CN1331408C - Powdered walnut oil, and its prepn. process - Google Patents
Powdered walnut oil, and its prepn. process Download PDFInfo
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- CN1331408C CN1331408C CNB2005100109503A CN200510010950A CN1331408C CN 1331408 C CN1331408 C CN 1331408C CN B2005100109503 A CNB2005100109503 A CN B2005100109503A CN 200510010950 A CN200510010950 A CN 200510010950A CN 1331408 C CN1331408 C CN 1331408C
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Abstract
The present invention relates to powdery walnut oil. Walnut oil, walnut powder and an additive of corn syrup are used as raw materials. The present invention comprises the components according to the weight percentage: 55 to 60% of walnut oil, 12 to 20% of walnut powder, 8 to 12 % of additive of corn syrup, 10 to 14% of malt dextrin, 2 to 5 % of emulsifying agent and 0.02 to 0.1 % of amylase; the sum of the weight ratio of the raw materials is 100%. Shell breaking and coat removing technology is adopted during preparation, and peeled walnut kernels can be obtained by removing impurities; pure wild walnut oil can be obtained by drying, cake pressing and squeezing; then, refined walnut oil can be obtained by filtration, separation and dehydration; pulp can be obtained by pulp mixing, filtering and concentrating walnut oil dregs; the refined walnut oil and the pulp of wild walnut powder are added with the corn syrup and the malt dextrin for uniformly mixing, homogenizing, spray drying and sieving, and the powdery walnut oil can be obtained. The present invention adopts perennial wild walnuts from Shangri-La as main raw materials; because pesticide and fertilizer are not needed in the growing process of wild walnuts, walnut kernels do not comprise residual pesticide and fertilizer. The present invention adopts modern processing technology to process green health care food of walnuts to the powdery walnut oil; additives are used as few as possible in the preparation technology; pigment and preservatives are not used. The product can be used as food and a food additive, and has the favorable performance of dissolution, emulsification, storage, transportation, dispersion, antioxidation, etc. The shelf life can be largely prolonged. The product does not have repulsive interaction with other raw materials in food processing, and has favorable mixing performance and compatibility capability.
Description
Technical field
The present invention relates to a kind of edible oil and processing method thereof, particularly a kind of powdered walnut oil and preparation technology thereof.
Background technology
Contain abundant unrighted acid in the walnut oil, its content near 80% wherein linoleic acid, linolenic content be other edible oil, and be rich in trace elements such as multivitamin and calcium, magnesium, to softening blood vessel, reduce the human cholesterol content, prevent that artery sclerosis and thrombosis from having positive role, can also prevent and treat multiple common modern rich man's diseases such as hypertension, high fat of blood, diabetes, obesity, in developed country, edible walnut oil has become a kind of propensity to consume, and the U.S. also is assigned therein as aerospace food.Problems such as common walnut oil is a fluid oil, exists storage, transportation inconvenience, and edible way is single, and takes inconvenience when using, is difficult to mix, easily sticks on hand with on container, the equipment with other raw material and be difficult to clean, and is perishable.
Summary of the invention
Order of the present invention is the weak point that exists in liquid walnut oil year for overcoming, and proposing a kind of is primary raw material with wild walnut, the powdered walnut oil and the preparation technology thereof that can be used as high-quality raw-food material or directly eat.
Technical scheme of the present invention is powdered walnut oil preparation technology, it is characterized in that be equipped with raw material in following ratio, the each component percentage by weight is, walnut oil 55-60%, walnut powder 12-20%, corn syrup 8-12%, maltodextrin 10-14%, emulsifying agent 2-5%, amylase 0.02-0.1%, each raw material weight is 100% than sum, concrete technology is:
(1) refining walnut oil
A, shelling are removed the peel wild walnut shell-breaking, are gone clothing to adopt centrifugal hulling device and air-flow hulling device shelling peeling, artificial selected impurity elimination;
B, prick cake equipment with walnut kernel be bundled into pie, squeezer squeezes out walnut oil;
C, filtration walnut oil keep 60 ℃, and 240 eye mesh screens filter;
D, protein isolate add 10% clear water, heat 20-40 ℃, stir 20-40 minute, and insulation was left standstill 4 hours at least, got the come-up walnut oil;
E, vacuum dehydration place walnut oil and are heated to 50-60 ℃ of maintenance dehydration in 1-4 hour under the vacuum state;
F, emulsification dehydration walnut oil add emulsifying agent at 60-70 ℃ of stirring, and the dissolving back is standby fully;
(2) lapping
The water that a, the walnut powder that feeds intake add 2 times of amounts stirs, and the limit adds the waterside and is stirred to and adds 3 times of amounts of water, and dnockout begins to heat to the pot of sizing mixing;
B, the material of sizing mixing enter the pot of sizing mixing, and beginning is heated gradually, and temperature remains on 105-120 ℃, continue to stir, and measure the material solid content greater than 20%, transfer PH=6-7 with sodium carbonate, add amylorrhexis starch, keep stirring 15-20 minute;
C, liquefaction keep stirring, and temperature keeps 105-120 ℃, steam pressure 0.3Mpa;
D, insulation material are incubated 18-22 hour in the insulation jar, keep D value=10-20 simultaneously;
E, filtration 240 eye mesh screens filter;
F, the concentrated economic benefits and social benefits that adopt are separated the film concentrator, and one imitates heated pressure 0.01-0.04Mpa, and two imitate heated pressure 0.5-0.74Mpa, and one imitates 68-78 ℃ of evaporating temperature, 45-58 ℃ of two effect evaporating temperature, and the heating pressurization is concentrated into concentration less than 6% with material;
(3) walnut oil powderization
A, get (1) resulting refining walnut oil, (2) resulting lapping, add corn syrup, maltodextrin;
B, material enter colloid mill, homogenizer, and the material temperature is lower than 65 ℃, and homogenization pressure 35-40Mpa surveys particle less than 1.0 μ m;
C, three grades of spray drying towers of employing are handled to such an extent that spray-drying gets powdered walnut oil to material, important technological parameters, feed liquid contains solid content reason 45-55%, feeding temperature is 60-80 ℃, EAT 150-175 ℃, leaving air temp 70-98 ℃, in the product moisture 4%, normal negative pressure is-0.015-0.02Mpa in the tower, the strong 0.2-0.3Mpa of used for air compressor air pressure, the steam normal pressure is controlled at 0.85-1.0Mpa, and fluid bed steam heated temperature is controlled at 90-105 ℃, and dehumidification air conditioner machine temperature is controlled at 30-50 ℃.
Walnut oil is a wild walnut oil in the raw material, and walnut powder is wild walnut oil dregs of rice powder or wild walnut meat powder.Emulsifying agent is at least a in single two mixed fatty glycerides, phosphatide, sucrose fat, the two caproic acid tartaric acid monoglycerides in the raw material.
A kind of powdered walnut oil is characterized in that, is made by above-mentioned preparation technology, and the each component percentage by weight is, walnut oil 55-60%, walnut powder 12-20%, corn syrup 8-12%, maltodextrin 10-14%, emulsifying agent 2-5%, amylase 0.02-0.1%, each raw material weight is 100% than sum.
The present invention adopts the perennial wild walnut in Shangri-la as primary raw material, and wild walnut does not need the applying pesticides chemical fertilizer in growth course, do not contain the residues of banned pesticides chemical fertilizer in the walnut kernel.The present invention adopts modern processing to be processed as powdered walnut oil this green health care food of walnut, and the use additive of trying one's best few in preparation technology does not use pigment, anticorrisive agent.Add in the raw material walnut powder can adjust the mouthfeel of powdered walnut oil and local flavor with and effective ingredient.This product not only can be made food but also can be used as food additives, have performances such as good dissolving, emulsification, storage, transportation, dispersion be anti-oxidant, shelf-life can prolong greatly, and uses with other raw material in food processing and do not have repulsive interaction, has good blending and compatibility ability.
The specific embodiment
Embodiment 1
Get the raw materials ready: the each component percentage by weight is, walnut oil 60%, and walnut powder 15%, corn syrup 10%, maltodextrin 1, emulsifying agent 4.9%, amylase 0.1%, each raw material weight is 100% than sum.Wherein, walnut oil is a wild walnut oil in the raw material, and walnut powder is wild walnut oil dregs of rice powder or wild walnut meat powder.In the raw material emulsifying agent be single two mixed fatty glycerides and two caproic acid tartaric acid monoglycerides each 1/2nd, amylase is food industry level amylase.
One, walnut oil core
1, getting wild walnut is raw material, adopts cylinder seperator and cyclopneumatic separator shelling and coat-eliminating, artificial selected impurity elimination, removes rotten kernel, wild walnut kernel;
2, prick the cake machine with walnut kernel be bundled into pie, squeezer squeezes out walnut oil;
3, walnut oil keeps 60 ℃, and 240 eye mesh screens filter;
4, add 10% clear water in the walnut oil, heat 20-40 ℃, stirred 20-40 minute, insulation was left standstill 4 hours at least at least, and a small amount of protein suction back proportion contained in the walnut oil is increased, and separated from walnut oil, got the come-up walnut oil;
5, there is certain moisture in the walnut oil behind the protein isolate, is unfavorable for walnut oil powderization, the walnut oil of handling is placed be heated to 50-60 ℃ under the vacuum state and keep dehydration in 1-4 hour, remove moisture and can remove peculiar smell in the walnut oil;
6, the dehydration walnut oil is standby after 60-70 ℃ of stirring adding emulsifying agent dissolves fully;
Two, lapping
1, walnut oil meal or the walnut meat powder water that adds 2 times of amounts stirs, and the limit adds the waterside and is stirred to and adds 3 times of amounts of water, and dnockout begins to heat to the pot of sizing mixing, and mixer continues to stir, and avoids material precipitation blocking pipe;
2, continue to stir, temperature remains on 105-120 ℃, measures the material solid content greater than 20%, transfers pH value less than 6-7 with sodium carbonate, adds amylorrhexis starch, keep stirring after 15-20 minute owing to the high temperature enzymolysis is liquefied,
3, adjustment equipment, it is stable that steam pressure is remained, 105 ℃-120 ℃ of temperature, steam pressure 0.3Mpa;
4, material insulation 18-22 hour in insulation jar keeps D value=10-20 simultaneously, if the D value does not reach requirement, opens and is incubated a jar cap relief valve, material is heated keep enzymolysis and proceed, and makes the D value reach requirement.
5, material enters leaf filter 240 eye mesh screens and filters through high-pressure pump;
6, adopt economic benefits and social benefits to separate the film concentrator, one imitates heated pressure 0.01-0.04Mpa, and two imitate heated pressure 0.5-0.74Mpa, and one imitates 68-78 ℃ of evaporating temperature, and two imitate 45-58 ℃ of evaporating temperature, and material is concentrated into concentration less than 6%; Concentrate the sodium hydroxide solution or the salpeter solution that finish use 2% and clean, it is standby that concentrated material enters basin;
Three, walnut oil powderization
1, getting walnut oil after emulsification walnut oil meal or walnut meat powder and corn syrup, the maltodextrin as core, after handling is lapping;
2, raw material enters colloid mill, homogenizer, and fully mixing and emulsifying expects that temperature is lower than 65 ℃, and homogenization pressure 35-40Mpa surveys particle less than 1.0 μ m, and the feed liquid behind the homogeneous can not produce lamination;
3, adopt three grades of spray drying towers to handle to such an extent that spray-drying gets powdered walnut oil to material, important technological parameters, feed liquid contains solid content reason 45-55%, feeding temperature is 60-80 ℃, EAT 150-175 ℃, leaving air temp 70-98 ℃, in the product moisture 4%, normal negative pressure is (0.015)-0.02Mpa in the tower, the strong 0.2-0.3Mpa of used for air compressor air pressure, the steam normal pressure is controlled at 0.85-1.0Mpa, and fluid bed steam heated temperature is controlled at 90-105 ℃, and dehumidification air conditioner machine temperature is controlled at 30-50 ℃.
Embodiment 2
(1) get the raw materials ready: the each component percentage by weight is, walnut oil 58%, and walnut powder 19%, corn syrup 8%, maltodextrin 12%, two caproic acid tartaric acid monoglyceride 2.92%, amylase 0.08%, each raw material weight is 100% than sum.
(2) technology and requirement are identical with embodiment 1.
Embodiment 3
(3) get the raw materials ready: the each component percentage by weight is, walnut oil 59%, and walnut powder 12%, corn syrup 11%, maltodextrin 14%, sucrose fat 3.95%, amylase 0.05%, each raw material weight is 100% than sum.
(4) technology and requirement are identical with embodiment 1.
Embodiment 4
(5) get the raw materials ready: the each component percentage by weight is, walnut oil 55%, and walnut powder 20%, corn syrup 10%, maltodextrin 13%, phosphatidase 11 .98%, amylase 0.02%, each raw material weight is 100% than sum.
(6) technology and requirement are identical with embodiment 1.
Embodiment 5
(7) get the raw materials ready: the each component percentage by weight is, walnut oil 57%, and walnut powder 14%, corn syrup 12%, maltodextrin 14%, single two mixed fatty glycerides 2.01%, amylase 0.09%, each raw material weight is 100% than sum.
(8) technology and requirement are identical with embodiment 1.
Claims (4)
1, a kind of powdered walnut oil preparation technology, it is characterized in that be equipped with raw material in following ratio, the each component percentage by weight is, walnut oil 55-60%, walnut powder 12-20%, corn syrup 8-12%, maltodextrin 10-14%, emulsifying agent 2-5%, amylase 0.02-0.1%, each raw material weight is 100% than sum, concrete technology is:
(1) refining walnut oil
A, shelling are removed the peel wild walnut shell-breaking, are gone clothing to adopt centrifugal hulling device and air-flow hulling device shelling peeling, artificial selected impurity elimination;
B, prick cake equipment with walnut kernel be bundled into pie, squeezer squeezes out walnut oil;
C, filtration walnut oil keep 60 ℃, and 240 eye mesh screens filter;
D, protein isolate add 10% clear water, heat 20-40 ℃, stir 20-40 minute, and insulation was left standstill 4 hours at least, got the come-up walnut oil;
E, vacuum dehydration place walnut oil and are heated to 50-60 ℃ of maintenance dehydration in 1-4 hour under the vacuum state;
F, emulsification dehydration walnut oil add emulsifying agent at 60-70 ℃ of stirring, and the dissolving back is standby fully;
(2) lapping
The water that a, the walnut powder that feeds intake add 2 times of amounts stirs, and the limit adds the waterside and is stirred to and adds 3 times of amounts of water, and dnockout begins to heat to the pot of sizing mixing;
B, the material of sizing mixing enter the pot of sizing mixing, and beginning is heated gradually, and temperature remains on 105-120 ℃, continue to stir, and measure the material solid content greater than 20%, transfer PH=6-7 with sodium carbonate, add amylorrhexis starch, keep stirring 15-20 minute;
C, liquefaction keep stirring, and temperature keeps 105-120 ℃, steam pressure 0.3Mpa;
D, insulation material are incubated 18-22 hour in the insulation jar, keep D value=10-20 simultaneously;
E, filtration 240 eye mesh screens filter;
F, the concentrated economic benefits and social benefits that adopt are separated the film concentrator, and one imitates heated pressure 0.01-0.04Mpa, and two imitate heated pressure 0.5-0.74Mpa, and one imitates 68-78 ℃ of evaporating temperature, 45-58 ℃ of two effect evaporating temperature, and the heating pressurization is concentrated into concentration less than 6% with material;
(3) walnut oil powderization
A, get (1) resulting refining walnut oil, (2) resulting lapping, add corn syrup, maltodextrin;
B, material enter colloid mill, homogenizer, and the material temperature is lower than 65 ℃, and homogenization pressure 35-40Mpa surveys particle less than 1.0 μ m;
C, adopt three grades of spray drying towers to material handle the spray-dried powders walnut oil, important technological parameters, feed liquid contain solid content 45-55%, and feeding temperature is 60-80 ℃, EAT 150-175 ℃, leaving air temp 70-98 ℃, in the product moisture 4%, normal negative pressure is-0.015-0.02Mpa in the tower, the strong 0.2-0.3Mpa of used for air compressor air pressure, the steam normal pressure is controlled at 0.85-1.0Mpa, and fluid bed steam heated temperature is controlled at 90-105 ℃, and dehumidification air conditioner machine temperature is controlled at 30-50 ℃.
2, the described powdered walnut oil preparation technology of claim 1 is characterized in that, walnut oil is a wild walnut oil in the raw material, and walnut powder is wild walnut oil dregs of rice powder or wild walnut meat powder.
3, powdered walnut oil preparation technology as claimed in claim 1 is characterized in that, emulsifying agent is at least a in single two mixed fatty glycerides, phosphatide, sucrose fat, the two caproic acid tartaric acid monoglycerides in the raw material.
4, a kind of powdered walnut oil, it is characterized in that, by the described either party's method preparation of claim 1-3, the each component percentage by weight is walnut oil 55-60%, walnut powder 12-20%, corn syrup 8-12%, maltodextrin 10-14%, emulsifying agent 2-5%, amylase 0.02-0.1%, each raw material weight is 100% than sum.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
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| CNB2005100109503A CN1331408C (en) | 2005-08-04 | 2005-08-04 | Powdered walnut oil, and its prepn. process |
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| CNB2005100109503A CN1331408C (en) | 2005-08-04 | 2005-08-04 | Powdered walnut oil, and its prepn. process |
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| CN1718028A CN1718028A (en) | 2006-01-11 |
| CN1331408C true CN1331408C (en) | 2007-08-15 |
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| CNB2005100109503A Expired - Fee Related CN1331408C (en) | 2005-08-04 | 2005-08-04 | Powdered walnut oil, and its prepn. process |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN101564180B (en) * | 2009-05-15 | 2012-06-27 | 中国科学院昆明植物研究所 | Walnut total nutriment and soft capsule and health products containing same |
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|---|---|---|---|---|
| CN100490660C (en) * | 2006-02-21 | 2009-05-27 | 北京市农林科学院 | Method for making high-embedding-ratio powder walnut oil |
| CN101942356B (en) * | 2010-08-18 | 2013-01-02 | 云南大地石业集团有限公司 | Walnut kernel cold pressing oil production method and walnut kernel cold pressing and cake-making devices specific thereof |
| CN106937680A (en) * | 2017-02-15 | 2017-07-11 | 广州白云山汉方现代药业有限公司 | A kind of walnut oil and water soluble powder powder composition and preparation method thereof |
| CN107751419A (en) * | 2017-11-10 | 2018-03-06 | 哈尔滨美森食品制造有限公司 | A kind of preparation method of baby walnut powdered oil |
| CN107969700B (en) * | 2017-11-22 | 2021-01-12 | 上海华宝孔雀香精有限公司 | Strong-fragrance walnut oil microcapsule and preparation method thereof |
| CN110432334A (en) * | 2019-09-10 | 2019-11-12 | 云南后谷咖啡有限公司 | One kind is dissolubility walnut powder and preparation method thereof |
| CN112889932A (en) * | 2021-01-25 | 2021-06-04 | 昆明生物制造研究院有限公司 | Preparation method of zero-trans-fatty acid walnut non-dairy creamer |
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| CN1718028A (en) | 2006-01-11 |
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