CN107648071A - A kind of slim and graceful not mascara of the content of wax and preparation method thereof - Google Patents
A kind of slim and graceful not mascara of the content of wax and preparation method thereof Download PDFInfo
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- CN107648071A CN107648071A CN201711038997.XA CN201711038997A CN107648071A CN 107648071 A CN107648071 A CN 107648071A CN 201711038997 A CN201711038997 A CN 201711038997A CN 107648071 A CN107648071 A CN 107648071A
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- Prior art keywords
- mascara
- parts
- graceful
- slim
- wax
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/81—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions involving only carbon-to-carbon unsaturated bonds
- A61K8/817—Compositions of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by a single or double bond to nitrogen or by a heterocyclic ring containing nitrogen; Compositions or derivatives of such polymers, e.g. vinylimidazol, vinylcaprolactame, allylamines (Polyquaternium 6)
- A61K8/8176—Homopolymers of N-vinyl-pyrrolidones. Compositions of derivatives of such polymers
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/60—Sugars; Derivatives thereof
- A61K8/604—Alkylpolyglycosides; Derivatives thereof, e.g. esters
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
- A61K8/731—Cellulose; Quaternized cellulose derivatives
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/81—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions involving only carbon-to-carbon unsaturated bonds
- A61K8/8141—Compositions of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides or nitriles thereof; Compositions of derivatives of such polymers
- A61K8/8152—Homopolymers or copolymers of esters, e.g. (meth)acrylic acid esters; Compositions of derivatives of such polymers
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q1/00—Make-up preparations; Body powders; Preparations for removing make-up
- A61Q1/02—Preparations containing skin colorants, e.g. pigments
- A61Q1/10—Preparations containing skin colorants, e.g. pigments for eyes, e.g. eyeliner, mascara
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/20—Chemical, physico-chemical or functional or structural properties of the composition as a whole
- A61K2800/30—Characterized by the absence of a particular group of ingredients
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- Life Sciences & Earth Sciences (AREA)
- Health & Medical Sciences (AREA)
- Animal Behavior & Ethology (AREA)
- General Health & Medical Sciences (AREA)
- Public Health (AREA)
- Veterinary Medicine (AREA)
- Birds (AREA)
- Epidemiology (AREA)
- Cosmetics (AREA)
Abstract
The invention discloses a kind of mascara of the slim and graceful not content of wax, the composition of following parts by weight is included：32~36 parts of acrylate copolymer, 4~6 parts of ethyl cellulose, 0.5~1.5 part of polyvinylpyrrolidone, 0.5~1.5 part of Surfhope SE Cosme C 1216,0.3~0.5 part of hydroxyethyl cellulose.Without wax stock in mascara formulation of the present invention, sense of not bearing a heavy burden, quality is slim and graceful, and skin sense is soft and moist, adornment effect is lasting, comfort is strong., can be low temperature emulsified after oil phase and Aqueous Phase Raw Material stir respectively meanwhile invention additionally discloses a kind of preparation method of the mascara, this formula is easy to make.
Description
Technical field
The present invention relates to a kind of mascara and preparation method thereof, the especially a kind of slim and graceful not mascara of the content of wax and its preparation
Method.
Background technology
Mascara is product more commonly used when female friend makes up.But using and manufacturing process among, exist with
Lower problem：(1) conventional mascara cream, eyelashes shape is moulded using substantial amounts of wax, skin sense is dry and astringent, and quality is harder, and comfort compares
Difference；(2) after conventional mascara cream makeup, eyelashes can be bent to side, and formation interlocks, it appears not natural enough；(3) conventional mascara cream needs
To be emulsified in high temperature, energy consumption is larger.
The content of the invention
Based on this, a kind of slim and graceful not content of wax is provided it is an object of the invention to overcome above-mentioned the deficiencies in the prior art part
Mascara.
To achieve the above object, the technical solution used in the present invention is：A kind of mascara of the slim and graceful not content of wax, comprising with
The composition of lower parts by weight：32~36 parts of acrylate copolymer, 4~6 parts of ethyl cellulose, polyvinylpyrrolidone 0.5~1.5
Part, 0.5~1.5 part of Surfhope SE Cosme C 1216,0.3~0.5 part of hydroxyethyl cellulose.
Not waxy feeds in the formula of mascara of the present invention, sense of not bearing a heavy burden, quality is slim and graceful, using ethyl cellulose
To be molded, skin sense is soft and moist, using ethyl cellulose and the adhesive force of hair, to prepare a kind of strong mascara of comfort；Due to third
Olefine acid ester polymer can form long-acting waterproof membrane on eyelashes；Ethyl cellulose has good affinity and attachment to eyelashes
Power, so product has good water resistance, make adornment effect lasting；Surfhope SE Cosme C 1216 has very strong emulsifying ability, is removing ornaments and formal dress
When, as long as will be dissolved in water, be washed by water with water or make up remover rubbing a moment, lotion.
Preferably, the acrylate copolymer, ethyl cellulose, the weight ratio of polyvinylpyrrolidone are：Acrylic acid
Ester copolymer：Ethyl cellulose：Polyvinylpyrrolidone=34：5：1.
Present inventor has found by substantial amounts of creative experiment, above-mentioned weight than three kinds of compositions compound, Ke Yijin
One step Synergistic, assign the mascara more longlasting waterproof efficacy.
Preferably, the mascara includes the composition of following parts by weight：34 parts of acrylate copolymer, ethyl cellulose 5
Part, 1 part of polyvinylpyrrolidone, 1 part of Surfhope SE Cosme C 1216,0.4 part of hydroxyethyl cellulose.The eyelashes of mentioned component and content
Cream, quality is slimmer and more graceful, and skin sense is more soft and moist, and waterproof is more lasting.
Preferably, the acrylate copolymer is COVACRYL MS11.
Preferably, the mascara also includes the solvent of following parts by weight：20~25 parts of deionized water, 8~12 parts of ethanol.
Preferably, the mascara also includes the composition of following parts by weight：0.5~1.5 part of butanediol, isostearic acid 9~
11 parts.The butanediol is NMF, assigns the mascara preferable moisture-keeping efficacy, and the isostearic acid is moisturizing agent, is assigned
The mascara is given preferably to moisten effect.
Preferably, the mascara also includes the PE9010 of 0.5~0.7 parts by weight.The PE9010 has preferably anti-
Rotten effect.
Preferably, the mascara also includes the colorant of 11~13 parts by weight, and the colorant is iron oxide black.
Meanwhile invention additionally discloses a kind of preparation method of the mascara, comprise the following steps：
1) water, Surfhope SE Cosme C 1216 are mixed in container A, is heated with stirring to 85 degrees Celsius, is uniformly dispersed, then cool
It is standby to 25 degrees Celsius of normal temperature；
2) polyvinylpyrrolidone, hydroxyethyl cellulose, butanediol, PE9010 are added in container A, are dispersed with stirring
It is even；
3) after being well mixed ethyl cellulose, ethanol, isostearic acid, it is added in container A, emulsifying；
4) iron oxide black is added in container A, homogeneous；
5) acrylate copolymer is added in container A, stirred；
6) normal temperature is sealed up for safekeeping, in case being filled into mascara packaging material.
Relative to prior art, beneficial effects of the present invention are：
Without wax stock in mascara formulation of the present invention, sense of not bearing a heavy burden, quality is slim and graceful.This patent uses ethyl cellulose usually
Shaping, skin sense is soft and moist, using ethyl cellulose and the adhesive force of hair, to prepare a kind of strong mascara of comfort.
Because acrylate polymer can form long-acting waterproof membrane on eyelashes；Ethyl cellulose has well to eyelashes
Affinity and adhesive force, so product has good water resistance, make adornment effect lasting, after tested, after lotion shaping, in water
Immersion will not fall off for 2 hours；Surfhope SE Cosme C 1216 has very strong emulsifying ability, in makeup removing, as long as being crumpled with water or make up remover
For a moment, lotion will be dissolved in water, washed by water.In addition, this formula is easy to make, oil phase and Aqueous Phase Raw Material stir respectively
, can be low temperature emulsified after even.
Embodiment
To better illustrate the object, technical solutions and advantages of the present invention, below in conjunction with specific embodiment to the present invention
It is described further.
Embodiment 1
A kind of embodiment of the slim and graceful not mascara of the content of wax of the present invention, mascara described in the present embodiment includes following heavy
Measure the composition of part：
34 parts of acrylate copolymer (COVACRYL MS11), 5 parts of ethyl cellulose, 1 part of polyvinylpyrrolidone, sugarcane
Sugared 1 part of laurate, 0.4 part of hydroxyethyl cellulose, 24.5 parts of deionized water, 10 parts of ethanol, 1 part of butanediol, isostearic acid 10
Part, 0.6 part of PE9010,12 parts of colorant (iron oxide black).
The preparation method of mascara described in the present embodiment is：
1) water, Surfhope SE Cosme C 1216 are mixed in container A, is heated with stirring to 85 degrees Celsius, is uniformly dispersed, then cool
It is standby to 25 degrees Celsius of normal temperature；
2) polyvinylpyrrolidone, hydroxyethyl cellulose, butanediol, PE9010 are added in container A, are dispersed with stirring
It is even；
3) after being well mixed ethyl cellulose, ethanol, isostearic acid, it is added in container A, emulsifying；
4) iron oxide black is added in container A, homogeneous；
5) film forming agent COVACRYL MS11 are added in container A, stirred；
6) normal temperature is sealed up for safekeeping, in case being filled into mascara packaging material.
Embodiment 2
A kind of embodiment of the slim and graceful not mascara of the content of wax of the present invention, mascara described in the present embodiment includes following heavy
Measure the composition of part：
32 parts of acrylate copolymer (COVACRYL MS11), 4 parts of ethyl cellulose, 0.5 part of polyvinylpyrrolidone,
0.5 part of Surfhope SE Cosme C 1216,0.3 part of hydroxyethyl cellulose, 20 parts of deionized water, 8 parts of ethanol, 0.5 part of butanediol, isostearic acid
9 parts, 0.5 part of PE9010,11 parts of colorant (iron oxide black).
The preparation method of mascara described in the present embodiment is：
1) water, Surfhope SE Cosme C 1216 are mixed in container A, is heated with stirring to 85 degrees Celsius, is uniformly dispersed, then cool
It is standby to 25 degrees Celsius of normal temperature；
2) polyvinylpyrrolidone, hydroxyethyl cellulose, butanediol, PE9010 are added in container A, are dispersed with stirring
It is even；
3) after being well mixed ethyl cellulose, ethanol, isostearic acid, it is added in container A, emulsifying；
4) iron oxide black is added in container A, homogeneous；
5) film forming agent COVACRYL MS11 are added in container A, stirred；
6) normal temperature is sealed up for safekeeping, in case being filled into mascara packaging material.
Embodiment 3
A kind of embodiment of the slim and graceful not mascara of the content of wax of the present invention, mascara described in the present embodiment includes following heavy
Measure the composition of part：
36 parts of acrylate copolymer (COVACRYL MS11), 6 parts of ethyl cellulose, 1.5 parts of polyvinylpyrrolidone,
1.5 parts of Surfhope SE Cosme C 1216,0.5 part of hydroxyethyl cellulose, 25 parts of deionized water, 12 parts of ethanol, 1.5 parts of butanediol, different tristearin
11 parts of acid, 0.7 part of PE9010,13 parts of colorant (iron oxide black).
The preparation method of mascara described in the present embodiment is：
1) water, Surfhope SE Cosme C 1216 are mixed in container A, is heated with stirring to 85 degrees Celsius, is uniformly dispersed, then cool
It is standby to 25 degrees Celsius of normal temperature；
2) polyvinylpyrrolidone, hydroxyethyl cellulose, butanediol, PE9010 are added in container A, are dispersed with stirring
It is even；
3) after being well mixed ethyl cellulose, ethanol, isostearic acid, it is added in container A, emulsifying；
4) iron oxide black is added in container A, homogeneous；
5) film forming agent COVACRYL MS11 are added in container A, stirred；
6) normal temperature is sealed up for safekeeping, in case being filled into mascara packaging material.
Embodiment 4
Waterproof lasting effects are verified
The present embodiment sets experimental group 1~3 and control group 1~6, and experimental group 1~3 is to be prepared in the embodiment of the present invention 1~3
Obtained mascara, except three kinds of acrylate copolymer, ethyl cellulose, polyvinylpyrrolidone compositions in control group 1~6
Weight is outer than different, and other compositions are same as Example 1, in addition, in every group of experiment, acrylate copolymer, ethyl cellulose
Element, total content of the polyvinylpyrrolidone three in mascara are identicals, and simply the ratio of three is different, specific control group
Acrylate copolymer, ethyl cellulose, the parts by weight content of three kinds of compositions of polyvinylpyrrolidone are as shown in table 1 in 1~6：
Acrylate copolymer, ethyl cellulose, three kinds of polyvinylpyrrolidone in the control group mascara of table 1
The weight ratio of composition
Waterproof effect is tested：Mascara in embodiment 1~3 and control group 1~6 is spread evenly across plastics false eyelashes
On, put in water at normal temperatures and soak, the time that observation mascara comes off, as a result as shown in table 2：
Hold adornment measure of merit：Mascara in embodiment 1~3 and control group 1~6 is spread evenly across plastics false eyelashes
On, the time of observation mascara dizziness, as a result as shown in table 2：
The mascara of table 2 holds shape waterproof test result
| Water-proofing time | Hold the adornment time | |
| Experimental group 1 | 2.5 hour | 9 hours |
| Experimental group 2 | 1.7 hour | 7.5 hour |
| Experimental group 3 | 1.8 hour | 8 hours |
| Control group 1 | 0.5 hour | 2 hours |
| Control group 2 | 0.3 hour | 1 hour |
| Control group 3 | 0.2 hour | 0.5 hour |
| Control group 4 | 1.0 hour | 5 hours |
| Control group 5 | 0.6 hour | 2 hours |
| Control group 6 | 0.8 hour | 3.5 hour |
As seen from Table 2, acrylate copolymer, ethyl cellulose, poly- second are comprised only in the mascara of control group 1~6
One kind in three kinds of compositions of alkene pyrrolidone, two kinds, hold adornment effect without good waterproof.And the mascara of experimental group 1~3
Containing three kinds of compositions, there is good waterproof to hold adornment effect.Thus it is provable, in mascara of the invention, acrylic ester copolymer
Three kinds of thing, ethyl cellulose, polyvinylpyrrolidone compositions have the function that to mutually promote, mutually cooperateed with, and can play significantly
Waterproof hold adornment effect.
Finally, it should be noted that the above embodiments are merely illustrative of the technical solutions of the present invention rather than the present invention is protected
The limitation of scope is protected, although being explained in detail with reference to preferred embodiment to the present invention, one of ordinary skill in the art should
Understand, technical scheme can be modified or equivalent substitution, without departing from the essence of technical solution of the present invention
And scope.
Claims (9)
1. a kind of mascara of the slim and graceful not content of wax, it is characterised in that include the composition of following parts by weight：Acrylate copolymer 32
~36 parts, 4~6 parts of ethyl cellulose, 0.5~1.5 part of polyvinylpyrrolidone, 0.5~1.5 part of Surfhope SE Cosme C 1216, hydroxyl second
0.3~0.5 part of base cellulose.
2. the mascara of the slim and graceful not content of wax as claimed in claim 1, it is characterised in that the acrylate copolymer, ethyl
Cellulose, the weight ratio of polyvinylpyrrolidone are：Acrylate copolymer：Ethyl cellulose：Polyvinylpyrrolidone=34：
5：1.
3. the mascara of the slim and graceful not content of wax as claimed in claim 1, it is characterised in that include the composition of following parts by weight：Third
34 parts of olefin(e) acid ester copolymer, 5 parts of ethyl cellulose, 1 part of polyvinylpyrrolidone, 1 part of Surfhope SE Cosme C 1216, hydroxyethyl cellulose
0.4 part.
4. the mascara of the not content of wax as claimed in claim 1 slim and graceful, it is characterised in that the acrylate copolymer is
COVACRYL MS11。
5. the mascara of the slim and graceful not content of wax as claimed in claim 1, it is characterised in that also include the solvent of following parts by weight：
20~25 parts of deionized water, 8~12 parts of ethanol.
6. the mascara of the slim and graceful not content of wax as described in any one of Claims 1 to 5, it is characterised in that also comprising following weight
The composition of part：0.5~1.5 part of butanediol, 9~11 parts of isostearic acid.
7. the mascara of the slim and graceful not content of wax as described in any one of Claims 1 to 5, it is characterised in that also comprising 0.5~0.7
The PE9010 of parts by weight.
8. the mascara of the slim and graceful not content of wax as described in any one of Claims 1 to 5, it is characterised in that also comprising 11~13 weights
The colorant of part is measured, the colorant is iron oxide black.
A kind of 9. preparation method of slim and graceful not mascara of the content of wax as described in any one of claim 1~8, it is characterised in that
Comprise the following steps：
1) water, Surfhope SE Cosme C 1216 are mixed in container A, is heated with stirring to 85 degrees Celsius, is uniformly dispersed, be then cooled to often
25 degrees Celsius of temperature is standby；
2) polyvinylpyrrolidone, hydroxyethyl cellulose, butanediol, PE9010 are added in container A, are dispersed with stirring uniformly；
3) after being well mixed ethyl cellulose, ethanol, isostearic acid, it is added in container A, emulsifying；
4) iron oxide black is added in container A, homogeneous；
5) acrylate copolymer is added in container A, stirred；
6) normal temperature is sealed up for safekeeping, in case being filled into mascara packaging material.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201711038997.XA CN107648071B (en) | 2017-10-27 | 2017-10-27 | Light and wax-free mascara and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201711038997.XA CN107648071B (en) | 2017-10-27 | 2017-10-27 | Light and wax-free mascara and preparation method thereof |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN107648071A true CN107648071A (en) | 2018-02-02 |
| CN107648071B CN107648071B (en) | 2020-10-23 |
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201711038997.XA Expired - Fee Related CN107648071B (en) | 2017-10-27 | 2017-10-27 | Light and wax-free mascara and preparation method thereof |
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| Country | Link |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109662914A (en) * | 2019-02-18 | 2019-04-23 | 广州卡迪莲化妆品有限公司 | A kind of no wax mascara and preparation method thereof |
| CN112618388A (en) * | 2021-01-06 | 2021-04-09 | 福建东亮生物科技有限公司 | Low-heavy metal eye shadow formula and processing technology |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1494891A (en) * | 2002-09-06 | 2004-05-12 | 莱雅公司 | Waxless washing-free face-beautifying keratin fibre nursing or cosmetic composition material |
| WO2017110872A1 (en) * | 2015-12-25 | 2017-06-29 | 三菱鉛筆株式会社 | Liquid cosmetic composition |
-
2017
- 2017-10-27 CN CN201711038997.XA patent/CN107648071B/en not_active Expired - Fee Related
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1494891A (en) * | 2002-09-06 | 2004-05-12 | 莱雅公司 | Waxless washing-free face-beautifying keratin fibre nursing or cosmetic composition material |
| WO2017110872A1 (en) * | 2015-12-25 | 2017-06-29 | 三菱鉛筆株式会社 | Liquid cosmetic composition |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109662914A (en) * | 2019-02-18 | 2019-04-23 | 广州卡迪莲化妆品有限公司 | A kind of no wax mascara and preparation method thereof |
| CN109662914B (en) * | 2019-02-18 | 2021-11-26 | 广州卡迪莲化妆品科技有限公司 | Soap-based wax-free mascara and preparation method thereof |
| CN112618388A (en) * | 2021-01-06 | 2021-04-09 | 福建东亮生物科技有限公司 | Low-heavy metal eye shadow formula and processing technology |
Also Published As
| Publication number | Publication date |
|---|---|
| CN107648071B (en) | 2020-10-23 |
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