CN107648071B - Light and wax-free mascara and preparation method thereof - Google Patents
Light and wax-free mascara and preparation method thereof Download PDFInfo
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- CN107648071B CN107648071B CN201711038997.XA CN201711038997A CN107648071B CN 107648071 B CN107648071 B CN 107648071B CN 201711038997 A CN201711038997 A CN 201711038997A CN 107648071 B CN107648071 B CN 107648071B
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- mascara
- light
- wax
- acrylate copolymer
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Classifications
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/81—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions involving only carbon-to-carbon unsaturated bonds
- A61K8/817—Compositions of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by a single or double bond to nitrogen or by a heterocyclic ring containing nitrogen; Compositions or derivatives of such polymers, e.g. vinylimidazol, vinylcaprolactame, allylamines (Polyquaternium 6)
- A61K8/8176—Homopolymers of N-vinyl-pyrrolidones. Compositions of derivatives of such polymers
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/60—Sugars; Derivatives thereof
- A61K8/604—Alkylpolyglycosides; Derivatives thereof, e.g. esters
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
- A61K8/731—Cellulose; Quaternized cellulose derivatives
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/81—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions involving only carbon-to-carbon unsaturated bonds
- A61K8/8141—Compositions of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides or nitriles thereof; Compositions of derivatives of such polymers
- A61K8/8152—Homopolymers or copolymers of esters, e.g. (meth)acrylic acid esters; Compositions of derivatives of such polymers
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q1/00—Make-up preparations; Body powders; Preparations for removing make-up
- A61Q1/02—Preparations containing skin colorants, e.g. pigments
- A61Q1/10—Preparations containing skin colorants, e.g. pigments for eyes, e.g. eyeliner, mascara
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/20—Chemical, physico-chemical or functional or structural properties of the composition as a whole
- A61K2800/30—Characterized by the absence of a particular group of ingredients
Abstract
The invention discloses light and wax-free mascara, which comprises the following components in parts by weight: 32-36 parts of acrylate copolymer, 4-6 parts of ethyl cellulose, 0.5-1.5 parts of polyvinylpyrrolidone, 0.5-1.5 parts of sucrose laurate and 0.3-0.5 part of hydroxyethyl cellulose. The mascara formula disclosed by the invention is free of wax raw materials, free of heavy feeling, light in texture, soft and moist in skin feeling, lasting in makeup effect and strong in comfort. Meanwhile, the invention also discloses a preparation method of the mascara, the formula is convenient to prepare, and the oil-phase raw materials and the water-phase raw materials can be emulsified at low temperature after being respectively stirred uniformly.
Description
Technical Field
The invention relates to mascara and a preparation method thereof, in particular to light and wax-free mascara and a preparation method thereof.
Background
Mascara is a product which is commonly used when women make up. However, in the using and manufacturing process, the following problems exist: (1) the traditional mascara adopts a large amount of wax to shape the shape of eyelashes, and has dry and astringent skin feel, hard texture and poor comfort; (2) after the traditional mascara is dressed up, eyelashes can be bent aside to form interlacing, which is not natural enough; (3) the traditional mascara needs to be emulsified at high temperature, and the energy consumption is large.
Disclosure of Invention
In view of this, the object of the present invention is to overcome the above-mentioned disadvantages of the prior art and to provide a light mascara free of wax.
In order to achieve the purpose, the technical scheme adopted by the invention is as follows: a light and wax-free mascara comprises the following components in parts by weight: 32-36 parts of acrylate copolymer, 4-6 parts of ethyl cellulose, 0.5-1.5 parts of polyvinylpyrrolidone, 0.5-1.5 parts of sucrose laurate and 0.3-0.5 part of hydroxyethyl cellulose.
The mascara formula disclosed by the invention does not contain wax raw materials, has no heavy feeling and light texture, is formed by adopting ethyl cellulose, has soft skin feeling, and is prepared by utilizing the adhesive force of the ethyl cellulose and hair; because the acrylate polymer can form a long-lasting waterproof film on eyelashes; the ethyl cellulose has good affinity and adhesive force to eyelashes, so that the product has good water resistance and lasting makeup effect; the sucrose laurate has strong emulsifying power, and when makeup is removed, the paste body can be dissolved in water and washed away by the water as long as the paste body is kneaded for a moment by water or makeup removing liquid.
Preferably, the weight ratio of the acrylate copolymer to the ethyl cellulose to the polyvinylpyrrolidone is: acrylate copolymer: ethyl cellulose: polyvinylpyrrolidone ═ 34: 5: 1.
through a large number of creative tests, the inventor of the application finds that the compounding of the three components in the weight ratio can further realize the synergistic effect, and the mascara is endowed with a more lasting waterproof effect.
Preferably, the mascara comprises the following ingredients in parts by weight: 34 parts of acrylate copolymer, 5 parts of ethyl cellulose, 1 part of polyvinylpyrrolidone, 1 part of sucrose laurate and 0.4 part of hydroxyethyl cellulose. The mascara with the components and the content has lighter texture, softer skin feel and longer water resistance.
Preferably, the acrylate copolymer is COVACRYL MS 11.
Preferably, the mascara further comprises the following solvents in parts by weight: 20-25 parts of deionized water and 8-12 parts of ethanol.
Preferably, the mascara further comprises the following ingredients in parts by weight: 0.5-1.5 parts of butanediol and 9-11 parts of isostearic acid. The butanediol is used as a humectant and endows the mascara with a better moisturizing effect, and the isostearic acid is used as a moisturizer and endows the mascara with a better moisturizing effect.
Preferably, the mascara further comprises 0.5-0.7 weight part of PE 9010. The PE9010 has a good anticorrosion effect.
Preferably, the mascara further comprises 11-13 parts by weight of a colorant, and the colorant is black iron oxide.
Meanwhile, the invention also discloses a preparation method of the mascara, which comprises the following steps:
1) mixing water and sucrose laurate in a container A, stirring and heating to 85 ℃, uniformly dispersing, and then cooling to the normal temperature of 25 ℃ for later use;
2) adding polyvinylpyrrolidone, hydroxyethyl cellulose, butanediol and PE9010 into the container A, and uniformly stirring and dispersing;
3) mixing ethyl cellulose, ethanol and isostearic acid uniformly, adding into a container A, homogenizing and emulsifying;
4) adding iron oxide black into the container A, and homogenizing;
5) adding the acrylate copolymer into the container A, and uniformly stirring;
6) and sealing at normal temperature for filling into the mascara package.
Compared with the prior art, the invention has the beneficial effects that:
the mascara formula disclosed by the invention is free of wax raw materials, free of heavy feeling and light in texture. This patent adopts ethyl cellulose element shaping, and the skin feels soft moist, utilizes the adhesive force of ethyl fibre and hair, prepares a mascara that the comfort is strong.
Because the acrylate polymer can form a long-lasting waterproof film on eyelashes; the ethyl cellulose has good affinity and adhesive force to eyelashes, so that the product has good water resistance and lasting makeup effect, and the cream does not fall off after being soaked in water for 2 hours after being tested to be formed; the sucrose laurate has strong emulsifying power, and when makeup is removed, the paste body can be dissolved in water and washed away by the water as long as the paste body is kneaded for a moment by water or makeup removing liquid. In addition, the formula is convenient to prepare, and the oil phase raw material and the water phase raw material can be emulsified at low temperature after being respectively stirred uniformly.
Detailed Description
To better illustrate the objects, aspects and advantages of the present invention, the present invention will be further described with reference to specific examples.
Example 1
An example of a light, wax-free mascara according to the present invention includes the following ingredients in parts by weight:
34 parts of acrylate copolymer (COVACRYL MS11), 5 parts of ethyl cellulose, 1 part of polyvinylpyrrolidone, 1 part of sucrose laurate, 0.4 part of hydroxyethyl cellulose, 24.5 parts of deionized water, 10 parts of ethanol, 1 part of butanediol, 10 parts of isostearic acid, 90100.6 parts of PE and 12 parts of pigment (black iron oxide).
The preparation method of the mascara according to the embodiment comprises the following steps:
1) mixing water and sucrose laurate in a container A, stirring and heating to 85 ℃, uniformly dispersing, and then cooling to the normal temperature of 25 ℃ for later use;
2) adding polyvinylpyrrolidone, hydroxyethyl cellulose, butanediol and PE9010 into the container A, and uniformly stirring and dispersing;
3) mixing ethyl cellulose, ethanol and isostearic acid uniformly, adding into a container A, homogenizing and emulsifying;
4) adding iron oxide black into the container A, and homogenizing;
5) adding a film forming agent COVACRYL MS11 into a container A, and uniformly stirring;
6) and sealing at normal temperature for filling into the mascara package.
Example 2
An example of a light, wax-free mascara according to the present invention includes the following ingredients in parts by weight:
32 parts of acrylate copolymer (COVACRYL MS11), 4 parts of ethyl cellulose, 0.5 part of polyvinylpyrrolidone, 0.5 part of sucrose laurate, 0.3 part of hydroxyethyl cellulose, 20 parts of deionized water, 8 parts of ethanol, 0.5 part of butanediol, 9 parts of isostearic acid, 90100.5 parts of PE (polyethylene glycol) and 11 parts of pigment (black iron oxide).
The preparation method of the mascara according to the embodiment comprises the following steps:
1) mixing water and sucrose laurate in a container A, stirring and heating to 85 ℃, uniformly dispersing, and then cooling to the normal temperature of 25 ℃ for later use;
2) adding polyvinylpyrrolidone, hydroxyethyl cellulose, butanediol and PE9010 into the container A, and uniformly stirring and dispersing;
3) mixing ethyl cellulose, ethanol and isostearic acid uniformly, adding into a container A, homogenizing and emulsifying;
4) adding iron oxide black into the container A, and homogenizing;
5) adding a film forming agent COVACRYL MS11 into a container A, and uniformly stirring;
6) and sealing at normal temperature for filling into the mascara package.
Example 3
An example of a light, wax-free mascara according to the present invention includes the following ingredients in parts by weight:
36 parts of acrylate copolymer (COVACRYL MS11), 6 parts of ethyl cellulose, 1.5 parts of polyvinylpyrrolidone, 1.5 parts of sucrose laurate, 0.5 part of hydroxyethyl cellulose, 25 parts of deionized water, 12 parts of ethanol, 1.5 parts of butanediol, 11 parts of isostearic acid, 90100.7 parts of PE (polyethylene glycol) and 13 parts of pigment (iron oxide black).
The preparation method of the mascara according to the embodiment comprises the following steps:
1) mixing water and sucrose laurate in a container A, stirring and heating to 85 ℃, uniformly dispersing, and then cooling to the normal temperature of 25 ℃ for later use;
2) adding polyvinylpyrrolidone, hydroxyethyl cellulose, butanediol and PE9010 into the container A, and uniformly stirring and dispersing;
3) mixing ethyl cellulose, ethanol and isostearic acid uniformly, adding into a container A, homogenizing and emulsifying;
4) adding iron oxide black into the container A, and homogenizing;
5) adding a film forming agent COVACRYL MS11 into a container A, and uniformly stirring;
6) and sealing at normal temperature for filling into the mascara package.
Example 4
Proof of water-proof lasting effect
In this embodiment, experimental groups 1 to 3 and control groups 1 to 6 are provided, the experimental groups 1 to 3 are mascaras prepared in the embodiments 1 to 3 of the present invention, the control groups 1 to 6 are the same as the embodiment 1 except for the weight ratios of the three components of the acrylate copolymer, the ethylcellulose and the polyvinylpyrrolidone, and in addition, in each group of experiments, the total content of the acrylate copolymer, the ethylcellulose and the polyvinylpyrrolidone in the mascaras is the same except for the different ratios of the three components, and the weight parts of the three components of the acrylate copolymer, the ethylcellulose and the polyvinylpyrrolidone in the specific control groups 1 to 6 are as shown in table 1:
TABLE 1 three kinds of acrylate copolymer, ethyl cellulose and polyvinylpyrrolidone in mascara of control group
Weight ratio of the ingredients
And (3) testing the waterproof effect: the mascaras of examples 1 to 3 and control groups 1 to 6 were uniformly coated on plastic false eyelashes, immersed in water at normal temperature, and the time for which the mascaras fell off was observed, with the results shown in table 2:
and (3) testing the makeup effect: the mascaras of examples 1 to 3 and control groups 1 to 6 were uniformly applied to plastic eyelash extensions, and the dizzy time of the mascaras was observed, and the results are shown in table 2:
TABLE 2 Mascara hold-on waterproofing test results
| Time to water | Make-up time | |
| Experimental group 1 | 2.5 hours | 9 hours |
| Experimental group 2 | 1.7 hours | 7.5 hours |
| Experimental group 3 | 1.8 hours | 8 hours |
| Control group 1 | 0.5 hour | 2 hours |
| Control group 2 | 0.3 hour | 1 hour |
| Control group 3 | 0.2 hour | 0.5 hour |
| Control group 4 | 1.0 hour | 5 hours |
| Control group 5 | 0.6 hour | 2 hours |
| Control group 6 | 0.8 hour | 3.5 hours |
As can be seen from Table 2, the mascaras of the control groups 1 to 6 only contain one or two of three components of acrylate copolymer, ethyl cellulose and polyvinylpyrrolidone, and do not have good waterproof makeup-holding effect. The mascara in the experimental groups 1-3 contains three components, and has a good waterproof makeup-holding effect. Therefore, the mascara disclosed by the invention has the effects of mutual promotion and mutual synergy of the three components, namely the acrylate copolymer, the ethyl cellulose and the polyvinylpyrrolidone, and can achieve a remarkable waterproof makeup-holding effect.
Finally, it should be noted that the above embodiments are only used for illustrating the technical solutions of the present invention and not for limiting the protection scope of the present invention, and although the present invention is described in detail with reference to the preferred embodiments, it should be understood by those skilled in the art that modifications or equivalent substitutions can be made on the technical solutions of the present invention without departing from the spirit and scope of the technical solutions of the present invention.
Claims (6)
1. A light and wax-free mascara is characterized by comprising the following components in parts by weight: 32-36 parts of acrylate copolymer, 4-6 parts of ethyl cellulose, 0.5-1.5 parts of polyvinylpyrrolidone, 0.5-1.5 parts of sucrose laurate, 0.3-0.5 part of hydroxyethyl cellulose and 0.7 part of PE 90100.5; the weight ratio of the acrylate copolymer to the ethyl cellulose to the polyvinylpyrrolidone is as follows: acrylate copolymer: ethyl cellulose: polyvinylpyrrolidone ═ 34: 5: 1, the acrylate copolymer is COVACRYL MS 11.
2. A light, wax-free mascara according to claim 1, comprising the following ingredients in parts by weight: 34 parts of acrylate copolymer, 5 parts of ethyl cellulose, 1 part of polyvinylpyrrolidone, 1 part of sucrose laurate and 0.4 part of hydroxyethyl cellulose.
3. A light, wax-free mascara according to claim 1, further comprising the following parts by weight of solvent: 20-25 parts of deionized water and 8-12 parts of ethanol.
4. A light, non-waxy mascara according to any of claims 1-3, further comprising the following ingredients in parts by weight: 0.5-1.5 parts of butanediol and 9-11 parts of isostearic acid.
5. A light, non-waxy mascara according to any one of claims 1 to 3, further comprising 11 to 13 parts by weight of a colorant, wherein said colorant is black iron oxide.
6. A method of making a light, wax-free mascara as claimed in any one of claims 1 to 5, comprising the steps of:
1) mixing water and sucrose laurate in a container A, stirring and heating to 85 ℃, uniformly dispersing, and then cooling to the normal temperature of 25 ℃ for later use;
2) adding polyvinylpyrrolidone, hydroxyethyl cellulose, butanediol and PE9010 into the container A, and uniformly stirring and dispersing;
3) mixing ethyl cellulose, ethanol and isostearic acid uniformly, adding into a container A, homogenizing and emulsifying;
4) adding iron oxide black into the container A, and homogenizing;
5) adding the acrylate copolymer into the container A, and uniformly stirring;
6) and sealing at normal temperature for filling into the mascara package.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201711038997.XA CN107648071B (en) | 2017-10-27 | 2017-10-27 | Light and wax-free mascara and preparation method thereof |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201711038997.XA CN107648071B (en) | 2017-10-27 | 2017-10-27 | Light and wax-free mascara and preparation method thereof |
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| Publication Number | Publication Date |
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| CN107648071A CN107648071A (en) | 2018-02-02 |
| CN107648071B true CN107648071B (en) | 2020-10-23 |
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| CN201711038997.XA Expired - Fee Related CN107648071B (en) | 2017-10-27 | 2017-10-27 | Light and wax-free mascara and preparation method thereof |
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Families Citing this family (2)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN109662914B (en) * | 2019-02-18 | 2021-11-26 | 广州卡迪莲化妆品科技有限公司 | Soap-based wax-free mascara and preparation method thereof |
| CN112618388A (en) * | 2021-01-06 | 2021-04-09 | 福建东亮生物科技有限公司 | Low-heavy metal eye shadow formula and processing technology |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| FR2844184B1 (en) * | 2002-09-06 | 2006-05-26 | Oreal | COSMETIC COMPOSITION FOR MAKE-UP OR CARE OF KERATINOUS FIBERS WITHOUT WAX |
| WO2017110872A1 (en) * | 2015-12-25 | 2017-06-29 | 三菱鉛筆株式会社 | Liquid cosmetic composition |
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Granted publication date: 20201023 Termination date: 20211027 |