CN110772457B - Anti-hair loss shampoo and preparation method thereof - Google Patents
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
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- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
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- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/67—Vitamins
- A61K8/673—Vitamin B group
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- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
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- A61K8/675—Vitamin B3 or vitamin B3 active, e.g. nicotinamide, nicotinic acid, nicotinyl aldehyde
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- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
- A61K8/89—Polysiloxanes
- A61K8/891—Polysiloxanes saturated, e.g. dimethicone, phenyl trimethicone, C24-C28 methicone or stearyl dimethicone
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
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- A61K8/00—Cosmetics or similar toiletry preparations
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- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/002—Preparations for repairing the hair, e.g. hair cure
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/02—Preparations for cleaning the hair
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q7/00—Preparations for affecting hair growth
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Abstract
The invention relates to an anti-hair loss shampoo and a preparation method thereof, wherein the anti-hair loss shampoo is prepared from the following substances in parts by weight: disodium ethylene diamine tetraacetate, guar gum hydroxypropyl trimethyl ammonium chloride, butanediol, disodium laureth sulfosuccinate, cocamide MEA, trihydroxystearin, cetyl alcohol, sodium cocamidopropionate, cocamidopropyl hydroxysultaine, vitamin B group raw materials, polydimethylsiloxane, laureth-23, laureth-3, an anti-dropping plant extract, phenoxyethanol, ethylhexyl glycerol, essence, citric acid, sodium chloride and deionized water. The anti-hair loss shampoo disclosed by the invention has the effects of nourishing and repairing hair, and can be used for moistening hair scales, enabling the hair to be difficult to break, enabling the hair to be black and bright, improving the growth activity of hair follicle cells, promoting hair regeneration, enhancing the metabolism function of hair follicles and effectively preventing hair loss after long-term use.
Description
Technical Field
The invention relates to the field of cosmetic washing and protection, and particularly relates to anti-hair loss shampoo and a preparation method thereof.
Background
As an important component of a human body, the hair not only can protect the head and adjust the body temperature, but also plays an important role in appearance instruments of the human body, and the hair loss problems such as the backward movement of a hairline, the withering of the hair and the like can seriously reduce the personal color value. At present, people suffering from alopecia are mainly concentrated on 20-40 years old, and most people are male. This is because seborrheic alopecia caused by androgens is the most common cause of alopecia, and excessive secretion of androgens causes excess sebum secretion, which presses hair roots, resulting in alopecia. In addition, endocrine disorders, immune dysfunction, nutritional imbalances, stress, genetics, sunlight, pollution, etc. can also lead to hair loss. The hair follicle is the root of hair growth, and the growth cycle of normal hair follicle cells is generally: anagen phase-catagen phase-telogen phase-shedding of old hair-anagen phase, most of the hair loss is due to abnormal cell cycle and morphology of hair follicles.
Theoretically, the most effective treatment for alopecia is to inhibit the catagen phase, prolong the anagen phase while maintaining the healthy hair follicle cells, and induce the telogen phase to transform into the anagen phase. However, at present, the goal is not perfectly achieved, the anti-hair loss performance of most anti-hair loss shampoos on the market cannot meet the actual requirement, and the anti-hair loss effect is poor.
The hair grows from the hair follicle, the healthy hair follicle is the fundamental guarantee of the hair growth, the ecological environment of the hair follicle is damaged, and particularly, the microcirculation of the hair follicle is disturbed and even blocked, and the hair follicle is the root cause of alopecia symptoms. Therefore, reducing scalp hair follicle damage, improving and repairing the hair follicle microenvironment is the first problem to be solved for hair loss prevention. The surfactant is used as an important functional raw material in shampoo, and the selection of the surfactant is important to the efficacy and the mild performance of the shampoo.
Disclosure of Invention
The anti-hair loss shampoo provided by the invention can reduce scalp injury, repair hair follicles, prevent hair loss and promote growth, has an obvious anti-hair loss effect, and can strengthen the hair follicles and hair roots after long-term use, so that the scalp is healthier and the hair is more nutritious.
The invention adopts the following technical scheme for solving the technical problems:
the anti-hair loss shampoo is composed of the following substances in parts by weight: 0.01-0.1 part of disodium ethylene diamine tetraacetate, 0.01-0.05 part of guar gum hydroxypropyl trimethyl ammonium chloride, 0.3-6 parts of butanediol, 10-30 parts of disodium laureth sulfosuccinate, 0.3-1 part of cocamide MEA, 0.1-0.8 part of trihydroxystearin, 0.2-1.2 parts of cetyl alcohol, 4-24 parts of sodium cocamidopropionate, 8-24 parts of cocamidopropyl hydroxysulfobetaine, 0.03-1.5 parts of vitamin B group raw materials, 0.8-6 parts of polydimethylsiloxane, 230.1-6 parts of laureth-230.1, 30.1-6 parts of laureth-30.1 parts of anti-dropping plant extract, 0.2-0.5 part of phenoxyethanol, 0.01-0.1 part of ethylhexylglycerin, 0.1-0.7 part of essence, 0-0.7 part of citric acid, 0-3 parts of sodium chloride and 20-40 parts of deionized water.
Preferably, the anti-hair loss shampoo is prepared from the following substances in parts by weight: 0.02-0.05 part of disodium ethylene diamine tetraacetate, 0.01-0.03 part of guar gum hydroxypropyl trimethyl ammonium chloride, 0.3-5 parts of butanediol, 15-30 parts of disodium laureth sulfosuccinate, 0.4-0.8 part of cocamide MEA, 0.2-0.6 part of trihydroxystearin, 0.4-1.0 part of cetyl alcohol, 5-20 parts of sodium cocamidopropionate, 10-20 parts of cocamidopropyl hydroxysulfobetaine, 0.06-1.2 parts of vitamin B group raw materials, 1-5 parts of polydimethylsiloxane, 230.1-5 parts of laureth-230.1, 30.1-5 parts of laureth-30.1, 2-10 parts of anti-dropping plant extract, 0.3-0.4 part of phenoxyethanol, 0.02-0.08 part of ethylhexylglycerin, 0.2-0.6 part of essence, 0-0.5 part of citric acid, 0-2 parts of sodium chloride and 25-35 parts of deionized water.
Most preferably, the anti-hair loss shampoo is prepared from the following substances in parts by weight: 0.04 part of disodium ethylene diamine tetraacetate, 0.02 part of guar gum hydroxypropyl trimethyl ammonium chloride, 4 parts of butanediol, 24 parts of disodium laureth sulfosuccinate, 0.6 part of cocamide MEA (membrane electrode assembly), 0.4 part of trihydroxystearin, 0.7 part of cetyl alcohol, 12 parts of sodium cocoamidopropionate, 15 parts of cocamidopropyl hydroxysulfobetaine, 0.6 part of vitamin B group raw material, 3 parts of polydimethylsiloxane, 233 parts of laureth-233 parts, 32.5 parts of laureth-32.5 parts, 6 parts of anti-dropping plant extract, 0.35 part of phenoxyethanol, 0.05 part of ethylhexyl glycerol, 0.4 part of essence, 0.1 part of citric acid, 0.5 part of sodium chloride and 27 parts of deionized water.
Preferably, the vitamin B group raw material comprises: 0.01-0.5 part of panthenol, 0.01-0.5 part of nicotinamide and 0.01-0.5 part of biotin.
Preferably, the anti-alopecia plant extract comprises: 0.5-6 parts of polygonum multiflorum extract and 0.5-6 parts of cacumen biotae extract.
The invention also provides a preparation method of the anti-hair loss shampoo, which comprises the following steps:
(1) adding deionized water into a stirring pot, heating to 70-90 ℃, adding ethylene diamine tetraacetic acid, disodium laureth sulfosuccinate, cocamide MEA, trihydroxystearin, cetyl alcohol, sodium cocamidopropionate and cocamidopropyl hydroxysultaine, and stirring until the raw materials are completely dissolved;
(2) adding guar gum hydroxypropyl trimethyl ammonium chloride dispersed by butanediol, stirring and preserving heat for 20-40 min;
(3) cooling to 50-70 ℃, adding polydimethylsiloxane, laureth-23 and laureth-3 for homogenizing and dispersing;
(4) cooling to 40-50 ℃, and sequentially adding the vitamin B group raw material, the anti-alopecia plant extract, the phenoxyethanol, the ethylhexyl glycerin and the essence;
(5) and finally, adding citric acid and sodium chloride, and uniformly stirring to obtain the anti-hair loss shampoo.
Preferably, the temperature in step (1) is raised to 85 ℃.
Preferably, the stirring and heat preservation in the step (2) are carried out for 30 min.
Preferably, the temperature in the step (3) is reduced to 60 ℃.
Preferably, the temperature in the step (4) is reduced to 45 ℃.
The invention has the beneficial effects that: (1) the anti-hair loss shampoo disclosed by the invention adopts a mild surfactant, is low in degreasing capability, small in irritation to scalp and free from damage to scalp; (2) the vitamin B group raw materials and the plant extracts are matched for use, so that the hair can be nourished, damaged hair follicles and hair roots can be repaired, and the hair growth can be effectively promoted; (3) the anti-hair loss shampoo disclosed by the invention has the effects of nourishing and repairing hair, and can be used for moistening hair scales, enabling the hair not to be easily broken and enabling the hair to be black and bright after being used for a long time; (4) the anti-hair loss shampoo disclosed by the invention can improve the growth and development of hair follicles, increase the proportion of the hair follicles in a growth period, improve the growth activity of hair follicle cells, promote hair regeneration, enhance the metabolism function of the hair follicles and effectively prevent hair loss.
Detailed Description
In order to make the objects, technical solutions and advantages of the embodiments of the present invention clearer, the technical solutions in the embodiments of the present invention will be clearly and completely described below, and it is obvious that the described embodiments are a part of the embodiments of the present invention, but not all of the embodiments. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.
Example 1
The anti-hair loss shampoo is composed of the following substances in parts by weight: 0.04 part of disodium ethylene diamine tetraacetate, 0.02 part of guar gum hydroxypropyl trimethyl ammonium chloride, 4 parts of butanediol, 24 parts of disodium laureth sulfosuccinate, 0.6 part of cocamide MEA (membrane electrode assembly), 0.4 part of trihydroxystearin, 0.7 part of cetyl alcohol, 12 parts of sodium cocoamidopropionate, 15 parts of cocamidopropyl hydroxysulfobetaine, 0.6 part of vitamin B group raw material, 3 parts of polydimethylsiloxane, 233 parts of laureth-233 parts, 32.5 parts of laureth-32.5 parts, 6 parts of anti-dropping plant extract, 0.35 part of phenoxyethanol, 0.05 part of ethylhexyl glycerol, 0.4 part of essence, 0.1 part of citric acid, 0.5 part of sodium chloride and 27 parts of deionized water.
The vitamin B group raw material comprises: 0.2 part of panthenol, 0.2 part of nicotinamide and 0.2 part of biotin.
The anti-alopecia plant extract comprises: 3 parts of polygonum multiflorum extract and 3 parts of cacumen biotae extract.
The preparation method of the anti-hair loss shampoo comprises the following steps:
(1) adding deionized water into a stirring pot, heating to 85 ℃, adding disodium ethylene diamine tetraacetic acid, disodium laureth sulfosuccinate, cocamide MEA, trihydroxystearin, cetyl alcohol, sodium cocamidopropionate and cocamidopropyl hydroxysultaine, and stirring until the raw materials are completely dissolved;
(2) adding guar gum hydroxypropyl trimethyl ammonium chloride dispersed by butanediol, stirring and keeping the temperature for 30 min;
(3) cooling to 60 deg.C, adding polydimethylsiloxane, laureth-23 and laureth-3, and homogenizing and dispersing;
(4) cooling to 45 deg.C, sequentially adding vitamin B group material, anti-alopecia plant extract, phenoxyethanol, ethylhexyl glycerol, and essence;
(5) and finally, adding citric acid and sodium chloride, and uniformly stirring to obtain the anti-hair loss shampoo.
Example 2
Example 2 is different from example 1 in the ratio of raw materials, and the other examples are the same.
The anti-hair loss shampoo is composed of the following substances in parts by weight: 0.01 part of disodium ethylene diamine tetraacetate, 0.05 part of guar gum hydroxypropyl trimethyl ammonium chloride, 1 part of butanediol, 30 parts of disodium laureth sulfosuccinate, 0.3 part of cocamide MEA (membrane electrode assembly), 0.8 part of trihydroxystearin, 0.2 part of cetyl alcohol, 20 parts of sodium cocamidopropionate, 8 parts of cocamidopropyl hydroxysulfobetaine, 1.5 parts of vitamin B group raw materials, 0.8 part of polydimethylsiloxane, 230.1 parts of laureth-230.1 parts, 36 parts of laureth-36 parts, 2 parts of an anti-dropping plant extract, 0.2 part of phenoxyethanol, 0.1 part of ethylhexyl glycerol, 0.1 part of essence, 0.2 part of citric acid, 0.3 part of sodium chloride and 20 parts of deionized water.
The vitamin B group raw material comprises: 0.5 part of panthenol, 0.5 part of nicotinamide and 0.5 part of biotin.
The anti-alopecia plant extract comprises: 1 part of polygonum multiflorum extract and 1 part of cacumen biotae extract.
Example 3
Example 3 differs from example 1 in the ratio of raw materials, and the other points are the same.
The anti-hair loss shampoo is composed of the following substances in parts by weight: 0.1 part of disodium ethylene diamine tetraacetate, 0.01 part of guar gum hydroxypropyl trimethyl ammonium chloride, 6 parts of butanediol, 10 parts of disodium laureth sulfosuccinate, 1 part of cocamide MEA, 0.1 part of trihydroxystearin, 1.2 parts of cetyl alcohol, 6 parts of sodium cocamidopropionate, 20 parts of cocamidopropyl hydroxysulfobetaine, 0.3 part of vitamin B group raw material, 6 parts of polydimethylsiloxane, 236 parts of laureth-236 parts, 30.1 parts of laureth-30.1 parts of anti-drop plant extract, 0.5 part of phenoxyethanol, 0.01 part of ethylhexyl glycerol, 0.5 part of essence, 0.1 part of citric acid, 0.4 part of sodium chloride and 40 parts of deionized water.
The vitamin B group raw material comprises: 0.1 part of panthenol, 0.1 part of nicotinamide and 0.1 part of biotin.
The anti-alopecia plant extract comprises: 6 parts of polygonum multiflorum extract and 6 parts of cacumen biotae extract.
Comparative example 1
Comparative example 1 is different from example 1 in that comparative example 1 does not contain the anti-alopecia plant extract.
Comparative example 2
Comparative example 2 differs from example 1 in that comparative example 2 does not contain a vitamin B group raw material.
Comparative example 3
Comparative example 3 is different from example 1 in that comparative example 3 does not contain a vitamin B group raw material and an anti-alopecia plant extract.
To further demonstrate the effect of the present invention, the following test methods were provided:
the experimental method comprises the following steps: 120 volunteers with alopecia troubling age of 18-45 years old are selected, male and female are not limited, and the volunteers are randomly divided into 5 groups of 20 people. The shampoo in the comparative example and the shampoo in the example are respectively used by all groups of volunteers, and the application period is 3 months every 2 days. During the test period, the subjects had no other cosmetics, health products and drugs that affected the experimental results. Because the experiment time is long and the seasonal alopecia in autumn and winter is obvious, the anti-alopecia test is recommended to avoid the season change in autumn and winter as much as possible so as to reduce the influence of the external environment change on the experiment.
Evaluation of anti-shedding effect: the subject combs the hair with a standard oak comb 10 before washing the hair each time, the number of fallen hairs is recorded, the number of effective, effective and ineffective people is counted, and the effective rate is calculated. The effective rate calculation method comprises the following steps: (the number of effective persons + the number of effective persons)/(the number of effective persons + the number of ineffective persons) × 100%.
The effect is shown: the hair loss after 3 months is reduced by more than 40 percent compared with that before the experiment, and the problems of head itching and scurf are solved;
the method has the following advantages: the hair falling quantity after 3 months is reduced by 20-40% compared with that before the experiment, and the problems of head itching and scurf are improved;
and (4) invalidation: the number of hair loss after 3 months is reduced by less than 20 percent compared with that before the experiment, and the problems of head itching and scurf are not improved.
The results of the anti-alopecia efficacy test are shown in Table 1
TABLE 1 results of efficacy test for alopecia
As can be seen from Table 1, different formulations affect the anti-hair loss performance of the shampoo, as can be seen from comparative examples 1, 2 and 3, the example 1 is the best mixture ratio and has the best anti-hair loss effect, and as can be seen from comparative example 1 and comparative examples 1 to 3, the vitamin B group raw material and the anti-hair loss plant extract can affect the anti-hair loss effect of the shampoo, wherein the anti-hair loss plant extract has a larger influence than the anti-hair loss effect.
In light of the foregoing description of preferred embodiments according to the invention, it is clear that many changes and modifications can be made by the person skilled in the art without departing from the scope of the invention. The technical scope of the present invention is not limited to the contents of the specification, and must be determined according to the scope of the claims.
Claims (6)
1. The anti-hair loss shampoo is characterized by comprising the following substances in parts by weight: 0.04 part of disodium ethylene diamine tetraacetate, 0.02 part of guar gum hydroxypropyl trimethyl ammonium chloride, 4 parts of butanediol, 24 parts of disodium laureth sulfosuccinate, 0.6 part of cocamide MEA (membrane electrode assembly), 0.4 part of trihydroxystearin, 0.7 part of cetyl alcohol, 12 parts of sodium cocoamidopropionate, 15 parts of cocamidopropyl hydroxysulfobetaine, 0.6 part of vitamin B group raw material, 3 parts of polydimethylsiloxane, 233 parts of laureth-233 parts, 32.5 parts of laureth-32.5 parts, 6 parts of anti-dropping plant extract, 0.35 part of phenoxyethanol, 0.05 part of ethylhexyl glycerol, 0.4 part of essence, 0.1 part of citric acid, 0.5 part of sodium chloride and 27 parts of deionized water;
the vitamin B group raw material comprises: 0.2 part of panthenol, 0.2 part of nicotinamide and 0.2 part of biotin;
the anti-alopecia plant extract comprises: 3 parts of polygonum multiflorum extract and 3 parts of cacumen biotae extract.
2. The method for preparing the hair loss prevention shampoo as defined in claim 1, comprising the steps of:
(1) adding deionized water into a stirring pot, heating to 70-90 ℃, adding ethylene diamine tetraacetic acid, disodium laureth sulfosuccinate, cocamide MEA, trihydroxystearin, cetyl alcohol, sodium cocamidopropionate and cocamidopropyl hydroxysultaine, and stirring until the raw materials are completely dissolved;
(2) adding guar gum hydroxypropyl trimethyl ammonium chloride dispersed by butanediol, stirring and preserving heat for 20-40 min;
(3) cooling to 50-70 ℃, adding polydimethylsiloxane, laureth-23 and laureth-3 for homogenizing and dispersing;
(4) cooling to 40-50 ℃, and sequentially adding the vitamin B group raw material, the anti-alopecia plant extract, the phenoxyethanol, the ethylhexyl glycerin and the essence;
(5) and finally, adding citric acid and sodium chloride, and uniformly stirring to obtain the anti-hair loss shampoo.
3. The preparation method of the anti-hair loss shampoo as claimed in claim 2, wherein the temperature is increased to 85 ℃ in the step (1).
4. The preparation method of the anti-hair loss shampoo as claimed in claim 2, wherein the stirring and heat preservation in the step (2) are carried out for 30 min.
5. The preparation method of the anti-hair loss shampoo as claimed in claim 2, wherein the temperature in the step (3) is reduced to 60 ℃.
6. The preparation method of the anti-hair loss shampoo as claimed in claim 2, wherein the temperature in the step (4) is reduced to 45 ℃.
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN111467277A (en) * | 2020-05-15 | 2020-07-31 | 广州路标科技有限公司 | Hair blackening essence capable of changing white hair into black hair and preparation method thereof |
| CN111956580A (en) * | 2020-09-15 | 2020-11-20 | 广州科盈化妆品有限公司 | Anti-hair loss shampoo and preparation method thereof |
| CN112006944A (en) * | 2020-09-21 | 2020-12-01 | 陆梦羽 | Formula and preparation method of active anti-hair loss and hair growth shampoo |
| CN112274463A (en) * | 2020-09-22 | 2021-01-29 | 广东嘉丹婷日用品有限公司 | Anti-hair loss shampoo and preparation method thereof |
| CN113143809A (en) * | 2021-06-10 | 2021-07-23 | 李晓娜 | Anti-hair loss shampoo and preparation method thereof |
| CN113350219A (en) * | 2021-06-28 | 2021-09-07 | 广州大唐化妆品有限公司 | Hair loss preventing and hair fixing composition, shampoo containing hair loss preventing and hair fixing composition and preparation method of shampoo |
| CN113633588A (en) * | 2021-08-14 | 2021-11-12 | 广州市丝露杰精细化工有限公司 | Anti-hair loss shampoo and preparation method thereof |
| CN113995709A (en) * | 2021-12-13 | 2022-02-01 | 广州市发歌精细化工有限公司 | Shampoo containing plant composite anti-shedding agent and preparation method thereof |
| CN115300439A (en) * | 2022-08-10 | 2022-11-08 | 沃淄(上海)生物科技有限公司 | Compound traditional Chinese medicine extract anti-hair loss and hair-plumping care solution and application thereof |
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| CN106667821A (en) * | 2015-11-10 | 2017-05-17 | 刘泽华 | Plant shampoo for preventing hair loss and promoting hair growth |
| CN108852940A (en) * | 2018-08-28 | 2018-11-23 | 广州乐草元生物科技有限公司 | A kind of anti-hair shampoo and preparation method thereof |
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| CN106667821A (en) * | 2015-11-10 | 2017-05-17 | 刘泽华 | Plant shampoo for preventing hair loss and promoting hair growth |
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