CN110840820A - Acne-removing purple perilla composite cream with sun-screening function and preparation method thereof - Google Patents
Acne-removing purple perilla composite cream with sun-screening function and preparation method thereof Download PDFInfo
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- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
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Abstract
The invention discloses acne-removing purple perilla composite cream with a sun-screening function, which is prepared from the following raw materials in parts by weight: 8-12 parts of seabuckthorn fruit oil, 0.7-1.2 parts of vitamin E oil, 0.4-0.6 part of emulsifier, 38-45 parts of lavender hydrosol, 0.3-0.8 part of urea capsule, 5-8 parts of glycerol, 1-3 parts of pentanediol, 18-24 parts of perilla seed extract, 8-10 parts of paper mulberry extract and 6-12 parts of spirulina extract, and also discloses a preparation method of the acne-removing perilla frutescens composite cream. The sea buckthorn fruit oil, the vitamin E oil, the perilla seed extract, the paper mulberry extract and the spirulina extract are used as functional components of the cream, natural components are adopted, and the cream does not contain preservatives.
Description
Technical Field
The invention belongs to the technical field of functional cosmetics, and particularly relates to development of acne-removing purple perilla composite cream with a sun-screening function.
Background
At present, natural plant extracts are added into cosmetic cream in the cosmetic industry to enable the cosmetic cream to have the effects of diminishing inflammation, resisting acne and the like, but scars of acne skin are difficult to recover due to the fact that scars appear due to solar ultraviolet rays after the skin is damaged, and components such as zinc oxide, titanium dioxide and octyl salicylate are added into existing sunscreen cosmetics. Therefore, it is necessary to develop a cream suitable for the people with acne muscle, especially in the seasons and areas of ultraviolet intensity.
Disclosure of Invention
The invention aims to solve the technical problem that the deficiency of the prior art is overcome, and provides a preparation method of acne-removing perilla frutescens composite cream with sun-screening function.
In order to solve the technical problems, the invention adopts the technical scheme that: the acne-removing purple perilla composite cream with the sun-screening function is characterized by being prepared from the following raw materials in parts by weight: 8-12 parts of seabuckthorn fruit oil, 0.7-1.2 parts of vitamin E oil, 0.4-0.6 part of emulsifier, 38-45 parts of lavender hydrosol, 0.3-0.8 part of urea capsule, 5-8 parts of glycerol, 1-3 parts of pentanediol, 18-24 parts of perilla seed extract, 8-10 parts of paper mulberry extract and 6-12 parts of spirulina extract.
The preparation method of the acne-removing purple perilla composite cream with the sun-screening function is characterized by comprising the following raw materials in parts by weight: 10 parts of seabuckthorn fruit oil, 1 part of vitamin E oil, 0.5 part of emulsifier, 40 parts of lavender hydrosol, 0.5 part of urea capsule, 6 parts of glycerol, 2 parts of pentanediol, 20 parts of perilla seed extract, 10 parts of paper mulberry extract and 10 parts of spirulina extract.
In addition, the invention also provides a method for preparing the acne-removing perilla frutescens composite cream with the sun-screening function, which is characterized by comprising the following steps of:
firstly, selecting seabuckthorn fruit oil, vitamin E oil and an emulsifier, and stirring and emulsifying in a water bath at 70 ℃ to obtain an oil phase;
step two, selecting lavender hydrosol, urea capsules, glycerin and pentanediol, and heating in a water bath at 70 ℃ to obtain a water phase;
and step three, mixing the oil phase obtained in the step one and the water phase obtained in the step two, emulsifying in a water bath at 70 ℃, adding the perilla seed extract, the paper mulberry extract and the spirulina extract after the emulsification is finished, and stirring uniformly to obtain the acne-removing perilla composite cream with the sun-screening function.
The preparation method is characterized in that the preparation method of the seabuckthorn fruit oil in the first step comprises the following steps: firstly, pulverizing fructus Hippophae to 100 mesh, placing into supercritical 5L charging barrel, and extracting at 50 deg.C under 30MPa with supercritical CO2The extraction method takes the crude product of the seabuckthorn fruit oil as an extract once every 30min, and the extraction time is 3h in total; then theSupercritical CO2Adding the crude product of the seabuckthorn fruit oil obtained by extraction into a molecular distillation feeding tank, performing molecular distillation, dehydration, deodorization and deacidification at the distillation temperature of 160 ℃ and the flow rate of 300g/h, and decoloring by using activated carbon at the temperature of 40 ℃; and finally, freezing for 4 hours at the temperature of-3-0 ℃ to obtain the seabuckthorn fruit oil.
The method is characterized in that the preparation method of the broussonetia papyrifera extract in the step three comprises the following steps: baking fresh folium Broussonetiae in oven at 110 deg.C for 15min, oven drying at 70 deg.C overnight, cutting into pieces, adding citric acid solution with mass content of 8%, soaking for 30min, filtering, and repeatedly washing with distilled water. Soaking dried folium Broussonetiae in 1.5 wt% hydrogen peroxide, heating in 50 deg.C water bath for 60min while stirring to decolorize uniformly, filtering, washing with water repeatedly, and drying in 80 deg.C oven to obtain treated folium Broussonetiae; adding distilled water into the treated folium Broussonetiae, and heating in 80 deg.C water bath for 30min to obtain decolorized Broussonetia papyrifera extract.
The method is characterized in that the preparation method of the spirulina extract in the step three comprises the following steps: putting spirulina powder into a container, adding water according to the ratio of material to liquid of 1:20, standing in ultrasonic wave for 5h, heating in water bath at 70 deg.C for 1.5h, taking out, centrifuging for 10min with a high-speed freezer at 4000r, and taking out supernatant to obtain spirulina extract.
The method is characterized in that the preparation method of the perilla seed extract in the step three comprises the following steps: taking the mass ratio of 1: 30, mixing the perilla seeds with distilled water, carrying out water bath for 30min at the temperature of 80 ℃ to obtain a coarse product of perilla seed extract, and then decoloring by adopting activated carbon to obtain a perilla seed extract; the method is characterized in that pretreatment is carried out before the active carbon is decolorized, and the pretreatment process comprises the following steps: firstly, soaking the activated carbon in distilled water for 24 hours, then filtering, adding a hydrochloric acid solution for soaking and boiling, repeatedly washing the activated carbon with water to be neutral after standing for 24 hours, filtering and then drying the activated carbon in an oven at 105 ℃.
The vitamin E oil, the emulsifier, the lavender hydrosol, the urea sac, the glycerol and the pentanediol which are used in the invention are all products sold in the market.
Compared with the prior art, the invention has the following advantages:
1. the principle of the invention is that pores are opened and impurities such as bacteria and the like in the pores are removed through the paper mulberry extract, the oxidation resistance of the seabuckthorn fruit oil and the perilla extract is obviously improved under the action of the moisturizing factor of the spirulina compound extract, and the flavone substance in the perilla extract strongly resists UV-B radiation. The compound use of the three components enhances the degerming, moisture retention and radiation resistance performance, and the skin care effect is optimal.
2. The sea buckthorn fruit oil, the vitamin E oil, the perilla seed extract, the paper mulberry extract and the spirulina extract are used as functional components of the cream, natural components are adopted, and no preservative is contained, so that the prepared composite cream has the functions of moisturizing, anti-acne, oxidation resistance and ultraviolet resistance, does not generate side effects on skin, and is suitable for most people.
3. The cream prepared by the invention has strong dirt-removing power, can remove acne dregs and bacteria, and can clean skin pores. The cream contains more than 200 bioactive substances, wherein the powerful antioxidant SOD enzyme and carotenoid contained in the seabuckthorn fruit oil can rapidly decompose and kill endotoxin and bacteria in skin pores, repair damaged tissues, convert partial substances into vitamin A in vivo, directly repair epithelial tissues, and enhance immunity so as to remove acne. In addition, the cream contains a large amount of antioxidant substances, flavonoid substances, terpenoid substances and transdermal penetration enhancers, which reach deep cells of skin through pore channels, and under the action of moisturizing factors, the synergistic effect of the antioxidant substances is exerted to the maximum, and meanwhile, the characteristic of water retention is also played in turn. Has effects of caring skin, nourishing and resisting oxidation, and can be used for removing acne.
The technical solution of the present invention will be described in further detail by examples.
Detailed Description
Example 1
The acne-removing purple perilla composite cream with the sun-screening function in the embodiment is prepared from the following raw materials in parts by weight: 10 parts of seabuckthorn fruit oil, 1 part of vitamin E oil, 0.5 part of emulsifier, 40 parts of lavender hydrosol, 0.5 part of urea capsule, 6 parts of glycerol, 2 parts of pentanediol, 20 parts of perilla seed extract, 10 parts of paper mulberry extract and 10 parts of spirulina extract. The emulsifier is lanolin.
The preparation method of the acne-removing perilla frutescens composite cream with the sun-screening function comprises the following steps:
firstly, selecting seabuckthorn fruit oil, vitamin E oil and an emulsifier, and stirring and emulsifying in a water bath at 70 ℃ to obtain an oil phase;
step two, selecting lavender hydrosol, urea capsules, glycerin and pentanediol, and heating in a water bath at 70 ℃ to obtain a water phase;
and step three, mixing the oil phase obtained in the step one and the water phase obtained in the step two, emulsifying in a water bath at 70 ℃, adding the perilla seed extract, the paper mulberry extract and the spirulina extract after the emulsification is finished, and stirring uniformly to obtain the acne-removing perilla composite cream with the sun-screening function.
In the embodiment, firstly, the seabuckthorn fruits are crushed to 100 meshes and then are put into a supercritical 5L charging barrel, and supercritical CO is adopted under the conditions that the extraction temperature is 50 ℃ and the extraction pressure is 30MPa2The extraction method takes the crude product of the seabuckthorn fruit oil as an extract once every 30min, and the extraction time is 3h in total; then supercritical CO is added2Adding the crude product of the seabuckthorn fruit oil obtained by extraction into a molecular distillation feeding tank, performing molecular distillation, dehydration, deodorization and deacidification at the distillation temperature of 160 ℃ and the flow rate of 300g/h, and decoloring by using activated carbon at the temperature of 40 ℃; and finally, freezing for 4 hours at the temperature of-3-0 ℃ to obtain the seabuckthorn fruit oil.
In this embodiment, the preparation method of the broussonetia papyrifera extract in step three comprises: baking fresh folium Broussonetiae in oven at 110 deg.C for 15min, oven drying at 70 deg.C overnight, cutting into pieces, adding citric acid solution with mass content of 8%, soaking for 30min, filtering, and repeatedly washing with distilled water. Soaking dried folium Broussonetiae in 1.5 wt% hydrogen peroxide, heating in 50 deg.C water bath for 60min while stirring to decolorize uniformly, filtering, washing with water repeatedly, and drying in 80 deg.C oven to obtain treated folium Broussonetiae; adding distilled water into the treated folium Broussonetiae, and heating in 80 deg.C water bath for 30min to obtain decolorized Broussonetia papyrifera extract.
In this embodiment, the preparation method of the spirulina extract in step three includes: putting spirulina powder into a container, adding water according to the ratio of material to liquid of 1:20, standing in ultrasonic wave for 5h, heating in water bath at 70 deg.C for 1.5h, taking out, centrifuging for 10min with a high-speed freezer at 4000r, and taking out supernatant to obtain spirulina extract.
In this embodiment, the preparation method of the perilla seed extract in step three includes: taking the mass ratio of 1: 30, mixing the perilla seeds with distilled water, carrying out water bath for 30min at the temperature of 80 ℃ to obtain a coarse product of perilla seed extract, and then decoloring by adopting activated carbon to obtain a perilla seed extract; the method is characterized in that pretreatment is carried out before the active carbon is decolorized, and the pretreatment process comprises the following steps: firstly, soaking the activated carbon in distilled water for 24 hours, then filtering, adding a hydrochloric acid solution for soaking and boiling, repeatedly washing the activated carbon with water to be neutral after standing for 24 hours, filtering and then drying the activated carbon in an oven at 105 ℃.
Comparative example 1
This comparative example is the same as the example except that: the composite cream of this comparative example does not contain broussonetia extract.
Comparative example 2
This comparative example is the same as the example except that: the composite cream of this comparative example does not contain perilla extract.
Comparative example 3
This comparative example is the same as the example except that: the composite cream of this comparative example did not contain spirulina extract.
Comparative example 4
This comparative example is the same as the example except that: the composite cream of this comparative example did not contain spirulina extract, perilla extract, and perilla extract.
Example 2
The acne-removing purple perilla composite cream with the sun-screening function in the embodiment is prepared from the following raw materials in parts by weight: 8 parts of seabuckthorn fruit oil, 0.7 part of vitamin E oil, 0.4 part of emulsifier, 38 parts of lavender hydrosol, 0.3 part of urea capsule, 5 parts of glycerol, 1 part of pentanediol, 18 parts of perilla seed extract, 8 parts of paper mulberry extract and 6 parts of spirulina extract. The emulsifier is lanolin.
The acne-removing perilla composite cream with the sun-screening function has the same preparation method as that of the example 1.
Example 3
The acne-removing purple perilla composite cream with the sun-screening function in the embodiment is prepared from the following raw materials in parts by weight: 12 parts of seabuckthorn fruit oil, 1.2 parts of vitamin E oil, 0.6 part of emulsifier, 45 parts of lavender hydrosol, 0.8 part of urea capsule, 8 parts of glycerol, 3 parts of pentanediol, 24 parts of perilla seed extract, 10 parts of paper mulberry extract and 12 parts of spirulina extract. The emulsifier is lanolin.
The acne-removing perilla composite cream with the sun-screening function has the same preparation method as that of the example 1.
The oxidation resistance, moisturizing ability, ultraviolet resistance and acne removal ability of the creams prepared in examples 1 to 3 and comparative examples 1 to 4 were examined.
(1) Detection of antioxidant capacity
Table 1 examples and comparative creams experimental results unit for antioxidant ability (%)
As can be seen from table 1, the perilla extract and the spirulina extract can improve the antioxidant capacity of the cream together, and the combination of the two can bring the antioxidant capacity of the cream to the utmost.
(2) Detection of moisturizing ability
The skin moisture content of the face of ten subjects was measured and averaged before the cosmetics were applied, then the skin of the face of ten subjects was applied using the creams of example 1 and comparative examples 1 to 4, the skin moisture content of the face of ten subjects was measured and averaged after 10 minutes, then the moisture content increase rates of the skin of the face before and after application were calculated, the skin moisture content of the face of subject was measured and averaged after 4 hours, then the moisture content increase rates of the skin of the face before and after application were calculated, and the obtained data are shown in table 2.
Table 2 examples and comparative examples unit (%) -test results on moisturizing ability of cream
As can be seen from table 2, the cream containing perilla extract, spirulina extract and broussonetia extract in example 1 was most effective in moisturizing skin, and the cream of example 1 was also most effective in moisturizing skin after long-term application.
(3) Ultraviolet resistance was measured
Table 3 examples and comparative creams uv protection test result unit (%)
As can be seen from table 3: the cream containing the perilla herb extract, the spirulina extract and the broussonetia papyrifera extract in example 1 was used to optimize the ultraviolet protection ability and the ultraviolet protection ability. The anti-ultraviolet capability mainly uses Fe3+Reduction method detection shows that after a large amount of ultraviolet radiation, the total antioxidant capacity of skin tissues is obviously reduced, and the accumulation of skin tissue lipid peroxidation products caused by ultraviolet radiation is related to the weakening of the function of a tissue antioxidant defense system.
(4) Acne removing ability test
Cream prepared using the creams of example 1 and comparative examples 1-4 were used to perform an acne removal experiment for 3 months on 5 groups of 140 volunteers, each group having 20 volunteers, of which 7 groups of volunteers used the creams prepared using the creams of example 1 and comparative examples 1-4, respectively
Table 4 results of cream acne removal experiments of examples 1 to 3 and comparative examples 1 to 4
The above description is only for the preferred embodiment of the present invention, and is not intended to limit the present invention in any way. Any simple modification, change and equivalent changes of the above embodiments according to the technical essence of the invention are still within the protection scope of the technical solution of the invention.
Claims (7)
1. The acne-removing purple perilla composite cream with the sun-screening function is characterized by being prepared from the following raw materials in parts by weight: 8-12 parts of seabuckthorn fruit oil, 0.7-1.2 parts of vitamin E oil, 0.4-0.6 part of emulsifier, 38-45 parts of lavender hydrosol, 0.3-0.8 part of urea capsule, 5-8 parts of glycerol, 1-3 parts of pentanediol, 18-24 parts of perilla seed extract, 8-10 parts of paper mulberry extract and 6-12 parts of spirulina extract.
2. The preparation method of the acne-removing perilla frutescens composite cream with the sun-screening function according to claim 1, which is characterized by being prepared from the following raw materials in parts by weight: 10 parts of seabuckthorn fruit oil, 1 part of vitamin E oil, 0.5 part of emulsifier, 40 parts of lavender hydrosol, 0.5 part of urea capsule, 6 parts of glycerol, 2 parts of pentanediol, 20 parts of perilla seed extract, 10 parts of paper mulberry extract and 10 parts of spirulina extract.
3. A method for preparing the acne-removing perilla frutescens composite cream with the sun-screening function as claimed in claim 1 or 2, wherein the method comprises the following steps:
firstly, selecting seabuckthorn fruit oil, vitamin E oil and an emulsifier, and stirring and emulsifying in a water bath at 70 ℃ to obtain an oil phase;
step two, selecting lavender hydrosol, urea capsules, glycerin and pentanediol, and heating in a water bath at 70 ℃ to obtain a water phase;
and step three, mixing the oil phase obtained in the step one and the water phase obtained in the step two, emulsifying in a water bath at 70 ℃, adding the perilla seed extract, the paper mulberry extract and the spirulina extract after the emulsification is finished, and stirring uniformly to obtain the acne-removing perilla composite cream with the sun-screening function.
4. The method of claim 3, wherein the preparation method of the seabuckthorn fruit oil in the first step comprises: firstly, pulverizing fructus Hippophae to 100 mesh, placing into supercritical 5L charging barrel, and extracting at 50 deg.C under 30MPa with supercritical CO2The extraction method takes the crude product of the seabuckthorn fruit oil as an extract once every 30min, and the extraction time is 3h in total; then supercritical CO is added2Adding the crude product of the seabuckthorn fruit oil obtained by extraction into a molecular distillation feeding tank, performing molecular distillation, dehydration, deodorization and deacidification at the distillation temperature of 160 ℃ and the flow rate of 300g/h, and decoloring by using activated carbon at the temperature of 40 ℃; and finally, freezing for 4 hours at the temperature of-3-0 ℃ to obtain the seabuckthorn fruit oil.
5. The method of claim 3, wherein the preparation method of the broussonetia papyrifera extract in step three comprises: baking fresh folium Broussonetiae in oven at 110 deg.C for 15min, oven drying at 70 deg.C overnight, cutting into pieces, adding citric acid solution with mass content of 8%, soaking for 30min, filtering, and repeatedly washing with distilled water. Soaking dried folium Broussonetiae in 1.5 wt% hydrogen peroxide, heating in 50 deg.C water bath for 60min while stirring to decolorize uniformly, filtering, washing with water repeatedly, and drying in 80 deg.C oven to obtain treated folium Broussonetiae; adding distilled water into the treated folium Broussonetiae, and heating in 80 deg.C water bath for 30min to obtain decolorized Broussonetia papyrifera extract.
6. The method of claim 3, wherein the Spirulina extract is prepared by the following steps: putting spirulina powder into a container, adding water according to the ratio of material to liquid of 1:20, standing in ultrasonic wave for 5h, heating in water bath at 70 deg.C for 1.5h, taking out, centrifuging for 10min with a high-speed freezer at 4000r, and taking out supernatant to obtain spirulina extract.
7. The method of claim 3, wherein the perilla seed extract in step three is prepared by: taking the mass ratio of 1: 30, mixing the perilla seeds with distilled water, carrying out water bath for 30min at the temperature of 80 ℃ to obtain a coarse product of perilla seed extract, and then decoloring by adopting activated carbon to obtain a perilla seed extract; the method is characterized in that pretreatment is carried out before the active carbon is decolorized, and the pretreatment process comprises the following steps: firstly, soaking the activated carbon in distilled water for 24 hours, then filtering, adding a hydrochloric acid solution for soaking and boiling, repeatedly washing the activated carbon with water to be neutral after standing for 24 hours, filtering and then drying the activated carbon in an oven at 105 ℃.
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Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2004131500A (en) * | 2002-09-19 | 2004-04-30 | Fancl Corp | Skin aging inhibitor or improver |
| CN107625668A (en) * | 2017-09-29 | 2018-01-26 | 武汉华士特工业生物技术开发有限公司 | A kind of anti-acne moisturizing sun cream and preparation method thereof |
-
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Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2004131500A (en) * | 2002-09-19 | 2004-04-30 | Fancl Corp | Skin aging inhibitor or improver |
| CN107625668A (en) * | 2017-09-29 | 2018-01-26 | 武汉华士特工业生物技术开发有限公司 | A kind of anti-acne moisturizing sun cream and preparation method thereof |
Non-Patent Citations (1)
| Title |
|---|
| 王建新等: "《化妆品植物原料大全》", 30 June 2012, 中国纺织出版社 * |
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| CN110840820B (en) | 2021-09-07 |
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