CN110628517A - Natural edible detergent and preparation method thereof - Google Patents
Natural edible detergent and preparation method thereof Download PDFInfo
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- CN110628517A CN110628517A CN201910926294.3A CN201910926294A CN110628517A CN 110628517 A CN110628517 A CN 110628517A CN 201910926294 A CN201910926294 A CN 201910926294A CN 110628517 A CN110628517 A CN 110628517A
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/66—Non-ionic compounds
- C11D1/662—Carbohydrates or derivatives
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/20—Organic compounds containing oxygen
- C11D3/22—Carbohydrates or derivatives thereof
- C11D3/222—Natural or synthetic polysaccharides, e.g. cellulose, starch, gum, alginic acid or cyclodextrin
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/38—Products with no well-defined composition, e.g. natural products
- C11D3/382—Vegetable products, e.g. soya meal, wood flour, sawdust
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/48—Medical, disinfecting agents, disinfecting, antibacterial, germicidal or antimicrobial compositions
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/50—Perfumes
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- Organic Chemistry (AREA)
- Health & Medical Sciences (AREA)
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- Emergency Medicine (AREA)
- Detergent Compositions (AREA)
Abstract
The invention discloses a natural edible detergent which comprises the following components in percentage by weight: 20-35% of soapberry peel extracting solution, 15-25% of tea seed powder extracting solution, 1-5% of thickening agent, 0.01-0.2% of preservative, 0.01-0.05% of essence and the balance of deionized water; the invention also discloses a preparation method of the natural edible detergent; the natural edible detergent is prepared by extracting plants containing natural active ingredients, has scientific formula and proportioning, does not add any artificially synthesized chemicals, has strong dirt-removing power, does not stimulate the body temperature of people, and has no toxic or side effect.
Description
Technical Field
The invention relates to the technical field of daily chemical products, in particular to a natural edible detergent and a preparation method thereof.
Background
The detergent is a common washing article in family life, is generally used for cleaning oil stains on tableware, and mainly comprises a surfactant. At present, components such as surfactants, preservatives and the like used in the liquid detergent are generally synthetic chemicals, and the surfactants have the advantages of strong detergency, good solubility and low cost, but chemical substances can be removed only by washing for many times after the liquid detergent is used, water resources are wasted, and the environment is polluted due to improper treatment of chemical excrement. When the detergent containing the synthetic chemicals is used for a long time, on one hand, trace detergent components remained on tableware can cause potential threat to human bodies, on the other hand, the detergent can generate negative effects on the skin of users of the detergent, the skin is easy to be rough and yellow, and particularly, uncomfortable symptoms such as red swelling and the like can be generated on hands of the users with sensitive skin after the detergent is used.
Disclosure of Invention
Aiming at the defects of the prior art, the invention aims to provide the natural edible detergent which is prepared by extracting plants containing natural active ingredients, has scientific formula and proportioning, does not add any artificially synthesized chemicals, has strong dirt-removing capability, does not stimulate the body temperature of people and has no toxic or side effect.
In order to achieve the purpose, the invention adopts the following technical scheme:
a natural edible detergent comprises the following components in percentage by weight: 20-35% of soapberry peel extracting solution, 15-25% of tea seed powder extracting solution, 1-5% of thickening agent, 0.01-0.2% of preservative, 0.01-0.05% of essence and the balance of deionized water;
the preparation method of the soapberry peel extracting solution comprises the following steps: weighing soapberry peel, adding the soapberry peel into water with the weight 5-10 times of that of the soapberry peel, leaching for 5-10h at 60-100 ℃, filtering and separating to obtain filtrate and filter residue, adding the filter residue into the water, leaching for 3-5h at 60-100 ℃, filtering and separating again to obtain filtrate, combining the filtrates of the two times, centrifuging, and collecting supernatant to obtain a soapberry peel extracting solution;
the preparation method of the tea seed powder extracting solution comprises the following steps: drying camellia seed meal in an electric heating forced air drying box at 60-80 ℃ until the moisture of the camellia seed meal is less than 6%, crushing the camellia seed meal by a crusher, sieving the camellia seed meal by a 40-80 mesh sieve to obtain camellia seed powder, mixing the camellia seed powder with petroleum ether, removing grease by Soxhlet extraction, adding the camellia seed powder without the grease into 60-80% ethanol according to the material-liquid ratio of 1:8-12(g/mL), leaching for 3-5h at 70-90 ℃, then carrying out suction filtration and centrifugation, collecting supernatant, carrying out reduced pressure distillation and recovering the ethanol to obtain a camellia seed powder extracting solution.
Preferably, the composition comprises the following components in percentage by weight: 25% of soapberry peel extracting solution, 20% of tea seed powder extracting solution, 3% of thickening agent, 0.1% of preservative, 0.03% of essence and the balance of deionized water.
Preferably, the composition comprises the following components in percentage by weight: 20% of soapberry peel extracting solution, 15% of tea seed powder extracting solution, 1% of thickening agent, 0.01% of preservative, 0.01% of essence and the balance of deionized water.
Preferably, the composition comprises the following components in percentage by weight: 35% of soapberry peel extracting solution, 25% of tea seed powder extracting solution, 5% of thickening agent, 0.2% of preservative, 0.05% of essence and the balance of deionized water.
Preferably, the thickening agent is one or more of alginic acid, sodium alginate, flaxseed gum, acacia gum and guar gum.
Preferably, the preservative is prepared by mixing lemongrass extract, honeysuckle extract and bamboo leaf extract according to the mass ratio of 1-3:1: 1.
Preferably, the essence is one or more of rose essence, jasmine essence, violet essence and clove essence.
In another aspect, the present invention also provides a preparation method of a natural edible detergent, comprising the following steps: mixing the soapberry peel extract, the tea seed powder extract, the thickening agent, the preservative, the essence and the deionized water uniformly according to a proportion, fully stirring for 30-60 mm, and standing for 4-5h to obtain the natural edible detergent.
Compared with the prior art, the invention has the beneficial technical effects that:
(1) the natural edible detergent is extracted from plants containing natural active ingredients, the formula proportion is scientific, and no artificially synthesized chemicals are added; the soapberry peel extracting solution contains rich saponin, the tea seed powder extracting solution contains rich tea saponin, and the tea saponin and the tea seed powder extracting solution are effectively combined and complemented to play a role in replacing the traditional chemical petroleum surfactant.
(2) According to the natural edible detergent, the plant extracting solution is selected as the preservative, so that the natural edible detergent has no toxic or side effect, and also has natural plant fragrance, wherein the lemon grass extracting solution mainly contains neral, geranial, limonene, citronellal, geraniol and the like, and has the effects of antibiosis, anticorrosion, antioxidation and the like; the honeysuckle extract mainly contains volatile oil, flavonoid, organic acid, triterpenes and inorganic elements, and has the effects of inhibiting bacteria, relieving allergy, delaying aging, preventing ultraviolet injury and the like; the bamboo leaf extract mainly contains flavonoid, phenols, esters and other components, has strong inhibiting effects on bacteria, mould, saccharomycetes and the like, particularly has a more remarkable inhibiting effect on the bacteria, can be used as a broad-spectrum antibacterial agent, is mixed according to a specific proportion and then used to play a synergistic effect, can effectively improve the antibacterial effect, not only reduces the antibacterial concentration, but also has a wider antibacterial range.
(3) The natural edible detergent is prepared by extracting plants containing natural active ingredients, has scientific formula and proportioning, does not add any artificially synthesized chemicals, has strong dirt-removing power, does not stimulate the body temperature of people, and has no toxic or side effect.
Detailed Description
The following further describes the embodiments of the present invention. It should be noted that the description of the embodiments is provided to help understanding of the present invention, but the present invention is not limited thereto. In addition, the technical features involved in the embodiments of the present invention described below may be combined with each other as long as they do not conflict with each other.
Example 1
A natural edible detergent comprises the following components in percentage by weight: 25% of soapberry peel extracting solution, 20% of tea seed powder extracting solution, 3% of thickening agent, 0.1% of preservative, 0.03% of essence and the balance of deionized water;
the preparation method of the soapberry peel extracting solution comprises the following steps: weighing soapberry peel, adding the soapberry peel into water with the weight 8 times that of the soapberry peel, leaching for 7 hours at 80 ℃, filtering and separating to obtain filtrate and filter residue, adding the filter residue into the water, leaching for 4 hours at 80 ℃, filtering and separating again to obtain filtrate, combining the filtrates of the two times, centrifuging, and collecting supernatant to obtain a soapberry peel extracting solution;
the preparation method of the tea seed powder extracting solution comprises the following steps: drying camellia seed meal in an electrothermal blowing drying box at 70 ℃ until the water content of the camellia seed meal is 4%, crushing the camellia seed meal by a crusher, sieving the camellia seed meal with a 60-mesh sieve to obtain camellia seed powder, mixing the camellia seed powder with petroleum ether, removing oil by Soxhlet extraction, adding the camellia seed powder without the oil into 70% ethanol according to the material-liquid ratio of 1:10(g/mL), extracting for 4 hours at 80 ℃, then carrying out suction filtration and centrifugation, collecting supernate, carrying out reduced pressure distillation, and recovering the ethanol to obtain a camellia seed powder extracting solution.
The thickening agent consists of alginic acid and sodium alginate.
The preservative is prepared by mixing a lemongrass extract, a honeysuckle extract and a bamboo leaf extract according to a mass ratio of 2:1: 1.
The essence is rose essence.
The preparation method of the natural edible detergent comprises the following steps: uniformly mixing the soapberry peel extract, the tea seed powder extract, alginic acid, sodium alginate, the lemon grass extract, the honeysuckle extract, the bamboo leaf extract, the rose essence and deionized water according to the weight percentage, fully stirring for 45 mm, and standing for 4.5h to obtain the natural edible detergent.
Example 2
A natural edible detergent comprises the following components in percentage by weight: 20% of soapberry peel extracting solution, 15% of tea seed powder extracting solution, 1% of thickening agent, 0.01% of preservative, 0.01% of essence and the balance of deionized water;
the preparation method of the soapberry peel extracting solution comprises the following steps: weighing soapberry peel, adding the soapberry peel into water with the weight 5 times that of the soapberry peel, leaching for 10 hours at 60 ℃, filtering and separating to obtain filtrate and filter residue, adding the filter residue into the water, leaching for 5 hours at 60 ℃, filtering and separating again to obtain filtrate, combining the filtrates of the two times, centrifuging, and collecting supernatant to obtain a soapberry peel extracting solution;
the preparation method of the tea seed powder extracting solution comprises the following steps: drying camellia seed meal in an electrothermal blowing drying box at 60 ℃ until the water content of the camellia seed meal is 5%, crushing the camellia seed meal by a crusher, sieving the camellia seed meal with a 40-mesh sieve to obtain camellia seed powder, mixing the camellia seed powder with petroleum ether, removing oil by Soxhlet extraction, adding the camellia seed powder without the oil into 60% ethanol according to the material-liquid ratio of 1:8(g/mL), extracting for 5 hours at 70 ℃, then carrying out suction filtration and centrifugation, collecting supernate, carrying out reduced pressure distillation, and recovering the ethanol to obtain a camellia seed powder extracting solution.
The thickening agent consists of linseed gum and Arabic gum.
The preservative is prepared by mixing a lemongrass extract, a honeysuckle extract and a bamboo leaf extract according to the mass ratio of 1:1: 1.
The essence is jasmine essence.
The preparation method of the natural edible detergent comprises the following steps: uniformly mixing the soapberry peel extract, the tea seed powder extract, the flaxseed gum, the Arabic gum, the lemon grass extract, the honeysuckle extract, the bamboo leaf extract, the jasmine essence and the deionized water in proportion according to the weight percentage, fully stirring for 30 mm, and standing for 4h to obtain the natural edible detergent.
Example 3
A natural edible detergent comprises the following components in percentage by weight: 35% of soapberry peel extracting solution, 25% of tea seed powder extracting solution, 5% of thickening agent, 0.2% of preservative, 0.05% of essence and the balance of deionized water;
the preparation method of the soapberry peel extracting solution comprises the following steps: weighing soapberry peel, adding the soapberry peel into water with the weight being 10 times of that of the soapberry peel, leaching for 5 hours at 100 ℃, filtering and separating to obtain filtrate and filter residue, adding the filter residue into the water, leaching for 3 hours at 100 ℃, filtering and separating again to obtain filtrate, combining the filtrates of the two times, centrifuging, and collecting supernatant to obtain a soapberry peel extracting solution;
the preparation method of the tea seed powder extracting solution comprises the following steps: drying camellia seed meal in an electrothermal blowing drying box at 80 ℃ until the water content of the camellia seed meal is 3%, crushing the camellia seed meal by a crusher, sieving the camellia seed meal with an 80-mesh sieve to obtain camellia seed powder, mixing the camellia seed powder with petroleum ether, removing oil by Soxhlet extraction, adding the camellia seed powder without the oil into 80% ethanol according to the material-liquid ratio of 1:12(g/mL), extracting for 3 hours at 90 ℃, then carrying out suction filtration and centrifugation, collecting supernate, carrying out reduced pressure distillation, and recovering the ethanol to obtain a camellia seed powder extracting solution.
The thickening agent is guar gum.
The preservative is prepared by mixing a lemongrass extract, a honeysuckle extract and a bamboo leaf extract according to a mass ratio of 3:1: 1.
The essence is violet essence and clove essence.
The preparation method of the natural edible detergent comprises the following steps: uniformly mixing the soapberry peel extract, the tea seed powder extract, the guar gum, the lemon grass extract, the honeysuckle extract, the bamboo leaf extract, the violet essence, the clove essence and deionized water according to the weight percentage, fully stirring for 45 mm, and standing for 4.5h to obtain the natural edible detergent.
Comparative example 1
A natural edible detergent comprises the following components in percentage by weight: 25% of soapberry peel extracting solution, 20% of tea seed powder extracting solution, 3% of thickening agent, 0.1% of preservative, 0.03% of essence and the balance of deionized water;
the preparation method of the soapberry peel extracting solution comprises the following steps: weighing soapberry peel, adding the soapberry peel into water with the weight 8 times that of the soapberry peel, leaching for 7 hours at 80 ℃, filtering and separating to obtain filtrate and filter residue, adding the filter residue into the water, leaching for 4 hours at 80 ℃, filtering and separating again to obtain filtrate, combining the filtrates of the two times, centrifuging, and collecting supernatant to obtain a soapberry peel extracting solution;
the preparation method of the tea seed powder extracting solution comprises the following steps: drying camellia seed meal in an electrothermal blowing drying box at 70 ℃ until the water content of the camellia seed meal is 4%, crushing the camellia seed meal by a crusher, sieving the camellia seed meal with a 60-mesh sieve to obtain camellia seed powder, mixing the camellia seed powder with petroleum ether, removing oil by Soxhlet extraction, adding the camellia seed powder without the oil into 70% ethanol according to the material-liquid ratio of 1:10(g/mL), extracting for 4 hours at 80 ℃, then carrying out suction filtration and centrifugation, collecting supernate, carrying out reduced pressure distillation, and recovering the ethanol to obtain a camellia seed powder extracting solution.
The thickening agent consists of alginic acid and sodium alginate.
The antiseptic is herba Cymbopogonis Citrari extractive solution.
The essence is rose essence.
The preparation method of the natural edible detergent comprises the following steps: uniformly mixing the soapberry peel extracting solution, the tea seed powder extracting solution, alginic acid, sodium alginate, the lemon grass extracting solution, the rose essence and deionized water according to the weight percentage, fully stirring for 45 mm, and standing for 4.5 hours to obtain the natural edible detergent.
Comparative example 2
A natural edible detergent comprises the following components in percentage by weight: 25% of soapberry peel extracting solution, 20% of tea seed powder extracting solution, 3% of thickening agent, 0.1% of preservative, 0.03% of essence and the balance of deionized water;
the preparation method of the soapberry peel extracting solution comprises the following steps: weighing soapberry peel, adding the soapberry peel into water with the weight 8 times that of the soapberry peel, leaching for 7 hours at 80 ℃, filtering and separating to obtain filtrate and filter residue, adding the filter residue into the water, leaching for 4 hours at 80 ℃, filtering and separating again to obtain filtrate, combining the filtrates of the two times, centrifuging, and collecting supernatant to obtain a soapberry peel extracting solution;
the preparation method of the tea seed powder extracting solution comprises the following steps: drying camellia seed meal in an electrothermal blowing drying box at 70 ℃ until the water content of the camellia seed meal is 4%, crushing the camellia seed meal by a crusher, sieving the camellia seed meal with a 60-mesh sieve to obtain camellia seed powder, mixing the camellia seed powder with petroleum ether, removing oil by Soxhlet extraction, adding the camellia seed powder without the oil into 70% ethanol according to the material-liquid ratio of 1:10(g/mL), extracting for 4 hours at 80 ℃, then carrying out suction filtration and centrifugation, collecting supernate, carrying out reduced pressure distillation, and recovering the ethanol to obtain a camellia seed powder extracting solution.
The thickening agent consists of alginic acid and sodium alginate.
The preservative is composed of honeysuckle extract and bamboo leaf extract.
The essence is rose essence.
The preparation method of the natural edible detergent comprises the following steps: uniformly mixing the soapberry peel extracting solution, the tea seed powder extracting solution, alginic acid, sodium alginate, the honeysuckle extracting solution, the bamboo leaf extracting solution, the rose essence and deionized water according to the weight percentage, fully stirring for 45 mm, and standing for 4.5h to obtain the natural edible detergent.
Comparative example 3
A natural edible detergent comprises the following components in percentage by weight: 25% of soapberry peel extracting solution, 20% of tea seed powder extracting solution, 3% of thickening agent, 0.1% of preservative, 0.03% of essence and the balance of deionized water;
the preparation method of the soapberry peel extracting solution comprises the following steps: weighing soapberry peel, adding the soapberry peel into water with the weight 8 times that of the soapberry peel, leaching for 7 hours at 80 ℃, filtering and separating to obtain filtrate and filter residue, adding the filter residue into the water, leaching for 4 hours at 80 ℃, filtering and separating again to obtain filtrate, combining the filtrates of the two times, centrifuging, and collecting supernatant to obtain a soapberry peel extracting solution;
the preparation method of the tea seed powder extracting solution comprises the following steps: drying camellia seed meal in an electrothermal blowing drying box at 70 ℃ until the water content of the camellia seed meal is 4%, crushing the camellia seed meal by a crusher, sieving the camellia seed meal with a 60-mesh sieve to obtain camellia seed powder, mixing the camellia seed powder with petroleum ether, removing oil by Soxhlet extraction, adding the camellia seed powder without the oil into 70% ethanol according to the material-liquid ratio of 1:10(g/mL), extracting for 4 hours at 80 ℃, then carrying out suction filtration and centrifugation, collecting supernate, carrying out reduced pressure distillation, and recovering the ethanol to obtain a camellia seed powder extracting solution.
The thickening agent consists of alginic acid and sodium alginate.
The preservative is prepared by mixing a lemongrass extract, a honeysuckle extract and a bamboo leaf extract according to a mass ratio of 4:1: 1.
The essence is rose essence.
The preparation method of the natural edible detergent comprises the following steps: uniformly mixing the soapberry peel extract, the tea seed powder extract, alginic acid, sodium alginate, the lemon grass extract, the honeysuckle extract, the bamboo leaf extract, the rose essence and deionized water according to the weight percentage, fully stirring for 45 mm, and standing for 4.5h to obtain the natural edible detergent.
Comparative example 4
A natural edible detergent comprises the following components in percentage by weight: 25% of soapberry peel extracting solution, 20% of tea seed powder extracting solution, 3% of thickening agent, 0.1% of preservative, 0.03% of essence and the balance of deionized water;
the preparation method of the soapberry peel extracting solution comprises the following steps: weighing soapberry peel, adding the soapberry peel into water with the weight 8 times that of the soapberry peel, leaching for 7 hours at 80 ℃, filtering and separating to obtain filtrate and filter residue, adding the filter residue into the water, leaching for 4 hours at 80 ℃, filtering and separating again to obtain filtrate, combining the filtrates of the two times, centrifuging, and collecting supernatant to obtain a soapberry peel extracting solution;
the preparation method of the tea seed powder extracting solution comprises the following steps: drying camellia seed meal in an electrothermal blowing drying box at 70 ℃ until the water content of the camellia seed meal is 4%, crushing the camellia seed meal by a crusher, sieving the camellia seed meal with a 60-mesh sieve to obtain camellia seed powder, mixing the camellia seed powder with petroleum ether, removing oil by Soxhlet extraction, adding the camellia seed powder without the oil into 70% ethanol according to the material-liquid ratio of 1:10(g/mL), extracting for 4 hours at 80 ℃, then carrying out suction filtration and centrifugation, collecting supernate, carrying out reduced pressure distillation, and recovering the ethanol to obtain a camellia seed powder extracting solution.
The thickening agent consists of alginic acid and sodium alginate.
The preservative is prepared by mixing lemongrass extract, honeysuckle extract and bamboo leaf extract according to the mass ratio of 0.5:1: 1.
The essence is rose essence.
The preparation method of the natural edible detergent comprises the following steps: uniformly mixing the soapberry peel extract, the tea seed powder extract, alginic acid, sodium alginate, the lemon grass extract, the honeysuckle extract, the bamboo leaf extract, the rose essence and deionized water according to the weight percentage, fully stirring for 45 mm, and standing for 4.5h to obtain the natural edible detergent.
Stain removal test
Refer to the detergency determination method of appendix B of "hand dishwashing detergents" of GB 9985-2000. The detergency of the natural edible detergents prepared in examples 1 to 3 of the present invention was measured. Wherein the judgment of the detergency is as follows: if the oil removal rate of the tested dish washing detergent is not less than that of the standard dish washing detergent, the tested dish washing detergent is qualified, otherwise, the tested dish washing detergent is unqualified, wherein the oil removal rate of the standard dish washing detergent is 36.4%, and the test results are shown in the following table 1.
TABLE 1 detergency results for oil removal of examples 1-3 from standard dishwashing detergent
| Example 1 | Example 2 | Example 3 | Standard tableware detergent | |
| Oil removal rate | 45.8 | 41.2 | 40.6 | 36.4 |
From table 1, it can be seen that the detergency of the natural edible detergent prepared according to the present invention can satisfy the detergency of tableware.
Skin irritation test
The skin irritation effect of the natural edible detergents prepared in examples 1 to 3 of the present invention was measured by referring to the skin irritation test method of the cosmetic hygiene code (2007 edition), and the skin irritation effect was generally expressed by scoring the skin reaction, and the test results are shown in table 2 below.
Table 2 examples 1-3 and standard dishwashing detergent skin irritation results
| Example 1 | Example 2 | Example 3 | Standard tableware detergent | |
| Skin response score | 0.25 | 0.3 | 0.28 | 0.42 |
From table 2, it can be seen that the integral evaluation of the natural edible detergent prepared by the present invention is less than 0.5, which indicates that the natural edible detergent prepared by the present invention has little or no irritation to skin.
Test of bacteriostatic Effect
The bactericidal effect of the natural edible detergents prepared in examples 1 to 3 and comparative examples 1 to 4 of the present invention was determined by referring to the method of "evaluation method of antibacterial and bacteriostatic effect of daily chemical products" of QB/T2738-2012, and the test results are shown in table 3 below.
TABLE 3 results of bactericidal effects of examples 1 to 3 and comparative examples 1 to 4 on Staphylococcus aureus, Pseudomonas aeruginosa, Candida albicans and Escherichia coli
| Staphylococcus aureus (%) | Pseudomonas aeruginosa (%) | Candida albicans (%) | Escherichia coli (%) | |
| Example 1 | 98.86 | 98.63 | 98.82 | 98.91 |
| Example 2 | 98.24 | 98.16 | 98.17 | 98.03 |
| Example 3 | 98.35 | 98.05 | 98.18 | 98.24 |
| Comparative example 1 | 80.31 | 80.62 | 80.43 | 80.27 |
| Comparative example 2 | 85.16 | 86.01 | 85.64 | 85.83 |
| Comparative example 3 | 90.62 | 90.35 | 90.81 | 90.74 |
| Comparative example 4 | 91.37 | 91.64 | 91.38 | 91.28 |
From the table 3, the sterilization rate of the natural edible detergent prepared by the invention on staphylococcus aureus, pseudomonas aeruginosa, candida albicans and escherichia coli reaches more than 98%, which shows that the natural edible detergent prepared by the invention meets the standard sterilization rate and can be preserved and inhibited; the bacteriostatic rates of the examples 1 to 3 are all higher than those of the comparative examples 1 to 4, which shows that the lemon grass extract, the honeysuckle extract and the bamboo leaf extract in the invention are mixed according to a specific proportion and then used, so that the synergistic effect is exerted, and the antibacterial effect can be effectively improved, wherein the proportion of the example 1 is most reasonable, and the antibacterial effect is optimal.
The embodiments of the present invention have been described in detail, but the present invention is not limited to the described embodiments. It will be apparent to those skilled in the art that various changes, modifications, substitutions and alterations can be made in these embodiments without departing from the principles and spirit of the invention, and the scope of protection is still within the scope of the invention.
Claims (8)
1. The natural edible detergent is characterized by comprising the following components in percentage by weight: 20-35% of soapberry peel extracting solution, 15-25% of tea seed powder extracting solution, 1-5% of thickening agent, 0.01-0.2% of preservative, 0.01-0.05% of essence and the balance of deionized water;
the preparation method of the soapberry peel extracting solution comprises the following steps: weighing soapberry peel, adding the soapberry peel into water with the weight 5-10 times of that of the soapberry peel, leaching for 5-10h at 60-100 ℃, filtering and separating to obtain filtrate and filter residue, adding the filter residue into the water, leaching for 3-5h at 60-100 ℃, filtering and separating again to obtain filtrate, combining the filtrates of the two times, centrifuging, and collecting supernatant to obtain a soapberry peel extracting solution;
the preparation method of the tea seed powder extracting solution comprises the following steps: drying camellia seed meal in an electric heating forced air drying box at 60-80 ℃ until the moisture of the camellia seed meal is less than 6%, crushing the camellia seed meal by a crusher, sieving the camellia seed meal by a 40-80 mesh sieve to obtain camellia seed powder, mixing the camellia seed powder with petroleum ether, removing grease by Soxhlet extraction, adding the camellia seed powder without the grease into 60-80% ethanol according to the material-liquid ratio of 1:8-12(g/mL), leaching for 3-5h at 70-90 ℃, then carrying out suction filtration and centrifugation, collecting supernatant, carrying out reduced pressure distillation and recovering the ethanol to obtain a camellia seed powder extracting solution.
2. The natural edible detergent according to claim 1, which is composed of the following components in percentage by weight: 25% of soapberry peel extracting solution, 20% of tea seed powder extracting solution, 3% of thickening agent, 0.1% of preservative, 0.03% of essence and the balance of deionized water.
3. The natural edible detergent according to claim 1, which is composed of the following components in percentage by weight: 20% of soapberry peel extracting solution, 15% of tea seed powder extracting solution, 1% of thickening agent, 0.01% of preservative, 0.01% of essence and the balance of deionized water.
4. The natural edible detergent according to claim 1, which is composed of the following components in percentage by weight: 35% of soapberry peel extracting solution, 25% of tea seed powder extracting solution, 5% of thickening agent, 0.2% of preservative, 0.05% of essence and the balance of deionized water.
5. The natural edible detergent as claimed in any one of claims 1 to 4, wherein the thickener is one or more of alginic acid, sodium alginate, flaxseed gum, gum arabic and guar gum.
6. The natural edible detergent as claimed in any one of claims 1 to 4, wherein the preservative is formed by mixing lemongrass extract, honeysuckle extract and bamboo leaf extract according to a mass ratio of 1-3:1: 1.
7. The natural edible detergent according to any one of claims 1-4, wherein the essence is one or more of rose essence, jasmine essence, violet essence and clove essence.
8. A method of preparing a natural edible liquid detergent according to any one of claims 1-7, comprising the steps of: mixing the soapberry peel extract, the tea seed powder extract, the thickening agent, the preservative, the essence and the deionized water uniformly according to a proportion, fully stirring for 30-60 mm, and standing for 4-5h to obtain the natural edible detergent.
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN112410134A (en) * | 2020-11-27 | 2021-02-26 | 简国新 | Green, safe and residue-free detergent and preparation method thereof |
| CN112430510A (en) * | 2020-12-01 | 2021-03-02 | 简国新 | Bacteriostatic detergent containing plant surfactant and preparation method thereof |
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|---|---|---|---|---|
| KR101108284B1 (en) * | 2011-04-08 | 2012-01-31 | 고도윤 | Multi-layered soap and method for preparing the same |
| CN105838520A (en) * | 2016-04-28 | 2016-08-10 | 郑州人造金刚石及制品工程技术研究中心有限公司 | Antibacterial botanic liquid detergent and preparing method thereof |
| CN106947615A (en) * | 2017-03-23 | 2017-07-14 | 广汉川西第泉饮品有限公司 | A kind of liquid detergent |
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Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| KR101108284B1 (en) * | 2011-04-08 | 2012-01-31 | 고도윤 | Multi-layered soap and method for preparing the same |
| CN105838520A (en) * | 2016-04-28 | 2016-08-10 | 郑州人造金刚石及制品工程技术研究中心有限公司 | Antibacterial botanic liquid detergent and preparing method thereof |
| CN106947615A (en) * | 2017-03-23 | 2017-07-14 | 广汉川西第泉饮品有限公司 | A kind of liquid detergent |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN112410134A (en) * | 2020-11-27 | 2021-02-26 | 简国新 | Green, safe and residue-free detergent and preparation method thereof |
| CN112430510A (en) * | 2020-12-01 | 2021-03-02 | 简国新 | Bacteriostatic detergent containing plant surfactant and preparation method thereof |
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