CN110755696A - Lubricant produced by adopting high-molecular polymer - Google Patents

Lubricant produced by adopting high-molecular polymer Download PDF

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Publication number
CN110755696A
CN110755696A CN201911248058.7A CN201911248058A CN110755696A CN 110755696 A CN110755696 A CN 110755696A CN 201911248058 A CN201911248058 A CN 201911248058A CN 110755696 A CN110755696 A CN 110755696A
Authority
CN
China
Prior art keywords
parts
water
mass ratio
stirring
molecular polymer
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201911248058.7A
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Chinese (zh)
Inventor
朱明亮
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Nantong Youhu Youjia Health Products Co ltd
Youhu Youjia Pharmaceutical Chuzhou Co ltd
Original Assignee
Nantong Excellent Health Care Products Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Nantong Excellent Health Care Products Co Ltd filed Critical Nantong Excellent Health Care Products Co Ltd
Priority to CN201911248058.7A priority Critical patent/CN110755696A/en
Publication of CN110755696A publication Critical patent/CN110755696A/en
Pending legal-status Critical Current

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Classifications

    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61LMETHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
    • A61L31/00Materials for other surgical articles, e.g. stents, stent-grafts, shunts, surgical drapes, guide wires, materials for adhesion prevention, occluding devices, surgical gloves, tissue fixation devices
    • A61L31/04Macromolecular materials
    • A61L31/048Macromolecular materials obtained by reactions only involving carbon-to-carbon unsaturated bonds
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/81Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions involving only carbon-to-carbon unsaturated bonds
    • A61K8/8141Compositions of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides or nitriles thereof; Compositions of derivatives of such polymers
    • A61K8/8158Homopolymers or copolymers of amides or imides, e.g. (meth) acrylamide; Compositions of derivatives of such polymers
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61LMETHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
    • A61L31/00Materials for other surgical articles, e.g. stents, stent-grafts, shunts, surgical drapes, guide wires, materials for adhesion prevention, occluding devices, surgical gloves, tissue fixation devices
    • A61L31/04Macromolecular materials
    • A61L31/042Polysaccharides
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61LMETHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
    • A61L31/00Materials for other surgical articles, e.g. stents, stent-grafts, shunts, surgical drapes, guide wires, materials for adhesion prevention, occluding devices, surgical gloves, tissue fixation devices
    • A61L31/14Materials characterised by their function or physical properties, e.g. injectable or lubricating compositions, shape-memory materials, surface modified materials
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61LMETHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
    • A61L2300/00Biologically active materials used in bandages, wound dressings, absorbent pads or medical devices
    • A61L2300/20Biologically active materials used in bandages, wound dressings, absorbent pads or medical devices containing or releasing organic materials
    • A61L2300/23Carbohydrates
    • A61L2300/232Monosaccharides, disaccharides, polysaccharides, lipopolysaccharides
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61LMETHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
    • A61L2300/00Biologically active materials used in bandages, wound dressings, absorbent pads or medical devices
    • A61L2300/40Biologically active materials used in bandages, wound dressings, absorbent pads or medical devices characterised by a specific therapeutic activity or mode of action
    • A61L2300/452Lubricants

Abstract

The invention relates to a lubricant produced by adopting high molecular polymer, the mass ratio of the raw materials is as follows, and the glycerol is 3.0-5.0; PEG-40 hydrogenated castor oil 0.5-2.0; 0.1-0.5 of essence; 0.5-1.0 parts of phenoxyethanol; 0.05-0.2 of ethylhexyl glycerol; 0.5-2.0% of hydroxyethyl cellulose; 3.0-5.0 parts of propylene glycol; 0.05-0.15 of citric acid; 0.5-1.0 parts of polyacrylamide methyl propane sulfonic acid; the remaining mass ratios are all water. The advantages that 1, the macromolecular material is difficult to be absorbed by the skin of the human body relative to the cellulose material, so the retention time on the surface of the skin of the human body is greatly prolonged compared with the cellulose, thereby achieving the effect of prolonging the duration time of the lubricating property; 2. the addition of the polymer can delay the absorption speed of the skin; 3. the lubricant has long time, almost no reduction of the lubricating performance and no harm to human body.

Description

Lubricant produced by adopting high-molecular polymer
Technical Field
The invention relates to the technical field of personal care products, in particular to a lubricant produced by adopting a high molecular polymer.
Background
Most of the personal lubricant products on the market today are cellulose-based formulations, but this type of product dries easily, while the duration of the lubricating properties is not long.
Disclosure of Invention
In order to solve the technical problems, the invention provides the lubricant produced by adopting the high molecular polymer, which has the advantages of reasonable formula, complete process, prolonged lubricant time, almost no reduction of the lubricating property and no harm to human bodies.
The lubricant is produced by adopting a high molecular polymer, and the mass ratio W/W% of raw materials is as follows:
3.0-5.0% of glycerin.
PEG-40 hydrogenated castor oil 0.5-2.0.
0.1-0.5 of essence.
0.5-1.0 part of phenoxyethanol.
0.05-0.2 of ethylhexyl glycerol.
0.5-2.0% of hydroxyethyl cellulose.
3.0-5.0 parts of propylene glycol.
0.05-0.15 of citric acid.
0.5-1.0 parts of polyacrylamide methyl propane sulfonic acid.
The water residual mass ratio is all water.
A preferable scheme is that the mass ratio W/W% of the raw materials is as follows:
and 5.0 of glycerol.
PEG-40 hydrogenated Castor oil 2.0.
0.5 of essence.
1.0 parts of phenoxyethanol.
And 0.2 of ethylhexyl glycerol.
Hydroxyethyl cellulose 2.0.
And 5.0 parts of propylene glycol.
Citric acid 0.15.
Polyacrylamide methyl propane sulfonic acid 1.0.
The water residual mass ratio is all water.
In another preferred scheme, the mass ratio W/W% of the raw materials is as follows:
and 3.0 of glycerol.
PEG-40 hydrogenated Castor oil 0.5.
0.1 of essence.
0.5 of phenoxyethanol.
And 0.05 of ethylhexyl glycerol.
0.5 of hydroxyethyl cellulose.
3.0 parts of propylene glycol.
Citric acid 0.05.
Polyacrylamide methyl propane sulfonic acid 0.5.
The water residual mass ratio is all water.
The raw materials are added according to the following process flow, and are uniformly stirred, and the method comprises the following steps:
1) adding water into a stirring pot, starting stirring at a rotating speed of 30-35 RPM/mmin, and starting heating at a set temperature of 85 ℃.
2) Slowly adding the hydroxyethyl cellulose when the water temperature rises to 60-65 ℃, and stirring for 50-60 min.
3) Adding polyacrylamide methyl propane sulfonic acid; stirring for 30-40 min.
4) When the temperature reached 85 ℃, it was held for 30 min.
5) Starting cooling and cooling to below 45 ℃.
6) Mixing essence, propylene glycol and PEG-40 hydrogenated castor oil in advance; adding into a pot; adding phenoxyethanol and ethylhexyl glycerol, and stirring for 20 min.
7) Adding citric acid, and adjusting pH value.
8) And (5) qualified detection and discharging.
The invention has the advantages that 1, the macromolecular material is difficult to be absorbed by the skin of a human body relative to the cellulose material, so the retention time on the surface of the skin of the human body is greatly prolonged compared with the cellulose, thereby achieving the effect of prolonging the duration time of the lubricating property; 2. the addition of the polymer can delay the absorption speed of the skin; 3. the lubricant has long time, almost no reduction of the lubricating performance and no harm to human body.
Detailed Description
Example 1
1) 8315g of water is added into a stirring pot, stirring is started, the rotating speed is set to be 30-35 RPM/mmin, heating is started, and the temperature is set to be 85 ℃.
2) When the water temperature rises to 60-65 ℃, slowly adding 200g of hydroxyethyl cellulose, and stirring for 50-60 min.
3) Adding 100g of polyacrylamide methyl propane sulfonic acid; stirring for 30-40 min.
4) When the temperature reached 85 ℃, it was held for 30 min.
5) Starting cooling and cooling to below 45 ℃.
6) 50g of essence, 500g of propylene glycol and 200g of PEG-40 hydrogenated castor oil are mixed in advance; adding into a pot; adding 100g of phenoxyethanol and 20g of ethylhexyl glycerol, and stirring for 20 min.
7) 15g of citric acid was added to adjust the pH.
8) And (5) qualified detection and discharging.
Example 2
1) 9480g of water is added into a stirring pot, stirring is started, the rotating speed is set to be 30-35 RPM/mmin, heating is started, and the temperature is set to be 85 ℃.
2) When the water temperature rises to 60-65 ℃, 50g of hydroxyethyl cellulose is slowly added, and the mixture is stirred for 50-60 min.
3) Adding 50g of polyacrylamide methyl propane sulfonic acid; stirring for 30-40 min.
4) When the temperature reached 85 ℃, it was held for 30 min.
5) Starting cooling and cooling to below 45 ℃.
6) 10g of essence, 300g of propylene glycol and 50g of PEG-40 hydrogenated castor oil are mixed in advance; adding into a pot; adding 50g of phenoxyethanol and 5g of ethylhexyl glycerol, and stirring for 20 min.
7) 5g of citric acid was added to adjust the pH.
8) And (5) qualified detection and discharging.
Example 3
1) Adding 9185g of water into a stirring pot, starting stirring, setting the rotating speed at 30-35 RPM/mmin, and starting heating, setting the temperature at 85 ℃.
2) When the water temperature rises to 60-65 ℃, slowly adding 150g of hydroxyethyl cellulose, and stirring for 50-60 min.
3) Adding 80g of polyacrylamide methyl propane sulfonic acid; stirring for 30-40 min.
4) When the temperature reached 85 ℃, it was held for 30 min.
5) Starting cooling and cooling to below 45 ℃.
6) Mixing 30g of essence, 400g of propylene glycol and 150g of PEG-40 hydrogenated castor oil in advance; adding into a pot; adding 80g of phenoxyethanol and 15g of ethylhexyl glycerol, and stirring for 20 min.
7) 10g of citric acid was added to adjust the pH.
8) And (5) qualified detection and discharging.
The product of the invention adopts HSP-1180 which is a copolymer of acrylamide and methyl propane sulfonic acid. HSP-1180 is designed to provide a highly lubricious, longer lasting product during use, even at low concentrations. In this way, the effect is twofold, firstly, an elegant, aesthetically pleasing glide is felt by the consumer during use, and moreover, HSP-1180 will act as a secondary thickener, especially in hydroalcoholic systems resistant to viscosity increase. In addition, HSP 1180 contains sulfonic acid groups in its molecular structure. It is soluble in strong acids and bases (in which it can be effectively neutralized by a large number of basic cations). The invention utilizes the high molecular material which is difficult to be absorbed by the skin of the human body relative to the cellulose material, so the retention time on the surface of the skin of the human body is greatly prolonged compared with the cellulose, thereby achieving the effect of prolonging the duration time of the lubricating property; according to the invention, 0.5-1.0% of high molecular polymer is added in the product formula of the original lubricant of the company, so that the lasting time of the lubricating property of the product can be obviously improved, and the lubricating effect is also improved. The invention is suitable for related products with requirements on the silky property and the lubricating property.

Claims (4)

1. A lubricant produced by adopting high molecular polymer is characterized in that the mass ratio W/W% of the raw materials is as follows,
3.0-5.0% of glycerin;
PEG-40 hydrogenated castor oil 0.5-2.0;
0.1-0.5 of essence;
0.5-1.0 parts of phenoxyethanol;
0.05-0.2 of ethylhexyl glycerol;
0.5-2.0% of hydroxyethyl cellulose;
3.0-5.0 parts of propylene glycol;
0.05-0.15 of citric acid;
0.5-1.0 parts of polyacrylamide methyl propane sulfonic acid;
the water residual mass ratio is all water.
2. The lubricant produced by using a high molecular polymer according to claim 1, wherein the raw materials are contained in a mass ratio of W/W% as follows,
5.0 of glycerin;
PEG-40 hydrogenated Castor oil 2.0;
0.5 of essence;
1.0 parts of phenoxyethanol;
0.2 parts of ethylhexyl glycerol;
2.0 parts of hydroxyethyl cellulose;
5.0 parts of propylene glycol;
0.15 parts of citric acid;
polyacrylamide methyl propane sulfonic acid 1.0;
the water residual mass ratio is all water.
3. The lubricant produced by using a high molecular polymer according to claim 1, wherein the raw materials are contained in a mass ratio of W/W% as follows,
3.0 parts of glycerin;
0.5 of PEG-40 hydrogenated castor oil;
0.1 of essence;
0.5 parts of phenoxyethanol;
ethyl hexyl glycerol 0.05;
0.5 of hydroxyethyl cellulose;
3.0 parts of propylene glycol;
0.05 parts of citric acid;
polyacrylamide methyl propane sulfonic acid 0.5;
the water residual mass ratio is all water.
4. The lubricant produced by adopting the high molecular polymer according to the claim 1, 2 or 3, characterized in that the raw materials are added and uniformly stirred according to the following process flow, and the steps are as follows:
1) adding water into a stirring pot, starting stirring, and setting the rotating speed at 30-35 RPM/mmin, starting heating, and setting the temperature at 85 ℃;
2) slowly adding hydroxyethyl cellulose when the water temperature rises to 60-65 ℃, and stirring for 50-60 min;
3) adding polyacrylamide methyl propane sulfonic acid; stirring for 30-40 min;
4) when the temperature reaches 85 ℃, keeping for 30 min;
5) starting cooling, and cooling to below 45 ℃;
6) mixing essence, propylene glycol and PEG-40 hydrogenated castor oil in advance; adding into a pot; adding phenoxyethanol and ethylhexyl glycerol, and stirring for 20 min;
7) adding citric acid, and adjusting the pH value;
8) and (5) qualified detection and discharging.
CN201911248058.7A 2019-12-09 2019-12-09 Lubricant produced by adopting high-molecular polymer Pending CN110755696A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201911248058.7A CN110755696A (en) 2019-12-09 2019-12-09 Lubricant produced by adopting high-molecular polymer

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201911248058.7A CN110755696A (en) 2019-12-09 2019-12-09 Lubricant produced by adopting high-molecular polymer

Publications (1)

Publication Number Publication Date
CN110755696A true CN110755696A (en) 2020-02-07

Family

ID=69341283

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201911248058.7A Pending CN110755696A (en) 2019-12-09 2019-12-09 Lubricant produced by adopting high-molecular polymer

Country Status (1)

Country Link
CN (1) CN110755696A (en)

Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US20030203991A1 (en) * 2002-04-30 2003-10-30 Hydromer, Inc. Coating composition for multiple hydrophilic applications
CN102920615A (en) * 2011-08-08 2013-02-13 陈明智 Gum composition for external use on skin
CN103100115A (en) * 2012-04-28 2013-05-15 尹颖 Obstetric canal lubrication composition
CN104922055A (en) * 2014-03-19 2015-09-23 张益寿 Semifluid composition used for lubrication, moisture retention, disinfection and sterilization and application method thereof
CN109536132A (en) * 2018-11-27 2019-03-29 南通优护优家卫生用品有限公司 It can be applied to the thickener of cationic sterilised products

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US20030203991A1 (en) * 2002-04-30 2003-10-30 Hydromer, Inc. Coating composition for multiple hydrophilic applications
CN102920615A (en) * 2011-08-08 2013-02-13 陈明智 Gum composition for external use on skin
CN103100115A (en) * 2012-04-28 2013-05-15 尹颖 Obstetric canal lubrication composition
CN104922055A (en) * 2014-03-19 2015-09-23 张益寿 Semifluid composition used for lubrication, moisture retention, disinfection and sterilization and application method thereof
CN109536132A (en) * 2018-11-27 2019-03-29 南通优护优家卫生用品有限公司 It can be applied to the thickener of cationic sterilised products

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PB01 Publication
SE01 Entry into force of request for substantive examination
SE01 Entry into force of request for substantive examination
TA01 Transfer of patent application right

Effective date of registration: 20200407

Address after: 239000 northwest side of the intersection of Zhongxin Avenue and Lanzhou Road, Suchu modern industrial park, Chuzhou City, Anhui Province

Applicant after: Youhu Youjia Pharmaceutical (Chuzhou) Co.,Ltd.

Applicant after: NANTONG YOUHU YOUJIA HEALTH PRODUCTS CO.,LTD.

Address before: North Street Rugao city 226500 Jiangsu city of Nantong Province Yu Xian Lu No. 118

Applicant before: NANTONG YOUHU YOUJIA HEALTH PRODUCTS Co.,Ltd.

TA01 Transfer of patent application right
RJ01 Rejection of invention patent application after publication

Application publication date: 20200207

RJ01 Rejection of invention patent application after publication