CN110358632A - A kind of tiger nut essential oil and preparation method thereof - Google Patents
A kind of tiger nut essential oil and preparation method thereof Download PDFInfo
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- CN110358632A CN110358632A CN201910715148.6A CN201910715148A CN110358632A CN 110358632 A CN110358632 A CN 110358632A CN 201910715148 A CN201910715148 A CN 201910715148A CN 110358632 A CN110358632 A CN 110358632A
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- essential oil
- brave nut
- brave
- nut
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/02—Recovery or refining of essential oils from raw materials
- C11B9/025—Recovery by solvent extraction
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- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Medicines Containing Plant Substances (AREA)
Abstract
The present invention provides a kind of brave nut essential oils and preparation method thereof, by the root, stem and leaf of brave nut be added organic enzyme solvent again by vacuum and low temperature extract method extract to obtain brave nut essential oil, most nutriment complete extractions in brave nut plant are come out, the destruction for avoiding nutriment has good effect in terms of the treatment and beauty for skin disease.
Description
Technical field
The present invention relates to plants essential oil fields, more particularly to a kind of brave nut essential oil and preparation method thereof.
Background technique
Essential oil is in the flower from plant, leaf, stem, root or fruit, passes through steam distillation, extrusion, cold-maceration or molten
Agent extraction method refines the oiliness aromatic substance of extraction.The earliest record about essential oil India, Persian and Egypt from ancient times;
Greece and Rome and Eastern countries have carried out a large amount of aromatic oil and ointment trade.It is all direct in most of ancient civilization
Use fragrant plant or its resin-like product to use as essential oil, until Arab culture golden age, just develop distillation
The technology of essential oil.Arabic distills out ethyl alcohol from the sugar of fermentation first, so that a kind of novel solvent for extracting essential oil is provided, it is existing
Also just come therefrom for essential oil.
Current existing essential oil is generally divided into two kinds, one is the folk prescription oil by single plant extract, it is another then be by
The compound oil that two kinds or more of folk prescription oil is tuned into, often effect is relatively simple for folk prescription oil, although and compound oil effect is more more
Sample, but allotment is sufficiently complex, need to could obtain by many experiments, and there are no a kind of allotments for not needing complexity just to have on the market
There is the essential oil of multi-efficiency.
Brave nut is a kind of plant for originating in Mediterranean Region, and last century is introduced into the country by the former Soviet Union, and starts big
Amount plantation, brave nut contain the nutritional ingredient there are many needed by human body, have good function to skin care, health care, prevention of disease etc.
Effect, but brave nut is normally only used for the processing of food at present, single by edible tiger nut product, can not be by brave nut the effect of
It maximizes.
The present invention is to provide a kind of brave nut essential oil and its preparation side to break through the barrier that brave nut can only be eaten
Method, to solve the problems, such as that current existing essential oil effect is single, allotment is complicated.
Summary of the invention
The object of the present invention is to provide a kind of brave nut essential oils and preparation method thereof, to solve above-mentioned existing essential oil effect
Problem single, allotment is complicated.
To achieve the above object, the present invention provides following schemes:
The present invention provides a kind of preparation method of brave nut essential oil, and the preparation method comprises the following steps:
(1) prepare brave nut root, stem and leaf: harvesting the root, stem and leaf of the brave nut of current growth, it is standby to clean drying surface moisture
With;
(2) organic enzyme solvent is added: organic enzyme solvent is added in brave nut root, stem and leaf, organic enzyme solvent is made not have brave nut
Root, stem and leaf;
(3) cryogenic vacuum extracts: the brave nut root, stem and leaf for being mixed with organic enzyme solvent being carried out cryogenic vacuum extraction, obtains tiger
Nut essential oil semi-finished product;
(4) it dispenses: brave nut essential oil semi-finished product being dispensed after ultraviolet disinfection, obtain brave nut essential oil.
Preferably, the harvest time of the root, stem and leaf of Hu Jianguo is 15~30 days before brave nut full maturity.
Preferably, organic enzyme solvent is water and alcohol, and the ratio of the two is 1: 0.5~1
Preferably, the method that the vacuum and low temperature extracts is Microwave Extraction, and extraction time is 1~5min.
Preferably, the method that the vacuum and low temperature extracts is ultrasonic wave extraction, and extraction time is 20~40min.
Preferably, the method that the vacuum and low temperature extracts be 1~3min of first Microwave Extraction again ultrasonic wave extraction 10~
30min。
A kind of tiger nut essential oil, the tiger nut essential oil are made by the preparation method of above-mentioned brave nut essential oil.
The present invention achieves following advantageous effects compared with the existing technology:
A kind of brave nut essential oil provided by the invention and preparation method thereof, is added organic enzyme solvent for the root, stem and leaf of brave nut
It extracts to obtain brave nut essential oil by the method that vacuum and low temperature extracts again, most nutriments in brave nut plant are complete
It is whole to extract, the destruction of nutriment is avoided, has good effect in terms of the treatment and beauty for skin disease.
Specific embodiment
The technical scheme in the embodiments of the invention will be clearly and completely described below, it is clear that described implementation
Example is only a part of the embodiment of the present invention, instead of all the embodiments.Based on the embodiments of the present invention, this field is common
Technical staff's every other embodiment obtained without making creative work belongs to the model that the present invention protects
It encloses.
The object of the present invention is to provide a kind of brave nut essential oils and preparation method thereof, are obtained by extracting brave nut root, stem and leaf
Essential oil provides a kind of brave nut essential oil and preparation method thereof to break through the barrier that brave nut can only be eaten, existing at present to solve
Essential oil effect is single, problem that allotment is complicated.
In order to make the foregoing objectives, features and advantages of the present invention clearer and more comprehensible, With reference to embodiment
The present invention is described in further detail.
Embodiment 1:
The present embodiment provides a kind of brave nut essential oils and preparation method thereof, harvest the root, stem and leaf of the brave nut of current growth,
The harvest time of the root, stem and leaf of brave nut is 15 days before brave nut full maturity, and effective component contains in brave nut root, stem and leaf at this moment
Amount is more, then cleans drying surface moisture, then take a Sterile vacuum container, brave nut root, stem and leaf is put into container, at it
The middle organic enzyme solvent of addition did not had brave nut root, stem and leaf, and organic enzyme solvent selects alcohol and water 1: 1 to deploy, in this way can be more
The effective component in brave nut root, stem and leaf is extracted well, by container vacuum-pumping, obtains brave nut essence using Microwave Extraction 3min
Oily semi-finished product, Microwave Extraction can rapidly extract to the maximum extent the effective component in brave nut root, stem and leaf, and not
Effective component is destroyed, brave nut essential oil semi-finished product are dispensed after ultraviolet disinfection finally, obtain brave nut essential oil.
Embodiment 2:
The present embodiment provides a kind of brave nut essential oils and preparation method thereof, harvest the root, stem and leaf of the brave nut of current growth,
The harvest time of the root, stem and leaf of brave nut is 25 days before brave nut full maturity, and effective component contains in brave nut root, stem and leaf at this moment
Amount is more, then cleans drying surface moisture, then take a Sterile vacuum container, brave nut root, stem and leaf is put into container, at it
The middle organic enzyme solvent of addition did not had brave nut root, stem and leaf, and organic enzyme solvent selects alcohol and water 0.7: 1 to deploy, in this way can
The effective component in brave nut root, stem and leaf is preferably extracted, by container vacuum-pumping, obtains Hu Jian using ultrasonic wave extraction 30min
Fruit essential oil semi-finished product, ultrasonic wave extraction can rapidly extract to the maximum extent the effective component in brave nut root, stem and leaf
Come, and do not destroy effective component, brave nut essential oil semi-finished product are dispensed after ultraviolet disinfection finally, obtain brave nut essential oil.
Embodiment 3:
The present embodiment provides a kind of brave nut essential oils and preparation method thereof, harvest the root, stem and leaf of the brave nut of current growth,
The harvest time of the root, stem and leaf of brave nut is 30 days before brave nut full maturity, and effective component contains in brave nut root, stem and leaf at this moment
Amount is more, then cleans drying surface moisture, then take a Sterile vacuum container, brave nut root, stem and leaf is put into container, at it
The middle organic enzyme solvent of addition did not had brave nut root, stem and leaf, and organic enzyme solvent selects alcohol and water 0.5: 1 to deploy, in this way can
The effective component in brave nut root, stem and leaf is preferably extracted, by container vacuum-pumping, Microwave Extraction 3min is first used, reuses super
Sound wave extracts 20min, obtains brave nut essential oil semi-finished product, and Microwave Extraction and ultrasonic wave extraction can will be in brave nut root, stem and leafs
Effective component rapidly extracts to the maximum extent, and does not destroy effective component, finally by brave nut essential oil semi-finished product through purple
It is dispensed after outside line sterilizing, obtains brave nut essential oil.
In tiger nut essential oil provided by the invention and preparation method thereof, the Microwave Extraction that is used when preparing brave nut essential oil
It is the prior art with ultrasonic wave extraction, therefore, the present invention only provides key parameter, and method detailed repeats no more.
Organic enzyme is added using brave nut root, stem and leaf as the raw material for preparing essential oil in tiger nut essential oil provided by the invention
Method that solvent is extracted through vacuum and low temperature extracts the effective component in brave nut root, stem and leaf, and retain to the maximum extent effectively at
Point, tiger nut essential oil obtained can be used in cosmetics and treat the addition of the drug of skin disease, have good effect to beauty
Fruit.
Invention applies a specific example illustrates the principle and implementation of the invention, above embodiments are said
It is bright to be merely used to help understand method and its core concept of the invention;At the same time, for those skilled in the art, foundation
Thought of the invention, there will be changes in the specific implementation manner and application range.To sum up, the content of the present specification should not manage
Solution is limitation of the present invention.
Claims (7)
1. a kind of preparation method of tiger nut essential oil, it is characterised in that: the preparation method comprises the following steps:
(1) prepare brave nut root, stem and leaf: harvesting the root, stem and leaf of the brave nut of current growth, it is spare to clean drying surface moisture;
(2) organic enzyme solvent is added: organic enzyme solvent is added in brave nut root, stem and leaf, organic enzyme solvent is made not have brave nut rhizome
Leaf;
(3) cryogenic vacuum extracts: the brave nut root, stem and leaf for being mixed with organic enzyme solvent being carried out cryogenic vacuum extraction, obtains brave nut
Essential oil semi-finished product;
(4) it dispenses: brave nut essential oil semi-finished product being dispensed after ultraviolet disinfection, obtain brave nut essential oil.
2. a kind of preparation method of brave nut essential oil according to claim 1, it is characterised in that: the root, stem and leaf of Hu Jianguo
Harvest time is 15~30 days before brave nut full maturity.
3. a kind of preparation method of brave nut essential oil according to claim 1, it is characterised in that: organic enzyme solvent is
Water and alcohol, and the ratio of the two is 1: 0.5~1.
4. a kind of preparation method of brave nut essential oil according to claim 1, it is characterised in that: the vacuum and low temperature extracts
Method be Microwave Extraction, extraction time be 1~5min.
5. a kind of preparation method of brave nut essential oil according to claim 1, it is characterised in that: the vacuum and low temperature extracts
Method be ultrasonic wave extraction, extraction time be 20~40min.
6. a kind of preparation method of brave nut essential oil according to claim 1, it is characterised in that: the vacuum and low temperature extracts
Method be first 1~3min of Microwave Extraction 10~30min of ultrasonic wave extraction again.
7. a kind of tiger nut essential oil, it is characterised in that: the tiger nut essential oil by the claims 1~6 preparation method system
?.
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Citations (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN102311867A (en) * | 2011-08-18 | 2012-01-11 | 新疆大学 | Method for extracting Cyperus esculentus oil by aqueous enzymatic extraction-freeze-thaw coupling technology |
CN102492542A (en) * | 2011-11-28 | 2012-06-13 | 四川大学 | Rapid extraction method of cyperus bean oil |
CN103789094A (en) * | 2014-01-21 | 2014-05-14 | 广州大学 | Method for extracting agilawood essential oil from agilawood chips |
CN107502444A (en) * | 2017-09-08 | 2017-12-22 | 安徽嘉旗粮油工程技术有限公司 | A kind of processing method of cyperus esculentus oil |
-
2019
- 2019-07-26 CN CN201910715148.6A patent/CN110358632A/en active Pending
Patent Citations (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN102311867A (en) * | 2011-08-18 | 2012-01-11 | 新疆大学 | Method for extracting Cyperus esculentus oil by aqueous enzymatic extraction-freeze-thaw coupling technology |
CN102492542A (en) * | 2011-11-28 | 2012-06-13 | 四川大学 | Rapid extraction method of cyperus bean oil |
CN103789094A (en) * | 2014-01-21 | 2014-05-14 | 广州大学 | Method for extracting agilawood essential oil from agilawood chips |
CN107502444A (en) * | 2017-09-08 | 2017-12-22 | 安徽嘉旗粮油工程技术有限公司 | A kind of processing method of cyperus esculentus oil |
Non-Patent Citations (3)
Title |
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刘雷等: "超声波辅助提取油莎豆油脂工艺研究", 《粮油加工》 * |
胡炜东等: "超声波辅助提取油莎豆油工艺的研究", 《食品与机械》 * |
陈星等: "油莎草根精油的提取与部分理化性质分析", 《粮油加工》 * |
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