CN107502444A - A kind of processing method of cyperus esculentus oil - Google Patents
A kind of processing method of cyperus esculentus oil Download PDFInfo
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- CN107502444A CN107502444A CN201710805956.2A CN201710805956A CN107502444A CN 107502444 A CN107502444 A CN 107502444A CN 201710805956 A CN201710805956 A CN 201710805956A CN 107502444 A CN107502444 A CN 107502444A
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B1/00—Production of fats or fatty oils from raw materials
- C11B1/02—Pretreatment
- C11B1/04—Pretreatment of vegetable raw material
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23D—EDIBLE OILS OR FATS, e.g. MARGARINES, SHORTENINGS, COOKING OILS
- A23D9/00—Other edible oils or fats, e.g. shortenings, cooking oils
- A23D9/007—Other edible oils or fats, e.g. shortenings, cooking oils characterised by ingredients other than fatty acid triglycerides
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23D—EDIBLE OILS OR FATS, e.g. MARGARINES, SHORTENINGS, COOKING OILS
- A23D9/00—Other edible oils or fats, e.g. shortenings, cooking oils
- A23D9/02—Other edible oils or fats, e.g. shortenings, cooking oils characterised by the production or working-up
- A23D9/04—Working-up
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B1/00—Production of fats or fatty oils from raw materials
- C11B1/02—Pretreatment
- C11B1/025—Pretreatment by enzymes or microorganisms, living or dead
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B1/00—Production of fats or fatty oils from raw materials
- C11B1/10—Production of fats or fatty oils from raw materials by extracting
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B3/00—Refining fats or fatty oils
- C11B3/16—Refining fats or fatty oils by mechanical means
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- Engineering & Computer Science (AREA)
- Oil, Petroleum & Natural Gas (AREA)
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- Chemical Kinetics & Catalysis (AREA)
- Microbiology (AREA)
- Food Science & Technology (AREA)
- Polymers & Plastics (AREA)
- Biochemistry (AREA)
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Abstract
The invention discloses a kind of processing method of cyperus esculentus oil, comprise the following steps：S1, Chinese yam, sweet osmanthus, peppermint added water to cook to obtain decoction liquor, fragrant Fructus Perillae quintessence oil and sclareol are added after cooling, obtains proportion liquid；S2, high-quality cyperue esculentus is chosen, dried, crushed, obtain material A；S3, material A mixed with proportion liquid, purified water, citric acid, be ultrasonically treated, then added enzyme preparation and digested, obtain cyperue esculentus crude oil after enzyme deactivation after centrifugation, then add modified montmorillonite used, stirred, filtering, obtain cyperus esculentus oil.A kind of processing method of cyperus esculentus oil proposed by the present invention, its oil yield is high, has the advantages that environmental protection, pollution-free, and obtained cyperus esculentus oil is easy to human consumption's absorption, and nutritive value is high, good health care effect, is not easy to become sour, long shelf-life.
Description
Technical field
The present invention relates to edible oil processing technique field, more particularly to a kind of processing method of cyperus esculentus oil.
Background technology
Cyperue esculentus category Cyperaceae, Cyperus annual herb plant, it is a kind of high-quality, high yield, adaptability is extremely strong, synthesis is sharp
With very high vegetable oil material resource is worth, cyperue esculentus has the plantation of large area in China at present, and annual production is about 30000t.Oily Sha
Fat content is up to 35% or so in beans, and content of starch is up to 30% or so, and sugar content is up to 25% or so, and protein content is high
Up to 10% or so, natural resin content is up to 7% or so, is a kind of excellent industrial crops.Because cyperue esculentus oil yield is higher,
And the quality of oil is better than rapeseed oil, therefore there are good market prospects.The extracting method of existing cyperus esculentus oil includes squeezing
Method, extraction method and supercritical extraction.But the nutritional ingredient that can be destroyed in cyperus esculentus oil after the high temperature in hot moulding, drop
The nutritive value and quality of low cyperus esculentus oil, and the oxidation stability of cyperus esculentus oil is less desirable after cold press, and squeezing be present
Residual oil content is higher in cake, and oil yield is low；Organic solvent extraction extracts cyperus esculentus oil, production equipment be present and operation requires more
Strictly, there is the problems such as potential safety hazard and pollution environment in extraction process.Supercritical extraction is produced grease and not destroyed in grease
Original composition, no chemical residues have the characteristics of safe efficient, but its to produce cost too high.
The content of the invention
Based on technical problem existing for background technology, the present invention proposes a kind of processing method of cyperus esculentus oil, and its is fuel-displaced
Rate is high, has the advantages that environmental protection, pollution-free, and obtained cyperus esculentus oil is easy to human consumption's absorption, and nutritive value is high, health care effect
Fruit is good, is not easy to become sour, long shelf-life.
A kind of processing method of cyperus esculentus oil proposed by the present invention, comprises the following steps：
S1, Chinese yam, sweet osmanthus, peppermint added water to cook to obtain decoction liquor, fragrant Fructus Perillae quintessence oil and sclareol added after cooling,
Obtain proportion liquid；
S2, high-quality cyperue esculentus is chosen, dried, crushed, obtain material A；
S3, material A mixed with proportion liquid, purified water, citric acid, is ultrasonically treated, then added enzyme preparation and digested,
Cyperue esculentus crude oil is obtained after enzyme deactivation after centrifugation, then add it is modified montmorillonite used, stir, filtering, obtain cyperus esculentus oil.
Preferably, digested in S3 enzymolysis process using aqueous enzymatic method.
Preferably, in S1, the weight ratio between Chinese yam, sweet osmanthus and peppermint is 10-20:15-25:8-15.
Preferably, in proportion liquid, the weight ratio between decoction liquor, fragrant Fructus Perillae quintessence oil and sclareol is 20-30:8-15:
6-12。
Preferably, in S2, the granularity of material A is 20-60 mesh.
Preferably, in S3, by weight by 20-30 parts material A and 10-20 parts proportion liquid, 80-100 parts purified water, 8-15
Part citric acid mixing, is ultrasonically treated, and then adds 0.1-0.2 part enzyme preparations and is digested, is obtained after enzyme deactivation after centrifugation
Cyperue esculentus crude oil, the modified montmorillonite used of the 1-2wt% on the basis of cyperue esculentus crude oil gross weight is then added, stirred, filtering, obtained
Cyperus esculentus oil.
Preferably, ultrasonic processing technique parameter is as follows：Ultrasonic power is 300-400W, ultrasonic time 10-18min.
Preferably, enzymolysis process parameter is as follows：Hydrolysis temperature is 42-48 DEG C, enzymolysis time 3-4h.
Preferably, it is modified montmorillonite used to be prepared according to following technique：Na-montmorillonite is crushed, is calcined, cooling, then
Mix, stirring reaction, filter with deionized water, microcrystalline cellulose, chitosan, tartaric acid, honey, calcium propionate, sorbic acid, do
It is dry, obtain modified montmorillonite used.
Preferably, it is modified montmorillonite used to be prepared according to following technique：By weight by 20-30 part na-montmorillonite powder
It is broken, it is calcined at 400-450 DEG C, cools down, then gather with 60-80 parts deionized water, 2-3 parts microcrystalline cellulose, 0.5-1 part shells
Sugar, the mixing of 1-2 parts tartaric acid, 1-2 parts honey, 0.01-0.02 parts calcium propionate, 0.002-0.01 parts sorbic acid, at 45-50 DEG C
Stirring reaction 40-60min, filter, dry, obtain modified montmorillonite used.
Cyperue esculentus after will be broken in the present invention mixes with proportion liquid, purified water, citric acid, is ultrasonically treated, passed through
Rationally set be ultrasonically treated technological parameter, make cyperue esculentus soft texture, make in effective proportion liquid absorb Chinese yam, sweet osmanthus, peppermint,
Active component in fragrant Fructus Perillae quintessence oil and sclareol, the flavor of cyperus esculentus oil of the present invention is effectively improved, while in cyperus esculentus oil
It can effectively protect grease not oxidized in process, effectively extend the shelf-life of cyperus esculentus oil of the present invention, while add this
The nutritional ingredient of invention cyperus esculentus oil, the health-care effect of inventive article is improved, and it is fuel-displaced beneficial to cyperue esculentus, greatly reduce enzymolysis
Reaction time；Then add enzyme preparation to be digested, obtain cyperue esculentus crude oil after enzyme deactivation after centrifugation, its oil yield is with carrying
Oil cut rate is high, then adds modified montmorillonite used agitation and filtration, it is added it is modified montmorillonite used be by by na-montmorillonite high-temperature roasting, removing
Na-montmorillonite per se with harmful components, improve food security, at the same be also effectively improved na-montmorillonite space knot
Structure, increase its aperture and specific surface area, strengthen its adsorption capacity and reactivity, then with microcrystalline cellulose, chitosan, winestone
Acid, honey, calcium propionate, sorbic acid are modifying agent, are effectively improved the structure of na-montmorillonite, play good take off in the present invention
Acid, decolourize and deodorising effect, simplify production technology, effectively reduce the production cost of cyperus esculentus oil, and it is modified montmorillonite used with
Enzymolysis process coordinates, and greatly reduces the content of the phosphatide and free fatty in cyperus esculentus oil, effectively suppresses cyperus esculentus oil and occurs
Become sour phenomenon, make inventive article fragrance dense, pure color, extend the period of storage of giving off a strong fragrance cyperus esculentus oil of the present invention.This
The processing method for inventing a kind of cyperus esculentus oil proposed, its oil yield is high, has the advantages that environmental protection, pollution-free, and obtained oil
Sha's soya-bean oil is easy to human consumption's absorption, and nutritive value is high, good health care effect, is not easy to become sour, long shelf-life.
Embodiment
Below, technical scheme is described in detail by specific embodiment.
Embodiment 1
A kind of processing method of cyperus esculentus oil proposed by the present invention, comprises the following steps：
S1, Chinese yam, sweet osmanthus, peppermint added water to cook to obtain decoction liquor, fragrant Fructus Perillae quintessence oil and sclareol added after cooling,
Obtain proportion liquid；
S2, high-quality cyperue esculentus is chosen, dried, crushed, obtain material A；
S3, material A mixed with proportion liquid, purified water, citric acid, is ultrasonically treated, then added enzyme preparation and digested,
Cyperue esculentus crude oil is obtained after enzyme deactivation after centrifugation, then add it is modified montmorillonite used, stir, filtering, obtain cyperus esculentus oil.
Wherein, na-montmorillonite is crushed, be calcined, cooling, then with deionized water, microcrystalline cellulose, chitosan, winestone
Acid, honey, calcium propionate, sorbic acid mixing, stirring reaction, filter, dry, obtain modified montmorillonite used.
Embodiment 2
A kind of processing method of cyperus esculentus oil proposed by the present invention, comprises the following steps：
S1, Chinese yam, sweet osmanthus, peppermint added water to cook to obtain decoction liquor, fragrant Fructus Perillae quintessence oil and sclareol added after cooling,
Obtain proportion liquid；Wherein, the weight ratio between Chinese yam, sweet osmanthus and peppermint is 10:25:8；Decoction liquor, fragrant Fructus Perillae quintessence oil and perfume (or spice) are purple
Weight ratio between Soviet Union's alcohol is 30:8:12；
S2, high-quality cyperue esculentus is chosen, dried, crushed, obtain the material A of 60 mesh；
S3,20 parts of material As are mixed with 10 parts of proportion liquids, 80 parts of purified waters, 8 parts of citric acids by weight, are ultrasonically treated,
Then add 0.1 part of enzyme preparation to be digested, obtain cyperue esculentus crude oil after enzyme deactivation after centrifugation, then add with cyperue esculentus
1wt%'s is modified montmorillonite used on the basis of crude oil gross weight, stirs, and filtering, obtains cyperus esculentus oil.
Wherein, in S3, ultrasonic processing technique parameter is as follows：Ultrasonic power is 300W, ultrasonic time 18min；
Enzymolysis process parameter is as follows：Hydrolysis temperature is 42 DEG C, enzymolysis time 4h；
It is modified montmorillonite used to be prepared according to following technique：20 parts of na-montmorillonites are crushed by weight, at 400 DEG C
Roasting, cooling, then with 60 parts of deionized waters, 2 parts of microcrystalline celluloses, 0.5 part of chitosan, 1 part of tartaric acid, 1 part of honey, 0.01
Part calcium propionate, 0.002 part of sorbic acid mixing, the stirring reaction 40min at 45 DEG C, filter, dry, obtain modified montmorillonite used.
Embodiment 3
A kind of processing method of cyperus esculentus oil proposed by the present invention, comprises the following steps：
S1, Chinese yam, sweet osmanthus, peppermint added water to cook to obtain decoction liquor, fragrant Fructus Perillae quintessence oil and sclareol added after cooling,
Obtain proportion liquid；Wherein, the weight ratio between Chinese yam, sweet osmanthus and peppermint is 15:20:12；Decoction liquor, fragrant Fructus Perillae quintessence oil and perfume (or spice) are purple
Weight ratio between Soviet Union's alcohol is 25:11:10；
S2, high-quality cyperue esculentus is chosen, dried, crushed, obtain the material A of 40 mesh；
S3,25 parts of material As are mixed with 15 parts of proportion liquids, 90 parts of purified waters, 12 parts of citric acids by weight, at ultrasound
Reason, then add 0.15 part of enzyme preparation and digested, obtain cyperue esculentus crude oil after enzyme deactivation after centrifugation, then add with oil
1.5wt%'s is modified montmorillonite used on the basis of Sha's beans crude oil gross weight, stirs, and filtering, obtains cyperus esculentus oil.
Wherein, in S3, ultrasonic processing technique parameter is as follows：Ultrasonic power is 350W, ultrasonic time 14min；
Enzymolysis process parameter is as follows：Hydrolysis temperature is 45 DEG C, enzymolysis time 3.4h；
It is modified montmorillonite used to be prepared according to following technique：25 parts of na-montmorillonites are crushed by weight, at 420 DEG C
Roasting, cooling, then with 70 parts of deionized waters, 2.5 parts of microcrystalline celluloses, 0.6 part of chitosan, 1.2 parts of tartaric acid, 1.8 parts of honeybees
Honey, 0.015 part of calcium propionate, 0.006 part of sorbic acid mixing, the stirring reaction 50min at 48 DEG C, filter, dry, obtain being modified illiteracy
De- stone.
Embodiment 4
A kind of processing method of cyperus esculentus oil proposed by the present invention, comprises the following steps：
S1, Chinese yam, sweet osmanthus, peppermint added water to cook to obtain decoction liquor, fragrant Fructus Perillae quintessence oil and sclareol added after cooling,
Obtain proportion liquid；Wherein, the weight ratio between Chinese yam, sweet osmanthus and peppermint is 20:15:15；Decoction liquor, fragrant Fructus Perillae quintessence oil and perfume (or spice) are purple
Weight ratio between Soviet Union's alcohol is 20:15:6；
S2, high-quality cyperue esculentus is chosen, dried, crushed, obtain the material A of 20 mesh；
S3,30 parts of material As are mixed with 20 parts of proportion liquids, 100 parts of purified waters, 15 parts of citric acids by weight, at ultrasound
Reason, then add 0.2 part of enzyme preparation and digested, obtain cyperue esculentus crude oil after enzyme deactivation after centrifugation, then add with oil
2wt%'s is modified montmorillonite used on the basis of Sha's beans crude oil gross weight, stirs, and filtering, obtains cyperus esculentus oil.
Wherein, in S3, ultrasonic processing technique parameter is as follows：Ultrasonic power is 400W, ultrasonic time 10min；
Enzymolysis process parameter is as follows：Hydrolysis temperature is 48 DEG C, enzymolysis time 3h；
It is modified montmorillonite used to be prepared according to following technique：30 parts of na-montmorillonites are crushed by weight, at 450 DEG C
Roasting, cooling, then with 80 parts of deionized waters, 3 parts of microcrystalline celluloses, 1 part of chitosan, 2 parts of tartaric acid, 2 parts of honey, 0.02 part
Calcium propionate, 0.01 part of sorbic acid mixing, the stirring reaction 60min at 50 DEG C, filter, dry, obtain modified montmorillonite used.
Embodiment 5
A kind of processing method of cyperus esculentus oil proposed by the present invention, comprises the following steps：
S1, Chinese yam, sweet osmanthus, peppermint added water to cook to obtain decoction liquor, fragrant Fructus Perillae quintessence oil and sclareol added after cooling,
Obtain proportion liquid；Wherein, the weight ratio between Chinese yam, sweet osmanthus and peppermint is 12:20:15；Decoction liquor, fragrant Fructus Perillae quintessence oil and perfume (or spice) are purple
Weight ratio between Soviet Union's alcohol is 22:15:10；
S2, high-quality cyperue esculentus is chosen, dried, crushed, obtain the material A of 50 mesh；
S3,22 parts of material As are mixed with 18 parts of proportion liquids, 85 parts of purified waters, 10 parts of citric acids by weight, at ultrasound
Reason, then add 0.12 part of enzyme preparation and digested, obtain cyperue esculentus crude oil after enzyme deactivation after centrifugation, then add with oil
1.2wt%'s is modified montmorillonite used on the basis of Sha's beans crude oil gross weight, stirs, and filtering, obtains cyperus esculentus oil.
Wherein, in S3, ultrasonic processing technique parameter is as follows：Ultrasonic power is 380W, ultrasonic time 12min；
Enzymolysis process parameter is as follows：Hydrolysis temperature is 46 DEG C, enzymolysis time 3.2h；
It is modified montmorillonite used to be prepared according to following technique：28 parts of na-montmorillonites are crushed by weight, at 440 DEG C
Roasting, cooling, then with 75 parts of deionized waters, 2.2 parts of microcrystalline celluloses, 0.8 part of chitosan, 1.2 parts of tartaric acid, 1.2 parts of honeybees
Honey, 0.012 part of calcium propionate, 0.005 part of sorbic acid mixing, the stirring reaction 50min at 48 DEG C, filter, dry, obtain being modified illiteracy
De- stone.
The cyperus esculentus oil that a kind of processing method of cyperus esculentus oil to being proposed in 3-4 of the embodiment of the present invention obtains and conventional work
Cyperus esculentus oil is tested made from skill, and test result is as follows：
| Embodiment 3 | Embodiment 4 | Common process | |
| Cyperue esculentus crude oil phosphorus content/ppm | 120 | 145 | 265 |
| Cyperus esculentus oil phosphorus content/ppm | 40 | 50 | 150 |
| Cyperus esculentus oil peroxide value/(mmol/Kg) | 1.2 | 1.6 | 3.5 |
As can be seen from the above experimental data, a kind of processing method of cyperus esculentus oil proposed by the present invention and common process phase
Than, the phosphorus content in cyperue esculentus crude oil and cyperus esculentus oil is all greatly reduced, and phosphorus content is no more than 50ppm in cyperus esculentus oil,
The cyperus esculentus oil peroxide value that the present invention obtains simultaneously is significantly lower than the cyperus esculentus oil that common process obtains, oily during liquefaction
Lipid oxidation degree is low, and obtained cyperus esculentus oil oxidation stability is good, good quality, effectively extends the storage time of inventive article.
The foregoing is only a preferred embodiment of the present invention, but protection scope of the present invention be not limited thereto,
Any one skilled in the art the invention discloses technical scope in, technique according to the invention scheme and its
Inventive concept is subject to equivalent substitution or change, should all be included within the scope of the present invention.
Claims (9)
1. a kind of processing method of cyperus esculentus oil, it is characterised in that comprise the following steps：
S1, Chinese yam, sweet osmanthus, peppermint added water to cook to obtain decoction liquor, fragrant Fructus Perillae quintessence oil and sclareol are added after cooling, is obtained
Proportion liquid；
S2, high-quality cyperue esculentus is chosen, dried, crushed, obtain material A；
S3, material A mixed with proportion liquid, purified water, citric acid, be ultrasonically treated, then added enzyme preparation and digested, enzyme deactivation
By cyperue esculentus crude oil is obtained after centrifugation, then add it is modified montmorillonite used, stir, filtering, obtain cyperus esculentus oil.
2. the processing method of cyperus esculentus oil according to claim 1, it is characterised in that in S1, between Chinese yam, sweet osmanthus and peppermint
Weight ratio be 10-20:15-25:8-15.
3. the processing method of cyperus esculentus oil according to claim 1, it is characterised in that in proportion liquid, decoction liquor, fragrant purple perilla essence
Weight ratio between oil and sclareol is 20-30:8-15:6-12.
4. according to the processing method of cyperus esculentus oil any one of claim 1-3, it is characterised in that in S2, the grain of material A
Spend for 20-60 mesh.
5. according to the processing method of cyperus esculentus oil any one of claim 1-4, it is characterised in that in S3, by weight
20-30 parts material A is mixed with 10-20 parts proportion liquid, 80-100 parts purified water, 8-15 part citric acids, is ultrasonically treated, Ran Houjia
Enter 0.1-0.2 part enzyme preparations to be digested, obtain cyperue esculentus crude oil after enzyme deactivation after centrifugation, then add with cyperue esculentus hair
1-2wt%'s is modified montmorillonite used on the basis of oily gross weight, stirs, and filtering, obtains cyperus esculentus oil.
6. according to the processing method of cyperus esculentus oil any one of claim 1-5, it is characterised in that ultrasonic processing technique is joined
Number is as follows：Ultrasonic power is 300-400W, ultrasonic time 10-18min.
7. according to the processing method of cyperus esculentus oil any one of claim 1-6, it is characterised in that enzymolysis process parameter is such as
Under：Hydrolysis temperature is 42-48 DEG C, enzymolysis time 3-4h.
8. according to the processing method of cyperus esculentus oil any one of claim 1-7, it is characterised in that it is modified montmorillonite used according to
It is prepared by following technique：Na-montmorillonite is crushed, be calcined, cooling, then with deionized water, microcrystalline cellulose, chitosan,
Tartaric acid, honey, calcium propionate, sorbic acid mixing, stirring reaction, filter, dry, obtain modified montmorillonite used.
9. according to the processing method of cyperus esculentus oil any one of claim 1-8, it is characterised in that it is modified montmorillonite used according to
It is prepared by following technique：20-30 parts na-montmorillonite is crushed by weight, is calcined at 400-450 DEG C, is cooled down, then
With 60-80 parts deionized water, 2-3 parts microcrystalline cellulose, 0.5-1 parts chitosan, 1-2 parts tartaric acid, 1-2 parts honey, 0.01-
0.02 part of calcium propionate, the mixing of 0.002-0.01 parts sorbic acid, the stirring reaction 40-60min at 45-50 DEG C, filter, dry, obtain
To modified montmorillonite used.
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN108998214A (en) * | 2018-08-30 | 2018-12-14 | 陕西杨凌陕特农业发展有限公司 | A kind of production method of Fructus Zanthoxyli oil |
| CN110041993A (en) * | 2019-03-28 | 2019-07-23 | 宋超 | A kind of tiger nut oil extract and its application in cosmetics edible oil |
| CN110358632A (en) * | 2019-07-26 | 2019-10-22 | 宋玉来 | A kind of tiger nut essential oil and preparation method thereof |
-
2017
- 2017-09-08 CN CN201710805956.2A patent/CN107502444A/en active Pending
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| 刘昌盛: "钠基蒙脱石对菜籽油中磷脂的吸附行为研究", 《中国油料作物学报》 * |
| 罗质: "《油脂精炼工艺学》", 30 June 2016, 中国轻工业出版社 * |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108998214A (en) * | 2018-08-30 | 2018-12-14 | 陕西杨凌陕特农业发展有限公司 | A kind of production method of Fructus Zanthoxyli oil |
| CN110041993A (en) * | 2019-03-28 | 2019-07-23 | 宋超 | A kind of tiger nut oil extract and its application in cosmetics edible oil |
| CN110358632A (en) * | 2019-07-26 | 2019-10-22 | 宋玉来 | A kind of tiger nut essential oil and preparation method thereof |
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