CN110507594A - A kind of toner and preparation method thereof - Google Patents
A kind of toner and preparation method thereof Download PDFInfo
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- CN110507594A CN110507594A CN201910875117.7A CN201910875117A CN110507594A CN 110507594 A CN110507594 A CN 110507594A CN 201910875117 A CN201910875117 A CN 201910875117A CN 110507594 A CN110507594 A CN 110507594A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/64—Proteins; Peptides; Derivatives or degradation products thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/81—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions involving only carbon-to-carbon unsaturated bonds
- A61K8/8141—Compositions of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides or nitriles thereof; Compositions of derivatives of such polymers
- A61K8/8152—Homopolymers or copolymers of esters, e.g. (meth)acrylic acid esters; Compositions of derivatives of such polymers
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
- A61K8/86—Polyethers
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9706—Algae
- A61K8/9717—Rhodophycota or Rhodophyta [red algae], e.g. Porphyra
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9728—Fungi, e.g. yeasts
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9789—Magnoliopsida [dicotyledons]
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9794—Liliopsida [monocotyledons]
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/98—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin
- A61K8/987—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin of species other than mammals or birds
- A61K8/988—Honey; Royal jelly, Propolis
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/48—Thickener, Thickening system
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Abstract
The present invention discloses a kind of toner and preparation method thereof.With the total weight of toner, the raw material for toner to be made includes: 1.0-40wt% water soluble humectants；0.01-0.5wt% water-soluble thickener；0.1-20wt% polyethylene glycol；With 55-95wt% water.
Description
Technical field
The present invention relates to cosmetic fields more particularly to a kind of toner and preparation method thereof.
Background technique
With the increasingly raising of economy, living standard, consumer is higher and higher for the demand degree of skin care.Toner
It is the basic steps during skin care, there is moisturizing, cleaning and the function of reinforcing subsequent product absorption.
Cosmetic field is full of stylishness, and product requirement has aesthetic characteristic, including color, skin sense, smell, use feeling
It will determine whether consumer can continue to use Deng, these characteristics.Currently, crowd has been increasingly becoming disappearing for cosmetics after young 95
Take main force, they are more easier interesting, and novel product attracts, and emphasis on personalized, the product of interest is also easier to pierce
Swash their desire to buy.Currently, toner different either in character or effect, it is generally low using upper interest, such as make
The gel shape skin care item prepared with the high molecular polymer of resistance to ionic difference, often consistency is higher for this kind of product, changes water and quick-fried water
Effect is unobvious；Or the water outlet cream of the W/O emulsified body or W/SI in critical stable state；Or soft bead or suspended oil is added
Rouge etc. has similar problem.
Moisturizing effect is demand one of of the consumer for toner, therefore there is an urgent need in the art to provide use when has
Visual droplet sense, smears the toner for continuing quick-fried water, not only to the feeling of people's water profit moisturizing, can also increase the entertaining of product
Property.
Summary of the invention
The present invention is intended to provide a kind of novel toner and preparation method thereof.
In the first aspect of the present invention, a kind of moisturizing lotion is provided, with the total weight of toner, for makeup to be made
The raw material of water includes:
1.0-40wt% water soluble humectants
0.01-0.5wt% water-soluble thickener
0.1-20wt% polyethylene glycol
55-95wt% water.
In another preferred example, the water-soluble thickener is selected from following one or more: carbomer, acrylic acid
(ester) class/C10-30 alkylol acrylamide acid esters cross-linked polymer, hydroxy-ethyl acrylate/sodium acryloyldimethyl taurate copolymers,
Ammonium acryloyl taurate/VP copolymer, Sodium Polyacrylate, xanthan gum, hydroxyethyl cellulose and cellulose gum.
In another preferred example, the polyethylene glycol is selected from following one or more: polyethylene glycol -6, poly- second two
Alcohol -8, polyethylene glycol -10, polyethylene glycol -32, polyethylene glycol -75, polyethylene glycol -14M, polyethylene glycol -20M, polyethylene glycol -
90M and polyethylene glycol -150.
In another preferred example, the water soluble humectants are selected from following one or more: glycerol, propylene glycol,
1,3-PD, dipropylene glycol, 1,3-BDO, methyl propanediol, sorb (sugar) alcohol, Sodium Hyaluronate, hyaluronan
Sodium hydrolyzes Sodium Hyaluronate, trehalose, glycine betaine, panthenol, glycerin polyether -26 and PEG/PPG-17/6 copolymer.
In another preferred example, the raw material further include:
0.1-10wt% skin conditioning agent
0.01-0.4wt%pH regulator
0.05-1.0wt% solubilizer
0.001-0.5wt% chelating agent
0.01-3.0wt% preservative
0.001-1.0wt% essence.
In another preferred example, the skin conditioning agent is selected from following one or more: Chondrus crispus extracts
Object, Tremella fructification extract, yam extract, Mel extract, oat kernel extract, inositol, acetyl group tetrapeptide -5, two are split
Yeast tunning lysis object and hydrolyzed wheat protein.
In another preferred example, the pH adjusting agent is selected from following one or more: sodium hydroxide, hydroxide
Potassium, triethanolamine, tromethamine, aminomethyl propanol and arginine.
In another preferred example, the solubilizer is selected from following one or more: Cremophor RH40,
PEG-60 rilanit special, octyl dodecanol polyethers -16, polysorbate -20, PPG-26- butylol polyether -26, Natrulon H-10
Laurate and PPG-13- decyl tetradecyl alcohol polyethers -24.
In another preferred example, the chelating agent is selected from following one or two: EDETATE SODIUM, tetra- sodium of EDTA, spray are replaced
Sour five sodium, sodium phytate and phytic acid.
In another preferred example, the preservative is selected from following one or more: 1,2- hexylene glycol, and 1,2- penta 2
Alcohol, benzyl alcohol, Phenoxyethanol, Sensiva SC50, parahydroxyacet-ophenone, pungent glycol, methyl hydroxybenzoate and Chlorphenesin.
In another preferred example, the water-soluble thickener is carbopol Ultrez 20；The polyethylene glycol is poly-
Ethylene glycol -90M and polyethylene glycol -75 or polyethylene glycol -150.
In another preferred example, with the total weight of toner, have in raw material 0.01-0.05wt% polyethylene glycol -90M and
1-3wt% polyethylene glycol -75 or polyethylene glycol -150.
In the second aspect of the present invention, a kind of preparation method of toner provided present invention as described above, institute are provided
State method comprising steps of by the water soluble humectants of formulation dosage, water-soluble thickener, water and polyethylene glycol mix, obtain as
The upper toner provided by the invention.
In another preferred example, the method includes the steps:
(1) water soluble humectants of formulation dosage, water-soluble thickener, chelating agent and water are mixed, obtains solution 1
(2) pH adjusting agent of solution 1 and formulation dosage is mixed, obtains mixture 1；With
(3) mixture 1 and the polyethylene glycol of formulation dosage, skin conditioning agent, solubilizer, essence and preservative are mixed,
The toner provided present invention as described above.
In another preferred example, step (1) is mixed at 75-85 DEG C.
In another preferred example, step (2) is mixed at 48-55 DEG C.
In another preferred example, step (3) is mixed at 42-48 DEG C.
In another preferred example, the change provided present invention as described above is obtained by filtration at 32-39 DEG C after step (3) mixing
Adornment water.
Accordingly, the present invention provides having visual droplet sense when using, the toner for continuing quick-fried water is smeared, is not only given
People's water moistens the feeling of moisturizing, also increases the interest of product.
Detailed description of the invention
Fig. 1 is the hand using renderings for the toner that the embodiment of the present invention 5 is prepared；Wherein,
A is that toner is just applied to hand, the case where gently beating；
B is after toner is gently patted, to start the case where bursting out droplet；
C is the effect picture that toner bursts out droplet.
Specific embodiment
After extensive and in-depth study, discovery uses medium rheology, the polymer and high molecular weight of resistance to ion to inventor
Polyethylene glycol can obtain the toner with quick-fried water effect.
As used in the present invention, " quick-fried water " refers to that the toner on skin can burst out the situation of droplet after gently patting.
The present invention provides a kind of toner with quick-fried water effect, and raw material therein is main in terms of the total weight of toner
Include:
Further, can also include:
Water soluble humectants used in the present invention include glycerol, propylene glycol, 1,3-PD, dipropylene glycol, 1,3- fourth
Glycol, methyl propanediol, sorb (sugar) alcohol, Sodium Hyaluronate, hyaluronan sodium hydrolyze Sodium Hyaluronate, trehalose, sweet tea
Dish alkali, panthenol, one or more of glycerin polyether -26 and PEG/PPG-17/6 copolymer；Preferably glycerine, 1,3- fourth
It is one or more kinds of in glycol, trehalose, Sodium Hyaluronate, glycine betaine and panthenol；More preferable glycerol, 1,3-BDO and
Trehalose.
With the total weight of toner, the additional amount of the water soluble humectants is 1-40wt%, preferably 5-30wt%；
When the additional amount of water soluble humectants is less than 1wt%, obtained toner performance of keeping humidity is poor, when adding for water soluble humectants
When entering amount greater than 40wt%, preparation-obtained toner is sticky and at high cost.
Water-soluble thickener used in the present invention includes carbomer, acrylic acid (ester) class/C10-30 alkylol acrylamide acid esters
Cross-linked polymer, hydroxy-ethyl acrylate/sodium acryloyldimethyl taurate copolymers, ammonium acryloyldime-thyltaurate/VP are total
Polymers, Sodium Polyacrylate, xanthan gum, one or more of hydroxyethyl cellulose and cellulose gum；It is preferred that carbomer,
One or both of Sodium Polyacrylate, xanthan gum and acrylic acid (ester) class/C10-30 alkylol acrylamide acid esters cross-linked polymer with
On；More preferable acrylic acid (ester) class/C10-30 alkylol acrylamide acid esters cross-linked polymer.
Inventors have found that acrylic acid (ester) class/C10-30 alkylol acrylamide acid esters cross-linked polymer has preferable resistance to ion
Property, there is good thickening capabilities, skin sense water profit after neutralization；Further, resistance to ionic preferable polymer, compared to it is resistance to from
The slightly worse polymer of sub- property, so that the wire-drawing effect of toner provided by the invention and quick-fried water effect are all more persistently.
In one embodiment of the invention, the carbomer used includes but is not limited to (the i.e. 2- first of carbopol 980
Base butyric acid homopolymer, No. CAS is 600-07-7), (i.e. prop-2-enoic acid homopolymer, No. CAS is carbopol 981
9063-87-0)。
In one embodiment of the invention, acrylic acid (ester) class used /C10-30 alkylol acrylamide acid esters crosslinking is poly-
Closing object includes but is not limited to carbopol Ultrez 20, carbopol Ultrez 21；Preferably ca rbopol Ultrez
20。
With the total weight of toner, the additional amount of the water-soluble thickener is 0.01-0.5wt%, preferably 0.08-
0.35wt%；When the additional amount of water-soluble thickener is less than 0.01wt%, obtained toner consistency is low, wire drawing and quick-fried water effect
Fruit is poor, and when the additional amount of water-soluble thickener is greater than 0.5wt%, the consistency of made obtained toner is high, spreadability and quick-fried water
Effect is poor.
Polyethylene glycol used in the present invention includes polyethylene glycol -6, polyethylene glycol-8, polyethylene glycol -10, polyethylene glycol -
32, polyethylene glycol -75, polyethylene glycol -14M, polyethylene glycol -20M, one of polyethylene glycol -90M and polyethylene glycol -150
Or it is two or more；It is preferred that polyethylene glycol -90M, polyethylene glycol -32, polyethylene glycol -75, polyethylene glycol -150, polyethylene glycol -
One or both of 14M and polyethylene glycol-8.
In one embodiment of the invention, the polyethylene glycol for the use of the number of repeat unit of ethylene glycol being 20-200000,
It is preferred that the number of repeat unit of ethylene glycol is 50-100000, as the number of repeat unit of ethylene glycol is 75,100,120,150,
1000-9000,10000-90000's etc., for example, one of polyethylene glycol -90M, polyethylene glycol -75 and polyethylene glycol -150
Or two or more, the combination of more preferable polyethylene glycol -75 or polyethylene glycol -150 and polyethylene glycol -90M.
With the total weight of toner, the additional amount of the polyethylene glycols is 0.1-20wt%, preferably 1-10wt%.
When the additional amount of polyethylene glycols is less than 0.1wt%, the performance of keeping humidity of obtained toner is low, and the persistence of wire drawing is poor；When
The additional amount of polyethylene glycols is greater than 20wt%, and the stringiness of obtained toner is strong, and skin sense is sticky.
Skin conditioning agent used in the present invention includes: Chondrus crispus extract, Tremella fructification extract, and Chinese yam mentions
Object is taken, Mel extract, oat kernel extract, inositol, acetyl group tetrapeptide -5, two splits yeast tunning lysis object, and hydrolyzes
One or more of wheat gluten.These substances can be used disclosed method and be prepared, can also be commercially available, such as
But it is not limited to, it is Chondrus crispus extract (trade name: Seamolient) purchased from BASF Corp. of Germany, public purchased from Shanghai brightness text
Tremella fructification extract (trade name: WSK), the Mel extract (commodity purchased from hundred Lang De biochemistry corporation,Ltd.s of department
Name: Mel extract) etc..
It is preferred that the real extract of tremella, one or both of Mel extract and Chondrus crispus extract.
With the total weight of toner, the additional amount of the skin conditioning agent is 0.1-10wt%, preferably 0.3-
5wt%；When the additional amount of skin conditioning agent is less than 0.1wt%, the effect of preparation-obtained toner conditioning skin, is poor.
PH adjusting agent used in the present invention includes sodium hydroxide, potassium hydroxide, triethanolamine, tromethamine, aminomethyl
One or more of propyl alcohol and arginine；Preferably triethanolamine, tromethamine, one of arginine.
With the total weight of toner, the additional amount of the pH adjusting agent is 0.01-0.4wt%.Preferably 0.05-
0.3wt%, when the additional amount of pH adjusting agent is less than 0.01wt%, the pH of obtained toner is too low, when pH adjusting agent
When additional amount is greater than 0.4wt%, the pH of toner is excessively high, the too high or too low stimulation for all easily causing skin of pH.
Solubilizer used in the present invention includes Cremophor RH40, PEG-60 rilanit special, octyl dodecanol
Polyethers -16, polysorbate -20, PPG-26- butylol polyether -26, Natrulon H-10 laurate, PPG-13- decyl tetradecyl alcohol
One or more of polyethers -24；Preferably octyl dodecanol polyethers -16, PEG-60 rilanit special and polysorbate
One or both of ester -20.
With the total weight of toner, the additional amount of the solubilizer is 0.05-1wt%.Preferably 0.1-0.5wt%；
When the additional amount of the solubilizer is less than 0.05wt%, the solubilising power for the toner being prepared is poor, poor transparency, works as institute
When stating the additional amount of solubilizer greater than 1wt%, the irritation for the toner being prepared is larger.
Chelating agent used in the present invention includes EDETATE SODIUM, tetra- sodium of EDTA, five sodium of Pentetic Acid, in sodium phytate and phytic acid
One or two；It is preferred that EDETATE SODIUM, one or both of five sodium of sodium phytate and Pentetic Acid.
With the total weight of toner, the additional amount of the chelating agent is 0.001-0.5wt%.Preferably 0.01-
0.3wt%；When the additional amount of the chelating agent is less than 0.001wt%, the ability of chelated metal ions is weak, when the chelating agent
When additional amount is greater than 0.5wt%, the pH for the toner being prepared is too high or too low, the stimulation of Yi Yinqi skin.
Preservative and essence are also used in the present invention.The preservative includes 1,2- hexylene glycol, 1,2- pentanediol, benzene first
Alcohol, Phenoxyethanol, Sensiva SC50, parahydroxyacet-ophenone, pungent glycol, one of methyl hydroxybenzoate and Chlorphenesin or two
Kind or more；Preferably 1,2- hexylene glycol, parahydroxyacet-ophenone, one or both of Phenoxyethanol and Sensiva SC50 with
On.
With the total weight of toner, the additional amount of the preservative is 0.01-3.0wt%, preferably 0.05-
2.0wt%；The additional amount of the essence is 0.001-1wt%, preferably 0.01-0.05wt%.
It is common that water used in the present invention can be cosmetic field, such as, but not limited to, deionized water.The present invention mentions
In the toner of confession, with the total weight of toner, the additional amount of deionized water is 55-95wt%, preferably 60-90wt%.
The present invention provides the preparation method of toner, the method includes the steps:
The first step is added water soluble humectants, water-soluble thickener, chelating agent, is stirred and heated in deionized water
75-85 DEG C of dissolution is complete；
Second step is cooled to 48-55 DEG C, and pH adjusting agent is added, and is dispersed with stirring uniformly；
Third step is cooled to 42-48 DEG C, and polyethylene glycols, skin conditioning agent, solubilizer, essence, preservative are added, stir
It mixes uniformly, obtains toner provided by the invention.
In one embodiment of the invention, above-mentioned each step carries out in the reaction vessel.
In one embodiment of the invention, third step is being cooled to 32-39 DEG C after mixing evenly, this hair is obtained by filtration
The toner of bright offer.The filtering can be carried out by conventional method in that art, such as, but not limited to, be filtered.
The feature that the features described above or embodiment that the present invention mentions are mentioned can be in any combination.Disclosed in this case specification
All features can be used in combination with any composition form, each feature disclosed in specification, any can provide it is identical,
The alternative characteristics of impartial or similar purpose replace.Therefore except there is special instruction, revealed feature is only impartial or similar spy
The general example of sign.
Main advantages of the present invention are:
Toner provided by the invention when in use, along with the slight beating of hand, has lasting wire-drawing effect, together
Shi Chijiu's bursts out macroscopic grain grain droplet, and after use, skin has softness, and the sliding sense of touch of silk does not stick clearly greasy.
Embodiment of the present invention is described in detail below in conjunction with embodiment, but those skilled in the art will
It will be appreciated that the following example is merely to illustrate the present invention, and should not be taken as limiting the scope of the invention.Tool is not specified in embodiment
Concrete conditions in the establishment of a specific crime person carries out according to conventional conditions or manufacturer's recommended conditions.Reagents or instruments used without specified manufacturer,
For can be with conventional products that are commercially available.
In embodiment,
The manufacturer of carbomer 1# is lubrizol, product grade: carbopol 980；
The manufacturer of carbomer 2# is lubrizol, product grade: carbopol 981；
Acrylic acid (ester) class/C10-30 alkylol acrylamide acid esters cross-linked polymer 1# manufacturer is lubrizol, product
The trade mark: carbopol Ultrez 20；
Acrylic acid (ester) class/C10-30 alkylol acrylamide acid esters cross-linked polymer 2# manufacturer is lubrizol, product
The trade mark: carbopol Ultrez 21；
Prepare embodiment
According to the content (number) of each component of embodiment 1-5 and comparative example 1-2 in the following table 1, and make as steps described below
It is standby to obtain toner.
The preparation method is as follows:
Step 1: deionized water being placed in reaction vessel, water soluble humectants, water-soluble thickener, and chelating is added
It is complete to be stirred and heated to 78 DEG C of dissolutions for agent；
Step 2: being cooled to 50 DEG C, pH adjusting agent is added in the reaction vessel, be dispersed with stirring uniformly；
Step 3: being cooled to 45 DEG C, polyethylene glycols are added in the reaction vessel, skin conditioning agent, solubilizer, essence, prevent
Rotten agent, stirs evenly；
Step 4: being cooled to 35 DEG C, the toner with quick-fried water effect is prepared in filtering.
Table 1
Effect example
The moisturizing lotion that the moisturizing lotion I-V and comparative example 1-2 for selecting embodiment 1-5 to be prepared are prepared
VI-VII carries out the test of consumer's usage experience, is assessed using the consumer that 30 average ages are 26 years old as object.Assessment
Method is in 1-5 component selections to projects degree of recognition (whether meeting description).Shown in the corresponding effect of each score value is described as follows:
Test result such as table 2
Table 2
Test result shows, toner provided by the embodiments of the present application is substantially better than pair in the usage experience of quick-fried water effect
The toner that ratio provides.By comparing the toner of different rheologies and resistance to ionic polymer formulation, show to imitate in quick-fried water
In the usage experience of fruit, in contrast medium rheology, the general performance of the toner of the polymer formulation of resistance to ion are good for use.It is logical
Being applied in combination for the polyglycol polymer of comparison different molecular weight is crossed, is shown in the usage experience of quick-fried water effect, is used
In contrast the general performance of the toner of the formulated in combination of the polyglycol polymer of high molecular weight is good.
The foregoing is merely illustrative of the preferred embodiments of the present invention, the substantial technological content model being not intended to limit the invention
It encloses, substantial technological content of the invention is broadly defined in the scope of the claims of application, any technology that other people complete
Entity or method also or a kind of equivalent change, will if identical with defined in the scope of the claims of application
It is considered as being covered by among the scope of the claims.
Claims (10)
1. a kind of moisturizing lotion, which is characterized in that with the total weight of toner, the raw material for toner to be made includes:
1.0-40wt% water soluble humectants
0.01-0.5wt% water-soluble thickener
0.1-20wt% polyethylene glycol
55-95wt% water.
2. toner as described in claim 1, which is characterized in that the water-soluble thickener is selected from following one or two
More than: carbomer, acrylic acid (ester) class/C10-30 alkylol acrylamide acid esters cross-linked polymer, hydroxy-ethyl acrylate/acryloyl diformazan
Base Taurate Copolymer, ammonium acryloyl taurate/VP copolymer, Sodium Polyacrylate, xanthan gum, hydroxy ethyl fiber
Element and cellulose gum.
3. toner as described in claim 1, which is characterized in that the polyethylene glycol be selected from it is following it is one or two kinds of with
Upper: polyethylene glycol -6, polyethylene glycol-8, polyethylene glycol -10, polyethylene glycol -32, polyethylene glycol -75, polyethylene glycol -14M gather
Ethylene glycol -20M, polyethylene glycol -90M and polyethylene glycol -150.
4. toner as described in claim 1, which is characterized in that the water soluble humectants are selected from following one or two
More than: glycerol, propylene glycol, 1,3-PD, dipropylene glycol, 1,3-BDO, methyl propanediol, sorb (sugar) alcohol, hyalomitome
Sour sodium, hyaluronan sodium hydrolyze Sodium Hyaluronate, trehalose, glycine betaine, panthenol, glycerin polyether -26 and PEG/PPG-
17/6 copolymer.
5. toner as described in claim 1, which is characterized in that the raw material further include:
0.1-10wt% skin conditioning agent
0.01-0.4wt%pH regulator
0.05-1.0wt% solubilizer
0.001-0.5wt% chelating agent
0.01-3.0wt% preservative
0.001-1.0wt% essence.
6. toner as described in any one in claim 1-5, which is characterized in that the water-soluble thickener is carbopol
Ultrez 20；The polyethylene glycol is polyethylene glycol -90M and polyethylene glycol -75 or polyethylene glycol -150.
7. toner as claimed in claim 6, which is characterized in that with the total weight of toner, have 0.01- in raw material
0.05wt% polyethylene glycol -90M and 1-3wt% polyethylene glycol -75 or polyethylene glycol -150.
8. a kind of preparation method of such as described in any item toners of claim 1-7, which is characterized in that the method includes steps
It is rapid: the water soluble humectants of formulation dosage, water-soluble thickener, water and polyethylene glycol being mixed, claim 1-7 such as is obtained and appoints
Toner described in one.
9. preparation method as claimed in claim 8, which is characterized in that the method includes the steps:
(1) water soluble humectants of formulation dosage, water-soluble thickener, chelating agent and water are mixed, obtains solution 1
(2) pH adjusting agent of solution 1 and formulation dosage is mixed, obtains mixture 1；
(3) mixture 1 and the polyethylene glycol of formulation dosage, skin conditioning agent, solubilizer, essence and preservative are mixed, is obtained
Such as the described in any item toners of claim 1-7.
10. preparation method as claimed in claim 9, which is characterized in that step (3) mixing after be obtained by filtration at 32-39 DEG C as
The described in any item toners of claim 1-7.
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| FR3118712A1 (en) * | 2020-11-20 | 2022-07-15 | L'oreal | COMPOSITION FOR THE CARE OF KERATIN MATERIALS |
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| CN110507594B (en) | 2022-06-17 |
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