CN103518856A - Production process of high-calcium pure walnut instant powder - Google Patents

Production process of high-calcium pure walnut instant powder Download PDF

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Publication number
CN103518856A
CN103518856A CN201310469505.8A CN201310469505A CN103518856A CN 103518856 A CN103518856 A CN 103518856A CN 201310469505 A CN201310469505 A CN 201310469505A CN 103518856 A CN103518856 A CN 103518856A
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walnut
calcium
walnut kernel
powder
production process
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朱兆云
丁江生
赵毅
王京昆
王宁
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Yunnan Pharmaceutical Institute
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Yunnan Pharmaceutical Institute
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Abstract

A production process of a high-calcium pure walnut instant powder is provided. The instant powder comprises the used raw and auxiliary materials by the weight percentage: 20-30% of walnut kernels, 0-1.0% of a calcium nutrition enhancer, 60-70% of a sweetening agent, 1.0-3.0% of a stabilizer, and 3.0-7.0% of a grease absorbent, wherein the sum of the weight percentage of the raw and auxiliary materials is 100%. The production process comprises the steps: after walnut kernels are boiled for sterilization in water, adding into an extruder to extrude, and thus obtaining peeled walnut kernel particles; adding cyclodextrin into water, grinding evenly, then adding the walnut kernel particles for grinding into a paste, mixing with other raw and auxiliary materials to prepare particles, drying, crushing, and carrying out ultramicro crushing to obtain the finished powder. The production process of the product is simple, adopts the mechanical method for the processes of peeling the walnut kernels, removing impurities and the like, completely avoids traditional methods of chemical peeling, chemical color protecting and the like, allows the product to have high technological content, and completely retains original nutritional components of the walnut kernels; and moreover, the production process supplements calcium nutrition, so as to achieve complete and balanced nutrition and improve health care and nutritional value of the product.

Description

The production technology of the pure instant walnut powder of a kind of high calcium
Technical field
The present invention relates to a kind of production technology of health beverages, the production technology of the pure instant walnut powder of especially a kind of instant-drink type high calcium.
Background technology
Walnut kernel is good invigorant and raw materials of food processing, fatty 65% left and right, and protein 15% left and right, carbohydrate is more than 10%, crude fibre 5.8%, the several mineral materials such as vitamin and phosphorus (0.32%), potassium (0.39%), calcium (0.10%).Walnut oil is containing unrighted acid up to 83%, and unrighted acid has special health care to human body, is the good source of cerebral tissue eucaryotic cell structure fat, improves the physiological function of brain, can also promote absorbing of calcium.Core is chosen and in benevolence protein, is contained 18 seed amino acids, except 8 kinds enter body essential amino acids content higher, also contain more arginine.Arginine and ornithine can irritate pituitary growth hormone, control unnecessary Adipogenesis.Therefore walnut protein is described as good protein.
In the bibliographical information that existing walnut powder is produced, the most close with the present invention is the patent No. 02113654.8, and name is called the patent of invention of " full content instant walnut powder and production technology thereof ".It is comprised of walnut kernel, sucrose and auxiliary material phosphate, polyglyceryl fatty acid ester, each component percentage by weight is walnut kernel 50-69%, sucrose 30-49%, phosphate 0.1-0.8%, polyglyceryl fatty acid ester 0.8-2.5%, each supplementary material percentage by weight sum is 100%.During preparation walnut-meat hulling adopt high-alkali, high temperature, in short-term and water under high pressure force to go clothing technology, sucrose water to be dissolved into after syrup and go the walnut kernel of clothing in 1~2: 1 ratio mixer mill pulping; After dissolving, add slurry to be uniformly mixed phosphate, polyglyceryl fatty acid ester water, through homogeneous, spraying, after being dried, sieve powder.Its preparation method is as follows:
1), walnut-meat hulling adopt high-alkali, high temperature, in short-term and water under high pressure force to go clothing technology, peeling liquid is 2%NaOH solution, peeling temperature (90 ± 2) ℃, time 1-1.5 minute, washes down and sloughs walnut clothing with water under high pressure immediately after alkali treatment; 2), sucrose water is dissolved into after syrup and goes the walnut kernel of clothing in 1~2: 1 ratio mixer mill pulping; 3), add after phosphate, polyglyceryl fatty acid ester water are dissolved and mix in the slurry that defibrination obtains, be uniformly mixed laggard homogenizer; 4), homogeneous carries out at twice, pressure 40-50Mpa, temperature is room temperature; 5) after the spray-dried tower of feed liquid, after homogeneous is dry, sieve powder, feed liquid enters tower concentration 45-50%, room temperature charging, and hot blast enters tower temperature 170-190 ℃, temperature of outgoing air 76-90 ℃.This technique exists walnut nutritious composition destroyed larger with loss, the problem that production procedure is long, energy consumption is higher.
Summary of the invention
The present invention proposes the production technology of the pure instant walnut powder of a kind of improved high calcium, and this process using machinery extruding technology peeling, inclusion are directly pulverized and produced after absorbing grease.The present invention absorbs the special techniques such as grease and processes by inclusion, greatly simplified production technology, and in product, do not add essence, pigment, anticorrisive agent and emulsifying agent, guarantee product safety and reliable in quality, become powder mobility, dispersiveness and dissolubility better, walnut nutritious composition, without destroying and loss, in the time of complete maintenance walnut all natural nutritional labeling, has also supplemented calcium nutritional labeling; Product has walnut delicate fragrance local flavor, and color is all good, has improved health care, the nutritive value of goods.
The present invention is raw materials used is walnut kernel, calcium-nutrition intensifying agent, sweetener, stabilizing agent and fat absorption agent, each component percentage by weight is walnut kernel 20-30%, calcium-nutrition intensifying agent 0-1.0%, sweetener 60-70%, stabilizing agent 1.0-3.0%, fat absorption agent 3.0-7.0%, each supplementary material percentage by weight sum is 100%; Concrete production technology is: (1) selects that meat is full, not damaged, free from insect pests, without going mouldy or without rotten fresh walnut kernel, removing the impurity such as broken shell and barrier film; (2) by the clear water rinsing of the walnut kernel after selecting, remove earth, dirt and impurity; (3) walnut kernel boils and within 20-45 minute, carries out sterilizing in aseptic purified water; (4) sterilizing walnut kernel joins and in extruder, extrudes the walnut kernel particle that obtains peeling; (5) in cyclodextrin, add the water of 5 times of amounts to grind well, add walnut kernel particle, in grinder, fully mix and grind to form pasty state, add all the other qualified supplementary materials fully to mix, cross 18 mesh sieves, dry under 45-80 ℃ of condition; (6) dried particles is pulverized, crossed 60 mesh sieves and remove residual walnut kernel skin, then make into powder through ultramicro grinding.
Calcium-nutrition intensifying agent in the present invention, comprise any in calcium gluconae, calcium phosphate, calcium carbonate, calcium sulfate, sweetener, comprise any one or several in sucrose, xylitol, maltodextrin, lactose, water soluble starch, auxiliary material is stabilizing agent, comprise any in sodium carboxymethylcellulose, colloidal microcrystalline cellulose sodium carboxymethylcellulose (MCC/NaCMC) compound, xanthans, carragheen, citric acid, malic acid and ascorbic acid, fat absorption agent, comprises one or both in superfine silica gel powder, beta-schardinger dextrin-.
According to above-mentioned production method, can be processed into the pure instant walnut powder of a kind of high calcium.
the present invention compared with the prior art tool has the following advantages or good effect:
1), the present invention adopts mechanical extruding technology peeling.High-alkali, high temperature peeling that prior art generally adopts, there is no mechanical extruding technology peeling report.Mechanism high-alkali, high temperature peeling is: by high-alkali, high temperature, walnut kernel clothing skin is corroded, then with water under high pressure, wash away Beancurd sheet.The weak point of art methods is: when falling walnut kernel clothing skin by high-alkali, high temperature corrosion, also can erode to pulp, cause walnut kernel surface corrosion, color burn, highly basic high temperature destruction can make walnut kernel composition destroy and produce harmful substance, walnut kernel quality deliquescing simultaneously, alkali lye can immerse pulp, produces alkali taste, affect its taste, be also unfavorable for following process utilization; The present invention adopts mechanical extruding technology peeling, and the complete original color of walnut and all natural nutritional labeling of having kept is not destroyed.
2), the present invention absorbs the special techniques such as grease and processes by inclusion, do not need the emulsion processes such as homogeneous, can directly pulverize and produce powder, the complete walnut oil composition that retained, has also improved the stability of unrighted acid greatly; The present invention has simplified production technology, when saving the energy, has significantly improved the nutritive value of goods, has also effectively improved production efficiency.Prior art generally adopts wet grinding mill sizing process, and walnut kernel is through immersion, defibrination, screenings separation and homogeneous and the process such as concentrated, then through vacuum drying spraying is dry or freeze drying after pulverize, sieve powder.The weak point of art methods is: immersion, defibrination affect raw material recovery rate, and long soaking time causes microbial reproduction growth, and protein and sugar class fermentation of materials decomposes generation tart flavour; Adopt defibrination, screenings separating technology, the fat, the protein that wrap in walnut kernel can not propose fully, thereby make walnut kernel magma concentration low; Homogeneous and concentrated and dry etc. need to heat link, causes the destruction of the thermal sensitivity compositions such as protein, unrighted acid, affects its quality, reduces nutritive value.
3), product of the present invention adopts advanced miniaturization technical finesse, raw material almost all utilizes, and product cost is reduced.Product of the present invention is well-designed to keep the contained nutritional labeling of walnut and functional characteristic thereof to carry out, and does not add essence, pigment, anticorrisive agent and emulsifying agent in formula, natural pure, is healthy beverage.This product is solid instant beverage, easy to carry.Adopting bag packing, is the product that adapts to family oriented.
4), product of the present invention has been broken through technological difficulties that can not ultra high temperature sterilization, a set of sterilizing and sterile working rules have been determined, utilize existing sterile working environment and sterilizing methods targetedly, realizing sterile working produces, by lab scale, suitability for industrialized production, test, reach and ensure the quality of products controlledly, can not run off by complete preservation alimentary health-care function material again.For example, for the fat in walnut kernel, under the effect of lipoxidase, can there is oxidative degradation, make to form hydroperoxides after undersaturated fatty acid oxidation.The present invention carries out sterilizing for 20-45 minute by walnut kernel is boiled in aseptic purified water, simultaneously can be by fat oxidation enzyme-deactivating.The heat resistance of this enzyme is lower, in aseptic purified water, boils 20-45 minute, and 45-80 ℃ is toasted walnut kernel particle simultaneously, and its effect is to destroy lipoxidase, can make walnut kernel flavouring simultaneously, gives walnut kernel special fragrance, produces the fragrant of walnut.
5), the present invention adopts the processing such as grease inclusion technique and miniaturization technology, and formula adopts new matrix colloid microcrystalline cellulose Avicel RC/CL thixotrope, making into powder adds after water reconstitutes and is uniformly dispersed, (more than 1 day) places not stratified for a long time, the fat-free floating in surface, bottom is without precipitation, delicate mouthfeel.
6), calcium is needed by human and the nutriment that very easily lacks.The present invention fills a prescription and has used calcium-nutrition intensifying agent, because the undersaturated aliphatic acid in walnut is conducive to absorption and the utilization of calcium nutritional labeling, has greatly improved health care and the nutritive value of product.
7), the product ,Jing Yunnan Province product quality supervision and inspection research institute that produces by the embodiment of the present invention 1 detects, fat content is 13.3%, protein content is 4.5%.By inventory, convert, in full accord in product in the content of fat and protein and ratio and walnut kernel, illustrates in process of production the nutriment in can complete preservation walnut kernel, and yield is high, and nutrition and health care material function is more balanced.
8), the one-tenth powder produced of the embodiment of the present invention 1, as follows its sense organ and physical and chemical index are detected, effect is as follows:
(1) the outward appearance uniformity: get into powder 0.5 g, put in glossy paper, about 5cm tiles 2, with glass plate, its surface is flattened, at bright place, to observe, result becomes powder to present uniform light yellow color and luster, without decorative pattern and color spot.Presentation of results the present invention becomes the powder outward appearance uniformity better, without visible impurity.
(2) mobility: one-tenth powder is poured in a funnel, made sample drop on by funnel the circle that below diameter is 20mm dull and stereotyped upper, powder is piled up gradually, until can not continue to pile height.From scale, read powder stack height h, by formula, obtain angle of repose α.Result angle of repose α is 35 °-36 °, and presentation of results the present invention becomes powder mobility better.
(3) melting: get into powder 10g, add 70-80 ℃ of hot water 200ml, stir 5 minutes, observe immediately.Reconstitute the rear liquid even suspension that is creamy white, outward appearance is fine and smooth, is uniformly dispersed.
(4) settling volume ratio: the liquid after 50ml is reconstituted is placed in graduated cylinder, close plug, firmly jolting is 1 minute, measures the height (H0) starting, and after standing 3 hours, records the final height of sedimentation face (H), and settling volume compares F=H/H0=1.Result shows this liquid stabilising, not stratified, surperficial fat-free floating, and bottom is without precipitation.
(5) accelerated stability is investigated: will become powder simulation listing packing, under the constant temperature and humidity condition of relative humidity (75 ± 5) %, temperature (40 ± 2) ℃, place 6 months, respectively at 0 month, January, February, March, June taking a sample to check, result becomes the powder outward appearance uniformity, mobility, melting, settling volume all more unchanged than indices, moisture is between 1.1% to 1.6%, without the moisture absorption, grumeleuse, also without rancidity, without going mouldy etc., presentation of results becomes powder stability better.
(6) smell and mouthfeel: get into powder and reconstitute rear trial test, drink has the fragrant of walnut, delicate mouthfeel, pure taste nature, free from extraneous odour, without coarse grittiness.
In addition, also observed 100 routine general populations' result of use, 100 examples are adult, age 25-65 year, and male 80 examples wherein, female's 20 examples, concrete result of use is as shown in table 1.
 
The satisfaction of table 1 100 routine drinking of said product
Number Sex Satisfied Satisfied Dissatisfied
80 Man 25 52 3
20 Female 8 10 2
To sum up, compare with existing walnut powder product and production technology, product processes of the present invention is simple, and yield is high; Fully take into account in process of production the safety problem of product, with mechanical means to raw material peel, the technique such as impurity elimination, avoided traditional Chemopeel completely, chemistry protects the methods such as look, product technology content is high, has retained the intrinsic nutritional labeling of walnut kernel completely, has also supplemented calcium nutritional labeling, make it to reach nutrition complete and balanced, improved health care, the nutritive value of goods.In addition, because the present invention has taked a series of technical measures such as fat oxidation enzyme-deactivating, grease inclusion technique, miniaturization technology in formula and production technology, on formula, do not add essence, pigment, anticorrisive agent and emulsifying agent etc., product of the present invention has higher quality.The technology of the present invention route is rationally advanced, and simple and direct practicality is easy to promote, and has good economic and social benefit.
The specific embodiment
embodiment 1
1) press 100Kg batching: barking walnut kernel: 20%, calcium gluconae 1.0%, sucrose 30%, maltodextrin 20%, lactose 20%, Avicel RC/CL 2.9%, citric acid 0.1%, superfine silica gel powder 1.0%, beta-schardinger dextrin-5.0%.
2) production technology
A. get the clear water rinsing of qualified walnut kernel, in aseptic purified water, boil sterilizing in 20-45 minute; B. get in sterilizing walnut kernel input extruder and extrude and obtain barking walnut kernel particle; C. in cyclodextrin, add the water of 5 times of amounts to grind well, add walnut kernel particle, in grinder, fully mix and grind to form pasty state, add all the other qualified supplementary materials fully to mix, cross 18 mesh sieves, dry under 45-80 ℃ of condition.D. dried particles is dropped in pulverizer and to pulverize, to cross 60 mesh sieves and remove residual walnut kernel skin, then drop into and in micronizer, pulverize and obtain into powder.
embodiment 2
1) press 100Kg batching: barking walnut kernel: 30%, calcium gluconae 0.3%, sucrose 21%, maltodextrin 20%, lactose 20%, sodium carboxymethylcellulose 1.6%, citric acid 0.1%, superfine silica gel powder 0.5%, beta-schardinger dextrin-6.5%.
2) production technology is with embodiment 1.
embodiment 3
1) press 100Kg batching: barking walnut kernel: 25%, calcium gluconae 0.5%, sucrose 25%, maltodextrin 20%, lactose 20%, Avicel RC/CL 2.2%, malic acid 0.3%, superfine silica gel powder 2.0%, beta-schardinger dextrin-5.0%.
2) production technology is with embodiment 1.
embodiment 4
1) press 100Kg batching: barking walnut kernel: 24%, calcium gluconae 0.7%, xylitol 30%, maltodextrin 20%, lactose 20%, Avicel RC/CL 2.25%, malic acid 0.05%, superfine silica gel powder 0.3%, beta-schardinger dextrin-2.7%.
2) production technology is with embodiment 1.
embodiment 5
1) press 100Kg batching: barking walnut kernel: 22%, calcium phosphate 0.2%, sucrose 30%, water soluble starch 20%, lactose 20%, xanthans 1.0%, citric acid 0.5%, superfine silica gel powder 1.5%, beta-schardinger dextrin-4.5%.
2) production technology is with embodiment 1.
embodiment 6
1) press 100Kg batching: barking walnut kernel: 28%, calcium sulfate 0.8%, sucrose 28%, maltodextrin 17%, water soluble starch 20%, Avicel RC/CL 2.0%, citric acid 0.3%, superfine silica gel powder 1.2%, beta-schardinger dextrin-3.0%.
2) production technology is with embodiment 1.
embodiment 7
1) press 100Kg batching: barking walnut kernel: 26%, calcium carbonate 0.6%, sucrose 30%, maltodextrin 20%, lactose 16%, carragheen 2.0%, citric acid 0.4%, superfine silica gel powder 1.0%, beta-schardinger dextrin-4.0%.
2) production technology is with embodiment 1.
embodiment 8
1) press 100Kg batching: barking walnut kernel: 20%, sucrose 30%, maltodextrin 20%, lactose 20%, Avicel RC/CL 2.7%, citric acid 0.3%, beta-schardinger dextrin-7.0%.
2) production technology is with embodiment 1.
embodiment 9
1) press 100Kg batching: barking walnut kernel: 24%, xylitol 30%, water soluble starch 20%, lactose 20%, sodium carboxymethylcellulose 1.5%, citric acid 0.5%, beta-schardinger dextrin-4.0%.
2) production technology is with embodiment 1.

Claims (3)

1. the production technology of the pure instant walnut powder of high calcium, it is characterized in that: raw materials used is walnut kernel, calcium-nutrition intensifying agent, sweetener, stabilizing agent and fat absorption agent, each component percentage by weight is walnut kernel 20-30%, calcium-nutrition intensifying agent 0-1.0%, sweetener 60-70%, stabilizing agent 1.0-3.0%, fat absorption agent 3.0-7.0%, each supplementary material percentage by weight sum is 100%; Concrete production technology is:
(1) select that meat is full, not damaged, free from insect pests, without going mouldy or without rotten fresh walnut kernel, removing the impurity such as broken shell and barrier film;
(2) by the clear water rinsing of the walnut kernel after selecting, remove earth, dirt and impurity;
(3) walnut kernel boils and within 20-45 minute, carries out sterilizing in aseptic purified water;
(4) sterilizing walnut kernel joins and in extruder, extrudes the walnut kernel particle that obtains peeling;
(5) in cyclodextrin, add the water of 5 times of amounts to grind well, add walnut kernel particle, in grinder, fully mix and grind to form pasty state, add all the other qualified supplementary materials fully to mix, cross 18 mesh sieves, dry under 45-80 ℃ of condition;
(6) dried particles is pulverized, crossed 60 mesh sieves and remove residual walnut kernel skin, then make into powder through ultramicro grinding.
2. the production technology of the pure instant walnut powder of high calcium as claimed in claim 1, it is characterized in that: calcium-nutrition intensifying agent is calcium gluconae, calcium phosphate, calcium carbonate, any in calcium sulfate, sweetener is sucrose, xylitol, maltodextrin, lactose, any one or several in water soluble starch, stabilizing agent is sodium carboxymethylcellulose, colloidal microcrystalline cellulose sodium carboxymethylcellulose (MCC/NaCMC) compound, xanthans, carragheen, citric acid, any one or several in malic acid, fat absorption agent is superfine silica gel powder, one or both in beta-schardinger dextrin-.
3. the pure instant walnut powder of high calcium, is characterized in that processing by production method claimed in claim 1.
CN201310469505.8A 2013-10-10 2013-10-10 Production process of high-calcium pure walnut instant powder Pending CN103518856A (en)

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CN103919220A (en) * 2014-03-20 2014-07-16 云南省药物研究所 Full-fat walnut high-concentration slurry and preparation method thereof
CN103989153A (en) * 2014-05-29 2014-08-20 丽江中源绿色食品有限公司 Method for processing bolete submicron powder
CN105661397A (en) * 2016-01-21 2016-06-15 南京呈鼎生物科技有限公司 Fruit, vegetable and cyclodextrin supermolecule micro-powder, method for preparing same and application of fruit, vegetable and cyclodextrin supermolecule micro-powder
CN106236713A (en) * 2016-08-30 2016-12-21 林州中农颖泰生物肽有限公司 A kind of seven relieve internal heat clearly effervescent granule and preparation method thereof
CN110432334A (en) * 2019-09-10 2019-11-12 云南后谷咖啡有限公司 One kind is dissolubility walnut powder and preparation method thereof

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CN103919220A (en) * 2014-03-20 2014-07-16 云南省药物研究所 Full-fat walnut high-concentration slurry and preparation method thereof
CN103989153A (en) * 2014-05-29 2014-08-20 丽江中源绿色食品有限公司 Method for processing bolete submicron powder
CN103989153B (en) * 2014-05-29 2015-12-30 丽江中源绿色食品有限公司 A kind of processing method of bolete Ultramicro-powder
CN105661397A (en) * 2016-01-21 2016-06-15 南京呈鼎生物科技有限公司 Fruit, vegetable and cyclodextrin supermolecule micro-powder, method for preparing same and application of fruit, vegetable and cyclodextrin supermolecule micro-powder
CN106236713A (en) * 2016-08-30 2016-12-21 林州中农颖泰生物肽有限公司 A kind of seven relieve internal heat clearly effervescent granule and preparation method thereof
CN110432334A (en) * 2019-09-10 2019-11-12 云南后谷咖啡有限公司 One kind is dissolubility walnut powder and preparation method thereof

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Application publication date: 20140122