmbh & Co. Kg | Aqueous composition and aqueous coating agent |
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2019
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| CN104804593A (en) * | 2015-05-12 | 2015-07-29 | 重庆市品胜涂料有限公司 | Water-based art paint and preparation method thereof |
| WO2019101799A1 (en) * | 2017-11-21 | 2019-05-31 | Brillux Gmbh & Co. Kg | Aqueous composition and aqueous coating agent |
| CN108285711A (en) * | 2018-02-10 | 2018-07-17 | 浙江德尔福涂料有限公司 | A kind of imitative lime fluorspar coating and preparation method thereof |
| CN108641499A (en) * | 2018-03-30 | 2018-10-12 | 浙江长兴凯士涂料有限公司 | A kind of imitative lime stone cobweb coating |
| CN109266145A (en) * | 2018-09-06 | 2019-01-25 | 江苏久诺建材科技股份有限公司 | A kind of lacquer of color inhibition |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111484781A (en) * | 2020-04-28 | 2020-08-04 | 天津德普威涂料有限公司 | Limestone-imitated multicolor paint and construction method thereof |
| CN113831810A (en) * | 2021-11-09 | 2021-12-24 | 浙江志强涂料有限公司 | As-cast finish concrete imitation coating and preparation method thereof |
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Application publication date: 20200421 |