CN110585094A - Miaoling cleansing mousse capable of deeply cleansing, refreshing and moisturizing and preparation method thereof - Google Patents
Miaoling cleansing mousse capable of deeply cleansing, refreshing and moisturizing and preparation method thereof Download PDFInfo
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Abstract
The wonderful face cleansing mousse capable of deeply cleansing, refreshing and moisturizing and the preparation method thereof comprise the following components in parts by weight: sodium cocoyl amino acid; total flavonoids of astragalus membranaceus; cocamidopropyl betaine; potassium laureth phosphate; cocamide DEA; extracting solution from the root of the sprouting vegetable; a humectant, essential oils; bis (hydroxymethyl) imidazolidinyl urea; and (3) water. In the formula, the extract liquid added to the root of the sprouting vegetable contains a large amount of VC, flavonoid and soluble polysaccharide active substances, so that the sprouting vegetable has the effects of a bactericide and an antioxidant, and meanwhile, the root of the sprouting vegetable is reused as a waste component, so that the sprouting vegetable meets the requirement of green production, and the material cost is greatly reduced; the total flavonoids of astragalus are added as a whitening agent, so that melanin deposition can be effectively printed; the effect is better when the total flavonoids of astragalus and the vitamins in the extract liquid of the root of the sprouting vegetable are used together; can effectively clean face deeply, does not need heating in the preparation process, and is suitable for industrial production and home-made self-use.
Description
Technical Field
The invention relates to the technical field of face cleaning materials, in particular to a wonderful age face cleaning mousse capable of deeply cleaning, refreshing and preserving moisture and a preparation method thereof.
Background
The traditional facial cleanser focuses on efficient cleaning, blackhead removal, oil removal and the like, the stimulation of the product to the skin is ignored, in order to improve the cleaning power and the oil removal capability, components such as a surfactant with extremely strong alkalinity, a foaming agent, a soap base and the like are added, because the skin of a human body is weakly acidic, the skin can be stimulated after long-time use, a sebum membrane is damaged, and once the sebum membrane is lost, the skin is easily damaged by the outside. The amino acid facial cleaning product is a novel concept facial cleaning product, adopts a weakly acidic amino acid surfactant, is mild and skin-friendly, and has little irritation. The most important characteristics of the cleansing cream are high-efficiency cleansing, mild skin friendliness, low irritation and applicability to both children and sensitive skin. However, the prior amino acid facial cleansing products generally have the technical problems of high cost and complex preparation process.
Sprouting vegetable is a new favorite in the planting field, is developed to the army in various fields at present, and has unlimited business opportunities, however, the root part of sprouting vegetable is low in utilization rate, and a large amount of materials are wasted. How to efficiently utilize the roots of the waste sprouting vegetables is a difficult technical problem. As a large consumption field in the cosmetic industry, no prior cases of using sprouting vegetables exist at present.
Disclosure of Invention
The invention aims to provide a wonderful-age face-cleaning mousse capable of deeply cleaning, refreshing and moisturizing face and a preparation method thereof, and aims to solve the technical problems of high cost and complex preparation process of the existing amino acid face-cleaning products and solve the problem of serious root waste of sprouting vegetables.
In order to achieve the technical purpose, the invention adopts the following technical scheme:
the wonderful face cleaning mousse capable of deeply cleaning, refreshing and moisturizing the face is characterized by comprising the following components in parts by weight: 10-20 parts of sodium cocoyl amino acid; 0.02-0.2 parts of astragalus total flavonoids; 10-15 parts of cocamidopropyl betaine; 10-15 parts of potassium laureth phosphate; 10-15 parts of cocamide DEA; 5-20 parts of a sprout root extract; 10-20 parts of a humectant and 0.5-1 part of essential oil; 0.5-2 parts of bis (hydroxymethyl) imidazolidinyl urea; 30-50 parts of water.
As a preferred technical scheme of the invention, the wonderful age cleansing mousse capable of deeply cleansing, refreshing and moisturizing is characterized by comprising the following components in parts by weight: 12 parts of sodium cocoyl amino acid; 0.1 part of astragalus total flavonoids; 12 parts of cocamidopropyl betaine; 15 parts of potassium laureth phosphate; 10 parts of cocamide DEA; 10 parts of bud seedling vegetable root extract liquor; 20 parts of humectant and 0.5 part of essential oil; 0.5 part of bis (hydroxymethyl) imidazolidinyl urea; and 40 parts of water.
Preferably, the humectant comprises natural methylglycine proline and glycerol in a weight ratio of 1: (0.5 to 3).
More preferably, the composition further comprises 2-5 parts of a pH regulator, 1-5 parts of a vitamin and 1-5 parts of hyaluronic acid.
Preferably, the extract of the root of the sprout seedling vegetable is a mixed extract of the root of one or more sprout seedling vegetables of wheat sprout seedling vegetable, medlar sprout seedling vegetable, barley sprout seedling vegetable, perilla sprout seedling vegetable, dandelion sprout seedling vegetable or wild chrysanthemum sprout seedling vegetable which are subjected to rutin enrichment culture.
The preparation method of the bud seedling vegetable root extract liquid comprises the following steps:
step one, drying and crushing: cleaning and airing the roots of the bud seedling vegetable cut from the complete bud seedling vegetable, drying the bud seedling vegetable in an oven, and crushing the bud seedling vegetable by using a plant crusher to obtain bud seedling vegetable root powder;
step two, leaching: mixing the bud seedling vegetable root powder obtained in the step one with 60% -80% of ethanol, performing reflux extraction at the temperature of 40-60 ℃ for 1-10 hours, and repeatedly extracting for 1-5 times;
step three, flocculating and precipitating: clarifying agent of the natural plant extract;
step four, first centrifugation: centrifuging the mixed solution obtained in the step three to obtain a liquid phase;
step five, cooling and standing: cooling the liquid phase obtained in the step four to below room temperature, and standing to separate out part of high molecular weight substances;
step six, centrifuging for the second time: centrifuging the mixed solution obtained in the fifth step to obtain a liquid phase;
step seven, concentration: and (5) concentrating the liquid phase obtained in the step six at the normal temperature until the rutin content is 5-10 mg/L, and completing the preparation to obtain the bud seedling vegetable root extract.
Further preferably, the mixing weight ratio of the sprout root powder and 60-80% ethanol in the second step is 1: 10-1: 25.
Preferably, in the third step, the natural plant extract clarifier is KBT-ZTC.
In addition, the extraction method of the astragalus total flavonoids comprises the following steps:
firstly, cutting astragalus roots into short rods of 1cm, and placing the short rods into a container;
step two, adding absolute alcohol, refluxing for 2 hours at 70 ℃, pouring out the extracting solution and cooling;
step three, adding 48% NaOH aqueous solution into the extracting solution while stirring, and filtering to obtain yellow viscous precipitate;
step four, repeating the step two and the step three for 2-4 times until no yellow viscous precipitate is generated;
adding concentrated hydrochloric acid into the yellow viscous precipitate to adjust the pH value to 2-3, volatilizing purified water, and leaching for 3 times by using absolute ethyl alcohol to obtain a red solution containing flavone and analogues thereof and a white precipitate containing salt and cane sugar;
and step six, volatilizing alcohol to obtain red precipitate, namely the astragalus total flavone.
Finally, the invention provides a preparation method of the wonderful age cleansing mousse capable of deeply cleansing, refreshing and moisturizing, which is characterized by comprising the following steps:
step one, material preparation: preparing or weighing the required components according to the parts by weight;
step two, adding half of water into a mixing container;
step three, adding the humectant, the astragalus total flavonoids and the sprouting vegetable root extract into a mixing container, and uniformly stirring until the mixture is transparent;
step four, sodium cocoyl amino acid, cocamidopropyl betaine, potassium laureth phosphate and cocamide DEA are added; adding into a mixing container, adding the rest water, and stirring uniformly;
step five, adding the other components except the essential oil, and uniformly stirring;
step six, adding the essential oil, and slightly and uniformly stirring;
and step seven, filling the prepared solution into a foaming bottle, and storing for later use, so that the preparation is finished.
The potassium laureth phosphate has excellent foamability as an amino acid foaming agent, has fine and durable foam, and is suitable for being used as a raw material of foaming agents of toothpaste and cosmetics, shampoos and shaving cream; has antibacterial and bactericidal properties, mildew resistance, corrosion resistance and antistatic ability; low toxicity and low irritation; good biodegradability and no pollution to the environment.
The natural methylglycine proline exists in organism tissues, is a natural moisturizing factor, has the characteristics of high purity, easiness in use, good stability and the like, and has excellent moisturizing capability with excellent moisturizing effect in cosmetics and detergent products; the hand feeling is particularly smooth, and the skin can quickly permeate into skin tissues, so that the skin has the effects of luster, freshness and moistening; the skin has rapid penetration, moistening skin, sunscreen and anti-inflammatory effects. It can be used in combination with glycerol to effectively retain water and achieve facial moisturizing effect.
The total flavonoids of astragalus have better inhibition effect on tyrosinase and can well inhibit the synthesis of melanin. The astragalus whitening skin care soap disclosed by the invention has low skin irritation, and can effectively whiten the skin and inhibit melanin deposition.
The cocamidopropyl betaine has the advantages of small irritation, mild performance, fine, smooth, rich and stable foam, viscosity regulation, skin softness enhancement and sterilization effect, can be compounded with an anionic surfactant to improve the viscosity of a material body under the condition of pH 5.5-6.5, has an obvious thickening effect, is a main component for preparing mild baby shampoo, baby foam bath and baby skin care products, and can also be used as a detergent, a wetting agent, a thickening agent, an antistatic agent, a bactericide and the like.
The sprouting vegetable is a generally edible health-care vegetable, the extract of the root of the sprouting vegetable subjected to rutin enrichment culture contains a large amount of health-care components, researchers study the antioxidant activity of the sprouting vegetable by comparing the clearance rate of 5 sprouting vegetable extracting solutions on superoxide anion free radicals (O2-) and hydroxyl free radicals (. OH), and the results show that the comparison results of the clearance rates of the sprouting vegetable extracting solutions with different concentrations and different parts on the superoxide anion free radicals (O2-) and the hydroxyl free radicals (. OH) are consistent. Rutin belongs to vitamin medicine, has effects of reducing capillary permeability and fragility, maintaining and recovering normal elasticity of capillary, and can be used for preventing and treating hypertension cerebral hemorrhage; diabetic retinal hemorrhage, hemorrhagic purpura, etc., and also as food antioxidant and pigment. Rutin is also a main raw material for synthesizing troxerutin, and the troxerutin is a cardiovascular and cerebrovascular medicine, can effectively inhibit the aggregation of blood platelets and has the function of preventing thrombosis.
In addition, bis (hydroxymethyl) imidazolidinyl urea as a preservative and essential oils as a fragrance modulator, neither of which inhibit the efficacy of the other ingredients.
Compared with the prior art, the invention has the technical advantages that:
1. the extracting solution of the root of the sprouting vegetable is added into the formula, the extracting solution of the root of the sprouting vegetable contains a large amount of VC, flavonoid and small-particle soluble polysaccharide active substances, and has the effects of a bactericide and an antioxidant, wherein rutin has an excellent health-care function, and meanwhile, the root of the sprouting vegetable is reused as a waste component, so that the sprouting vegetable meets the requirement of green production, and the material cost is greatly reduced;
2. the natural plant extract clarifier is added in the extraction process of the bud seedling vegetable root extract, so that the bud seedling vegetable root extract has the characteristics of less dosage, low use cost, quick floc formation, thorough impurity removal, high safety and no harmful residues, and the particle state of the bud seedling vegetable root extract accords with the requirements of the cleansing mousse on the components;
2. the natural methylglycine proline and the glycerol are used in a matching manner and used as the humectant, so that the moisture can be effectively locked, and a good facial moisturizing effect is achieved;
3. the astragalus total flavonoids are added as a whitening agent, so that the melanin deposition can be effectively printed, and the effect is better when the astragalus total flavonoids are used in combination with vitamins in the extract liquid of the root of the sprouting vegetable;
4. the combination of sodium cocoyl amino acid, cocamidopropyl betaine, potassium laureth phosphate and cocamide DEA effectively achieves the effect of deep face cleaning, does not need heating in the preparation process, and is suitable for industrial production and home-made self-use.
Detailed Description
Hereinafter, an example of a musically aged cleansing mousse capable of deep cleansing, refreshing and moisturizing and a method for preparing the same according to the present invention will be described. The examples described herein are specific embodiments of the present invention, are intended to be illustrative and exemplary in nature, and are not to be construed as limiting the scope of the invention. In addition to the embodiments described herein, those skilled in the art will be able to employ other technical solutions which are obvious based on the disclosure of the claims and the specification of the present application, and these technical solutions include technical solutions which make any obvious replacement or modification for the embodiments described herein.
The principles and features of this invention are described below in conjunction with examples which are set forth to illustrate, but are not to be construed to limit the scope of the invention.
Example 1
The wonderful face cleaning mousse capable of deeply cleaning, refreshing and moisturizing the face comprises the following components in parts by weight: 10 parts of sodium cocoyl amino acid; 0.02 part of astragalus total flavonoids; 10 parts of cocamidopropyl betaine; 15 parts of potassium laureth phosphate; 10 parts of cocamide DEA; 20 parts of bud seedling vegetable root extract liquid; 10 parts of humectant and 0.5 part of essential oil; 0.5 part of bis (hydroxymethyl) imidazolidinyl urea; 50 parts of water. The sprouting vegetable is prepared from wheat sprouting vegetable and wild chrysanthemum sprouting vegetable in a ratio of 1: 1.
Wheat sprout, Chinese wolfberry sprout, barley sprout, perilla sprout, dandelion sprout or wild chrysanthemum sprout
The preparation method of the bud seedling vegetable root extract liquid comprises the following steps: cleaning and airing the roots of the bud seedling vegetable cut from the complete bud seedling vegetable, drying the bud seedling vegetable in an oven, and crushing the bud seedling vegetable by using a plant crusher to obtain bud seedling vegetable root powder; mixing the obtained sprout root powder with 60-80% ethanol at a weight ratio of 1:10, reflux-extracting at 40 deg.C for 6 hr, and repeatedly extracting for 3 times; adding a natural plant extract clarifying agent KBT-ZTC; centrifuging the obtained mixed solution to obtain a liquid phase; cooling the obtained liquid phase to below room temperature, and standing to separate out part of high molecular weight substances; and (3) second centrifugation: the resulting mixed solution was centrifuged to obtain a liquid phase.
The extraction method of the total flavonoids in astragalus comprises the following steps: cutting radix astragali into 1cm short rods, and placing into a container; adding anhydrous alcohol, refluxing at 70 deg.C for 2 hr, pouring out the extractive solution, and cooling; adding 48% NaOH aqueous solution into the extract while stirring, and filtering to obtain yellow viscous precipitate; repeating the second step and the third step for 2-4 times until no yellow viscous precipitate is generated; adding concentrated hydrochloric acid into the yellow viscous precipitate to adjust the pH value to 2-3, volatilizing purified water, and leaching for 3 times by using absolute ethyl alcohol to obtain a red solution containing flavone and analogues thereof and a white precipitate containing salt and cane sugar; volatilizing alcohol to obtain red precipitate, i.e. total flavonoids of astragalus.
The preparation method of the integral face cleaning mousse comprises the following steps: preparing or weighing the required components according to the parts by weight; adding one-half of the water into a mixing container; adding the humectant, the astragalus total flavonoids and the bud seedling vegetable root extract into a mixing container, and uniformly stirring until the mixture is transparent; adding sodium cocoyl amino acid, cocamidopropyl betaine, potassium laureth phosphate and cocamide DEA into a mixing container, adding the rest water, stirring uniformly, wherein heating is generally not needed, if the indoor temperature is extremely low or the solid is not dissolved, heating properly, adding the other components except the essential oil after the components are completely dissolved, stirring uniformly, adding the essential oil, and stirring slightly; and (4) filling the prepared solution into a foaming bottle, and storing for later use, thus finishing the preparation.
Example 2
The wonderful face cleaning mousse capable of deeply cleaning, refreshing and moisturizing the face comprises the following components in parts by weight: 12 parts of sodium cocoyl amino acid; 0.1 part of astragalus total flavonoids; 12 parts of cocamidopropyl betaine; 15 parts of potassium laureth phosphate; 10 parts of cocamide DEA; 10 parts of bud seedling vegetable root extract liquor; 20 parts of humectant and 0.9 part of essential oil; 0.5 part of bis (hydroxymethyl) imidazolidinyl urea; and 40 parts of water. The humectant comprises natural methylglycine proline and glycerol, and the weight mixing ratio of the natural methylglycine proline to the glycerol is 1: 0.5. the sprouting vegetable is prepared from barley sprouting vegetable, medlar sprouting vegetable and wild chrysanthemum sprouting vegetable in a ratio of 1:1: 1.
The preparation method of the bud seedling vegetable root extract liquid comprises the following steps: cleaning and airing the roots of the bud seedling vegetable cut from the complete bud seedling vegetable, drying the bud seedling vegetable in an oven, and crushing the bud seedling vegetable by using a plant crusher to obtain bud seedling vegetable root powder; mixing the obtained sprout root powder with 60-80% ethanol at a weight ratio of 1:25, reflux-extracting at 50 deg.C for 2 hr, and repeatedly extracting for 3 times; adding a natural plant extract clarifying agent KBT-ZTC; centrifuging the obtained mixed solution to obtain a liquid phase; cooling the obtained liquid phase to below room temperature, and standing to separate out part of high molecular weight substances; and (3) second centrifugation: the resulting mixed solution was centrifuged to obtain a liquid phase.
The extraction method of the total flavonoids in astragalus comprises the following steps: cutting radix astragali into 1cm short rods, and placing into a container; adding anhydrous alcohol, refluxing at 70 deg.C for 2 hr, pouring out the extractive solution, and cooling; adding 48% NaOH aqueous solution into the extract while stirring, and filtering to obtain yellow viscous precipitate; repeating the second step and the third step for 4 times until no yellow viscous precipitate is generated; adding concentrated hydrochloric acid into the yellow viscous precipitate to adjust pH to 2, volatilizing purified water, and leaching with anhydrous alcohol for 3 times to obtain red solution containing flavone and its analogues and white precipitate containing salt and sucrose; volatilizing alcohol to obtain red precipitate, i.e. total flavonoids of astragalus.
The overall cleansing mousse was prepared as in example 1.
Example 3
The wonderful face cleaning mousse capable of deeply cleaning, refreshing and moisturizing the face comprises the following components in parts by weight: 13 parts of sodium cocoyl amino acid; 0.05 part of astragalus total flavonoids; 10 parts of cocamidopropyl betaine; 15 parts of potassium laureth phosphate; 15 parts of cocamide DEA; 15 parts of bud seedling vegetable root extract liquor; 12 parts of humectant and 0.7 part of essential oil; 0.8 part of bis (hydroxymethyl) imidazolidinyl urea; 35 parts of water; 1 part of hyaluronic acid. The humectant comprises natural methylglycine proline and glycerol, and the weight mixing ratio of the natural methylglycine proline to the glycerol is 1: 1. the sprouting vegetable is prepared from barley sprouting vegetable, dandelion sprouting vegetable and wild chrysanthemum sprouting vegetable in a ratio of 1:1: 1.
The preparation method of the bud seedling vegetable root extract liquid comprises the following steps: cleaning and airing the roots of the bud seedling vegetable cut from the complete bud seedling vegetable, drying the bud seedling vegetable in an oven, and crushing the bud seedling vegetable by using a plant crusher to obtain bud seedling vegetable root powder; mixing the obtained sprout root powder with 60-80% ethanol at a weight ratio of 1:25, reflux-extracting at 40 deg.C for 6 hr, and repeatedly extracting for 3 times; adding a natural plant extract clarifying agent KBT-ZTC; centrifuging the obtained mixed solution to obtain a liquid phase; cooling the obtained liquid phase to below room temperature, and standing to separate out part of high molecular weight substances; and (3) second centrifugation: and (4) centrifuging the obtained mixed solution, and finally concentrating the liquid phase obtained in the step six at the normal temperature until the rutin content is 5-10 mg/L, so that the preparation is finished, and thus the bud seedling vegetable root extract is obtained.
A liquid phase is obtained.
The extraction method of the total flavonoids in astragalus comprises the following steps: cutting radix astragali into 1cm short rods, and placing into a container; adding anhydrous alcohol, refluxing at 70 deg.C for 2 hr, pouring out the extractive solution, and cooling; adding 48% NaOH aqueous solution into the extract while stirring, and filtering to obtain yellow viscous precipitate; repeating the second step and the third step for 2 times until no yellow viscous precipitate is generated; adding concentrated hydrochloric acid into the yellow viscous precipitate to adjust pH to 2.5, volatilizing purified water, and leaching with anhydrous alcohol for 3 times to obtain red solution containing flavone and its analogues and white precipitate containing salt and sucrose; volatilizing alcohol to obtain red precipitate, i.e. total flavonoids of astragalus.
The overall cleansing mousse was prepared as in example 1.
Example 4
The wonderful face cleaning mousse capable of deeply cleaning, refreshing and moisturizing the face comprises the following components in parts by weight: 20 parts of sodium cocoyl amino acid; 0.2 part of astragalus total flavonoids; 15 parts of cocamidopropyl betaine; 15 parts of potassium laureth phosphate; 13 parts of cocamide DEA; 18 parts of bud seedling vegetable root extract liquor; 10 parts of humectant and 0.5 part of essential oil; 2 parts of bis (hydroxymethyl) imidazolidinyl urea; 40 parts of water; 2 parts of sodium hydroxide; 5 parts of vitamins; 4 parts of hyaluronic acid. The humectant comprises natural methylglycine proline and glycerol, and the weight mixing ratio of the natural methylglycine proline to the glycerol is 1: 0.5. the sprouting vegetable is prepared from perilla sprouting vegetable, dandelion sprouting vegetable and medlar sprouting vegetable in a ratio of 1:2: 1.
The preparation method of the bud seedling vegetable root extract liquid comprises the following steps: cleaning and airing the roots of the bud seedling vegetable cut from the complete bud seedling vegetable, drying the bud seedling vegetable in an oven, and crushing the bud seedling vegetable by using a plant crusher to obtain bud seedling vegetable root powder; mixing the obtained sprout root powder with 60-80% ethanol at a weight ratio of 1:15, reflux-extracting at 55 deg.C for 1 hr, and repeatedly extracting for 5 times; adding a natural plant extract clarifying agent KBT-ZTC; centrifuging the obtained mixed solution to obtain a liquid phase; cooling the obtained liquid phase to below room temperature, and standing to separate out part of high molecular weight substances; and (3) second centrifugation: and (4) centrifuging the obtained mixed solution, and finally concentrating the liquid phase obtained in the step six at the normal temperature until the rutin content is 5-10 mg/L, so that the preparation is finished, and thus the bud seedling vegetable root extract is obtained.
The extraction method of the total flavonoids in astragalus comprises the following steps: cutting radix astragali into 1cm short rods, and placing into a container; adding anhydrous alcohol, refluxing at 70 deg.C for 2 hr, pouring out the extractive solution, and cooling; adding 48% NaOH aqueous solution into the extract while stirring, and filtering to obtain yellow viscous precipitate; repeating the second step and the third step for 2 times until no yellow viscous precipitate is generated; adding concentrated hydrochloric acid into the yellow viscous precipitate to adjust pH to 3, volatilizing purified water, and leaching with anhydrous alcohol for 3 times to obtain red solution containing flavone and its analogues and white precipitate containing salt and sucrose; volatilizing alcohol to obtain red precipitate, i.e. total flavonoids of astragalus.
The overall cleansing mousse was prepared as in example 1.
Example 5
The wonderful face cleaning mousse capable of deeply cleaning, refreshing and moisturizing the face comprises the following components in parts by weight: 18 parts of sodium cocoyl amino acid; 0.15 part of astragalus total flavonoids; 16 parts of cocamidopropyl betaine; 15 parts of potassium laureth phosphate; 15 parts of cocamide DEA; 18 parts of bud seedling vegetable root extract liquor; 15 parts of humectant and 0.9 part of essential oil; 1.5 parts of bis (hydroxymethyl) imidazolidinyl urea; 45 parts of water; 2 parts of sodium hydroxide; 3 parts of vitamin and 3 parts of hyaluronic acid. The humectant comprises natural methylglycine proline and glycerol, and the weight mixing ratio of the natural methylglycine proline to the glycerol is 1: 1.5. the sprouting vegetable is prepared by matching perilla sprouting vegetable and wild chrysanthemum sprouting vegetable in a ratio of 2: 1.
The preparation method of the bud seedling vegetable root extract liquid comprises the following steps: cleaning and airing the roots of the bud seedling vegetable cut from the complete bud seedling vegetable, drying the bud seedling vegetable in an oven, and crushing the bud seedling vegetable by using a plant crusher to obtain bud seedling vegetable root powder; mixing the obtained sprout root powder with 60-80% ethanol at a weight ratio of 1:10, reflux-extracting at 60 deg.C for 8 hr, and repeatedly extracting for 5 times; adding a natural plant extract clarifying agent KBT-ZTC; centrifuging the obtained mixed solution to obtain a liquid phase; cooling the obtained liquid phase to below room temperature, and standing to separate out part of high molecular weight substances; and (3) second centrifugation: and (4) centrifuging the obtained mixed solution, and finally concentrating the liquid phase obtained in the step six at the normal temperature until the rutin content is 5-10 mg/L, so that the preparation is finished, and thus the bud seedling vegetable root extract is obtained.
The extraction method of the total flavonoids in astragalus comprises the following steps: cutting radix astragali into 1cm short rods, and placing into a container; adding anhydrous alcohol, refluxing at 70 deg.C for 2 hr, pouring out the extractive solution, and cooling; adding 48% NaOH aqueous solution into the extract while stirring, and filtering to obtain yellow viscous precipitate; repeating the second step and the third step for 3 times until no yellow viscous precipitate is generated; adding concentrated hydrochloric acid into the yellow viscous precipitate to adjust pH to 2, volatilizing purified water, and leaching with anhydrous alcohol for 3 times to obtain red solution containing flavone and its analogues and white precipitate containing salt and sucrose; volatilizing alcohol to obtain red precipitate, i.e. total flavonoids of astragalus.
The overall cleansing mousse was prepared as in example 1.
Example 6
The wonderful face cleaning mousse capable of deeply cleaning, refreshing and moisturizing the face comprises the following components in parts by weight: 20 parts of sodium cocoyl amino acid; 0.18 part of astragalus total flavone; 13 parts of cocamidopropyl betaine; 15 parts of potassium laureth phosphate; 14 parts of cocamide DEA; 20 parts of bud seedling vegetable root extract liquid; 120 parts of humectant and 1 part of essential oil; 1 part of bis (hydroxymethyl) imidazolidinyl urea; 50 parts of water; 3 parts of vitamin and 3 parts of hyaluronic acid. The humectant comprises natural methylglycine proline and glycerol, and the weight mixing ratio of the natural methylglycine proline to the glycerol is 1: 2.5. the sprouting vegetable is wild chrysanthemum sprouting vegetable.
The preparation method of the bud seedling vegetable root extract liquid comprises the following steps: cleaning and airing the roots of the bud seedling vegetable cut from the complete bud seedling vegetable, drying the bud seedling vegetable in an oven, and crushing the bud seedling vegetable by using a plant crusher to obtain bud seedling vegetable root powder; mixing the obtained sprout root powder with 60-80% ethanol at a weight ratio of 1:20, reflux-extracting at 45 deg.C for 10 hr, and repeatedly extracting for 5 times; adding a natural plant extract clarifying agent KBT-ZTC; centrifuging the obtained mixed solution to obtain a liquid phase; cooling the obtained liquid phase to below room temperature, and standing to separate out part of high molecular weight substances; and (3) second centrifugation: and (4) centrifuging the obtained mixed solution, and finally concentrating the liquid phase obtained in the step six at the normal temperature until the rutin content is 5-10 mg/L, so that the preparation is finished, and thus the bud seedling vegetable root extract is obtained.
The extraction method of the total flavonoids in astragalus comprises the following steps: cutting radix astragali into 1cm short rods, and placing into a container; adding anhydrous alcohol, refluxing at 70 deg.C for 2 hr, pouring out the extractive solution, and cooling; adding 48% NaOH aqueous solution into the extract while stirring, and filtering to obtain yellow viscous precipitate; repeating the second step and the third step for 4 times until no yellow viscous precipitate is generated; adding concentrated hydrochloric acid into the yellow viscous precipitate to adjust pH to 3, volatilizing purified water, and leaching with anhydrous alcohol for 3 times to obtain red solution containing flavone and its analogues and white precipitate containing salt and sucrose; volatilizing alcohol to obtain red precipitate, i.e. total flavonoids of astragalus.
The overall cleansing mousse was prepared as in example 1.
The extract liquid of the bud seedling vegetable root in the embodiment is a mixed extract liquid of one or more bud seedling vegetable roots of wheat bud seedling vegetable, medlar bud seedling vegetable, barley bud seedling vegetable, perilla bud seedling vegetable, dandelion bud seedling vegetable or wild chrysanthemum bud seedling vegetable which are subjected to rutin enrichment culture. The rutin enrichment culture method comprises the following steps: firstly, extracting rutin from the tartary buckwheat sprout vegetable waste by adopting an ethanol extraction and ultrasonic auxiliary extraction method; then, preparing the extracted rutin extracting solution into a rutin solution with the weight percentage of 5 percent; then soaking the white newsprint in the solution for 5 minutes; and taking out the soaked newsprint, and drying the newsprint by using an infrared dryer to prepare the nutrient paper for cultivating the sprouting vegetables. Through determination, the rutin content of the prepared sprouting vegetable cultivation nutrient paper can reach 1.5 mg/g. The nutrient paper is used for cultivating according to a conventional cultivation method of the wheat sprout vegetables, and the rutin content of the roots of the wheat sprout vegetables is measured to be 0.113mg/g after harvesting.
Comparative example 1
The wonderful face cleaning mousse capable of deeply cleaning, refreshing and moisturizing the face comprises the following components in parts by weight: 20 parts of sodium cocoyl amino acid; 13 parts of cocamidopropyl betaine; 15 parts of potassium laureth phosphate; 14 parts of cocamide DEA; 120 parts of glycerol; 1 part of bis (hydroxymethyl) imidazolidinyl urea; 50 parts of water.
Comparative example 2
The wonderful face cleaning mousse capable of deeply cleaning, refreshing and moisturizing the face comprises the following components in parts by weight: 20 parts of sodium cocoyl amino acid; 0.18 part of astragalus total flavone; 13 parts of cocamidopropyl betaine; 15 parts of potassium laureth phosphate; 15 parts of cocamide DEA; 120 parts of glycerol; 1 part of bis (hydroxymethyl) imidazolidinyl urea; 50 parts of water; 3 parts of hyaluronic acid.
And (3) testing the product effect: the products of examples 1-6 were distributed to 50 subjects, wherein the subjects were between 30-55 years of age, female 30 in gender, male 20, and had healthy skin, no history of skin allergy, and met the test inclusion criteria.
The test method comprises the following steps: the subjects used the products of examples 1-6 and comparative examples 1 and 2 on their faces, respectively, once every morning and evening, for about one month continuously, followed by collecting visits and observing and feeling the effect of use. The test evaluation results are as follows (10 points full):
as can be seen from the above table, the testers had comprehensive advantages in terms of product appearance odor, foaming effect, cleansing effect, moisturizing effect, sunscreen effect and health care effect, and had significant benefits.
The above examples are only for describing the preferred embodiments of the present invention, and are not intended to limit the scope of the present invention, and various modifications and improvements made to the technical solution of the present invention by those skilled in the art without departing from the spirit of the present invention should fall within the protection scope defined by the claims of the present invention.
Claims (10)
1. The wonderful face cleaning mousse capable of deeply cleaning, refreshing and moisturizing the face is characterized by comprising the following components in parts by weight: 10-20 parts of sodium cocoyl amino acid; 0.02-0.2 parts of astragalus total flavonoids; 10-15 parts of cocamidopropyl betaine; 10-15 parts of potassium laureth phosphate; 10-15 parts of cocamide DEA; 5-20 parts of a sprout root extract; 10-20 parts of a humectant and 0.5-1 part of essential oil; 0.5-2 parts of bis (hydroxymethyl) imidazolidinyl urea; 30-50 parts of water.
2. The wonderful age mildy wash mousse capable of deeply cleansing, refreshing and moisturizing according to claim 1, which is characterized by comprising the following components in parts by weight: 12 parts of sodium cocoyl amino acid; 0.1 part of astragalus total flavonoids; 12 parts of cocamidopropyl betaine; 15 parts of potassium laureth phosphate; 10 parts of cocamide DEA; 10 parts of bud seedling vegetable root extract liquor; 20 parts of humectant and 0.5 part of essential oil; 0.5 part of bis (hydroxymethyl) imidazolidinyl urea; and 40 parts of water.
3. The wonderful age mildy wash mousse capable of deeply cleansing, refreshing and moisturizing as claimed in claim 1, wherein the moisturizing agent comprises natural methylglycine proline and glycerol in a weight ratio of 1: (0.5 to 3).
4. The wonderful age cleansing mousse capable of deeply cleansing, refreshing and moisturizing according to claim 1, further comprising 2-5 parts of a pH regulator, 1-5 parts of vitamins and 1-5 parts of hyaluronic acid.
5. The wonderful age mildy wash mousse capable of deeply cleansing, refreshing and moisturizing as claimed in claim 1, wherein the sprout seedling root extract is a mixed extract of the root of one or more sprout seedlings selected from wheat sprout seedling vegetable, medlar sprout seedling vegetable, barley sprout seedling vegetable, perilla sprout seedling vegetable, dandelion sprout seedling vegetable and wild chrysanthemum sprout seedling vegetable which are subjected to rutin enrichment culture.
6. The wonderful age mildy wash mousse capable of deeply cleansing, refreshing and moisturizing according to claim 1, wherein the sprout vegetable root extract is prepared by the following method:
step one, drying and crushing: cleaning and airing the roots of the bud seedling vegetable cut from the complete bud seedling vegetable, drying the bud seedling vegetable in an oven, and crushing the bud seedling vegetable by using a plant crusher to obtain bud seedling vegetable root powder;
step two, leaching: mixing the bud seedling vegetable root powder obtained in the step one with 60% -80% of ethanol, performing reflux extraction at the temperature of 40-60 ℃ for 1-10 hours, and repeatedly extracting for 1-5 times;
step three, flocculating and precipitating: clarifying agent of the natural plant extract;
step four, first centrifugation: centrifuging the mixed solution obtained in the step three to obtain a liquid phase;
step five, cooling and standing: cooling the liquid phase obtained in the step four to below room temperature, and standing to separate out part of high molecular weight substances;
step six, centrifuging for the second time: centrifuging the mixed solution obtained in the fifth step to obtain a liquid phase;
step seven, concentration: and (5) concentrating the liquid phase obtained in the step six at the normal temperature until the rutin content is 5-10 mg/L, and thus, completing the preparation.
7. The wonderful age mildy wash mousse capable of deeply cleansing, refreshing and moisturizing as claimed in claim 6, wherein in the second step, the mixing weight ratio of the sprout vegetable root powder and 60% -80% of ethanol is 1: 10-1: 25.
8. The wonderful age mildy wash mousse capable of deeply cleansing, refreshing and moisturizing as claimed in claim 6, wherein in the third step, the natural plant extract clarifier is KBT-ZTC.
9. The wonderful age cleansing mousse capable of deeply cleansing, refreshing and moisturizing according to claim 1, wherein the method for extracting the total flavonoids in astragalus mongholicus comprises the following steps:
firstly, cutting astragalus roots into short rods of 1cm, and placing the short rods into a container;
step two, adding absolute alcohol, refluxing for 2 hours at 70 ℃, pouring out the extracting solution and cooling;
step three, adding 48% NaOH aqueous solution into the extracting solution while stirring, and filtering to obtain yellow viscous precipitate;
step four, repeating the step two and the step three for 2-4 times until no yellow viscous precipitate is generated;
adding concentrated hydrochloric acid into the yellow viscous precipitate to adjust the pH value to 2-3, volatilizing purified water, and leaching for 3 times by using absolute ethyl alcohol to obtain a red solution containing flavone and analogues thereof and a white precipitate containing salt and cane sugar;
and step six, volatilizing alcohol to obtain red precipitate, namely the astragalus total flavone.
10. The preparation method of the wonderful age mildy wash mousse capable of deeply cleansing, refreshing and moisturizing according to any one of claims 1-9, which is characterized by comprising the following steps:
step one, material preparation: preparing or weighing the required components according to the parts by weight;
step two, adding half of water into a mixing container;
step three, adding the humectant, the astragalus total flavonoids and the sprouting vegetable root extract into a mixing container, and uniformly stirring until the mixture is transparent;
step four, adding sodium cocoyl amino acid, cocamidopropyl betaine, potassium laureth phosphate and cocamide DEA into a mixing container, adding all the rest water, and stirring uniformly;
step five, adding the other components except the essential oil, and uniformly stirring;
step six, adding the essential oil, and slightly and uniformly stirring;
and step seven, pouring the prepared solution into a foaming container, so as to finish the preparation.
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