CN110699025B - 一种螺纹锁固脂 - Google Patents

一种螺纹锁固脂 Download PDF

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CN110699025B
CN110699025B CN201910986275.XA CN201910986275A CN110699025B CN 110699025 B CN110699025 B CN 110699025B CN 201910986275 A CN201910986275 A CN 201910986275A CN 110699025 B CN110699025 B CN 110699025B
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任晓辰
吴韦岐
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Xi'an Marcott New Material Technology Co ltd
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Abstract

本发明属于螺纹锁固密封技术领域,特别是涉及一种螺纹锁固脂。包括组分A和组分B,组分A按其重量份数计,由E‑51环氧树脂11‑14份、液体羧基丁腈橡胶3‑3.9份、AG‑80环氧树脂30‑35份、活性稀释剂501 2‑3.5份、丁腈‑40 6.8‑8份、2#白钢玉微粉30‑32份、铝粉6‑9份和气相二氧化硅2‑3份组成;组分B为缩胺105环氧树脂12‑15份。解决了现有技术中的螺纹锁固脂粘结强度、相容性、润滑性和防腐能力都较差的技术问题。相比现有技术中的螺纹锁固脂具有更好的润滑性以及粘结强度。

Description

一种螺纹锁固脂
技术领域
本发明属于螺纹锁固密封技术领域,特别是涉及一种螺纹锁固脂。
背景技术
现有技术中的石油套管以及尾管等的连接都是通过螺纹连接,或者焊接及铆接来实现的,该连接方式施工量大施工工艺复杂。螺纹锁固脂是类似于黏胶一样的产品,其可应用于金属与金属的连接及密封。但现有技术中关于螺纹锁固脂配方公开的还较少,且螺纹锁固脂的润滑性较差,并且其这对小型材质的锁固粘结尚且可以满足,但石油套管以及尾管,在工作过程中其经常需要下放各种仪器及设备,因此对于石油套管以及尾管上的螺纹锁固脂,其对螺纹锁固脂的相容性、润滑性、防腐性以及粘结强度都具有更高的要求,目前现有技术中还没有能够很好的满足其需求的。
发明内容
本发明目的是,提供了一种螺纹锁固脂,解决了现有技术中的螺纹锁固脂粘结强度、相容性、润滑性和防腐能力都较差的技术问题。
为了实现上述发明目的,本发明的具体技术方案是:一种螺纹锁固脂,包括组分A和组分B,组分A按其重量份数计,由E-51环氧树脂11-14份、液体羧基丁腈橡胶3-3.9份、AG-80环氧树脂30-35份、活性稀释剂501 2-3.5份、丁腈-40 6.8-8份、2#白钢玉微粉30-32份、铝粉6-9份和气相二氧化硅2-3份组成;组分B为缩胺105环氧树脂12-15份。
进一步的,组分A按其重量份数计,由E-51环氧树脂11份、液体羧基丁腈橡胶3份、AG-80环氧树脂30份、活性稀释剂501 2份、丁腈-40 6.8份、2#白钢玉微粉30份、铝粉6份和气相二氧化硅2份组成;
进一步的,组分A按其重量份数计,由E-51环氧树脂13份、液体羧基丁腈橡胶3.9份、AG-80环氧树脂33份、活性稀释剂501 3.2份、丁腈-40 6.8份、2#白钢玉微粉30份、铝粉6份和气相二氧化硅2.5份组成。
进一步的,组分A按其重量份数计,由E-51环氧树脂14份、液体羧基丁腈橡胶3.9份、AG-80环氧树脂35份、活性稀释剂501 3.5份、丁腈-40 8份、2#白钢玉微粉32份、铝粉9份和气相二氧化硅3份组成。
进一步的,铝粉为工业级250目。
有益效果:通过整体配方的组合从而使产品的闪点更高,达到了265℃,使用更加安全;组分A与B完成复配后有效使用时间更长,在25℃温度下可达到46分钟-120分钟;通过丁腈-40的加入从而使得E-51环氧树脂和AG-80环氧树脂得到了一定的改性,通过丁腈-40中的活性端基与环氧树脂中的活性基团,反应形成链段,从而显著提高了其固化性能、剪切强度、拉伸强度和抗冲强度,剪切强度32MPa,拉伸强度26MPa,抗冲强度6578J/㎡;通过2#白钢玉微粉的加入从而使其与铝粉、气相二氧化硅结合后,从而显著提高螺纹锁固脂的润滑性;通过E-51环氧树脂和AG-80环氧树脂的加入从而使螺纹锁固脂的防腐性能和粘结性更强,通过液体羧基丁腈橡胶的加入从而使螺纹锁固脂具有更好的耐油性,更好的适用于油管套管的连接。
具体实施方式
下面结合具体实施例对本发明作进一步的详细描述。
一种螺纹锁固脂,包括组分A和组分B,组分A按其重量份数计,由E-51环氧树脂11-14份、液体羧基丁腈橡胶3-3.9份、AG-80环氧树脂30-35份、活性稀释剂501 2-3.5份、丁腈-40 6.8-8份、2#白钢玉微粉30-32份、铝粉6-9份和气相二氧化硅2-3份组成;组分B为缩胺105环氧树脂12-15份。
E-51环氧树脂为黄色粘稠液体,具有环氧值高、粘度低、色泽浅,广泛用作粘接剂、无溶剂涂料、自流平地坪料、浇注料。
液体羧基丁腈橡胶由丁二烯、丙烯腈和有机酸(丙烯酸、甲基丙烯酸等)三元共聚而成。简称XNBR,相对密度0.98~0.99。引入羧基增加了极性,增大NBR与PVC和酚醛树脂的相容性,赋予高强度,具有良好的粘接性和耐老化性,改进耐磨性和撕裂强度。
AG-80环氧树脂是一种工业生产的四缩水甘油胺型环氧树脂的实际官能度大约为3-3.5,可用芳香胺、酸酐、双氰胺及咪唑类固化剂固化的物品。高耐热、耐化学药品性优良,固化后的树脂表现出很好的耐热性和化学稳定性。覆铜板中主要用于遮蔽紫外线。UV涂料、无溶剂涂料、高耐热乙烯基树脂、重防腐涂料树脂,电工浇注,PCB层压板、印刷电路板,成型材料、风电复合材料;涂料,粘接剂等,已用作飞机次结构的复合材料和宇航结构复合材料。还可用作耐热胶粘剂的导电胶粘剂。
丁腈-40国产丁腈橡胶的一种。
活性稀释剂501是一种环氧活性稀释剂一般是指带有一个或两个以上环氧基的低分子化合物,它们可以直接参与环氧树脂的固化反应,成为环氧树脂固化物交联网络结构的一部分,对固化产物的性能几乎无影响,有时还能增加固化体系的韧性。
铝粉为工业级250目。
实施例1,所述螺纹锁固脂,包括组分A和组分B,其中组分A按其重量计,由E-51环氧树脂110g、液体羧基丁腈橡胶30g、AG-80环氧树脂300g、活性稀释剂501 20g、丁腈-4068g、2#白钢玉微粉300g、铝粉60g和气相二氧化硅20g组成;B组分缩胺105环氧树脂134.38g。
实施例2,所述螺纹锁固脂,包括组分A和组分B,其中组分A按其重量计,由E-51环氧树脂140g、液体羧基丁腈橡胶39g、AG-80环氧树脂350g、活性稀释剂501 35g、丁腈-4080g、2#白钢玉微粉320g、铝粉90g和气相二氧化硅30g组成,B组分缩胺105环氧树脂160g。
最优实施例,所述螺纹锁固脂,包括组分A和组分B,其中组分A按其重量计,由E-51环氧树脂130g、液体羧基丁腈橡胶39g、AG-80环氧树脂330g、活性稀释剂501 32g、丁腈-4068g、2#白钢玉微粉300g、铝粉60g和气相二氧化硅25g组成;B组分缩胺105环氧树脂146g。
使用过程中将组分B以10:1.38~10:15.5的比例混合,然后处理油管或套管表面,然后涂抹本发明所述螺纹锁固脂,10分钟后将油管或套管螺纹结合固定,然后保持静止24小时,螺纹锁固完成。
通过对本发明所述螺纹锁固脂进行检测报告,以及结合参照一与参照二,实验结果记录如下,其中参照一:青岛拓普石油化工有限公司生产的螺纹锁固脂;参照二:乐泰268螺纹锁固脂肪;两个厂家的螺纹锁固作为参照一与参照二与本申请中所述的实施例1、实施例2以及最优实施例实验结果对比如下。
Figure BDA0002236800540000051
Figure BDA0002236800540000061
通过本发明所述的螺纹锁固脂检测报告,以及与现有市场上的产品的对比,发现本申请技术方案中所述的螺纹锁固脂,实施例1、2以及最优实施例,各项指标都明显优于现有参照产品。其中最优实施例的闪点达到了265℃;组分A与B完成复配后有效使用时间更长,在25℃温度下可达到分钟;通过丁腈-40的加入从而使得E-51环氧树脂和AG-80环氧树脂得到了一定的改性,通过丁腈-40中的活性端基与环氧树脂中的活性基团,反应形成链段,从而显著提高了其固化性能、剪切强度、拉伸强度和抗冲强度,剪切强度32MPa,拉伸强度26MPa,抗冲强度6578J/㎡;通过2#白钢玉微粉的加入从而使其与铝粉、气相二氧化硅结合后,从而显著提高螺纹锁固脂的润滑性;通过E-51环氧树脂和AG-80环氧树脂的加入从而使螺纹锁固脂的防腐性能和粘结性更强,通过液体羧基丁腈橡胶的加入从而使螺纹锁固脂具有更好的耐油性,更好的适用于油管套管的连接。

Claims (1)

1.一种螺纹锁固脂,其特征在于:所述螺纹锁固脂,包括组分A和组分B,其中组分A按其重量计,由E-51树脂130g、液体羧基丁腈橡胶39g、AG-80环氧树脂330g、活性稀释剂50132g、丁腈-40 68g、2#白钢玉微粉300g、铝粉60g和气相二氧化硅25g组成;组分B缩胺105环氧树脂146g。
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CN1613888A (zh) * 2003-11-05 2005-05-11 北京航空航天大学 一种环氧树脂超低温胶粘剂及其制备方法
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