CN108619410A - A kind of Mt. Ai spirit Ai Aicao essential oils and its extraction process - Google Patents
A kind of Mt. Ai spirit Ai Aicao essential oils and its extraction process Download PDFInfo
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- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/88—Liliopsida (monocotyledons)
- A61K36/899—Poaceae or Gramineae (Grass family), e.g. bamboo, corn or sugar cane
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- A61K36/28—Asteraceae or Compositae (Aster or Sunflower family), e.g. chamomile, feverfew, yarrow or echinacea
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- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
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Abstract
The invention discloses a kind of Mt. Ai spirit Ai Aicao essential oils and its extraction processes, it is made of pure water and Chinese medicine, wherein, the Chinese medicine is by herding chaste tree, elscholtiza, soil melon root, needle juniper, oenothera biennis, holy basil, japanese ampelopsis fruit, omei linden root-bark, Finger-millet, Bi Collettii composition, using the method for Chinese traditional treatment theory and orthogonal test and the extraction of half Biomimetic Immersion, determine rational formula and processing technology, the present invention can effectively extract the volatile effective component contained in wormwood, extend the process time of wormwood extraction of essential oil, more traditional extracting mode is compared, the yield of wormwood volatile effective component is improved 20% or so, improve the economic value added of wormwood, effective for wormwood essential oil provides technological guidance, extend the industrial chain of wormwood exploitation.
Description
Technical field
The present invention relates to essential oil fields, more particularly to a kind of Mt. Ai spirit Ai Aicao essential oils and its extraction process.
Background technology
In nature, all plants can all carry out photosynthesis, its cell can secret out of the molecule of fragrant, these points
It is sub then sachet can be gathered into, it is dispersed on the petal, leaf or trunk of plant.After sachet is refined extraction, our institutes are become
" plants essential oil " claimed.Essential oil can be combined by 250 kinds or more different molecules.Under the arrangement of the Nature, these molecules
With perfect ratio jointly there is so that each plant has its particularity, and also therefore essential oil is to the profound effect of human body
Incomparable broadness.
Essential oil（Essential oil) it is made of chemical moleculars such as terpenes, aldehydes, esters, alcohols.Because of height flowing
Property, so being known as " oil ", but there is this qualitative difference with our the daily vegetable oil seen.The main component of vegetable oil is three acid
Glyceride and aliphatic acid composition.First batch of record India, Persian and Egypt from ancient times about essential oil；Greece and Rome and east
Square various countries have carried out a large amount of aromatic oil and ointment trade.Be likely to these products be by flower, root and leaf immerse fatty oil in and
The extract made.In most of ancient civilization, fragrant plant or its resin-like product are directly used.Until Arab culture
Golden age, just develop distillation essential oil technology.Arabic distills out pure water from the sugar of fermentation first, to provide
A kind of novel solvent of extraction essential oil, to replace that thousands of years of fatty oil may have been used.
Essential oil is in the flower from plant, leaf, stem, root or fruit, passes through steam distillation, extrusion, cold-maceration or molten
Agent extraction method refines the volatile flavor of extraction.Essential oil has point diluted（Compound essential oil）With it is not diluted（Folk prescription essence
Oil）.The volatility of essential oil is very strong, once ingress of air will volatilize quickly, also based on this reason, essential oil must be used can be close
The bottle of envelope stores, once corkage uses, also to cover back lid as early as possible.Not all plant can output essential oil, only
Plant containing face cream gland is likely to output essential oil.The face cream gland distribution of different plants is had any different, and has plenty of petal, leaf, root
On stem or trunk.By sachet refine extraction after, become we so-called " plants essential oil ".In essential oil comprising it is many it is different at
Part, some essential oils, such as rose, it can be combined by 250 kinds or more different molecules.Essential oil has lipophilicity, it is easy to molten
In grease, because the strand of essential oil is usually shorter, this makes them easily permeate in skin, and by under subcutaneous fat
Abundant capillary and enter internal.Essential oil is made of the molecule of some very littles, these high volatile substances, can be by nasal cavity
Mucosal tissue is absorbed into body, and message is directly sent to brain, by the limbic system of brain, adjusts the life of mood and body
Manage function.So in aromatotherapy, essential oil can strengthen the function of physiology and psychology.All there are one chemistry for each plants essential oil
Structure come determine it fragrance, color, mobility and it and system operation mode, but also each plants essential oil respectively has one
Cover special function speciality.
Current studies have shown that essential oil also has more new effects to be mined out constantly.Such as the laboratories Gal é nic
It was found that the Argan oil extracted from the berry of arganier trees has effects that the magical of anti-aging；The laboratories Dec1 é or are then found
A kind of beauty of the essential oil mixed by essential oils such as fibert, wheat malt, damesca roses, camomile and bourbon fish pelargoniums
Special effect.The purpose that cosmetologists study essential oil is to allow this natural holy product more to contribute to beauty, and effectively prevent and resist
UV sunlight.The effect of diversified essential oil product, has his own strong points, we should each takes what he needs according to actual conditions.And
And the penetration of essential oil is rapid and powerful, therefore make sure to keep in mind to be excessively used, only need several drops just much of that every time, once excessive make
With can only run counter to desire.
Essential oil essence can anti-communicable disease, to antibacterium, virus, mould, can anti-inflammation, anti-spasm promotes cell new old generation
It thanks and cytothesis function, makes life finer.And certain essential oils can adjust endocrine organ, promote hormone secretion, allow people
The physiology and psychological activity of body, obtain good development.The effect of essential oil is relatively known from, nothing more than releiving and inspire enthusiasm
It is this to be relatively biased to psychological effect, but not only in this effect of essential oil.Different types of essential oil also has a variety of different work(
Effect, for some diseases, also there is the function of releiving and mitigate symptom.Essential oil is all helpful to many diseases, matches composite medicine
Treatment, can allow disease recovery faster.And it uses in daily life, purification air, disinfection, sterilization can be played
Effect, while some communicable diseases can be prevented.Therapeutic effect of the essential oil to following disease：1. nervous system and spiritual disease
Disease；2. eye, ear, nose, oral cavity, odontopathy；3. the disease in terms of respiratory system；4. the disease in terms of blood circulation system；⑤
Disease in terms of digestive system；6. the disease in terms of endocrine, metabolism, urinary system；7. in terms of venereal disease, immune system
Disease；8. gynecological disease；9. muscle, skeletal diseases；10. skin disease.
Folium artemisiae argyi is exactly the leaf of wormwood, perennial herb or slightly at suffruticose, and plant has enhanced aroma.Stem list is raw or few
Number, brown or grey yellowish-brown, base portion slightly lignifying, top Bi matter, and have a small number of short branches, leaf ground paper matter is greyish white above
Color pubescence, base portion is usually without pseudostipule or minimum pseudostipule；Upper leaf is partly split with bract leaf pinniform, capitulum is oval
There are a gland point in shape, corolla tubulose or goblet shape, outside, anther narrow line shape, and style and corolla be close isometric or slightly longer than corolla.Achene
Long avette or oblong, the flowering fruit bearing stage 9-10 months.All herbal medicine, have Wen Jing, dry, cold dispelling, hemostasis, anti-inflammatory, relieving asthma, cough-relieving, peace
The effects that tire, antiallergy.Wormwood essential oil is the extract of leaf from wormwood, stem, and extrusion and solvent extraction method refine extraction
Volatile flavor, generally pale yellow or green-yellow.Natural folium artemisiae argyi extracting refining forms, and appearance is pale yellow or green-yellow.
Warming and activating meridian, qi and activate blood circulation, cold-dispelling pain-relieving improve local circulation, increase immunity.It is coated on acupuncture point or affected part, rubs repeatedly
To absorption.
Invention content
The purpose of the present invention is to provide a kind of Mt. Ai spirit Ai Aicao essential oils and its extracting methods, pass through the preceding place to Chinese medicine
Manage, set suitable extracting parameter, half Biomimetic Immersion extraction etc. technologies come achieve the purpose that extract wormwood essential oil volatile ingredient,
Improve the recovery rate of existing extractive technique.The essential oil, which has, to boost metabolism, anti-inflammatory of subsiding a swelling, promotes the work(such as skin immunity
Effect, can warming and activating meridian, cold-dispelling pain-relieving, improve local circulation, essential oil can be in eight to ten minutes can penetrate to the skin, then reach blood
Essential oil is transported to internal each organ by liquid and lymph, and cell is made to obtain sufficient nutrient, thus essential oil can accelerate body
Metabolism promotes skin to absorb, and promotes the generation of skin neoblast, the growth of the internal cell of stimulation, maintenance improves gradually old
The skin of change, skin-moisturizing, skin can also sterilize injured skin, mediate the infection that skin is caused by injury, and flesh is promoted in anti-inflammatory of subsiding a swelling
The biochemical vigor of skin also assists in the reparation of scar and the healing of wound, reinforces resistance of the skin to foreign aggression.
What the object of the invention was achieved through the following technical solutions：
A kind of Mt. Ai spirit Ai Aicao essential oils, are made of the raw material of following weight ratio：
100-200 parts of pure water, 40-60 parts of Chinese medicine；Wherein, the Chinese medicine includes：40-60 parts of wormwood herds chaste tree 40-60
Part, 40-50 parts of elscholtiza, 40-50 parts of soil melon root, 20-40 parts of needle juniper, 20-40 parts of oenothera biennis, 10-30 parts of holy basil, japanese ampelopsis fruit
10-30 parts, omei linden root-bark 20-30 Fen 20-30 parts of, Bi Collettiis of 20-30 parts of, Finger-millet.
In a preferred embodiment in accordance with this invention, the raw material is fabricated to by following parts by weight：
100-190 parts of pure water, 40-50 parts of Chinese medicine；Wherein, the Chinese medicine includes：40-50 parts of wormwood herds chaste tree 40-50
Part, 40-45 parts of elscholtiza, 40-45 parts of soil melon root, 20-30 parts of needle juniper, 20-30 parts of oenothera biennis, 10-20 parts of holy basil, japanese ampelopsis fruit
10-20 parts, omei linden root-bark 20-25 Fen 20-25 parts of, Bi Collettiis of 20-25 parts of, Finger-millet.
In another preferred embodiment of the present invention, the raw material is made by following parts by weight：
150-200 parts of pure water, 50-60 parts of Chinese medicine；Wherein, the Chinese medicine includes：50-60 parts of wormwood herds chaste tree 50-60
Part, 45-50 parts of elscholtiza, 45-50 parts of soil melon root, 30-40 parts of needle juniper, 30-40 parts of oenothera biennis, 20-30 parts of holy basil, japanese ampelopsis fruit
20-30 parts, omei linden root-bark 25-30 Fen 25-30 parts of, Bi Collettiis of 25-30 parts of, Finger-millet.
In another preferred embodiment of the present invention, the raw material is made by following parts by weight：
200 parts of pure water, 60 parts of Chinese medicine；Wherein, the Chinese medicine includes：60 parts of wormwood herds 60 parts of chaste tree, 50 parts of elscholtiza, soil
50 parts of melon root, 40 parts of needle juniper, 40 parts of oenothera biennis, 30 parts of holy basil, 30 parts of japanese ampelopsis fruit, 30 30 parts of, Bi Collettiis 30 of Fen, Finger-millet of omei linden root-bark
Part.
In a preferred embodiment in accordance with this invention, the raw material is fabricated to by following parts by weight：
180 parts of pure water, 40 parts of Chinese medicine；Wherein, the Chinese medicine includes：40 parts of wormwood herds 40 parts of chaste tree, 40 parts of elscholtiza, soil
40 parts of melon root, 20 parts of needle juniper, 20 parts of oenothera biennis, 10 parts of holy basil, 10 parts of japanese ampelopsis fruit, 20 20 parts of, Bi Collettiis 20 of Fen, Finger-millet of omei linden root-bark
Part.
In a preferred embodiment in accordance with this invention, the raw material is fabricated to by following parts by weight：
170 parts of pure water, 50 parts of Chinese medicine；Wherein, the Chinese medicine includes：50 parts of wormwood herds 50 parts of chaste tree, 45 parts of elscholtiza, soil
45 parts of melon root, 30 parts of needle juniper, 30 parts of oenothera biennis, 20 parts of holy basil, 20 parts of japanese ampelopsis fruit, 25 25 parts of, Bi Collettiis 25 of Fen, Finger-millet of omei linden root-bark
Part.
On the other hand, the present invention provides a kind of extraction processes of Mt. Ai spirit Ai Aicao essential oils：
The raw material is to be prepared from the following steps：
Step 1：Metering, removal of impurities are cleaned, are cleaned, mixing
A, it measures：Corresponding Chinese medicine and pure water are weighed by above-mentioned raw materials parts by weight proportioning, it is spare；
B, removal of impurities cleans：Clean processing by screening is carried out in Chinese medicine that step a is obtained merging ultrasonic wave, after being cleaned in
Medicinal material；
C, it cleans：The obtained Chinese medicines of step b are herded into chaste tree, elscholtiza, soil melon root, needle juniper, oenothera biennis, holy basil, japanese ampelopsis fruit, white youth
It is cleaned in Hua, Finger-millet, Bi Collettiis merging high pressure cleaning showers equipment, the Chinese medicine after being cleaned；
D, it mixes：The Chinese medicine that step c is obtained is placed in three-dimensional oscillating mixer and is mixed, mixed Chinese medicine is obtained
Material；
Step 2：Drying crushes, sterilizing
E, it dries：The obtained Chinese medicines of step d are placed in desiccation in tunnel dryer, so that Chinese medicine is come into full contact with hot wind, obtains
Chinese medicine after to drying；
F, it crushes：The Chinese medicine that step e is obtained is placed in ultramicro high-efficient grinding device and is crushed, the Chinese medicine after being crushed；
G, it sterilizes：In the Chinese medicine merging microwave drying sterilizing equipment that step f is obtained, using the effect of microwave energy, to Chinese medicine
Material carries out heating and sterilization treatment, the Chinese medicine after being sterilized；
Step 3：It is heated to reflux, extracts
H, step g obtained Chinese medicines are separately added into 6 times, 4 times and 2 times of pure water, it is anti-using being heated to reflux at normal temperatures
Kettle equipment is answered to be heated to reflux, number is 3 times, and heating time is respectively 30 minutes, 20 minutes, 10 minutes, heating temperature point
It does not control at 90 DEG C, 95 DEG C, 100 DEG C, obtains Chinese medicine stoste；
I, the Chinese medicine stoste that step h is obtained is extracted for 3 times using dual-effect concentrator point, respectively obtains extracting solution；
Step 4：Filtering merges
J, the extracting solution that step i is obtained is filtered respectively using superfinishing oil filter plant, obtains filtered fluid；It will obtain respectively
Filtered fluid merge, obtain test liquid；
Step 5：Steam distillation, drying
The test liquid that step j is obtained carries out steam distillation using half biomimetic method, and vapour pressure is controlled in 0.4MPa, internal temperature
It at 90 DEG C, uses ethyl acetate for absorbent, obtains essential oil distillate；
Obtained essential oil distillate is placed in oil water separator, anhydrous sodium sulfate is added, separation is dried, sponge essential oil
Moisture in liquid obtains consummate Mt. Ai spirit Ai Aicao essential oils；
Step 6：It collects, sealed storage
Essential oil is volatilized, is aoxidized, the Mt. Ai spirit Ai Aicao essential oils that step 5 is obtained in order to prevent, is collected in closed brown bottle,
Low temperature seal storage is carried out, finished product Mt. Ai spirit Ai Aicao essential oils are obtained；
Step 9, ultra-high pressure sterilization, detection
Finished product Mt. Ai spirit Ai Aicao essential oils are placed in batches in ultra-high pressure sterilization equipment, mould, bacterium are destroyed using super-pressure
Tissue, without heating, does not interfere with the active ingredient of essential oil, after sterilizing to keep the principle of product freshness to sterilize
Finished product essential oil is placed in safety detector in batches to be detected, using advanced cold light source, digital control and data processing technique,
It ensure that the stability of light source and the accuracy of data；
Step 10, labeling, vanning
The product after detecting qualification is labelled using high-speed automatic labeling machine, then packing and binding in batch, have been made one kind
Mt. Ai spirit Ai Aicao essential oils.
The pharmacological action of each bulk pharmaceutical chemicals is as follows：
Folium artemisiae argyi：Property bitter, acrid in flavour and warm in nature, Return liver, spleen, kidney channel.Energy warming and activating meridian, promoting blood circulation and removing blood stasis, anti-inflammatory analgetic, adjustment physiological function increase
The immunity of strong man's body keeps fit and healthy.
Herd chaste tree：It is mild-natured, it is mildly bitter flavor, pungent.Effect：Dysmenorrhoea, irregular menstruation, herria, wet what is said or talked about gonorrhoea, deafness, toothache；It is anti-
Oxidation is the rare natural good medicine of mankind's anti-aging.Eliminating the phlegm, cough-relieving are relievingd asthma, and chronic bronchitis is used for.
Elscholtiza：Meridian distribution of property and flavor：Pungent, tepor.It attaches to the lung and stomach meridians.Effect：Inducing sweat and dispelling exogenous evils, in, inducing diuresis for removing edema is anti-inflammatory for dampness elimination
Effect inhibits virus function, cures mainly：For summer-heat and damp exterior syndrome, oedema, difficult urination.
Soil melon root：It is bitter, cold in nature.It contains the Multiple components such as abundant aliphatic acid, amino acid, carrotene, choline, tool
There are clearing heat and detoxicating, dispersing swelling and dissipating binds, promoting circulation of blood to break the effect of becoming silted up, the blood circulation of skin can be improved, eliminates facial spot, treat acne
And acne print.
Needle juniper：It is acrid in flavour and warm in nature.Major function：Sweating, diuresis, analgesia.Cure mainly rheumatic arthralgia.
Oenothera biennis：Major function：Removing toxic substances；Stagnation resolvation；Wind-damp dispelling；Strengthening the bones and muscles.Main wind-cold-dampness arthralgia；Soreness of bones and muscles.
Holy basil：Pungent sweet, warm.Cold-dispelling is warded off foul.Cure the wound cold, cold headache, fullness and oppression of chest and abdomen, lower profit, passes out semen, nasal obstruction,
Toothache.
Japanese ampelopsis fruit：It is bitter；It is cold, liver；The spleen channel.
Omei linden root-bark：It is bitterly, it is cool in nature, it is nontoxic.Promoting menstruation qi-regulating.
Finger-millet：Sweet, warm.Major function：Tonifying middle-Jiao and Qi, thick stomach.
Bi Collettii：Nature and flavor：Hardship is put down.Effect：Dampness removing removes turbid, wind expelling stagnation removing.
The beneficial effects of the invention are as follows：The present invention is made of pure water and Chinese medicine, wherein the Chinese medicine be by
It herds chaste tree, elscholtiza, soil melon root, needle juniper, oenothera biennis, holy basil, japanese ampelopsis fruit, omei linden root-bark, Finger-millet, Bi Collettii to form, be cured in
The method for treating theoretical and orthogonal test and the extraction of half Biomimetic Immersion determines that rational formula and processing technology, the present invention can have
The volatile effective component contained in effect extraction wormwood, extends the process time of wormwood extraction of essential oil, more traditional extracting mode phase
Than improving the yield of wormwood volatile effective component 20% or so, improving the economic value added of wormwood, be wormwood essential oil
Effectively extraction provides technological guidance, extends the industrial chain of wormwood exploitation.
Clinical data
To confirm that Mt. Ai spirit Ai Aicao essential oils of the present invention are boosting metabolism, anti-inflammatory of subsiding a swelling, promoting skin immunity, Wen Jingtong
The effect of network, cold-dispelling pain-relieving, improvement local circulation etc., with by traditional Chinese herbal decoction made from embodiment, following clinic is carried out
Experimental study：
One, rancid experiment
| Phenomenon | |
| Embodiment 1 | 130 days no abnormality seens, fragrance are pure |
| Embodiment 2 | 115 days no abnormality seens, fragrance are pure |
| Embodiment 3 | 96 days no abnormality seens, fragrance are pure |
Respectively by the Mt. Ai spirit Ai Aicao essential oils of embodiment 1-3, carried out with brown bottle filling, open wide bottle cap, be placed in 25 DEG C of room temperature,
Under 75% environment of relative humidity, continuous observation, concrete outcome see the table below 1.
Two, physical and chemical experiment
Table 2
Three, clinical data
To confirm that Mt. Ai spirit Ai Aicao essential oils of the present invention are boosting metabolism, anti-inflammatory of subsiding a swelling, promoting skin immunity, Wen Jingtong
The effect of network, cold-dispelling pain-relieving, improvement local circulation etc., is carried out with by Mt. Ai spirit Ai Aicao essential oils made from embodiment
Following clinical experimental study：
Data and method
1, general information
Be diagnosed as dermatosis patient by Histopathology and cytolgical examination, the age between 25-55, important organ tissue work(
Can be normal, the patient for meeting this research inclusion criteria is 103.Man 49, female 54, average age 38.43 years old.
2, clinical symptoms
Clinical manifestation is the symptoms such as oedema, metabolic slow, skin dimness, acne acne print, soreness of bones and muscles occur.
3, therapy
Daily using wormwood essential oil made from embodiment, once a day, each 3-5 drops, 7 days are a cycle.
4, therapeutic effect
Clinical observation dermatosis patient 103, after inventive formulation treats 1-2 period, symptom improves effective 84, effectively
Rate 81.6%.
The present invention is treatment group through two groups of clinical verifications, one of which, uses the present invention daily 1 time, and 7 days are a week
Phase, another group is control group, and using related oral medicine, 7 days as a course for the treatment of, 103 is randomly selected in volunteer, clinical table
It is now the symptoms such as oedema, metabolic slow, skin dimness, acne acne print, soreness of bones and muscles occur.
Table 3 takes front and back two groups of courses for the treatment of and compares (unit：People)
There were significant differences for treatment group and control group, it will thus be seen that the application of the present invention clinically has notable curative effect.
Specific implementation mode
Pass through the following implementation technical solution that present invention be described in more detail.It should be pointed out that following explanation
Only to claimed technical solution for example, not to any restrictions of these technical solutions.This hair
Bright protection domain be subject to the appended claims record content.
Embodiment 1
A kind of Mt. Ai spirit Ai Aicao essential oils, are made of the raw material of following weight ratio：
200 parts of pure water, 60 parts of Chinese medicine；Wherein, the Chinese medicine includes：60 parts of wormwood herds 60 parts of chaste tree, 50 parts of elscholtiza, soil
50 parts of melon root, 40 parts of needle juniper, 40 parts of oenothera biennis, 30 parts of holy basil, 30 parts of japanese ampelopsis fruit, 30 30 parts of, Bi Collettiis 30 of Fen, Finger-millet of omei linden root-bark
Part.
On the other hand, the present invention provides a kind of extraction processes of Mt. Ai spirit Ai Aicao essential oils：
The raw material is to be prepared from the following steps：
Step 1：Metering, removal of impurities are cleaned, are cleaned, mixing
A, it measures：Corresponding Chinese medicine and pure water are weighed by above-mentioned raw materials parts by weight proportioning, it is spare；
B, removal of impurities cleans：Clean processing by screening is carried out in Chinese medicine that step a is obtained merging ultrasonic wave, after being cleaned in
Medicinal material；
C, it cleans：The obtained Chinese medicines of step b are herded into chaste tree, elscholtiza, soil melon root, needle juniper, oenothera biennis, holy basil, japanese ampelopsis fruit, white youth
It is cleaned in Hua, Finger-millet, Bi Collettiis merging high pressure cleaning showers equipment, the Chinese medicine after being cleaned；
D, it mixes：The Chinese medicine that step c is obtained is placed in three-dimensional oscillating mixer and is mixed, mixed Chinese medicine is obtained
Material；
Step 2：Drying crushes, sterilizing
E, it dries：The obtained Chinese medicines of step d are placed in desiccation in tunnel dryer, so that Chinese medicine is come into full contact with hot wind, obtains
Chinese medicine after to drying；
F, it crushes：The Chinese medicine that step e is obtained is placed in ultramicro high-efficient grinding device and is crushed, the Chinese medicine after being crushed；
G, it sterilizes：In the Chinese medicine merging microwave drying sterilizing equipment that step f is obtained, using the effect of microwave energy, to Chinese medicine
Material carries out heating and sterilization treatment, the Chinese medicine after being sterilized；
Step 3：It is heated to reflux, extracts
H, step g obtained Chinese medicines are separately added into 6 times, 4 times and 2 times of pure water, it is anti-using being heated to reflux at normal temperatures
Kettle equipment is answered to be heated to reflux, number is 3 times, and heating time is respectively 30 minutes, 20 minutes, 10 minutes, heating temperature point
It does not control at 90 DEG C, 95 DEG C, 100 DEG C, obtains Chinese medicine stoste；
I, the Chinese medicine stoste that step h is obtained is extracted for 3 times using dual-effect concentrator point, respectively obtains extracting solution；
Step 4：Filtering merges
J, the extracting solution that step i is obtained is filtered respectively using superfinishing oil filter plant, obtains filtered fluid；It will obtain respectively
Filtered fluid merge, obtain test liquid；
Step 5：Steam distillation, drying
The test liquid that step j is obtained carries out steam distillation using half biomimetic method, and vapour pressure is controlled in 0.4MPa, internal temperature
It at 90 DEG C, uses ethyl acetate for absorbent, obtains essential oil distillate；
Obtained essential oil distillate is placed in oil water separator, anhydrous sodium sulfate is added, separation is dried, sponge essential oil
Moisture in liquid obtains consummate Mt. Ai spirit Ai Aicao essential oils；
Step 6：It collects, sealed storage
Essential oil is volatilized, is aoxidized, the Mt. Ai spirit Ai Aicao essential oils that step 5 is obtained in order to prevent, is collected in closed brown bottle,
Low temperature seal storage is carried out, finished product Mt. Ai spirit Ai Aicao essential oils are obtained；
Step 9, ultra-high pressure sterilization, detection
Finished product Mt. Ai spirit Ai Aicao essential oils are placed in batches in ultra-high pressure sterilization equipment, mould, bacterium are destroyed using super-pressure
Tissue, without heating, does not interfere with the active ingredient of essential oil, after sterilizing to keep the principle of product freshness to sterilize
Finished product essential oil is placed in safety detector in batches to be detected, using advanced cold light source, digital control and data processing technique,
It ensure that the stability of light source and the accuracy of data；
Step 10, labeling, vanning
The product after detecting qualification is labelled using high-speed automatic labeling machine, then packing and binding in batch, have been made one kind
Mt. Ai spirit Ai Aicao essential oils.
Embodiment 2
A kind of Mt. Ai spirit Ai Aicao essential oils, are made of the raw material of following weight ratio：
180 parts of pure water, 40 parts of Chinese medicine；Wherein, the Chinese medicine includes：40 parts of wormwood herds 40 parts of chaste tree, 40 parts of elscholtiza, soil
40 parts of melon root, 20 parts of needle juniper, 20 parts of oenothera biennis, 10 parts of holy basil, 10 parts of japanese ampelopsis fruit, 20 20 parts of, Bi Collettiis 20 of Fen, Finger-millet of omei linden root-bark
Part.
On the other hand, the present invention provides a kind of extraction processes of Mt. Ai spirit Ai Aicao essential oils：
The raw material is to be prepared from the following steps：
Step 1：Metering, removal of impurities are cleaned, are cleaned, mixing
A, it measures：Corresponding Chinese medicine and pure water are weighed by above-mentioned raw materials parts by weight proportioning, it is spare；
B, removal of impurities cleans：Clean processing by screening is carried out in Chinese medicine that step a is obtained merging ultrasonic wave, after being cleaned in
Medicinal material；
C, it cleans：The obtained Chinese medicines of step b are herded into chaste tree, elscholtiza, soil melon root, needle juniper, oenothera biennis, holy basil, japanese ampelopsis fruit, white youth
It is cleaned in Hua, Finger-millet, Bi Collettiis merging high pressure cleaning showers equipment, the Chinese medicine after being cleaned；
D, it mixes：The Chinese medicine that step c is obtained is placed in three-dimensional oscillating mixer and is mixed, mixed Chinese medicine is obtained
Material；
Step 2：Drying crushes, sterilizing
E, it dries：The obtained Chinese medicines of step d are placed in desiccation in tunnel dryer, so that Chinese medicine is come into full contact with hot wind, obtains
Chinese medicine after to drying；
F, it crushes：The Chinese medicine that step e is obtained is placed in ultramicro high-efficient grinding device and is crushed, the Chinese medicine after being crushed；
G, it sterilizes：In the Chinese medicine merging microwave drying sterilizing equipment that step f is obtained, using the effect of microwave energy, to Chinese medicine
Material carries out heating and sterilization treatment, the Chinese medicine after being sterilized；
Step 3：It is heated to reflux, extracts
H, step g obtained Chinese medicines are separately added into 6 times, 4 times and 2 times of pure water, it is anti-using being heated to reflux at normal temperatures
Kettle equipment is answered to be heated to reflux, number is 3 times, and heating time is respectively 30 minutes, 20 minutes, 10 minutes, heating temperature point
It does not control at 90 DEG C, 95 DEG C, 100 DEG C, obtains Chinese medicine stoste；
I, the Chinese medicine stoste that step h is obtained is extracted for 3 times using dual-effect concentrator point, respectively obtains extracting solution；
Step 4：Filtering merges
J, the extracting solution that step i is obtained is filtered respectively using superfinishing oil filter plant, obtains filtered fluid；It will obtain respectively
Filtered fluid merge, obtain test liquid；
Step 5：Steam distillation, drying
The test liquid that step j is obtained carries out steam distillation using half biomimetic method, and vapour pressure is controlled in 0.5MPa, internal temperature
It at 95 DEG C, uses ethyl acetate for absorbent, obtains essential oil distillate；
Obtained essential oil distillate is placed in oil water separator, anhydrous sodium sulfate is added, separation is dried, sponge essential oil
Moisture in liquid obtains consummate Mt. Ai spirit Ai Aicao essential oils；
Step 6：It collects, sealed storage
Essential oil is volatilized, is aoxidized, the Mt. Ai spirit Ai Aicao essential oils that step 5 is obtained in order to prevent, is collected in closed brown bottle,
Low temperature seal storage is carried out, finished product Mt. Ai spirit Ai Aicao essential oils are obtained；
Step 9, ultra-high pressure sterilization, detection
Finished product Mt. Ai spirit Ai Aicao essential oils are placed in batches in ultra-high pressure sterilization equipment, mould, bacterium are destroyed using super-pressure
Tissue, without heating, does not interfere with the active ingredient of essential oil, after sterilizing to keep the principle of product freshness to sterilize
Finished product essential oil is placed in safety detector in batches to be detected, using advanced cold light source, digital control and data processing technique,
It ensure that the stability of light source and the accuracy of data；
Step 10, labeling, vanning
The product after detecting qualification is labelled using high-speed automatic labeling machine, then packing and binding in batch, have been made one kind
Mt. Ai spirit Ai Aicao essential oils.
Embodiment 3
A kind of Mt. Ai spirit Ai Aicao essential oils, are made of the raw material of following weight ratio：
170 parts of pure water, 50 parts of Chinese medicine；Wherein, the Chinese medicine includes：50 parts of wormwood herds 50 parts of chaste tree, 45 parts of elscholtiza, soil
45 parts of melon root, 30 parts of needle juniper, 30 parts of oenothera biennis, 20 parts of holy basil, 20 parts of japanese ampelopsis fruit, 25 25 parts of, Bi Collettiis 25 of Fen, Finger-millet of omei linden root-bark
Part.
On the other hand, the present invention provides a kind of extraction processes of Mt. Ai spirit Ai Aicao essential oils：
The raw material is to be prepared from the following steps：
Step 1：Metering, removal of impurities are cleaned, are cleaned, mixing
A, it measures：Corresponding Chinese medicine and pure water are weighed by above-mentioned raw materials parts by weight proportioning, it is spare；
B, removal of impurities cleans：Clean processing by screening is carried out in Chinese medicine that step a is obtained merging ultrasonic wave, after being cleaned in
Medicinal material；
C, it cleans：The obtained Chinese medicines of step b are herded into chaste tree, elscholtiza, soil melon root, needle juniper, oenothera biennis, holy basil, japanese ampelopsis fruit, white youth
It is cleaned in Hua, Finger-millet, Bi Collettiis merging high pressure cleaning showers equipment, the Chinese medicine after being cleaned；
D, it mixes：The Chinese medicine that step c is obtained is placed in three-dimensional oscillating mixer and is mixed, mixed Chinese medicine is obtained
Material；
Step 2：Drying crushes, sterilizing
E, it dries：The obtained Chinese medicines of step d are placed in desiccation in tunnel dryer, so that Chinese medicine is come into full contact with hot wind, obtains
Chinese medicine after to drying；
F, it crushes：The Chinese medicine that step e is obtained is placed in ultramicro high-efficient grinding device and is crushed, the Chinese medicine after being crushed；
G, it sterilizes：In the Chinese medicine merging microwave drying sterilizing equipment that step f is obtained, using the effect of microwave energy, to Chinese medicine
Material carries out heating and sterilization treatment, the Chinese medicine after being sterilized；
Step 3：It is heated to reflux, extracts
H, step g obtained Chinese medicines are separately added into 6 times, 4 times and 2 times of pure water, it is anti-using being heated to reflux at normal temperatures
Kettle equipment is answered to be heated to reflux, number is 3 times, and heating time is respectively 30 minutes, 20 minutes, 10 minutes, heating temperature point
It does not control at 90 DEG C, 95 DEG C, 100 DEG C, obtains Chinese medicine stoste；
I, the Chinese medicine stoste that step h is obtained is extracted for 3 times using dual-effect concentrator point, respectively obtains extracting solution；
Step 4：Filtering merges
J, the extracting solution that step i is obtained is filtered respectively using superfinishing oil filter plant, obtains filtered fluid；It will obtain respectively
Filtered fluid merge, obtain test liquid；
Step 5：Steam distillation, drying
The test liquid that step j is obtained carries out steam distillation using half biomimetic method, and vapour pressure is controlled in 0.6MPa, internal temperature
It at 100 DEG C, uses ethyl acetate for absorbent, obtains essential oil distillate；
Obtained essential oil distillate is placed in oil water separator, anhydrous sodium sulfate is added, separation is dried, sponge essential oil
Moisture in liquid obtains consummate Mt. Ai spirit Ai Aicao essential oils；
Step 6：It collects, sealed storage
Essential oil is volatilized, is aoxidized, the Mt. Ai spirit Ai Aicao essential oils that step 5 is obtained in order to prevent, is collected in closed brown bottle,
Low temperature seal storage is carried out, finished product Mt. Ai spirit Ai Aicao essential oils are obtained；
Step 9, ultra-high pressure sterilization, detection
Finished product Mt. Ai spirit Ai Aicao essential oils are placed in batches in ultra-high pressure sterilization equipment, mould, bacterium are destroyed using super-pressure
Tissue, without heating, does not interfere with the active ingredient of essential oil, after sterilizing to keep the principle of product freshness to sterilize
Finished product essential oil is placed in safety detector in batches to be detected, using advanced cold light source, digital control and data processing technique,
It ensure that the stability of light source and the accuracy of data；
Step 10, labeling, vanning
The product after detecting qualification is labelled using high-speed automatic labeling machine, then packing and binding in batch, have been made one kind
Mt. Ai spirit Ai Aicao essential oils.
The content of present invention merely illustrates some claimed specific embodiments, one of them or more skill
Recorded technical characteristic can be combined with arbitrary one or more technical solutions in art scheme, these are combined and obtain
Technical solution also in the application protection domain, technical solution is disclosed in the present invention just as obtained from these are combined
It is specifically recorded in content the same.
Claims (7)
1. a kind of Mt. Ai spirit Ai Aicao essential oils, it is characterised in that：The raw material is fabricated to by following parts by weight：Pure water 100-
200 parts, 40-60 parts of Chinese medicine；Wherein, the Chinese medicine includes：40-60 parts of wormwood, herd 40-60 parts of chaste tree, 40-50 parts of elscholtiza,
40-50 parts of soil melon root, 20-40 parts of needle juniper, 20-40 parts of oenothera biennis, 10-30 parts of holy basil, 10-30 parts of japanese ampelopsis fruit, omei linden root-bark 20-
30 20-30 parts of, Bi Collettiis of 20-30 parts of Fen, Finger-millet.
2. a kind of Mt. Ai spirit Ai Aicao essential oils according to claim 1, it is characterised in that：The raw material presses following parts by weight
It is fabricated to：100-190 parts of pure water, 40-50 parts of Chinese medicine；Wherein, the Chinese medicine includes：40-50 parts of wormwood herds chaste tree 40-
50 parts, 40-45 parts of elscholtiza, 40-45 parts of soil melon root, 20-30 parts of needle juniper, 20-30 parts of oenothera biennis, 10-20 parts of holy basil, japanese ampelopsis fruit
10-20 parts, omei linden root-bark 20-25 Fen 20-25 parts of, Bi Collettiis of 20-25 parts of, Finger-millet.
3. a kind of Mt. Ai spirit Ai Aicao essential oils according to claim 1, it is characterised in that：The raw material presses following parts by weight
It is fabricated to：150-200 parts of pure water, 50-60 parts of Chinese medicine；Wherein, the Chinese medicine includes：50-60 parts of wormwood herds chaste tree 50-
60 parts, 45-50 parts of elscholtiza, 45-50 parts of soil melon root, 30-40 parts of needle juniper, 30-40 parts of oenothera biennis, 20-30 parts of holy basil, japanese ampelopsis fruit
20-30 parts, omei linden root-bark 25-30 Fen 25-30 parts of, Bi Collettiis of 25-30 parts of, Finger-millet.
4. a kind of Mt. Ai spirit Ai Aicao essential oils according to claim 1, it is characterised in that：The raw material presses following parts by weight
It is fabricated to：200 parts of pure water, 60 parts of Chinese medicine；Wherein, the Chinese medicine includes：60 parts of wormwood, herd 60 parts of chaste tree, 50 parts of elscholtiza,
50 parts of soil melon root, 40 parts of needle juniper, 40 parts of oenothera biennis, 30 parts of holy basil, 30 parts of japanese ampelopsis fruit, 30 30 parts of, Bi Collettiis of Fen, Finger-millet of omei linden root-bark
30 parts.
5. a kind of Mt. Ai spirit Ai Aicao essential oils according to claim 1, it is characterised in that：The raw material presses following parts by weight
It is fabricated to：180 parts of pure water, 40 parts of Chinese medicine；Wherein, the Chinese medicine includes：40 parts of wormwood, herd 40 parts of chaste tree, 40 parts of elscholtiza,
40 parts of soil melon root, 20 parts of needle juniper, 20 parts of oenothera biennis, 10 parts of holy basil, 10 parts of japanese ampelopsis fruit, 20 20 parts of, Bi Collettiis of Fen, Finger-millet of omei linden root-bark
20 parts.
6. a kind of Mt. Ai spirit Ai Aicao essential oils according to claim 1, it is characterised in that：The raw material presses following parts by weight
It is fabricated to：170 parts of pure water, 50 parts of Chinese medicine；Wherein, the Chinese medicine includes：50 parts of wormwood, herd 50 parts of chaste tree, 45 parts of elscholtiza,
45 parts of soil melon root, 30 parts of needle juniper, 30 parts of oenothera biennis, 20 parts of holy basil, 20 parts of japanese ampelopsis fruit, 25 25 parts of, Bi Collettiis of Fen, Finger-millet of omei linden root-bark
25 parts.
7. a kind of extraction process of Mt. Ai spirit Ai Aicao essential oils according to claim 1-6 any one, it is characterised in that：
The raw material is to be prepared from the following steps：
Step 1：Metering, removal of impurities are cleaned, are cleaned, mixing
A, it measures：Corresponding Chinese medicine and pure water are weighed by above-mentioned raw materials parts by weight proportioning, it is spare；
B, removal of impurities cleans：Clean processing by screening is carried out in Chinese medicine that step a is obtained merging ultrasonic wave, after being cleaned in
Medicinal material；
C, it cleans：The obtained Chinese medicines of step b are herded into chaste tree, elscholtiza, soil melon root, needle juniper, oenothera biennis, holy basil, japanese ampelopsis fruit, white youth
It is cleaned in Hua, Finger-millet, Bi Collettiis merging high pressure cleaning showers equipment, the Chinese medicine after being cleaned；
D, it mixes：The Chinese medicine that step c is obtained is placed in three-dimensional oscillating mixer and is mixed, mixed Chinese medicine is obtained
Material；
Step 2：Drying crushes, sterilizing
E, it dries：The obtained Chinese medicines of step d are placed in desiccation in tunnel dryer, so that Chinese medicine is come into full contact with hot wind, obtains
Chinese medicine after to drying；
F, it crushes：The Chinese medicine that step e is obtained is placed in ultramicro high-efficient grinding device and is crushed, the Chinese medicine after being crushed；
G, it sterilizes：In the Chinese medicine merging microwave drying sterilizing equipment that step f is obtained, using the effect of microwave energy, to Chinese medicine
Material carries out heating and sterilization treatment, the Chinese medicine after being sterilized；
Step 3：It is heated to reflux, extracts
H, step g obtained Chinese medicines are separately added into 6 times, 4 times and 2 times of pure water, it is anti-using being heated to reflux at normal temperatures
Kettle equipment is answered to be heated to reflux, number is 3 times, and heating time is respectively 30 minutes, 20 minutes, 10 minutes, heating temperature point
It does not control at 90 DEG C, 95 DEG C, 100 DEG C, obtains Chinese medicine stoste；
I, the Chinese medicine stoste that step h is obtained is extracted for 3 times using dual-effect concentrator point, respectively obtains extracting solution；
Step 4：Filtering merges
J, the extracting solution that step i is obtained is filtered respectively using superfinishing oil filter plant, obtains filtered fluid；It will obtain respectively
Filtered fluid merge, obtain test liquid；
Step 5：Steam distillation, drying
The test liquid that step j is obtained carries out steam distillation using half biomimetic method, and vapour pressure is controlled in 0.4MPa, internal temperature
It at 90 DEG C, uses ethyl acetate for absorbent, obtains essential oil distillate；
Obtained essential oil distillate is placed in oil water separator, anhydrous sodium sulfate is added, separation is dried, sponge essential oil
Moisture in liquid obtains consummate Mt. Ai spirit Ai Aicao essential oils；
Step 6：It collects, sealed storage
Essential oil is volatilized, is aoxidized, the Mt. Ai spirit Ai Aicao essential oils that step 5 is obtained in order to prevent, is collected in closed brown bottle,
Low temperature seal storage is carried out, finished product Mt. Ai spirit Ai Aicao essential oils are obtained；
Step 9, ultra-high pressure sterilization, detection
Finished product Mt. Ai spirit Ai Aicao essential oils are placed in batches in ultra-high pressure sterilization equipment, mould, bacterium are destroyed using super-pressure
Tissue, without heating, does not interfere with the active ingredient of essential oil, after sterilizing to keep the principle of product freshness to sterilize
Finished product essential oil is placed in safety detector in batches to be detected, using advanced cold light source, digital control and data processing technique,
It ensure that the stability of light source and the accuracy of data；
Step 10, labeling, vanning
The product after detecting qualification is labelled using high-speed automatic labeling machine, then packing and binding in batch, have been made one kind
Mt. Ai spirit Ai Aicao essential oils.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
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| CN201810611463.XA CN108619410A (en) | 2018-06-14 | 2018-06-14 | A kind of Mt. Ai spirit Ai Aicao essential oils and its extraction process |
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| CN201810611463.XA CN108619410A (en) | 2018-06-14 | 2018-06-14 | A kind of Mt. Ai spirit Ai Aicao essential oils and its extraction process |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN110055132A (en) * | 2019-03-28 | 2019-07-26 | 广州白云山维一实业股份有限公司 | The method of purification of plants essential oil |
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| CN104127500A (en) * | 2014-06-27 | 2014-11-05 | 郑州华信学院 | Aromatic essential oil and aromatic nose plaster both preventing cold, and preparation method of two |
| CN107446702A (en) * | 2017-08-12 | 2017-12-08 | 安徽楚艾农业科技有限公司 | A kind of extracting method of wormwood essential oil |
| CN107638431A (en) * | 2017-09-19 | 2018-01-30 | 广州暨南生物医药研究开发基地有限公司 | A kind of preparation technology of P-Cymene and its application |
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| CN104127500A (en) * | 2014-06-27 | 2014-11-05 | 郑州华信学院 | Aromatic essential oil and aromatic nose plaster both preventing cold, and preparation method of two |
| CN107446702A (en) * | 2017-08-12 | 2017-12-08 | 安徽楚艾农业科技有限公司 | A kind of extracting method of wormwood essential oil |
| CN107638431A (en) * | 2017-09-19 | 2018-01-30 | 广州暨南生物医药研究开发基地有限公司 | A kind of preparation technology of P-Cymene and its application |
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| CN110055132A (en) * | 2019-03-28 | 2019-07-26 | 广州白云山维一实业股份有限公司 | The method of purification of plants essential oil |
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