CN110432334A - One kind is dissolubility walnut powder and preparation method thereof - Google Patents

One kind is dissolubility walnut powder and preparation method thereof Download PDF

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Publication number
CN110432334A
CN110432334A CN201910852771.6A CN201910852771A CN110432334A CN 110432334 A CN110432334 A CN 110432334A CN 201910852771 A CN201910852771 A CN 201910852771A CN 110432334 A CN110432334 A CN 110432334A
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CN
China
Prior art keywords
walnut
dissolubility
walnut kernel
added
walnut powder
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Pending
Application number
CN201910852771.6A
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Chinese (zh)
Inventor
熊相人
王翰龙
山云辉
杨强国
段炳意
杨亚仙
陈碧峰
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COFFEE ENGINEERING RESEARCH CENTER OF CHINA
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Hougu Coffee Co Ltd Yunnan Province
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Priority to CN201910852771.6A priority Critical patent/CN110432334A/en
Publication of CN110432334A publication Critical patent/CN110432334A/en
Pending legal-status Critical Current

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    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23CDAIRY PRODUCTS, e.g. MILK, BUTTER OR CHEESE; MILK OR CHEESE SUBSTITUTES; MAKING THEREOF
    • A23C11/00Milk substitutes, e.g. coffee whitener compositions
    • A23C11/02Milk substitutes, e.g. coffee whitener compositions containing at least one non-milk component as source of fats or proteins
    • A23C11/10Milk substitutes, e.g. coffee whitener compositions containing at least one non-milk component as source of fats or proteins containing or not lactose but no other milk components as source of fats, carbohydrates or proteins
    • A23C11/103Milk substitutes, e.g. coffee whitener compositions containing at least one non-milk component as source of fats or proteins containing or not lactose but no other milk components as source of fats, carbohydrates or proteins containing only proteins from pulses, oilseeds or nuts, e.g. nut milk

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  • Chemical & Material Sciences (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Food Science & Technology (AREA)
  • Polymers & Plastics (AREA)
  • Medicines Containing Plant Substances (AREA)
  • Cosmetics (AREA)

Abstract

It is dissolubility walnut powder and preparation method thereof the invention discloses one kind, i.e. the dissolubility walnut powder includes 50 ~ 80 parts and 20 ~ 30 parts of auxiliary material of 100 ~ 200 parts of walnut kernel, syrup of parts by weight of raw materials.Method is to obtain walnut kernel after former fruit CRACKING WALNUT to be gone to folder film, and walnut kernel is cleaned and is dried, the walnut kernel of formulation ratio is weighed, 40 ~ 60 DEG C of water mixing defibrinations 2 ~ 3 times for being added 2 ~ 3 times of walnut kernel weight obtain material a, and slurries b is obtained by filtration in material a;The emulsifier and stabilizer that formulation ratio is added in slurries b, which are mixed, obtains feed liquid c through high speed shear and emulsification;The syrup of formulation ratio is heated to 60 ~ 80 DEG C and obtains material d;Material d is added to be uniformly mixed in feed liquid c and obtains mixed serum e;Mixed serum e is sterilized to obtain mixed serum f through homogeneous;Mixed serum f is refrigerated to -40 DEG C hereinafter, then Freezing smashing obtains material g in the rate of temperature fall of 5 ~ 10 DEG C/min;Material g is obtained into object i.e. dissolubility walnut powder through lyophilization to moisture content≤3%.

Description

One kind is dissolubility walnut powder and preparation method thereof
Technical field
The invention belongs to technical field of food deep processing, and in particular to one kind is dissolubility walnut powder and preparation method thereof.
Background technique
Walnut powder product belongs to solid beverage class, and high-quality walnut powder is using based on high-quality walnut kernel, white granulated sugar, whole-fat milk powder Raw material is wanted, is killed through walnut kernel immersion, grinding, screenings separation (the bitter brown crust of removal), deodorant, ingredient, homogeneous, concentration Bacterium, spray drying are made.Walnut can be rated as anti-oxidant its " king ", the unusual height of the nutritive value of walnut.U.S. diet association builds People are discussed, weekly most nice walnut two or three times, the especially middle-aged and the old and menopausal women, because arginine contained in walnut, Oleic acid, antioxidant etc. are cardiovascular to protection, and prevention coronary heart disease, apoplexy, senile dementia etc. are that quite have benifit.Existing market On walnut powder have that be dissolved in the lotion that obtains after water uneven, unstable, place and lamination occur for a moment, or The technical problem of the multiple nutritional components missing of walnut kernel, therefore develop a kind of walnut powder product that can solve above-mentioned technical problem It is very important.
Summary of the invention
The first object of the present invention is to provide a kind of i.e. dissolubility walnut powder;Second is designed to provide the i.e. dissolubility The preparation method of walnut powder.
The first object of the present invention is achieved in that the i.e. dissolubility walnut powder includes the walnut kernel of parts by weight of raw materials 100 ~ 200 parts, 50 ~ 80 parts and 20 ~ 30 parts of auxiliary material of syrup.
The second object of the present invention is achieved in that including pre-treatment, homogeneous sterilizing, Freezing smashing and post-processing step Suddenly, it specifically includes:
A, pre-treatment:
1) walnut kernel is obtained after former fruit CRACKING WALNUT being removed folder film, walnut kernel is cleaned and is dried, the walnut kernel of formulation ratio is weighed, 40 ~ 60 DEG C of water mixing defibrinations 2 ~ 3 times for being added 2 ~ 3 times of walnut kernel weight obtain material a, and slurries b is obtained by filtration in material a;
2) emulsifier and stabilizer that formulation ratio is added in slurries b, which are mixed, obtains feed liquid c through high speed shear and emulsification;
3) syrup of formulation ratio is heated to 60 ~ 80 DEG C and obtains material d;
4) material d is added to be uniformly mixed in feed liquid c and obtains mixed serum e;
B, mixed serum e is sterilized to obtain mixed serum f through homogeneous;
C, mixed serum f is refrigerated to -40 DEG C hereinafter, then Freezing smashing obtains material g in the rate of temperature fall of 5 ~ 10 DEG C/min;
D, material g is obtained into object i.e. dissolubility walnut powder through lyophilization to moisture content≤3%.
The present invention handles walnut kernel by deep processing, and the walnut kernel slurries dry particle that can be redissolved in water is made, both complete The multiple nutritional components of walnut kernel are remained entirely, and the particle after drying can be dissolved in the water quickly, be reduced to uniform and stable Lotion, free from admixture and precipitating are long placed in no layering.The present invention not only solves the core of soluble walnut product from engineering technology Technique, and develop a kind of novel healthy food can be with since the unsaturated fat and protein content of the product are higher Substitute milk replacer --- the vegetable fat powder for thering is side effect to be produced with hydrogenated vegetable oil human body.
Specific embodiment
Below with reference to embodiment, the present invention is further illustrated, but the present invention is limited in any way, Based on present invention teach that it is made it is any transform or replace, all belong to the scope of protection of the present invention.
I.e. dissolubility walnut powder of the present invention include parts by weight of raw materials 50 ~ 80 parts of 100 ~ 200 parts of walnut kernel, syrup and 20 ~ 30 parts of auxiliary material.
The syrup is corn syrup.
The auxiliary material is made of emulsifier and stabilizer.
The quality proportioning of the emulsifier and stabilizer is 1:1.
The emulsifier is sucrose fatty ester, diacetyl tartaric acid monodiglyceride or single, double fatty acid glyceride.
The stabilizer is Sodium Caseinate, dipotassium hydrogen phosphate, microcrystalline cellulose or Karaya Gum.
The preparation method of i.e. dissolubility walnut powder of the present invention, including pre-treatment, homogeneous sterilizing, Freezing smashing and rear place Step is managed, is specifically included:
A, pre-treatment:
1) walnut kernel is obtained after former fruit CRACKING WALNUT being removed folder film, walnut kernel is cleaned and is dried, the walnut kernel of formulation ratio is weighed, 40 ~ 60 DEG C of water mixing defibrinations 2 ~ 3 times for being added 2 ~ 3 times of walnut kernel weight obtain material a, and slurries b is obtained by filtration in material a;
2) emulsifier and stabilizer that formulation ratio is added in slurries b, which are mixed, obtains feed liquid c through high speed shear and emulsification;
3) syrup of formulation ratio is heated to 60 ~ 80 DEG C and obtains material d;
4) material d is added to be uniformly mixed in feed liquid c and obtains mixed serum e;
B, mixed serum e is sterilized to obtain mixed serum f through homogeneous;
C, mixed serum f is refrigerated to -40 DEG C hereinafter, then Freezing smashing obtains material g in the rate of temperature fall of 5 ~ 10 DEG C/min;
D, material g is obtained into object i.e. dissolubility walnut powder through lyophilization to moisture content≤3%.
The solid content of the mixed serum e needs to control 30% or more to be conducive in subsequent drying process The formation of grain skin covering of the surface.
The granularity of the Freezing smashing is 2 ~ 3mm.
The vacuum degree control of the lyophilization is in 3 ~ 5mbar.
The preparation method concrete operations of i.e. dissolubility walnut powder of the present invention are as follows:
1, prepare walnut kernel: by CRACKING WALNUT go folder film after leave walnut kernel clean drain;
2, defibrination: taking appropriate walnut kernel, and suitable water mixing is added, walnut kernel is worn into slurries, while removing high microsteping residue;
3, emulsifier is added in slurries, is integrated grease and water mixing in walnut kernel, while appropriate colloidal substance is added And modified cellulose, the free oil in lotion is embedded;
4, appropriate corn syrup mixing, heating, absorption grease is added;
5, the solid content of slurries is adjusted to 30% or more, and is heated to 60 DEG C -65 DEG C, to be conducive to particle in drying process The formation of skin covering of the surface;
6, by deployed slurries pressure be 15-20MPa under conditions of homogeneous;
7, it freezes: being refrigerated to -48 DEG C or so after homogenizing fluid is sterilized, and be ground into the particle of 2-3mm, by ice particle in low temperature item It is fitted into aluminium dish under part, is put into lyophilization in the distillation cabin that vacuum degree is 4mbar or so, makes the final moisture content in particle ≤3%;
8, illustrate: emulsifier, stabilizer and embedding medium of the invention optionally uses other substances with same nature Substitution, drying means can also realize that inlet air temperature is 180 degrees Celsius or more, temperature of outgoing air 80 under thermal spray drying condition Degree Celsius or more, granulation or directly spray drying technique can be used in drying process.
9, anticaking agent and wetting agent can be added in the particle after drying or powder.
Case is embodied, the invention will be further described below:
Embodiment 1
1, prepare walnut kernel: by CRACKING WALNUT go folder film after leave walnut kernel clean drain;
2, defibrination: taking walnut kernel 100g, and the mixing of 270mL water is added, walnut kernel is worn into slurries, while removing high microsteping residue;
3,10g emulsifier is added in slurries, is integrated grease and water mixing in walnut kernel, while 10g colloid substances are added Matter and modified cellulose embed the free oil in lotion;
4, the mixing of 50g corn syrup, heating, absorption grease is added;
5, the solid content of slurries is adjusted to 30% or more, and is heated to 60 DEG C -65 DEG C;
6, by deployed slurries pressure be 15-20MPa under conditions of homogeneous;
7, it freezes: being refrigerated to -48 DEG C or so after homogenizing fluid is sterilized, and be ground into the particle of 2-3mm, by ice particle in low temperature item It is fitted into aluminium dish under part, is put into lyophilization in the distillation cabin that vacuum degree is 4mbar or so, makes the final moisture content in particle ≤3%。
Embodiment 2
1, prepare walnut kernel: by CRACKING WALNUT go folder film after leave walnut kernel clean drain;
2, defibrination: taking walnut kernel 150g, and the mixing of 450mL water is added, walnut kernel is worn into slurries, while removing high microsteping residue;
3,18g emulsifier is added in slurries, is integrated grease and water mixing in walnut kernel, while 18g colloid substances are added Matter and modified cellulose embed the free oil in lotion;
4, the mixing of 100g corn syrup, heating, absorption grease is added;
5, the solid content of slurries is adjusted to 30% or more, and is heated to 60 DEG C -65 DEG C;
6, by deployed slurries pressure be 15-20MPa under conditions of homogeneous;
7, it freezes: being refrigerated to -48 DEG C or so after homogenizing fluid is sterilized, and be ground into the particle of 2-3mm, by ice particle in low temperature item It is fitted into aluminium dish under part, is put into lyophilization in the distillation cabin that vacuum degree is 4mbar or so, makes the final moisture content in particle ≤3%。
Embodiment 3
1, prepare walnut kernel: by CRACKING WALNUT go folder film after leave walnut kernel clean drain;
2, defibrination: taking walnut kernel 100g, and the mixing of 250mL water is added, walnut kernel is worn into slurries, while removing high microsteping residue;
3,12g emulsifier is added in slurries, is integrated grease and water mixing in walnut kernel, while 12g colloid substances are added Matter and modified cellulose embed the free oil in lotion;
4, the mixing of 80g corn syrup, heating, absorption grease is added;
5, the solid content of slurries is adjusted to 30% or more, and is heated to 60 DEG C -65 DEG C;
6, by deployed slurries pressure be 15-20MPa under conditions of homogeneous;
7, it freezes: being refrigerated to -48 DEG C or so after homogenizing fluid is sterilized, and be ground into the particle of 2-3mm, by ice particle in low temperature item It is fitted into aluminium dish under part, is put into lyophilization in the distillation cabin that vacuum degree is 4mbar or so, makes the final moisture content in particle ≤3%。
Embodiment 4
1, prepare walnut kernel: by CRACKING WALNUT go folder film after leave walnut kernel clean drain;
2, defibrination: taking walnut kernel 200g, and the mixing of 600mL water is added, walnut kernel is worn into slurries, while removing high microsteping residue;
3,10g emulsifier is added in slurries, is integrated grease and water mixing in walnut kernel, while 10g colloid substances are added Matter and modified cellulose embed the free oil in lotion;
4, the mixing of 100g corn syrup, heating, absorption grease is added;
5, the solid content of slurries is adjusted to 30% or more, and is heated to 60 DEG C -65 DEG C;
6, by deployed slurries pressure be 15-20MPa under conditions of homogeneous;
7, it freezes: being refrigerated to -48 DEG C or so after homogenizing fluid is sterilized, and be ground into the particle of 2-3mm, by ice particle in low temperature item It is fitted into aluminium dish under part, is put into lyophilization in the distillation cabin that vacuum degree is 4mbar or so, makes the final moisture content in particle ≤3%。

Claims (10)

1. one kind is dissolubility walnut powder, it is characterised in that the described i.e. dissolubility walnut powder include parts by weight of raw materials walnut kernel 100 ~ 200 parts, 50 ~ 80 parts and 20 ~ 30 parts of auxiliary material of syrup.
2. i.e. dissolubility walnut powder according to claim 1, it is characterised in that the syrup is corn syrup.
3. i.e. dissolubility walnut powder according to claim 1, it is characterised in that the auxiliary material is by emulsifier and stabilizer group At.
4. i.e. dissolubility walnut powder according to claim 3, it is characterised in that the quality of the emulsifier and stabilizer Proportion is 1:1.
5. i.e. dissolubility walnut powder according to claim 3 or 4, it is characterised in that the emulsifier is sucrose-fatty Ester, diacetyl tartaric acid monodiglyceride or single, double fatty acid glyceride.
6. i.e. dissolubility walnut powder according to claim 3 or 4, it is characterised in that the stabilizer is Sodium Caseinate, phosphorus Sour hydrogen dipotassium, microcrystalline cellulose or Karaya Gum.
7. a kind of preparation method of any i.e. dissolubility walnut powder of claim 1 ~ 6, it is characterised in that including pre-treatment, Matter sterilizing, Freezing smashing and post-processing step, specifically include:
A, pre-treatment:
1) walnut kernel is obtained after former fruit CRACKING WALNUT being removed folder film, walnut kernel is cleaned and is dried, the walnut kernel of formulation ratio is weighed, 40 ~ 60 DEG C of water mixing defibrinations 2 ~ 3 times for being added 2 ~ 3 times of walnut kernel weight obtain material a, and slurries b is obtained by filtration in material a;
2) emulsifier and stabilizer that formulation ratio is added in slurries b, which are mixed, obtains feed liquid c through high speed shear and emulsification;
3) syrup of formulation ratio is heated to 60 ~ 80 DEG C and obtains material d;
4) material d is added to be uniformly mixed in feed liquid c and obtains mixed serum e;
B, mixed serum e is sterilized to obtain mixed serum f through homogeneous;
C, mixed serum f is refrigerated to -40 DEG C hereinafter, then Freezing smashing obtains material g in the rate of temperature fall of 5 ~ 10 DEG C/min;
D, material g is obtained into object i.e. dissolubility walnut powder through lyophilization to moisture content≤3%.
8. preparation method according to claim 7, it is characterised in that the solid content of the mixed serum e needs to control Make the formation for being conducive to particle surface film in subsequent drying process 30% or more.
9. preparation method according to claim 7, it is characterised in that the granularity of the Freezing smashing is 2 ~ 3mm.
10. preparation method according to claim 7, it is characterised in that the vacuum degree control of the lyophilization 3 ~ 5mbar。
CN201910852771.6A 2019-09-10 2019-09-10 One kind is dissolubility walnut powder and preparation method thereof Pending CN110432334A (en)

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Citations (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1377612A (en) * 2002-04-23 2002-11-06 云南省轻工业科学研究所 Full content instant walnut powder and its producing process
CN1718028A (en) * 2005-08-04 2006-01-11 迪庆香格里拉天然营养植物有机食品开发有限责任公司 Powdered walnut oil, and its prepn. process
EP2342980A1 (en) * 2010-01-11 2011-07-13 Liquats Vegetals SA Process for the preparation of a beverage from nuts
CN102524416A (en) * 2012-02-10 2012-07-04 无锡超科食品有限公司 Preparation method of vegetable fat powder
CN103518856A (en) * 2013-10-10 2014-01-22 云南省药物研究所 Production process of high-calcium pure walnut instant powder
CN105285155A (en) * 2015-09-11 2016-02-03 无锡超科食品科技有限公司 Vegetable oil powder as well as preparation method and purposes thereof
CN109757562A (en) * 2019-03-22 2019-05-17 云南摩尔农庄生物科技开发有限公司 The processing method of bad oil smell is generated after preventing walnut dairy protein drinks from sterilizing

Patent Citations (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1377612A (en) * 2002-04-23 2002-11-06 云南省轻工业科学研究所 Full content instant walnut powder and its producing process
CN1718028A (en) * 2005-08-04 2006-01-11 迪庆香格里拉天然营养植物有机食品开发有限责任公司 Powdered walnut oil, and its prepn. process
EP2342980A1 (en) * 2010-01-11 2011-07-13 Liquats Vegetals SA Process for the preparation of a beverage from nuts
CN102524416A (en) * 2012-02-10 2012-07-04 无锡超科食品有限公司 Preparation method of vegetable fat powder
CN103518856A (en) * 2013-10-10 2014-01-22 云南省药物研究所 Production process of high-calcium pure walnut instant powder
CN105285155A (en) * 2015-09-11 2016-02-03 无锡超科食品科技有限公司 Vegetable oil powder as well as preparation method and purposes thereof
CN109757562A (en) * 2019-03-22 2019-05-17 云南摩尔农庄生物科技开发有限公司 The processing method of bad oil smell is generated after preventing walnut dairy protein drinks from sterilizing

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
李翔 等: "速溶核桃营养粉的制作工艺研究", 《农产品加工》 *

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Effective date of registration: 20210811

Address after: 678400 in PADI Industrial Park, mang City, Dehong Dai and Jingpo Autonomous Prefecture, Yunnan Province

Applicant after: COFFEE ENGINEERING RESEARCH CENTER OF CHINA

Address before: 678400 room 17D, building a, Taoyuan garden, No. 31, caoxiao lane, Kunming, Yunnan

Applicant before: Yunnan Hougu Coffee Co.,Ltd.

RJ01 Rejection of invention patent application after publication
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Application publication date: 20191112