CN110721119A - Cosmetic stock solution, preparation method and application thereof, and face cream - Google Patents

Cosmetic stock solution, preparation method and application thereof, and face cream Download PDF

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Publication number
CN110721119A
CN110721119A CN201810777542.8A CN201810777542A CN110721119A CN 110721119 A CN110721119 A CN 110721119A CN 201810777542 A CN201810777542 A CN 201810777542A CN 110721119 A CN110721119 A CN 110721119A
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Prior art keywords
sodium hyaluronate
stock solution
cosmetic
cosmetic stock
linseed oil
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陈其亮
陈明夕
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Huludao Zhensugu Biotechnology Co Ltd
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Huludao Zhensugu Biotechnology Co Ltd
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Priority to CN201810777542.8A priority Critical patent/CN110721119A/en
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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/92Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
    • A61K8/922Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/73Polysaccharides
    • A61K8/735Mucopolysaccharides, e.g. hyaluronic acid; Derivatives thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • A61Q19/08Anti-ageing preparations

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  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Veterinary Medicine (AREA)
  • Animal Behavior & Ethology (AREA)
  • General Health & Medical Sciences (AREA)
  • Public Health (AREA)
  • Birds (AREA)
  • Epidemiology (AREA)
  • Dermatology (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Chemical & Material Sciences (AREA)
  • Gerontology & Geriatric Medicine (AREA)
  • Cosmetics (AREA)

Abstract

The invention provides a cosmetic stock solution, a preparation method and application thereof, and a face cream, wherein each liter of the cosmetic stock solution comprises the following components: 50-200 g of linseed oil; 10-300 g of emulsifier; 1-20 g of sodium hyaluronate; 5-300 g of a humectant; 1-5 g of preservative; the balance of water. The cosmetic stock solution and the face cream provided by the invention can really enter the surface layer of the skin, permeate into the cells of a human body and nourish the cells.

Description

Cosmetic stock solution, preparation method and application thereof, and face cream
Technical Field
The invention relates to the technical field of cosmetics, in particular to a cosmetic stock solution, a preparation method and application thereof, and a face cream.
Background
The facial mask liquid, essence and cream are various in types, and mainly comprise cleaning, moisturizing, whitening, freckle removing and the like. The facial mask liquid, essence and cream are covered on the face for a short time, so that the external air and pollution are temporarily isolated, the skin temperature is increased, pores of the skin are promoted to expand, and sweat gland secretion and metabolism are promoted. The facial mask liquid and the essence are beneficial to the skin to remove products of epidermal cell metabolism and accumulated grease substances, and the facial cream is moist, moisturized and whitened and is adopted by women who love beauty for a long time.
However, the skin surface layer of human is very compact in structure, and the stratum corneum layer is protected by a film made of non-hydrophilic substances such as fatty acid, lactic acid, amino acid and the like, so that the skin surface layer of human cannot enter water, and most cosmetics are nutritional substances added into human, which cannot enter the skin surface layer due to the large molecular structure. According to scientific tests, the nutrient substances which can really enter the surface layer of the skin are less than 5 percent at best, namely 95 percent of the nutrient substances cannot enter the surface layer of the skin and provide nutrient substances for skin cells. Moreover, some cheap cosmetics in the market are not only not helpful for facial skin care, but also cause damage to sensitive skin.
Disclosure of Invention
The invention aims to provide a cosmetic stock solution, a preparation method and application thereof, and a face cream.
In order to achieve the above object, the present invention provides the following technical solutions:
the invention provides a cosmetic stock solution, each liter of which comprises the following components:
Figure BDA0001731711480000011
preferably, the linseed oil is cold-rolled linseed oil, and the alpha-linolenic acid content in the cold-rolled linseed oil is more than 45 wt.%.
Preferably, the emulsifier comprises one or more of olive oil emulsifier, wheat germ emulsifier, cetearyl alcohol, cetearyl glucoside, cetyl glucoside and polyglyceryl-3-methylglucdistearate.
Preferably, the sodium hyaluronate is a compound of high-molecular sodium hyaluronate and small-molecular sodium hyaluronate; the molecular weight of the high-molecular sodium hyaluronate is 100-170 ten thousand; the molecular weight of the micromolecular sodium hyaluronate is 20-40 ten thousand.
Preferably, when the sodium hyaluronate is a compound of high-molecular sodium hyaluronate and small-molecular sodium hyaluronate, the mass ratio of the high-molecular sodium hyaluronate to the small-molecular sodium hyaluronate is 1: 1-1: 10.
preferably, the humectant comprises one or more of glycerin, 1, 3-propanediol, an amino acid humectant, 1, 3-butanediol, squalane, and sorbitol.
The invention also provides a preparation method of the cosmetic stock solution, which comprises the following steps:
(1) dissolving an emulsifier in water to obtain an emulsion;
(2) mixing linseed oil with the emulsion obtained in the step (1) to obtain a mixed solution;
(3) and (3) mixing sodium hyaluronate, a humectant and a preservative with the mixed solution obtained in the step (2) to obtain a cosmetic stock solution.
The invention also provides application of the cosmetic stock solution in the technical scheme or the cosmetic stock solution prepared by the preparation method in the technical scheme in facial mask liquid or essence.
The invention also provides a face cream which comprises the cosmetic stock solution in the technical scheme or the cosmetic stock solution prepared by the preparation method in the technical scheme and a gelling agent.
Preferably, the gelling agent comprises one or more of AVC ice crystals, carrageenan, and agar powder.
The invention provides a cosmetic stock solution, which comprises the following components per liter: 50-200 g of linseed oil; 10-300 g of emulsifier; 1-20 g of sodium hyaluronate; 5-300 g of a humectant; 1-5 g of preservative; the balance of water. The linseed oil is added into the cosmetic stock solution, and the linseed oil is rich in alpha-linolenic acid, has a molecular structure similar to fatty acid ester in a skin cuticle, can really enter the skin surface layer and deeply permeate into human cells to nourish the cells, can greatly slow down the aging of skin cells under the action of being matched with other components of the cosmetic, effectively improves the dull state of the skin, and has the effects of resisting skin chronic inflammation and smoothing facial skin micro wrinkles.
The cream provided by the invention contains linseed oil, so that the cream also has the effects of greatly slowing down skin cell aging, effectively improving the dull state of skin, and resisting chronic inflammation of the skin and smoothing fine wrinkles of the facial skin.
Detailed Description
The invention provides a cosmetic stock solution, each liter of which comprises the following components:
Figure BDA0001731711480000031
the cosmetic stock solution provided by the invention comprises 50-200 g of linseed oil, preferably 80-200 g, and more preferably 100-170 g in total amount of 1L. In the present invention, the linseed oil is preferably cold-rolled linseed oil; the content of alpha-linolenic acid in the cold-rolled linseed oil is preferably more than 45 wt.%, and more preferably 53 wt.% to 58 wt.%. The source of the linseed oil is not particularly required in the invention, and the linseed oil with the source well known to those skilled in the art can be adopted. The linseed oil is rich in alpha-linolenic acid, the alpha-linolenic acid belongs to omega-3 series polyene fatty acid, is essential fatty acid for human body, has a molecular structure similar to fatty acid ester in skin cuticle, and can enter the skin surface layer and deeply permeate into human body cells to nourish the cells. In addition, the linseed oil enables the alpha-linolenic acid (omega-3) to be ingested in a sufficient amount to maintain the stability of facial skin cell membranes and form a layer of protective film on the skin cell membranes, so that the contact of inflammation and cancer factors formed by excessive ingestion of linoleic acid (omega-6) with skin cells is prevented, the stability and the safety of the skin cell membranes are ensured, the activity of the skin cells is greatly improved, and the aging and death of the skin cells are delayed; secondly, the alpha-linolenic acid (omega-3) in the linseed oil can prevent platelet winding, reduce blood viscosity in capillaries, promote blood circulation, improve oxygen carrying capacity of red blood cells, and further improve the dark state of skin; thirdly, the alpha-linolenic acid (omega-3) in the linseed oil also has the effect of resisting chronic inflammation of the skin; after the alpha-linolenic acid (omega-3) in the linseed oil enters human cells, the secretion of collagen is stimulated, and the gradually reduced collagen is supplemented from inside, so that the appearance of wrinkles can be effectively slowed down, and the smoothing effect on the appeared fine wrinkles can be realized.
The cosmetic stock solution provided by the invention comprises 10-300 g of emulsifier, preferably 10-200 g, and more preferably 20-150 g in total amount of 1L. In the present invention, the emulsifier preferably includes one or more of olive oil emulsifier, wheat germ emulsifier, cetearyl alcohol, cetearyl glucoside, cetyl glucoside, and polyglyceryl-3-methylglucdistearate. The source of the emulsifier is not particularly required in the present invention, and the source of the emulsifier known to those skilled in the art can be used, specifically, a commercially available emulsifier. The emulsifier of the invention has excellent skin affinity, is easy to absorb, can form a liquid crystal structure, is easy to spread, obtains fresh and silky hand feeling and has long-term moisture retention, thereby enhancing the elasticity and the smoothness of skin.
The cosmetic stock solution provided by the invention comprises 1-20 g of sodium hyaluronate, preferably 5-20 g, and more preferably 10-20 g, calculated by total amount of 1L. In the invention, the sodium hyaluronate is preferably a compound of high molecular sodium hyaluronate and small molecular sodium hyaluronate; the relative molecular weight of the high molecular sodium hyaluronate is preferably 100 to 170 ten thousand, and more preferably 120 to 170 ten thousand; the relative molecular weight of the small molecule sodium hyaluronate is preferably 20 to 40 ten thousand, and more preferably 25 to 35 ten thousand. In the invention, when the sodium hyaluronate is a compound of high-molecular sodium hyaluronate and small-molecular sodium hyaluronate, the mass ratio of the high-molecular sodium hyaluronate to the small-molecular sodium hyaluronate is preferably 1: 1-1: 10, most preferably 1: 1. The macromolecular sodium hyaluronate can form a breathable film on the surface of skin, so that the skin is smooth and moist, and invasion of external bacteria, dust and the like is blocked; the small molecule sodium hyaluronate can permeate into dermis, and has the effects of slightly dilating capillary vessels, increasing blood circulation, improving intermediate metabolism and promoting skin nutrition absorption; the two are compounded for use, can keep skin moist, smooth, fine, tender and elastic, and simultaneously has the effects of preventing wrinkles, resisting wrinkles, beautifying, protecting health and recovering the physiological function of the skin. The source of the sodium hyaluronate is not particularly required in the invention, and the sodium hyaluronate from which the source is well known to those skilled in the art can be adopted.
The cosmetic stock solution provided by the invention comprises 5-300 g of humectant, preferably 50-300 g, and more preferably 100-200 g, calculated by total 1L. In the present invention, the humectant preferably includes one or more of glycerin, 1, 3-propanediol, an amino acid humectant, 1, 3-butanediol, squalane, and sorbitol. The source of the humectant is not particularly required in the present invention, and humectants of sources well known to those skilled in the art can be used. The moisturizing agent provided by the invention can increase the permeability and moisture retention of facial mask liquid.
The cosmetic stock solution provided by the invention comprises 1-5 g of preservative, preferably 1-3 g, and more preferably 2-3 g, calculated by total 1L. In the present invention, the preservative preferably includes one or more of suma K220, ethylparaben, methylparaben, propylparaben, phenoxyethanol, suma K100, suma K350 and 2-methyl-4-isothiazolin-3-one, and more preferably suma K220. The invention does not require any particular source of preservative, and preservatives of a source well known to those skilled in the art, such as commercially available preservatives, may be used. The preservative has a broad-spectrum balanced inhibition function on bacteria, saccharomycetes and mould.
The cosmetic stock solution provided by the invention comprises the balance of water in a total amount of 1L. In the present invention, the water is preferably deionized water. The invention has no special requirement on the source of the deionized water, and the deionized water with the source known by the technicians in the field can be adopted.
The invention provides a preparation method of the cosmetic stock solution, which comprises the following steps:
(1) dissolving an emulsifier in water to obtain an emulsion;
(2) mixing linseed oil with the emulsion obtained in the step (1) to obtain a mixed solution;
(3) and (3) mixing sodium hyaluronate, a humectant and a preservative with the mixed solution obtained in the step (2) to obtain a cosmetic stock solution.
The invention melts the emulsifier in water to obtain the emulsion. In the invention, the temperature of the water is preferably 60-90 ℃, and more preferably 70-75 ℃. The invention preferably adopts a stirring mode for melting, has no special requirements on the stirring time and speed, and can achieve the effect of uniform melting. According to the invention, the emulsifier is preferably added into water for melting; before the emulsifier is added into water, the emulsifier is preferably heated and melted; the invention has no special requirement on the heating and melting temperature, and can realize the purpose of melting.
After the emulsion is obtained, the linseed oil is mixed with the emulsion to obtain a mixed solution. In the invention, the mixing is preferably stirring mixing, and the invention has no special requirements on the stirring mixing time and speed, and can achieve the effect of uniform mixing. In the present invention, the temperature of the emulsion during mixing is preferably 30 to 60 ℃, and more preferably 35 to 40 ℃. In the invention, if the temperature of the emulsion is higher than 60 ℃, the linseed oil is added, and the unsaturated acid content of the linseed oil is high, so that the linseed oil is oxidized under the condition of higher than 60 ℃ and the skin care effect is influenced.
After the mixed solution is obtained, the sodium hyaluronate, the humectant and the preservative are mixed with the mixed solution to obtain the cosmetic stock solution. In the present invention, the mixing is preferably stirring mixing; the invention has no special requirements on the stirring and mixing time and speed, and can achieve the effect of uniform mixing. The adding sequence of the sodium hyaluronate, the humectant and the preservative has no special requirement, and any substance can be added firstly. The sodium hyaluronate, the humectant and the preservative are preferably added into the mixed solution to be mixed; before the sodium hyaluronate and the humectant are added into the mixed solution, preferably, the sodium hyaluronate and the humectant are respectively or together dissolved in water to obtain water solutions respectively containing the sodium hyaluronate and the humectant or mixed water solutions containing the sodium hyaluronate and the humectant, and then the water solutions are added into the mixed solution; when the method that the sodium hyaluronate and the humectant are dissolved in water and then added into the mixed solution is adopted, the method has no special requirement on the water dosage for dissolving the sodium hyaluronate and the humectant, and the total volume of the obtained cosmetic stock solution can meet the requirement together with water used in other preparation steps.
The invention also provides application of the cosmetic stock solution in the technical scheme or the cosmetic stock solution prepared by the preparation method in the technical scheme in facial mask liquid or essence. The facial mask liquid or essence can be cosmetic stock solution only, or can be added with a thickening agent on the basis of the cosmetic stock solution. In the present invention, the thickener preferably includes one or more of synthetic egg white powder, carbomer, hydroxyethyl cellulose and hydroxymethyl cellulose. The source of the thickener is not particularly required in the present invention, and thickeners of sources well known to those skilled in the art may be used. The amount of the thickener is not particularly required, and is determined according to the actual requirement of the cosmetic stock solution in the production or application process.
The invention also provides a face cream which comprises the cosmetic stock solution in the technical scheme or the cosmetic stock solution and the gel prepared by the preparation method in the technical scheme.
The cream provided by the invention preferably comprises 5-12 g of gelling agent, and more preferably 6-10 g, calculated by total 1L. In the present invention, the gelling agent preferably comprises one or more of AVC ice crystals, carrageenan and agar powder, and more preferably AVC ice crystals. The source of the gelling agent is not particularly required in the invention, and the gelling agent with the source well known to those skilled in the art can be adopted. The gel provided by the invention has rheological property and can bring pleasant skin feeling to people.
The preparation method of the facial cream has no special requirements, and the gel is directly added into the cosmetic stock solution in the technical scheme. Preferably, in the preparation scheme of the cosmetic stock solution, the linseed oil and the emulsion are mixed to obtain a mixed solution, and a gelling agent is added simultaneously; other steps are the same as the technical scheme for preparing the cosmetic stock solution, and are not repeated. The addition mode of the gel agent has no special requirement, and the addition mode known by the technicians in the field can be adopted.
The present invention provides a cosmetic raw liquid, a preparation method and application thereof, and a cream, which will be described in detail with reference to the following examples, but they should not be construed as limiting the scope of the present invention.
Example 1
Respectively weighing 2.5g of Freyda small molecule sodium hyaluronate (relative molecular weight of 30W) and 2.5g of high molecule sodium hyaluronate (relative molecular weight of 150W), 50g of amino acid humectant, and dissolving with deionized water to 400ml for later use;
weighing olive oil emulsifier olym 100050g, heating for melting, slowly adding into 300ml of 75 ℃ hot water under stirring, and emulsifying uniformly to obtain an emulsion;
cooling the emulsion to 40 ℃, adding weighed 100g of linseed oil into the emulsion under stirring, and uniformly dispersing to obtain a mixed solution;
adding dissolved sodium hyaluronate and amino acid humectant into the mixed solution, adding 1, 3-propylene glycol and glycerol each 50g and antiseptic K2202g, adding deionized water to 1000ml, and stirring to obtain cosmetic stock solution.
The cosmetic stock solution can be directly used as facial mask solution or essence.
Example 2
Respectively weighing 5g of Freyda small molecule sodium hyaluronate (relative molecular weight of 20W) and 5g of high molecule sodium hyaluronate (molecular weight of 140W), 100g of amino acid humectant, and dissolving with deionized water to 400ml for later use;
weighing olive oil emulsifier olym 100050g, heating for melting, slowly adding into 300ml of 75 ℃ hot water under stirring, and emulsifying uniformly to obtain an emulsion;
slowly cooling the emulsion to 35 ℃, slowly adding the weighed 100g of linseed oil into the emulsion under stirring, and uniformly dispersing to obtain a mixed solution;
adding dissolved sodium hyaluronate and amino acid humectant into the mixed solution, adding 100g of 1, 3-propylene glycol and glycerol respectively and preservative K2205g, adding 1000ml of egg white powder and deionized water 1g, and stirring uniformly to obtain the facial mask solution.
Example 3
Respectively weighing 2.5g of Freyda small molecule sodium hyaluronate (relative molecular weight of 40W) and 2.5g of high molecule sodium hyaluronate (molecular weight of 170W), 80g of amino acid humectant, and dissolving with deionized water to 400ml for later use;
weighing olive oil emulsifier olym 100050g, heating for melting, slowly adding into 300ml of hot water at 90 ℃ while stirring, and emulsifying uniformly to obtain an emulsion;
slowly cooling the emulsion to 35 ℃, slowly adding the weighed 100g of linseed oil and 10g of AVC ice crystal gel into the emulsion under stirring, and uniformly dispersing to obtain a mixed solution;
adding dissolved sodium hyaluronate and amino acid humectant into the mixed solution, adding 1, 3-propylene glycol and glycerin each 50g and preservative K2202g, adding deionized water to 1000ml, stirring and dispersing uniformly, standing for gel forming, and making into facial cream.
The foregoing is only a preferred embodiment of the present invention, and it should be noted that, for those skilled in the art, various modifications and decorations can be made without departing from the principle of the present invention, and these modifications and decorations should also be regarded as the protection scope of the present invention.

Claims (10)

1. A cosmetic stock solution comprising per litre the following components:
Figure FDA0001731711470000011
2. the cosmetic stock solution of claim 1, wherein the linseed oil is cold-rolled linseed oil, and the alpha-linolenic acid content of the cold-rolled linseed oil is more than 45 wt.%.
3. The cosmetic stock solution of claim 1 wherein the emulsifier comprises one or more of olive oil emulsifier, wheat germ emulsifier, cetearyl alcohol, cetearyl glucoside, cetyl glucoside, and polyglyceryl-3-methylglucdistearate.
4. The cosmetic bulk according to claim 1, wherein the sodium hyaluronate is a complex of a polymeric sodium hyaluronate and a small molecule sodium hyaluronate; the relative molecular weight of the high molecular sodium hyaluronate is 100-170 ten thousand; the relative molecular weight of the small molecule sodium hyaluronate is 20-40 ten thousand.
5. The cosmetic stock solution according to claim 4, wherein when the sodium hyaluronate is a compound of high molecular sodium hyaluronate and small molecular sodium hyaluronate, the mass ratio of the high molecular sodium hyaluronate to the small molecular sodium hyaluronate is 1: 1-1: 10.
6. the cosmetic stock solution of claim 1, wherein the humectant comprises one or more of glycerin, 1, 3-propanediol, an amino acid humectant, 1, 3-butanediol, squalane, and sorbitol.
7. A process for preparing a cosmetic stock solution according to any one of claims 1 to 6, comprising the steps of:
(1) dissolving an emulsifier in water to obtain an emulsion;
(2) mixing linseed oil with the emulsion obtained in the step (1) to obtain a mixed solution;
(3) and (3) mixing sodium hyaluronate, a humectant and a preservative with the mixed solution obtained in the step (2) to obtain a cosmetic stock solution.
8. Use of a cosmetic raw liquid according to any one of claims 1 to 7 in a facial mask liquid or essence.
9. A cream comprising the cosmetic stock solution of any one of claims 1 to 7 and a gelling agent.
10. The cream of claim 9, wherein the gelling agent comprises one or more of AVC ice crystals, carrageenan, and agar powder.
CN201810777542.8A 2018-07-16 2018-07-16 Cosmetic stock solution, preparation method and application thereof, and face cream Pending CN110721119A (en)

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN112438905A (en) * 2020-12-03 2021-03-05 澳思美日用化工(广州)有限公司 Moisturizing and skin-brightening composition and application thereof

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CN105233270A (en) * 2015-11-12 2016-01-13 上海昊海生物科技股份有限公司 Medicine composition for water-optical treatment and application of medicine composition
CN107375039A (en) * 2017-09-04 2017-11-24 银川凤仪堂生物工程有限公司 Add the skin care item and preparation technology of egg yolk lecithin

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Publication number Priority date Publication date Assignee Title
KR20110128707A (en) * 2010-05-24 2011-11-30 박의신 Functional Cosmetics Using Estrogen
CN105233270A (en) * 2015-11-12 2016-01-13 上海昊海生物科技股份有限公司 Medicine composition for water-optical treatment and application of medicine composition
CN107375039A (en) * 2017-09-04 2017-11-24 银川凤仪堂生物工程有限公司 Add the skin care item and preparation technology of egg yolk lecithin

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN112438905A (en) * 2020-12-03 2021-03-05 澳思美日用化工(广州)有限公司 Moisturizing and skin-brightening composition and application thereof
CN112438905B (en) * 2020-12-03 2021-09-07 澳思美日用化工(广州)有限公司 Moisturizing and skin-brightening composition and application thereof

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Application publication date: 20200124