KR101771421B1 - Water Dispersed Type Makeup Cosmetic Composition - Google Patents

Water Dispersed Type Makeup Cosmetic Composition Download PDF

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KR101771421B1
KR101771421B1 KR1020150169905A KR20150169905A KR101771421B1 KR 101771421 B1 KR101771421 B1 KR 101771421B1 KR 1020150169905 A KR1020150169905 A KR 1020150169905A KR 20150169905 A KR20150169905 A KR 20150169905A KR 101771421 B1 KR101771421 B1 KR 101771421B1
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South Korea
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cosmetic composition
water
weight
makeup cosmetic
present
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KR1020150169905A
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Korean (ko)
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KR20170064596A (en
Inventor
김기백
지진구
박명삼
우영화
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코스맥스 주식회사
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    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/81—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions involving only carbon-to-carbon unsaturated bonds
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/02—Cosmetics or similar toiletry preparations characterised by special physical form
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/81—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions involving only carbon-to-carbon unsaturated bonds
    • A61K8/8141—Compositions of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides or nitriles thereof; Compositions of derivatives of such polymers
    • A61K8/8152—Homopolymers or copolymers of esters, e.g. (meth)acrylic acid esters; Compositions of derivatives of such polymers
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q1/00—Make-up preparations; Body powders; Preparations for removing make-up
    • A61Q1/02—Preparations containing skin colorants, e.g. pigments
    • A61Q1/04—Preparations containing skin colorants, e.g. pigments for lips
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00—Preparations for care of the skin
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
    • A61K2800/48—Thickener, Thickening system

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  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Animal Behavior & Ethology (AREA)
  • General Health & Medical Sciences (AREA)
  • Public Health (AREA)
  • Veterinary Medicine (AREA)
  • Birds (AREA)
  • Epidemiology (AREA)
  • Dermatology (AREA)
  • Cosmetics (AREA)

Abstract

The present invention relates to a process for the preparation of polyacrylate crosspolymer-6, ammonium acryloyldimethyltaurate / Vpicopolymer, and a polymer which is used as an incremental agent in combination with a Pigment-240 / HIDA copolymer bis-decyltetradeceth- To a makeup cosmetic composition of a dispersion type. INDUSTRIAL APPLICABILITY According to the present invention, it is possible to provide a water dispersion type makeup cosmetic composition which imparts soft spreadability, moist moisture and excellent gloss.

Description

Water Dispersed Type Makeup Cosmetic Composition

The present invention relates to a water-dispersible make-up cosmetic composition containing a water-dispersible polymer and imparting a moisturizing sensation and a gloss, and more particularly, to a water-dispersive make-up cosmetic composition comprising a polyacrylate crosspolymer- 6, an ammonium acryloyldimethyltaurate / And a fat-240 / HCI copolymer bis-decyltetradeceth-20etel. The present invention relates to a makeup cosmetic composition in which the formulations are maintained.

In general, a cosmetic composition of water dispersion type has a moist feeling due to the content of water. However, due to the rapid evaporation of water, the moisture sensation disappears over time, resulting in a dry feeling, and the problem of weakening the glossiness with evaporation of water. In case of increasing the content of the polymer used as the conventional thickening agent, the problem is reduced to some extent, but there are problems such as stickiness and heavy use feeling, so there is no satisfactory improvement.

In addition, most of the lip make-ups of the prior art have a problem that the carbomer used as an increasing agent is dried at a high rate and the keratinous sphere (angle) appears and the glossiness is poor. In the course of the synthesis of the carbomer, Is controversial because of its environmental pollution and its use in organic and natural cosmetics is limited

The present inventors have made intensive researches to overcome the problems of the prior art as described above. As a result, they have found that polyacrylate crosspolymer-6 and ammonium acryloyldimethyltaurate / Vpicopolymer, which are not conventional carbomer- -240 / HCI copolymer bis-decyltetradeceth-20-ethene are mixed to produce a cosmetic composition which is excellent in softness, excellent adhesion, moisturizing and glossiness upon application of a lip. Completed.

KR 10-2014-0110400 A

Therefore, a main object of the present invention is to provide a polymer such as polyacrylate crosspolymer-6 and ammonium acryloylmethyltaurate / Vpicopolymer, Pigment-240 / HI Dia Copolymer bis-decyltetradeceth- And to provide a cosmetic composition which is excellent in wetting ability, excellent adhesion, moisturizing and glossiness upon application of a lip.

According to one aspect of the present invention, there is provided a water-dispersed makeup cosmetic composition comprising a purified water, a thickener, and a pigment, wherein the thickener is selected from the group consisting of polyacrylate crosspolymer-6, ammonium acryloyldimethyltaurate / A water-dispersible type make-up cosmetic composition characterized by using a combination of a picolinic acid, a dicyclohexylmethane dicarboxylic acid, a picolymer, and a water-240 /

In the examples of the present invention, it has been proved that when the three polymers are used in combination, the moisturizing power and the gloss are remarkably superior to those of the conventional carbohydrase thickener, and the stability of the cosmetic composition is also improved. The lip cosmetic composition according to the present invention has softness and dampness at the time of application, and is excellent in spreadability.

In the present invention, preferably 80 to 95% by weight of purified water and 0.1 to 5% by weight of polyacrylate crosspolymer-6 based on the total weight of the composition. 0.1 to 5% by weight of ammonium acryloyldimethyltaurate / Vpicopolymer, 0.1 to 5% by weight of Pigment-240 / HI Dia Copolymer bis-decyltetradeceth-20 ether, and 0.01 to 5% by weight of pigment The present invention provides a makeup cosmetic composition comprising a water-dispersible type makeup cosmetic composition.

In the present invention, the purified water may be 80 to 95% by weight based on the total weight of the composition. In addition to purified water, it may further include butylene glycol, glycerin, etc. which are widely used as cosmetics in cosmetics.

In the present invention, the polyacrylate crosspolymer-6 may be 0.1 to 5% by weight based on the total weight of the composition. When the content of the polymer is less than 0.1% by weight, it does not increase, and it is difficult to achieve the expected effect. When the content of the polymer exceeds 5% by weight, the hardness is high and the spreadability may be lowered. Preferably, it is used in an amount of 5% by weight or less, more preferably 4% by weight or less, based on the total weight of the composition.

The polyacrylate crosspolymer-6 has a soft, fluffy feel and minimizes water loss, so that a moist feel can be felt. It also has excellent gloss. However, if the content of the polyacrylate crosspolymer-6 is excessively high, the spreadability may be deteriorated. Specifically, when the content of the polyacrylate crosspolymer-6 alone exceeds 5% by weight based on the total weight of the composition, spreadability may be impaired. The content of the polyacrylate crosspolymer-6 is set in consideration of soft skin feel.

In the present invention, the ammonium acryloyldimethyltaurate / Vpicopolymer may be present in an amount of 0.1 to 5% by weight based on the total weight of the composition. If the content of the polymer component is less than 0.1% by weight, it is difficult to form an incremental formation, and it is difficult to achieve the expected effect. When the content of the polymer component exceeds 5% by weight, stickiness is deteriorated.

The ammonium acryloyldimethyltaurate / vpicopolymer exhibits good scaling ability in low PH (4-9) and ethanol (30% or more), superior in solubility than other thickeners, and sticky And the feeling of initial feeling is thick, so that the relative humidity can be felt. Concretely, when the content of ammonium acryloyldimethyltaurate / Vpicopolymer alone exceeds 5% by weight based on the total weight of the composition, the hardness may be high due to high hardness. The content of the ammonium acryloyldimethyltaurate / VIPICO polymer is set in consideration of soft skin feel.

In the present invention, the above-mentioned Pigment-240 / HDI copolymer bis-decyltetradeceth-20etel may be 0.1 to 5% by weight based on the total weight of the composition. The above-mentioned Pigment-240 / HDI copolymer Bis-decyltetradeceth-20etel can improve the feeling of use and softness as a raw material having a shape memory phenomenon. The above-mentioned Pigment-240 / HISD copolymer may be used together with bis-decyltetradeceth-20-ether, potassium laurate, and VITATE.

In the present invention, the content of the pigment may be 0.01 to 5% by weight, based on the total weight of the composition. In one embodiment, the pigments may be used in combination with various types of pigments. For example, coloring pigments such as Red No. 102, Orange No. 205, Red No. 104, (1), Red No. 227, Yellow No. 4, Yellow No. 5, and Blue No. 1 may be used in combination. The kind of the pigment is not limited to the above-mentioned pigment but includes a water-soluble pigment soluble in water.

The makeup cosmetic composition of the present invention may contain a preservative, a moisturizing agent, a film-forming agent, a perfume, and the like, which are used in cosmetics of the present invention, within the range that does not impair the effects of the present invention.

The makeup cosmetic composition of the present invention may be used as a solid foundation, a concealer, a base, a lip balm, and the like, but is preferably a lip makeup cosmetic composition for lips.

In the makeup cosmetic composition according to the present invention, the above-mentioned components can be prepared by a conventional method such as heating, mixing and agitation. Such a manufacturing process is obvious in view of the technical level of a person skilled in the art.

The cosmetic composition of the present invention is a cosmetic composition comprising a polyacrylate crosspolymer-6 and an ammonium acryloyldimethyltaurate / Vipicopolymer, a Pigment-240 / HI Dia Copolymer bis-decyltetradeceth- When applied, it gives a soft feeling of flourishness and a moist feeling, and it improves the gloss power, thereby solving the problem of using existing carbomer.

Figs. 1A and 1B are graphs comparing the amount of skin moisture and the rate of change in Examples and Comparative Examples of the present invention.
Fig. 2 is a graph comparing the reflectance before and after coating of the examples of the present invention and the comparative example.

Hereinafter, the present invention will be described in more detail with reference to Examples. These embodiments are only for illustrating the present invention, and thus the scope of the present invention is not construed as being limited by these embodiments.

[Examples and Comparative Examples 1 to 3]

The ingredients of Table 1 below were blended to prepare a lip cosmetic composition.

First, the ingredients shown in the table were added in order, dispersed and dissolved. The contents of the following Table 1 were prepared on the basis of% by weight.

Raw material name Example Comparative Example 1 Comparative Example 2 Comparative Example 3 Comparative Example 4 One Purified water 83.500 96.380 87.380 86.200 86.200 2 Butylene glycol 5.000 1,000 5.000 5.000 5.000 3 glycerin 5.000 - 5.000 5.000 5.000 4 Polyacrylate Crosspolymer-6 2.500 - - 2.500 - 5 Ammonium acryloyldimethyltaurate / Vpicopolymer 2.500 - - - 2.500 6 Phenoxyethanol 0.500 0.500 0.500 0.500 0.500 7 Methylparaben 0.300 0.300 0.300 0.300 0.300 8 Carbomer - 0.700 0.700 - - 9 ≪ tb > ______________________________________ < tb > ______________________________________ < tb > 0.200 - - - - 10 Spices 0.100 0.100 0.100 0.100 0.100 11 Pentyleneglycol 0.080 - - 0.080 0.080 12 Tromethamine - 0.700 0.700 - - 13 Pigment 0.320 0.320 0.320 0.320 0.320

In the case of the above-mentioned Examples and Comparative Examples, water dispersion formulations of the same formulation were compared.

In the case of Comparative Examples 1 and 2, a formulation of a conventional water dispersion formulation was used, and a carbomer type polymer was used. In Comparative Example 3, polyacrylate crosspolymer-6 alone was used. In the case of Comparative Example 4, the ammonium acryloyldimethyltaurate / Vpicopolymer was used alone. The manufacturing process of the comparative example is similar to the embodiment.

In the case of Comparative Example 3 in which polyacrylate crosspolymer-6 alone was used, when the sensory evaluation was carried out after the preparation, the contents were aggregated and the color of Bali was worsened, and pigment bleeding phenomenon was remarkably confirmed.

When sensory evaluation of the result of using ammonium acryloyldimethyltaurate / VIPICO polymer alone showed good initial sensation of coolness, the sensation of moisture decreased rapidly and dry feeling was strong. Also, pigment blurring was confirmed. Due to these problems, it was considered that it would be difficult to commercialize. In Comparative Examples 3 and 4, additional tests other than hardness and pH measurement were excluded.

[Test Example 1] Hardness and pH measurement

The pH and hardness of the prepared contents of the above Examples and Comparative Examples 1 and 2 were compared and evaluated. Each sample was stored in a 25 ° C thermostat for 24 hours, and the hardness was measured using a Rheometer CR-500DX. The pH was measured using a pH meter (Bench pH meter HI 4221). The measurement results are shown in Table 2.

Example Comparative Example 1 Comparative Example 2 Comparative Example 3 Comparative Example 4 pH 6.62 6.45 6.58 6.51 6.45 Hardness 8.5 7 8 6.5 6.1

Referring to Table 2, it can be seen that there is not a large difference in hardness when comparing the contents of the examples of the present invention and the contents of Comparative Examples 1 and 2.

The pH value is a factor affecting formulation stability and flotation power, and it can be confirmed that the pH part is not significantly different.

[Test Example 2]

In the above Examples and Comparative Examples 1 and 2, a Corneometer CM825 (CK electronic, Germany) instrument was used to evaluate the moisture resistance of the makeup cosmetic composition.

 Five adult healthy women (mean age 26.2 years) were measured for their moisturizing power after application and the results are shown in Graph 1.

The moisture content of the test area (22 cm 2 ) was measured at the test site (20 cm 2 ), and 20 μl of the product was applied to the test site and absorbed. After 30 minutes, 2 hours, 4 hours , And skin moisture after 8 hours were measured three times, respectively.

The results of the measurements were obtained by calculating the skin moisture content and the rate of change using the average value of the three measurements, and then compared with the non-attrition value. Figs. 1A and 1B are graphs comparing the amount of skin moisture and the rate of change in Examples and Comparative Examples of the present invention.

As a result of the moisture test, the moisturizing power of the three groups was improved compared to the non - mousse, and the moisturizing power of the examples was the highest. The results are shown in Table 1. The results are shown in Table 1. The results are shown in Table 1. The results are shown in Table 1. It was found that the skin moisturizing ability was maintained up to 8 hours. In Comparative Example 1, no significant difference was observed between the unopened skin after about 4 hours,

Results of moisturisation test Examples> Comparative Example 2> It was confirmed that the moisturizing power was good in the order of Comparative Example 1, and in the case of the Examples, it is found that the polymer of the existing Carbomer type has better moisture holding power.

[Test Example 3]

Micro-TRI-gloss (BYK Gardner, Germany) was used to evaluate the glossiness of the make-up cosmetic compositions in the above Examples and Comparative Examples 1 and 2.

Artificial leather was used for the test. The glossiness of the artificial leather test area (48 cm 2 ) was measured three times before applying the product, and the product was applied to the test area by 120 μl, and the gloss of the spot was measured three times .

The measured results were compared with the before and after values at 20 ° reflectance at 70 ° C or higher and 85 ° C reflectance at 10 ° C or below based on the measured reflectance at 60 ° C. Fig. 2 is a graph comparing the reflectance before and after coating of the examples of the present invention and the comparative example.

As a result of the gloss test, the glossiness of the embodiment was most excellent as shown in Graph 2. It has a glossiness improved by about 2.7 times as compared with that before coating, and is improved by about 2 times in Comparative Example 1 and 1.6 times in Comparative Example 2.

It is confirmed that it has an excellent gloss power comparing with the base product using the existing Carbomer polymer.

[Test Example 4]

In the Examples and Comparative Examples 1 and 2, the stability of the makeup cosmetic composition was evaluated.

The temperature was kept for 14 days in a thermostatic chamber according to the temperature shown in Table 3, and the appearance change was visually observed. The results are shown in Table 3 (O: no appearance change at all, B: slight appearance change (color separation), X: significant change in appearance).

Example Comparative Example 1 Comparative Example 2 25 ℃ ○ ○ ○ 37 ℃ ○ ○ △ 45 ° C ○ △ △ cycle ○ △ X

As a result, as shown in Table 3, it was confirmed that the stability of the embodiment of the present invention was generally stable under various conditions.

The embodiments described above are merely illustrative of the present invention and are used for the purpose of describing the present invention only and not for limiting the scope of the present invention described in the claims or the claims. Therefore, those skilled in the art will appreciate that various modifications and equivalent embodiments are possible without departing from the scope of the present invention.

As described above, the cosmetic material of the present invention can be obtained by mixing polyacrylate crosspolymer-6 and ammonium acryloyldimethyltaurate / Vipicopolymer, Pigment-240 / HI Dia Copolymer bis-decyltetradeceth- The cosmetic composition of the present invention provides softness and moist feel when applied, and improves the polishing power, thereby solving the problem of using existing carbomers.

Claims (6)

Wherein the thickener is selected from the group consisting of polyacrylate crosspolymer-6, ammonium acryloyldimethyltaurate / Vipicopolymer, and a water-dispersible type makeup cosmetic composition comprising a water- 80 to 95% by weight of purified water and 0.1 to 5% by weight of polyacrylate crosspolymer-6 based on the total weight of the composition. 0.1 to 5% by weight of ammonium acryloyldimethyltaurate / Vpicopolymer, 0.1 to 5% by weight of Pigment-240 / HI Dia Copolymer bis-decyltetradeceth-20 ether, and 0.01 to 5% by weight of pigment Wherein the water-dispersible type make-up cosmetic composition is a water-dispersion type make-up cosmetic composition. delete The water dispersion type makeup cosmetic composition according to claim 1, further comprising a moisturizing agent, a film forming agent, and a perfume. The makeup cosmetic composition according to claim 1, which is a lip makeup cosmetic composition for lips. The water dispersion type makeup cosmetic composition according to claim 1, wherein a softness and a moist feel are imparted to the composition during application, and the glossiness is improved. delete
KR1020150169905A 2015-12-01 2015-12-01 Water Dispersed Type Makeup Cosmetic Composition KR101771421B1 (en)

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP3791855A1 (en) 2019-09-16 2021-03-17 Amorepacific Corporation Cosmetic composition comprising solubilized pigment and method for preparing the same
KR20220127083A (en) 2021-03-10 2022-09-19 (주)아모레퍼시픽 Agent for modifying pigment to dye, and colorant composition comprising the dye

Families Citing this family (2)

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Publication number Priority date Publication date Assignee Title
KR102211754B1 (en) * 2019-06-05 2021-02-04 (주)이미인 Elongational cosmetic composition with shape restoration ability and manufacturing method thereof
KR102436827B1 (en) * 2021-12-15 2022-08-26 한국콜마주식회사 Lip cosmetic composition having a large amount of pearls

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP3791855A1 (en) 2019-09-16 2021-03-17 Amorepacific Corporation Cosmetic composition comprising solubilized pigment and method for preparing the same
KR20210032142A (en) 2019-09-16 2021-03-24 (주)아모레퍼시픽 Cosmetic composition comprising solubilized pigment and method for preparing the same
US11065190B2 (en) 2019-09-16 2021-07-20 Amorepacific Corporation Cosmetic composition comprising solubilized pigment and method for preparing the same
KR20220127083A (en) 2021-03-10 2022-09-19 (주)아모레퍼시픽 Agent for modifying pigment to dye, and colorant composition comprising the dye

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