KR20210133795A - Cosmetic composition containning encapsulated cooling agent and method thereof - Google Patents

Cosmetic composition containning encapsulated cooling agent and method thereof Download PDF

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KR20210133795A
KR20210133795A KR1020200052882A KR20200052882A KR20210133795A KR 20210133795 A KR20210133795 A KR 20210133795A KR 1020200052882 A KR1020200052882 A KR 1020200052882A KR 20200052882 A KR20200052882 A KR 20200052882A KR 20210133795 A KR20210133795 A KR 20210133795A
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cosmetic composition
lips
cooling agent
weight
lip
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KR102394034B1 (en
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박진오
김기백
우영화
박명삼
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코스맥스 주식회사
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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/40Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
    • A61K8/42Amides
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/02Cosmetics or similar toiletry preparations characterised by special physical form
    • A61K8/11Encapsulated compositions
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/33Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
    • A61K8/37Esters of carboxylic acids
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/40Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
    • A61K8/44Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q1/00Make-up preparations; Body powders; Preparations for removing make-up
    • A61Q1/02Preparations containing skin colorants, e.g. pigments
    • A61Q1/04Preparations containing skin colorants, e.g. pigments for lips
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q1/00Make-up preparations; Body powders; Preparations for removing make-up
    • A61Q1/02Preparations containing skin colorants, e.g. pigments
    • A61Q1/04Preparations containing skin colorants, e.g. pigments for lips
    • A61Q1/06Lipsticks
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • A61Q19/001Preparations for care of the lips

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  • Life Sciences & Earth Sciences (AREA)
  • Animal Behavior & Ethology (AREA)
  • General Health & Medical Sciences (AREA)
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  • Veterinary Medicine (AREA)
  • Birds (AREA)
  • Epidemiology (AREA)
  • Emergency Medicine (AREA)
  • Dermatology (AREA)
  • Cosmetics (AREA)

Abstract

The present invention relates to a cosmetic composition for lips. The cosmetic composition for lips comprises an encapsulated cooling agent which comprises: 0.01 to 1 wt% of methyl diisopropyl propionamide; 0.01 to 1 wt% of menthyl lactate; and 0.01 to 1 wt% of ethyl methane carboxamide. The cosmetic composition for lips has an excellent moisturizing effect by reducing dryness after applying the cosmetic composition compared to the existing water dispersion type cosmetic composition for lips and can maintain a feeling of refreshing for a long time.

Description

캡슐화된 쿨링제를 포함하는 화장료 조성물 및 그 제조방법{COSMETIC COMPOSITION CONTAINNING ENCAPSULATED COOLING AGENT AND METHOD THEREOF}COSMETIC COMPOSITION CONTAINNING ENCAPSULATED COOLING AGENT AND METHOD THEREOF TECHNICAL FIELD

캡슐화된 쿨링제를 포함하는 화장료 조성물 및 그 제조방법에 관한 것이다.It relates to a cosmetic composition comprising an encapsulated cooling agent and a method for manufacturing the same.

입술의 화장을 위한 제품으로는 립스틱, 립글로스, 립틴트 및 립락커 등 다양한 제품이 있다. 이러한 입술용 화장료 조성물들은 기본적인 입술의 보호 및 미용의 목적 외에도, 입술에 청량감을 지속시켜 온도 감소 효과를 나타내기도 한다.There are various products for lip makeup, such as lipstick, lip gloss, lip tint, and lip lacquer. In addition to the basic lip protection and cosmetic purposes, these cosmetic compositions for lips also exhibit a temperature reduction effect by maintaining a refreshing feeling on the lips.

수분산 타입 리퀴드 립은 첫 도포 시 물 자체의 시원한 느낌이 있지만 시간이 경과할 수록 물의 휘발로 인해 건조한 느낌이 든다는 문제가 있으며, 그러한 건조함으로 인해 수분산 타입의 리퀴드 립 제품이 선호 받지 못하고 있다. 그러나 유분산 타입의 리퀴드 립은 물의 휘발로 건조한 느낌이 들지는 않지만, 시원한 쿨링감을 갖지 못한다. 또한 쿨링감이 든다고 해도 그 지속시간이 매우 짧다.Water-dispersion type liquid lip has a cool feeling of water itself when first applied, but there is a problem that it feels dry due to volatilization of water as time goes by, and due to such dryness, liquid lip products of water-dispersion type are not preferred. However, the oil-dispersion type liquid lip does not feel dry due to the volatilization of water, but it does not have a cooling feeling. Also, even if you feel a cooling sensation, the duration is very short.

이러한 기술적 배경 하에서, 물의 휘발로 인해 건조한 느낌 없이도 쿨링제가 캡슐화되어 쿨링감을 갖는 입술용 화장료 조성물에 대한 연구가 활발히 진행되고 있으나(KR등록번호 10-1701239), 아직은 미비한 실정이다.Under this technical background, research on a cosmetic composition for lips having a cooling feeling in which a cooling agent is encapsulated without a feeling of dryness due to volatilization of water is being actively conducted (KR Registration No. 10-1701239), but it is still insufficient.

일 양상은 화장료 조성물 총 중량 대비 쿨링제를 0.1 내지 2중량% 포함하는 것인 입술용 화장료 조성물을 제공하는 것이다.One aspect is to provide a cosmetic composition for lips comprising 0.1 to 2% by weight of a cooling agent relative to the total weight of the cosmetic composition.

일 양상은 화장료 조성물 총 중량 대비 쿨링제를 0.1 내지 2중량% 포함하는 것인 입술용 화장료 조성물을 제공한다.One aspect provides a cosmetic composition for lips comprising 0.1 to 2% by weight of a cooling agent relative to the total weight of the cosmetic composition.

상기 쿨링제의 중량 범위가 0.1중량% 이하일 경우에는 효과가 미미하고, 2중량% 이상일 경우에는 자극성이 높아 바람직하지 않다.When the weight range of the cooling agent is 0.1 wt% or less, the effect is insignificant, and when it is 2 wt% or more, irritation is high, which is not preferable.

일 구체예에 있어서, 상기 쿨링제는 메틸디이소프로필 프로피온아미드, 멘틸락테이트 및 에틸멘탄 카복사아미드를 포함할 수 있다.In one embodiment, the cooling agent may include methyldiisopropyl propionamide, menthyl lactate and ethylmentane carboxamide.

일 구체예에 있어서, 상기 쿨링제는 화장료 조성물 총 중량 대비 메틸디이소프로필 프로피온아미드 0.01 내지 1중량%, 멘틸락테이트 0.01 내지 1중량% 및 에틸멘탄 카복사아미드 0.01 내지 1중량% 포함할 수 있다.In one embodiment, the cooling agent may include 0.01 to 1% by weight of methyldiisopropyl propionamide, 0.01 to 1% by weight of menthyl lactate, and 0.01 to 1% by weight of ethylmentane carboxamide, based on the total weight of the cosmetic composition .

상기 메틸디이소프로필 프로피온아미드는 0.01 내지 0.08중량%, 0.01 내지 0.06중량%, 0.01 내지 0.04중량% 또는 0.01 내지 0.02중량%일 수 있으며, 멘틸락테이트 0.01 내지 0.08중량%, 0.01 내지 0.06중량%, 0.01 내지 0.04중량% 또는 0.01 내지 0.02중량%일 수 있고, 에틸멘탄 카복사아미드 0.01 내지 0.08중량%, 0.01 내지 0.06중량%, 0.01 내지 0.04중량% 또는 0.01 내지 0.02중량%일 수 있다.The methyldiisopropyl propionamide may be 0.01 to 0.08% by weight, 0.01 to 0.06% by weight, 0.01 to 0.04% by weight or 0.01 to 0.02% by weight, menthyl lactate 0.01 to 0.08% by weight, 0.01 to 0.06% by weight, 0.01 to 0.04% by weight or 0.01 to 0.02% by weight, and 0.01 to 0.08% by weight of ethylmentane carboxamide, 0.01 to 0.06% by weight, 0.01 to 0.04% by weight or 0.01 to 0.02% by weight.

상기 메틸디이소프로필 프로피온아미드, 멘틸락테이트 및 에틸멘탄 카복사아미드의 특정한 혼합 중량으로 인하여, 본 화장료 조성물은 더 높은 보습 효과 및 청량감을 가진다.Due to the specific mixed weight of methyldiisopropyl propionamide, menthyllactate and ethylmentane carboxamide, the cosmetic composition has a higher moisturizing effect and a refreshing feeling.

일 구체예에 있어서, 상기 쿨링제는 캡슐화된 것일 수 있다. 상기 쿨링제가 캡슐화됨으로써, 더 높은 제형 안정도를 가지는 화장료 조성물을 얻을 수 있다.In one embodiment, the cooling agent may be encapsulated. By encapsulating the cooling agent, it is possible to obtain a cosmetic composition having higher formulation stability.

일 구체예에 있어서, 상기 화장료 조성물은 립스틱, 립글로스, 립틴트 또는 립락커 중 어느 하나일 수 있다.In one embodiment, the cosmetic composition may be any one of lipstick, lip gloss, lip tint or lip lacquer.

당업자는 본 명세서에 따른 조성물의 유리한 특성이 예상된 첨가에 의해 악영향을 받지 않거나 실질적으로 받지 않도록, 임의의 추가 성분 및/또는 이의 양을 선택할 수 있다.A person skilled in the art can select any additional ingredients and/or amounts thereof such that the advantageous properties of the composition according to the present disclosure are not adversely or substantially not adversely affected by the expected addition.

본 명세서에 기재된 수치는 명시하지 않아도 "약"의 의미를 포함하는 것으로 간주한다. 예를 들어, 상기 기재된 수치는 10%, 5%, 2%, 또는 1%로 변할 수 있다. 어떤 구체예에서, 상기 값은 5%, 2%, 또는 1%로 변할 수 있다. 예를 들어, 5의 값은 대략 5의 범위는 갖는 4.5 및 5.5 사이, 4.75 및 5.25 사이, 또는 4.9 및 5.1 사이, 또는 4.95 및 5.05 사이의 임의의 값을 포함하는 것을 의미한다.Numerical values set forth herein are intended to include the meaning of “about” even if not specified. For example, the numerical values set forth above may vary by 10%, 5%, 2%, or 1%. In some embodiments, the value may vary by 5%, 2%, or 1%. For example, a value of 5 is meant to include any value between 4.5 and 5.5, between 4.75 and 5.25, or between 4.9 and 5.1, or between 4.95 and 5.05 having a range of approximately 5.

본 명세서에서 사용된 화장료 조성물은 입술용 화장료 조성물은 예를 들어, 립스틱, 립글로스, 립밤, 립크림, 립펜슬, 립라이너펜슬, 또는 액상루즈로 제형화될 수 있으나, 이에 한정되는 것은 아니며, 예를 들어 사용 목적에 따라 아이섀도(eye shadow), 치크(cheek), 또는 블러셔(Blusher) 등의 다양한 색조 메이크업 용도로 사용될 수 있다.The cosmetic composition used herein may be formulated as a cosmetic composition for lips, for example, lipstick, lip gloss, lip balm, lip cream, lip pencil, lip liner pencil, or liquid rouge, but is not limited thereto, for example, Depending on the purpose of use, it can be used for various color makeup purposes such as eye shadow, cheek, or blusher.

다른 양상은 상기 입술용 화장료 조성물을 제조하는 방법을 제공한다.Another aspect provides a method for preparing the cosmetic composition for lips.

당해 기술분야의 통상의 지식을 가진 자의 기술수준에 비추어 볼 때, 상기 가열, 혼합 및 냉각을 포함하는 통상의 제조 방법에 의해 입술용 화장료 조성물을 제조할 수 있다.In view of the technical level of those of ordinary skill in the art, a cosmetic composition for lips can be prepared by a conventional manufacturing method including the heating, mixing and cooling.

이상 사용된 모든 기술용어는, 달리 정의되지 않는 이상, 관련 분야에서 통상의 당업자가 일반적으로 이해하는 바와 같은 의미로 사용된다.All technical terms used above have the same meaning as commonly understood by those skilled in the art, unless otherwise defined.

본 발명은 쿨링제를 포함하는 화장료 조성물 및 그 제조방법에 관한 것으로써, 온도 감소 및 지속력, 사용감, 수분도 및 제형 안정도가 뛰어난 입술용 화장료 조성물을 제공할 수 있다.The present invention relates to a cosmetic composition containing a cooling agent and a method for manufacturing the same, and it is possible to provide a cosmetic composition for lips excellent in temperature reduction and durability, feeling of use, moisture content and formulation stability.

도 1은 입술용 화장료 조성물을 피부에 도포 후 5분간 온도 감소 및 지속력을 측정한 결과이다.
도 2는 입술용 화장료 조성물을 피부에 도포 후 5분간 피부온도를 적외선 카메라로 촬영하여 비교 측정한 결과이다.
도 3은 입술용 화장료 조성물을 시험부위에 적용 후 피부수분도를 비교 측정한 결과이다.
도 4는 입술용 화장료 조성물을 피부에 도포 후 피부 수분도를 측정한 결과이다.
1 is a result of measuring the temperature reduction and durability for 5 minutes after applying a cosmetic composition for lips to the skin.
2 is a comparison measurement result by photographing the skin temperature with an infrared camera for 5 minutes after applying a cosmetic composition for lips to the skin.
3 is a result of comparing and measuring skin moisture after applying a cosmetic composition for lips to a test site.
4 is a result of measuring the moisture content of the skin after applying the cosmetic composition for lips to the skin.

이하 본 발명을 실시예를 통하여 보다 상세하게 설명한다. 그러나, 본 발명에 따른 실시예 및 실험예는 여러 가지 다른 형태로 변형될 수 있으며, 본 발명의 범위가 아래에서 상술하는 실시예 및 실험예에 한정되는 것으로 해석되어서는 안 된다. 본 발명의 실시예 및 실험예는 당 업계에서 평균적인 지식을 가진 자에게 본 발명을 보다 완전하게 설명하기 위해서 제공되는 것이다. 또한, 본 명세서에는 바람직한 방법이나 시료가 기재되나, 이와 유사하거나 동등한 것들도 본 명세서의 범주에 포함된다.Hereinafter, the present invention will be described in more detail through examples. However, the Examples and Experimental Examples according to the present invention may be modified in various other forms, and the scope of the present invention should not be construed as being limited to the Examples and Experimental Examples described below. The Examples and Experimental Examples of the present invention are provided to more completely explain the present invention to those of ordinary skill in the art. In addition, although preferred methods and samples are described herein, similar or equivalent ones are also included in the scope of the present specification.

1. 입술용 화장료 조성물의 제조1. Preparation of cosmetic composition for lips

입술용 화장료 조성물의 제조는 다음과 같이 이루어졌다. 하기 표 1의 용량에 따라 원료를 비이커에 계량하여 준비하고, 수상부 원료를 차례로 첨가하여 아지믹서를 이용하여 5분간 균일하게 분산, 용해시켜 수분산 제형을 제조하였다. 그 후 수분산 제형에 수상부 분산이 가능하며, Methyl Diisopropyl Propionamide, Menthyl Lactate, Ethyl Menthane Carboxamide를 각각 4.75% (100% 기준)로 캡슐화 시킨 쿨링제를 첨가하여 분산하는 과정을 거쳐 입술용 화장료 조성물인 실시예 1 내지 5 및 쿨링제를 포함하지 않는 비교예를 제조하였다.The preparation of the cosmetic composition for lips was made as follows. The raw materials were prepared by measuring them in a beaker according to the capacity shown in Table 1 below, and the aqueous phase part raw materials were sequentially added and uniformly dispersed and dissolved for 5 minutes using an azimuth to prepare an aqueous dispersion formulation. After that, the aqueous dispersion can be dispersed in the aqueous phase, and the cooling agent encapsulated at 4.75% (based on 100%) of Methyl Diisopropyl Propionamide, Menthyl Lactate, and Ethyl Menthane Carboxamide, respectively, is added and dispersed. Examples 1 to 5 and Comparative Examples not including a cooling agent were prepared.

쿨링제의 함량은, 실시예 1에서 0.01425 (Methyl Diisopropyl Propionamide, Menthyl Lactate, Ethyl Menthane Carboxamide 각각 0.00475%), 실시예 2에서 0.057 (Methyl Diisopropyl Propionamide, Menthyl Lactate, Ethyl Menthane Carboxamide 각각 0.019%%), 실시예 3에서 0.09975 (Methyl Diisopropyl Propionamide, Menthyl Lactate, Ethyl Menthane Carboxamide 각각 0.03325%), 실시예 4에서 0.1425(Methyl Diisopropyl Propionamide, Menthyl Lactate, Ethyl Menthane Carboxamide 각각 0.0475%) 및 실시예 5에서 0.18525 (Methyl Diisopropyl Propionamide, Menthyl Lactate, Ethyl Menthane Carboxamide 각각 0.06175%) 첨가하였다.The content of the cooling agent is 0.01425 (Methyl Diisopropyl Propionamide, Menthyl Lactate, Ethyl Menthane Carboxamide 0.00475% each) in Example 1, 0.057 in Example 2 (Methyl Diisopropyl Propionamide, Menthyl Lactate, Ethyl Menthane Carboxamide 0.019% each) In Example 3 0.09975 (Methyl Diisopropyl Propionamide, Menthyl Lactate, Ethyl Menthane Carboxamide 0.03325% each), Example 4 0.1425 (Methyl Diisopropyl Propionamide, Menthyl Lactate, Ethyl Menthane Carboxamide 0.0475% each) and Example 5 0.18525 (Methyl Diisopropyl Propionamide) , Menthyl Lactate, and Ethyl Menthane Carboxamide (0.06175% each) were added.

성분명Ingredient name 실시예1Example 1 실시예2Example 2 실시예3Example 3 실시예4Example 4 실시예5Example 5 비교예comparative example 정제수Purified water To 100To 100 To 100To 100 To 100To 100 To 100To 100 To 100To 100 To 100To 100 보습제moisturizer 부틸렌 글라이콜Butylene Glycol 5.75.7 5.75.7 5.75.7 5.75.7 5.75.7 5.75.7 글리세린glycerin 5.75.7 5.75.7 5.75.7 5.75.7 5.75.7 5.75.7 컨디셔닝제conditioning agent 디메치콘dimethicone 0.50.5 0.50.5 0.50.5 0.50.5 0.50.5 0.50.5 레시틴lecithin 0.50.5 0.50.5 0.50.5 0.50.5 0.50.5 0.50.5 피막형성제film forming agent 글리세릴 폴리메타아크릴레이트Glyceryl Polymethacrylate 8.68.6 8.68.6 8.68.6 8.68.6 8.68.6 8.68.6 착색제coloring agent 1.181.18 1.181.18 1.181.18 1.181.18 1.181.18 1.181.18 점증제thickener 암모늄 아크릴로일디메틸타우레이트/VP 코폴리머Ammonium Acryloyldimethyltaurate/VP Copolymer 1.01.0 1.01.0 1.01.0 1.01.0 1.01.0 1.01.0 폴리아크릴레이트 크로스폴리머-6Polyacrylate crosspolymer-6 1.01.0 1.01.0 1.01.0 1.01.0 1.01.0 1.01.0 방부제antiseptic 페녹시에탄올Phenoxyethanol 0.90.9 0.90.9 0.90.9 0.90.9 0.90.9 0.90.9 1, 2-헥산디올1,2-Hexanediol 0.90.9 0.90.9 0.90.9 0.90.9 0.90.9 0.90.9 계면활성제Surfactants PEG-60 하이드로제네이티드 캐스터 오일PEG-60 Hydrogenated Castor Oil 0.40.4 0.40.4 0.40.4 0.40.4 0.40.4 0.40.4 쿨링제cooling agent 메틸 디이소프로필 프로피온아마이드, 멘틸 락테이트 및 에틸 멘탄 카복사마이드Methyl diisopropyl propionamide, menthyl lactate and ethyl menthane carboxamide 0.014250.01425 0.0570.057 0.099750.09975 0.14250.1425 0.185250.18525 -- 착향제flavoring agent 0.10.1 0.10.1 0.10.1 0.10.1 0.10.1 0.10.1

실험예 1: 쿨링제 함량에 따른 사용감 평가Experimental Example 1: Evaluation of feeling of use according to cooling agent content

상기 실시예의 메이크업 화장료 조성물의 쿨링제 함량에 따른 사용감을 평가하였다.The feeling of use according to the content of the cooling agent of the makeup cosmetic composition of the above example was evaluated.

테스트를 위하여 실시예 1 내지 5의 화장료 조성물을 시험부위에 24시간 폐쇄첩포한 후 패치를 제거하여 피부 반응을 판정하였고, 그 결과를 하기 표 2에 나타내었다.For the test, the cosmetic composition of Examples 1 to 5 was occluded on the test site for 24 hours, and the patch was removed to determine the skin reaction, and the results are shown in Table 2 below.

중량 (%)weight (%) 0.10.1 0.40.4 0.70.7 1.01.0 1.31.3 청량감refreshment 22 44 44 55 55 자극감irritation 00 1One 33 44 55 사용감 총 점수total score 22 44 22 1One 1One

청량감(0-아무느낌없음 5-매우상쾌) / 자극감(0-자극없음 5-자극매우강함) / 사용감 총점수(1-좋지않음 5-자극이없으면서도매우상쾌함)Refreshing feeling (0 - no feeling 5 - very refreshing) / irritation (0 - no irritation 5 - very strong) / total feeling of use (1 - bad 5 - very refreshing without irritation)

그 결과, 상기 표 2에서 확인되는 바와 같이 실시예 2의 화장료 조성물이 청량감을 주면서도 자극감이 적어 사용감에서 가장 뛰어남을 알 수 있다.As a result, as shown in Table 2, it can be seen that the cosmetic composition of Example 2 is the most excellent in the feeling of use because it gives a refreshing feeling and has less irritation.

실험예 2: 온도 감소 및 지속력 평가Experimental Example 2: Temperature reduction and durability evaluation

실험예 1에서 가장 뛰어난 사용감을 나타냈던 실시예 2의 입술용 화장료 조성물의 온도 감소 및 지속력을 평가하였다.The temperature reduction and durability of the cosmetic composition for lips of Example 2, which showed the best feeling of use in Experimental Example 1, was evaluated.

건강한 성인 5명 (평균 연령 26.6세)의 온도 감소 및 지속력을 측정하기 위하여, 시험 부위의 무도포 시 피부 온도를 적외선 카메라로 촬영하였으며, 같은 부위에 실시예를 적용하여 도포 직후, 1분, 3분, 5분 후의 피부 온도를 적외선 카메라 촬영하였다.In order to measure the temperature reduction and durability of 5 healthy adults (average age 26.6 years old), the skin temperature at the time of no application of the test site was photographed with an infrared camera. The skin temperature after minutes and 5 minutes was photographed with an infrared camera.

도 1 및 2에 나타난 바와 같이, 온도 감소 및 지속 테스트 결과 종래의 문제점을 가지고 있던 수분산 제형인 비교예와 비교할시, 피부 온도 감소율이 향상된 결과를 나타내었다.As shown in FIGS. 1 and 2 , the temperature reduction and lasting test results showed an improved skin temperature reduction rate when compared with the comparative example, which is an aqueous dispersion formulation having problems in the prior art.

실험예 3: 수분도 평가Experimental Example 3: Moisture level evaluation

상기 실시예의 입술용 화장료 조성물의 피부 수분도를 평가하였다.The skin moisture level of the cosmetic composition for lips of the above example was evaluated.

테스트를 위하여 시험부위를 미온수로 세정하고 10분간 항온항습실(22±2℃,40~60% RH)에서 대기한 뒤, 시험부위의 무도포 시 피부 수분도를 각각 3회씩 측정하였으며, 같은 부위에 제품을 도포하여 피부 수분도를 각각 3회씩 측정하여 비교하였다.For the test, the test site was washed with lukewarm water and waited in a constant temperature and humidity room (22±2℃, 40~60% RH) for 10 minutes. was applied and the skin moisture level was measured three times each for comparison.

측정 결과 도 3과 도 4에서 보이는 바와 같이 실시예 2의 화장료 조성물의 사용 후 피부수분도가 각각 708.0, 746.8% 증가하는 것으로 나타남에 따라, 실시예의 피부수분도가 비교예와 비교 시 높은 것으로 확인하였다.As shown in FIGS. 3 and 4, the skin moisture level of Example 2 was found to increase by 708.0 and 746.8%, respectively, after use of the cosmetic composition of Example 2, as shown in FIGS.

실험예 4: 제형 안정도 평가Experimental Example 4: Formulation stability evaluation

상기 실시예 1 내지 5의 입술용 화장료 조성물에 대한 제형 안정도 평가를 수행하였다.Formulation stability evaluation was performed for the cosmetic compositions for lips of Examples 1 to 5.

하기 표 3에 주어진 온도에 따라, 항온조에서 30일 동안 보관하여 외관변화를 육안으로 관찰하였다. 하기 <평가 기준>에 따라 평가하여 그 결과를 표 3에 나타내었다.According to the temperature given in Table 3, it was stored in a constant temperature bath for 30 days, and the change in appearance was visually observed. It was evaluated according to the following <Evaluation Criteria>, and the results are shown in Table 3.

<평가기준><Evaluation criteria>

안정성 우수 : ○Excellent stability: ○

약간의 제형 변화 : △Slight change in formulation: △

제형 분리 및 변색 : XFormulation separation and discoloration: X

온도Temperature 실시예1Example 1 실시예2Example 2 실시예3Example 3 실시예4Example 4 실시예5Example 5 4℃4℃ 25℃25℃ 37℃37℃ 45℃45℃ 50℃50℃ CycleCycle

상기 표 3에 나타난 바와 같이, 실시예 1 내지 5의 화장료 조성물의 안정도는 전반적으로 양호한 편이었으며, 이 중에서도 실시예 1, 2의 화장료 조성물의 제형 안정도가 가장 뛰어난 것으로 나타났다.As shown in Table 3, the stability of the cosmetic compositions of Examples 1 to 5 was generally good, and among them, the formulation stability of the cosmetic compositions of Examples 1 and 2 was found to be the most excellent.

Claims (5)

화장료 조성물 총 중량 대비 쿨링제를 0.1 내지 2중량% 포함하는 것인 입술용 화장료 조성물.A cosmetic composition for lips comprising 0.1 to 2% by weight of a cooling agent based on the total weight of the cosmetic composition. 청구항 1에 있어서, 상기 쿨링제는 메틸디이소프로필 프로피온아미드, 멘틸락테이트 및 에틸멘탄 카복사아미드를 포함하는 것인 입술용 화장료 조성물. The cosmetic composition for lips according to claim 1, wherein the cooling agent includes methyldiisopropyl propionamide, menthyl lactate and ethylmentane carboxamide. 청구항 1에 있어서, 상기 쿨링제는 화장료 조성물 총 중량 대비 메틸디이소프로필 프로피온아미드 0.01 내지 1중량%, 멘틸락테이트 0.01 내지 1중량% 및 에틸멘탄 카복사아미드 0.01 내지 1중량% 포함하는 것인 입술용 화장료 조성물. The lip of claim 1 , wherein the cooling agent comprises 0.01 to 1% by weight of methyldiisopropyl propionamide, 0.01 to 1% by weight of menthyl lactate, and 0.01 to 1% by weight of ethylmentane carboxamide, based on the total weight of the cosmetic composition cosmetic composition for use. 청구항 1에 있어서, 상기 쿨링제는 캡슐화된 것인 입술용 화장료 조성물. The cosmetic composition for lips according to claim 1, wherein the cooling agent is encapsulated. 청구항 1에 있어서, 상기 화장료 조성물은 립스틱, 립글로스, 립틴트 또는 립락커 중 어느 하나인 입술용 화장료 조성물.

The cosmetic composition for lips according to claim 1, wherein the cosmetic composition is any one of lipstick, lip gloss, lip tint, and lip lacquer.

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* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN115089503A (en) * 2022-07-19 2022-09-23 吴成林 Water-soluble cool agent and preparation method thereof

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* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2017058594A1 (en) * 2015-10-01 2017-04-06 Senomyx, Inc. Compounds useful as modulators of trpm8
KR20180117035A (en) * 2017-04-18 2018-10-26 코스맥스 주식회사 matt type cosmetic compostion for lips

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2017058594A1 (en) * 2015-10-01 2017-04-06 Senomyx, Inc. Compounds useful as modulators of trpm8
KR20180117035A (en) * 2017-04-18 2018-10-26 코스맥스 주식회사 matt type cosmetic compostion for lips

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN115089503A (en) * 2022-07-19 2022-09-23 吴成林 Water-soluble cool agent and preparation method thereof

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