CN110302110A - A kind of preparation process and its mask product of whitening antioxidation white tea facial mask - Google Patents

A kind of preparation process and its mask product of whitening antioxidation white tea facial mask Download PDF

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CN110302110A
CN110302110A CN201910664720.0A CN201910664720A CN110302110A CN 110302110 A CN110302110 A CN 110302110A CN 201910664720 A CN201910664720 A CN 201910664720A CN 110302110 A CN110302110 A CN 110302110A
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facial mask
white tea
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preparation process
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杨建忠
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Anji Ming Tablet Technology Co Ltd
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Anji Ming Tablet Technology Co Ltd
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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/60Sugars; Derivatives thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/64Proteins; Peptides; Derivatives or degradation products thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/67Vitamins
    • A61K8/671Vitamin A; Derivatives thereof, e.g. ester of vitamin A acid, ester of retinol, retinol, retinal
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/67Vitamins
    • A61K8/673Vitamin B group
    • A61K8/675Vitamin B3 or vitamin B3 active, e.g. nicotinamide, nicotinic acid, nicotinyl aldehyde
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/67Vitamins
    • A61K8/678Tocopherol, i.e. vitamin E
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/73Polysaccharides
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/92Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
    • A61K8/922Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
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    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • A61K8/9783Angiosperms [Magnoliophyta]
    • A61K8/9789Magnoliopsida [dicotyledons]
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • A61Q19/02Preparations for care of the skin for chemically bleaching or whitening the skin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • A61Q19/08Anti-ageing preparations

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Abstract

A kind of preparation process and its mask product of whitening antioxidation white tea facial mask, facial mask essence the preparation method is as follows: (1) takes white tea to be crushed, filtered after extraction, collect filtrate;(2) filtrate of collection is crossed into column, concentration, obtains white tea extracting solution;(3) obtained white tea extracting solution and emulsifier A, SIMMONDSIA CHINENSIS SEED OIL and/or borage oil and/or evening primrose oil are mixed, water is added in mixing while, obtains emulsion I;(4) thickener, moisturizer, emulsifier B, pH adjusting agent, additive are mixed, obtain mixture;(5) emulsion I is added in obtained mixture; after mixing evenly; obtain facial mask essence; this programme protects the active material in white tea by adding stabilizer; the mask product being prepared contains the alkaloids, flavonoids and phenols active material of high concentration; whitening, anti-oxidant and moisture retention are good, and stability is strong, good absorption effect.

Description

A kind of preparation process and its mask product of whitening antioxidation white tea facial mask
Technical field
The invention belongs to household chemicals preparation technical fields, and in particular to a kind of preparation of whitening antioxidation white tea facial mask Technique and its mask product.
Background technique
Facial mask market has become that China's daily use chemicals industry is fastest-rising one of to segment market at present.The development speed of facial mask it Closely bound up with its effect fastly, facial mask can solve the Five problems of skin simultaneously: moisturizing, whitening, oil-control, antiallergic sense and anti-ageing Always, and everyday skincare can not quickly improve skin condition often just for subproblem therein comprehensively.Facial mask utilizes covering In the of short duration time of face, it is temporarily isolating extraneous air and pollution, skin temperature and expansion pore is improved, promotes sweat gland secretion Increase skin oxygen content with metabolism;Moisture in facial mask penetrates into skin cuticula, so that it is become soft, increases elasticity; Gluing ingredient or powdered absorbent in facial mask can stick dirt, metabolic waste and excessive grease in skin and pore etc., And it is thoroughly removed.
Facial mask can be classified as moisture saver mask according to effect, whitening mask, spot-relieving face mask, compact facial mask, anti-wrinkle face mask, shine Skin facial mask, cleaning pack, compact pore facial mask and local facial mask;Tear-pull facial mask, mud can be divided into according to the dosage form classification of facial mask Cream facial mask, creams facial mask, gel facial mask and mounted facial mask;The effect of facial mask and added active constituent have much relations, together The facial mask of one effect may be there are many category, and the facial mask of different dosage forms represents the fashion trend of different times, also signifies The development course of facial mask.
Mounted facial mask includes facial mask cloth and Essence, and facial mask cloth adsorbs Essence as medium, can be fixed on face spy Positioning is set, and is formed confining bed, is promoted the absorption of Essence;Mounted facial mask possesses moisturizing at once, bright color and improves skin line The effect of reason is the category that sales volume is maximum in facial mask class product, growth rate is most fast.
Natural plants and its extract species skin care item, it is mild effectively, irritation it is small, such skin care item are quite liked by consumer Love;Anji white tea mainly originates in Anji, is treasure in tea, is one of Chinese six big teas, has and support mesh, foster the spirit of nobility, repose, beauty treatment The effect of, green tea, black tea are compared, amino acid, theanine, caffeine, the soluble sugar content in the white tea of Anji are high, especially ammonia Base acid content is apparently higher than other teas;Catechin in white tea has the function of anti-oxidant, antibacterial, strengthen immunity;Coffee Alkali and flavanol compound ingredient can promote blood circulation, eliminate fatigue;Organized enzyme can significantly improve internal esterase active, promote Catabolism of fat plays the role of oil-control;Tea polysaccharide has anti-radiation, anticancer and enhancing body self-protection power effect;Flavones Constituents have anti-oxidant and improvement blood circulation effect;The special aroma of white tea itself can also releive pressure, make one to loosen.
Application No. is the files of CN109010170A to disclose a kind of white tea facial mask and preparation method thereof, according to mass fraction It include: that 1-10 parts of white tea leaf extracts, 1.11-11 parts of moisturizer, 0.8-1 parts of additives, 1-5 parts of theanine, 1-5 parts of tea are more Phenol, 0.15-1 part thickener, 0.1-2 parts of niacinamide, 1-10 part two split yeast tunning lysis object, and disclose its preparation side Said components are simply mixed method;But tea polyphenols material stability is low, is easily oxidized, simply by itself and other preparations The facial mask liquid effect being mixed with is difficult to play.
Summary of the invention
In view of the above problems, the object of the present invention is to provide a kind of preparation processes of whitening antioxidation white tea facial mask And its mask product, the active material oxygen in white tea is reduced by the processing step for first mixing stabilizer and white tea extracting solution Change inactivation, the mask product being prepared contains the alkaloids, flavonoids and phenols active material of high concentration, whitening, antioxygen Change and moisture retention is good, and stability is strong, good absorption effect.
To achieve the goals above, technical scheme is as follows:
A kind of preparation process of whitening antioxidation white tea facial mask, including facial mask essence, facial mask essence the preparation method is as follows:
Step 1: taking white tea to be crushed, and filters after extraction, collects filtrate;
Step 2: the filtrate of collection is crossed into column, concentration, obtains white tea extracting solution;
Step 3: obtained white tea extracting solution is mixed with emulsifier A, SIMMONDSIA CHINENSIS SEED OIL and/or borage oil and/or evening primrose oil Water is added in stirring, mixing while, obtains emulsion I;
Step 4: thickener, moisturizer, emulsifier B, pH adjusting agent, additive are mixed, mixture is obtained;
Step 5: emulsion I is added in obtained mixture and obtains facial mask essence after mixing evenly.
In this programme design, tea polyphenols substance has the function of excellent removing free radical, can effectively prevent skin Cell membrane is damaged because of oxidation, while also having the effect of whitening, anti-inflammation and sterilization, and coffee alkaloids have quelling to skin Effect;But such as tea polyphenols, coffee bases of the active material in white tea extracting solution are oxidizable, decompose, and adopt SIMMONDSIA CHINENSIS SEED OIL, Common Borage The stabilizers such as oil, evening primrose oil are used to carry out active material inclusion protection and efficient emulsifier are cooperated to make stabilizer and activity The mixed system of substance is stablized, and tea polyphenols, coffee bases active material non-inactivation can be effectively protected, and used in this programme The stabilizers such as SIMMONDSIA CHINENSIS SEED OIL, borage oil, evening primrose oil have a variety of skin makeup effects, preferably lotus to skin-safe and easily absorption Lotus bar oil compares borage oil, evening primrose oil as stabilizer, and SIMMONDSIA CHINENSIS SEED OIL clearly moistens, moistening effect is good, and skin-friendly is very Height is alternatively arranged as medium for the active material in white tea extracting solution and brings skin promotion absorption into.
Further, step 3 specifically: (1) by obtained white tea extracting solution and SIMMONDSIA CHINENSIS SEED OIL and/or borage oil and/ Or evening primrose oil, emulsifier A stir 8 ~ 12min with 6000 ~ 6500r/min of revolving speed, it is 220 ~ 300r/ that (2), which reduce mixing speed, Water is added dropwise in mixture, the emulsion matter that the amount of ultimately joining of water is by min with 45 ~ 50 drops/min speed The 58% ~ 64% of amount, obtains emulsion I.
In this programme design, stable nanometer can be prepared to micro- using above-mentioned constant temperature phase inversion emulsification (EIP) The emulsion of meter level, since its partial size is small, stronger Brownian movement can greatly offset the effect of gravity, therefore floating/coagulation Stability it is good;Meanwhile compared to for droplet size, adsorption layer of surface active agent is very thick, prevents liquid film between drop Thinning, destruction, the deformation of drop itself, therefore coagulation stability is good, finally, the transparent nature and increasing of micron order emulsion system Consistence makes it have good appearance and dermal sensation;Therefore, the use feeling and using effect of facial mask are greatly improved.
Preferably, emulsifier A is spans emulsifier, such as sorbitan fatty acid ester etc., preferred dehydration mountain Pears alcohol fatty acid ester is lipophilic strong, and to skin-safe, is obtained surely using the transient change of the spontaneous curvature of its surfactant layer The stabilizers such as white tea extracting solution and SIMMONDSIA CHINENSIS SEED OIL can be formed stable Water-In-Oil mixture to micron emulsion by fixed nanometer System.
Preferably, emulsifier B be N- amide groups and its salt compounds and/or betaines zwitterionic compound and/ Or tween emulsifier type, such as polyoxyethylene sorbitan fatty acid ester and/or cocamidopropyl propyl amide hydroxy sulfo lycine and/ Or dodecanamide propyl hydroxy sulfo lycine etc..
In this programme design, emulsifier B selects thickening property, hydrophily excellent and surfactant to skin-safe, Be conducive to for emulsion being sufficiently mixed with other auxiliary agents, additive, disperse, the good facial mask essence of stabilization, the consistency of formation mentions High use feeling.
Preferably, carbomer and/or xanthan gum and/or algaroba glue can be selected in thickener.
Preferably, beta glucan and/or transdermal peptide EFG and/or trehalose and/or niacinamide can be selected in additive.
In this programme design, as additive, transdermal peptide EFG can promote active material and be absorbed by the skin, poly- with β-Portugal Sugar synergistic effect, can increase the maintenance function of facial mask essence, reduce the sensibility of face;Trehalose can be further to facial mask essence Active constituent in magnificent liquid plays a protective role;Niacinamide, which has, mitigates and prevents skin aging, whitening and water lock moisture-keeping efficacy.
Further, additive further includes vitamin A and/or vitamin E, and vitamin A facilitates skin as additive It is soft and full;Vitamin E can play the role of oxidation resistant, further protect the substances such as tea polyphenols not oxidized, while but also with Auxiliary removes the effect of free radical.
Preferably, pH adjusting agent is triethanolamine, triethanolamine can in the carboxyl of acid high-molecular gel carbomer etc. With form stable macromolecular structure, reach the application effect of thickening and moisturizing.
Further, step 4 specifically: (1) carbomer is added to the water stirring and dissolving, then be added Sodium Hyaluronate, Trehalose, cocamidopropyl propyl amide hydroxy sulfo lycine, polyoxyethylene sorbitan fatty acid ester, 85 ~ 95 DEG C, 500 ~ 520r/ 8 ~ 12min is mixed in min, obtains mixture II;(2) the addition triethanolamine, propylene glycol, butanediol in mixture II, 58 ~ 62 DEG C, 500 ~ 520r/min, 8 ~ 12min of mixing, obtain mixture III;(3) xanthan is added in obtained mixture III Glue, beta glucan, 35 ~ 40 DEG C, 500 ~ 520r/min, 12 ~ 18min of mixing, obtain mixture IV;(4) in obtained mixing Be added in object IV transdermal peptide EFG, 28 ~ 32 DEG C, after 500 ~ 520r/min is stirred 8 ~ 12min, obtain mixture VI.
Further, step 5 specifically: the emulsion I is added in obtained mixture VI, maintains 28 ~ 32 DEG C, It is stirred 20 ~ 25min with the speed of 780 ~ 850r/min, obtains the facial mask essence.
It is whitening antioxidation white tea facial mask using product prepared by the above method.
The invention has the following advantages:
White tea extracting solution containing high-content in the facial mask essence that this programme uses, tea polyphenols, coffee in white tea extracting solution Alkali isoreactivity content of material is high, and anti-oxidant, calm effect is good, while also can be reduced the generation of melanin, reaches the effect of whitening Fruit.
This programme compares traditional white tea face pack prescription, is added to the shakinesses such as tea polyphenols, caffeine in dialogue tea extract The stabilizer that fixed, oxidizable active material plays a protective role has excellent protecting effect skin can be promoted to work again simultaneously The absorption of property substance, and to skin-safe.
Using constant temperature phase inversion emulsification stable nanometer can be prepared to micron-sized emulsion in this programme, can be significantly Improve the use feeling and using effect of facial mask.
This programme additionally uses the Multiple components such as moisturizer, thickener, additive, and facial mask essence is made to have whitening, resist Oxidation, moisturizing effect, while the system of facial mask is more stable, has good use feeling and skin sense.
Specific embodiment
Embodiment 1
A kind of preparation process of whitening antioxidation white tea facial mask, the proportion of facial mask essence are as follows: 8% white tea extracting solution, 5% lotus Lotus bar oil, 2.5% sorbitan fatty acid ester, 0.08% vitamin A, 0.1% vitamin E, 0.1% Sodium Hyaluronate, 1% nicotinoyl Amine, 4.5% propylene glycol, 2% butanediol, 0.3% carbomer, 0.2% xanthan gum, 0.3% triethanolamine, 0.5% transdermal peptide EFG, 1% β- Glucan, 1.5% trehalose, 1% cocamidopropyl propyl amide hydroxy sulfo lycine, 1.5% polyoxyethylene sorbitan fatty acid ester, 70.42% purified water.
The preparation process of facial mask essence the following steps are included:
Step 1: taking white tea to be crushed, and crosses 60 meshes, and purified water, white tea powder and purifying is added after sieving in white tea powder The solid-liquid ratio of water is 1g:20ml, is warming up to 60 ~ 70 DEG C, and manganese hydrogen sodium regulating solution pH is added in 7.5 ~ 9.0 sections, extracts 1h After filter, collect filtrate;The filtrate of collection is crossed absorption Resin A B-8 column to adsorb, upper column flow rate is 1BV/h, is then used 100% ethyl alcohol is desorbed, and the stripping liquid of collection is concentrated and dried to 1/8 or so of original volume, obtains white tea extracting solution;
Step 2: white tea extracting solution, VitAVitE, SIMMONDSIA CHINENSIS SEED OIL and sorbitan fatty acid ester are mixed according to the ratio It closes, 30 DEG C of revolving speeds with 6000r/min stir 10min, keep temperature-resistant, and then reducing mixing speed is 250r/min, will Purified water with 45 ~ 50 drops/point speed be added dropwise in mixture, the amount of ultimately joining of purified water is total emulsion quality 60%, obtain emulsion I;
Step 3: according to the ratio by carbomer be added purified water in, 50 DEG C of stirring and dissolvings, then be added Sodium Hyaluronate, trehalose, Cocamidopropyl propyl amide hydroxy sulfo lycine, polyoxyethylene sorbitan fatty acid ester, 90 DEG C, 500r/min mixing 10min obtains mixture II;
Step 4: the addition triethanolamine, propylene glycol, butanediol in mixture II, 60 DEG C, 500r/min mixing 10min, Obtain mixture III;
Step 5: the addition xanthan gum, beta glucan in obtained mixture III, 40 DEG C, 500r/min mixing 15min, Obtain mixture IV;
Step 6: being added transdermal peptide EFG, niacinamide in obtained mixture IV, 30 DEG C, 500r/min be stirred 10min Afterwards, the emulsion I that step 2 obtains is added, maintains 30 DEG C, 20min is stirred with the speed of 800r/min, obtains facial mask essence Magnificent liquid;
Step 7: the facial mask essence of above-mentioned preparation cooperates common mask substrate such as non-woven fabrics, silk base fabric, concept in the market A kind of whitening antioxygen is prepared in stealthy silk base fabric, tencel or bamboo charcoal fiber base fabric, biological fiber or viscose fiber base fabric etc. Change white tea mask product, the product since Essence is more on mask substrate, is more easily absorbed by the skin, have good whitening, Anti-oxidant, moistening effect.
The detection of appearance and fragrance is carried out to facial mask essence according to QB/T2872-2007;According to QB/T2872-2007 points It is other to mercury, lead, arsenic, total plate count, mould and yeast sum, colibacillus of excrement, staphylococcus aureus, pseudomonas aeruginosa into Row detection, testing result are as follows:
By the testing result of table 1 it is found that the organoleptic indicator of facial mask essence manufactured in the present embodiment and hygienic chemistry index are closed Lattice.
Embodiment 2
A kind of preparation process of whitening antioxidation white tea facial mask, the proportion of facial mask essence are as follows: 12% white tea extracting solution, 8% SIMMONDSIA CHINENSIS SEED OIL, 2.5% sorbitan fatty acid ester, 1.0% vitamin A, 1.5% vitamin E, 1% Sodium Hyaluronate, 6% the third two Alcohol, 3% butanediol, 1.0% carbomer, 0.5% xanthan gum, 0.5% triethanolamine, 0.5% transdermal peptide EFG, 1% niacinamide, 1.5% β- Glucan, 2% trehalose, 4% cocamidopropyl propyl amide hydroxy sulfo lycine, 2.5% polyoxyethylene sorbitan fatty acid ester, 51.5% purified water.
The preparation process of facial mask essence the following steps are included:
Step 1: taking white tea to be crushed, and crosses 60 meshes, and purified water, white tea powder and purifying is added after sieving in white tea powder The solid-liquid ratio of water is 1g:20ml, is warming up to 60 ~ 70 DEG C, and manganese hydrogen sodium regulating solution pH is added in 7.5 ~ 9.0 sections, extracts 1h After filter, collect filtrate;The filtrate of collection is crossed absorption Resin A B-8 column to adsorb, upper column flow rate is 1BV/h, is then used 100% ethyl alcohol is desorbed, and the stripping liquid of collection is concentrated and dried to 1/8 or so of original volume, obtains white tea extracting solution;
Step 2: white tea extracting solution, VitAVitE, SIMMONDSIA CHINENSIS SEED OIL and sorbitan fatty acid ester are mixed according to the ratio It closes, 30 DEG C of revolving speeds with 6500r/min stir 12min, keep temperature-resistant, and then reducing mixing speed is 220r/min, will Purified water with 45 ~ 50 drops/point speed be added dropwise in mixture, the amount of ultimately joining of purified water is total emulsion quality 60%, obtain emulsion I;
Step 3: according to the ratio by carbomer be added purified water in, 50 DEG C of stirring and dissolvings, then be added Sodium Hyaluronate, trehalose, Cocamidopropyl propyl amide hydroxy sulfo lycine, polyoxyethylene sorbitan fatty acid ester, 95 DEG C, 520r/min mixing 12min obtains mixture II;
Step 4: the addition triethanolamine, propylene glycol, butanediol in mixture II, 62 DEG C, 520r/min mixing 12min, Obtain mixture III;
Step 5: the addition xanthan gum, beta glucan in obtained mixture III, 35 DEG C, 520r/min mixing 18min, Obtain mixture IV;
Step 6: being added transdermal peptide EFG, niacinamide in obtained mixture IV, 32 DEG C, 520r/min be stirred 12min Afterwards, the emulsion I that step 2 obtains is added, maintains 32 DEG C, 22min is stirred with the speed of 850r/min, obtains facial mask essence Magnificent liquid;
Step 7: the facial mask essence of above-mentioned preparation cooperates common mask substrate such as non-woven fabrics, silk base fabric, concept in the market A kind of whitening antioxygen is prepared in stealthy silk base fabric, tencel or bamboo charcoal fiber base fabric, biological fiber or viscose fiber base fabric etc. Change white tea mask product, the product since Essence is more on mask substrate, is more easily absorbed by the skin, have good whitening, Anti-oxidant, moistening effect.
The organoleptic indicator of facial mask essence manufactured in the present embodiment and hygienic chemistry index are qualified, and test method is the same as implementation Example 1.
Embodiment 3
A kind of preparation process of whitening antioxidation white tea facial mask, the proportion of facial mask essence are as follows: 12% white tea extracting solution, 8% SIMMONDSIA CHINENSIS SEED OIL, 2.5% sorbitan fatty acid ester, 1% Sodium Hyaluronate, 6% propylene glycol, 3% butanediol, 1.0% carbomer, 0.5% xanthan gum, 0.5% triethanolamine, 0.5% transdermal peptide EFG, 1% niacinamide, 1.5% beta glucan, 2% trehalose, 4% cocounut oil acyl Amine hydroxysultaine, 2.5% polyoxyethylene sorbitan fatty acid ester, 54% purified water.
The preparation process of facial mask essence the following steps are included:
Step 1: taking white tea to be crushed, and crosses 60 meshes, and purified water, white tea powder and purifying is added after sieving in white tea powder The solid-liquid ratio of water is 1g:20ml, is warming up to 60 ~ 70 DEG C, and manganese hydrogen sodium regulating solution pH is added in 7.5 ~ 9.0 sections, extracts 1h After filter, collect filtrate;The filtrate of collection is crossed absorption Resin A B-8 column to adsorb, upper column flow rate is 1BV/h, is then used 100% ethyl alcohol is desorbed, and the stripping liquid of collection is concentrated and dried to 1/8 or so of original volume, obtains white tea extracting solution;
Step 2: white tea extracting solution, SIMMONDSIA CHINENSIS SEED OIL are mixed according to the ratio with sorbitan fatty acid ester, 30 DEG C with 6500r/ The revolving speed of min stirs 12min, keeps temperature-resistant, and then reducing mixing speed is 220r/min, by purified water with 45 ~ 50 drops/ The speed divided is added dropwise in mixture, and the amount of ultimately joining of purified water is the 60% of total emulsion quality, obtains emulsion I;
Step 3: according to the ratio by carbomer be added purified water in, 50 DEG C of stirring and dissolvings, then be added Sodium Hyaluronate, trehalose, Cocamidopropyl propyl amide hydroxy sulfo lycine, polyoxyethylene sorbitan fatty acid ester, 85 DEG C, 500r/min mixing 8min obtains mixture II;
Step 4: the addition triethanolamine, propylene glycol, butanediol in mixture II, 58 DEG C, 500r/min mixing 8min, Obtain mixture III;
Step 5: the addition xanthan gum, beta glucan in obtained mixture III, 40 DEG C, 500r/min mixing 12min, Obtain mixture IV;
Step 6: being added transdermal peptide EFG, niacinamide in obtained mixture IV, 28 DEG C, 500r/min be stirred 8min Afterwards, the emulsion I that step 2 obtains is added, maintains 28 DEG C, 25min is stirred with the speed of 780r/min, obtains facial mask essence Magnificent liquid;
Step 7: the facial mask essence of above-mentioned preparation cooperates common mask substrate such as non-woven fabrics, silk base fabric, concept in the market A kind of whitening antioxygen is prepared in stealthy silk base fabric, tencel or bamboo charcoal fiber base fabric, biological fiber or viscose fiber base fabric etc. Change white tea mask product, the product since Essence is more on mask substrate, is more easily absorbed by the skin, have good whitening, Anti-oxidant, moistening effect.
The organoleptic indicator of facial mask essence manufactured in the present embodiment and hygienic chemistry index are qualified, and test method is the same as implementation Example 1.
Comparative example 1 is set, difference from example 1 is that, do not add SIMMONDSIA CHINENSIS SEED OIL.
Comparative example 2 is set, difference from example 1 is that, the processing of step 2 is by white tea extracting solution, Jojoba Oil, sorbitan fatty acid ester, pure water mix according to the ratio, and 30 DEG C of revolving speeds with 6500r/min stir 12min, purified water The amount of ultimately joining is the 60% of total emulsion quality, obtains emulsion I.
Comparative example 3 is set, difference from example 1 is that, do not add triethanolamine.
Evaluation test is carried out to facial mask made from embodiment 1 ~ 3 and comparative example 1 ~ 3, chooses skin health volunteer 12, Age distribution was randomly divided into A ~ F group, every group of a man and a woman at 25 ~ 30 years old, male to female ratio 1:1;First 2 weeks of test does not use product And similar product, detection is primary weekly;Every 2 days attaching facial masks when test, each 15min, test is primary weekly, follow-on test 3 Other similar products were changed without or shared during test week;Wherein, the facial mask that A group uses is the face prepared using embodiment 1 Film, the facial mask that B group uses are the facial mask prepared using embodiment 2, and the facial mask that C group uses is to adopt facial mask prepared with embodiment 3, The facial mask that D group uses is the facial mask prepared using comparative example 1, and the facial mask that E group uses is the facial mask prepared using comparative example 2, F group The facial mask used is the facial mask prepared using comparative example 3;It is surveyed respectively with CM825 skin moisture tester, MPA580 skin elasticity It tries instrument and the full face analysis instrument of VISIA and test evaluation is carried out to volunteer respectively, wherein highest is divided into 5 points, and it is minimum to be divided into 0 point, it comments Valence result is as follows:
As can be seen from the table above, the facial mask that prepared by embodiment 1 ~ 3 has excellent moisture retention, can increase the elasticity of skin, reduces sensitive Property, and there is excellent calmness, whitening effect;By comparative example 1 it is found that being not added with SIMMONDSIA CHINENSIS SEED OIL stabilizer, therefore the work of white tea Property material part inactivation so that the calmness of product, whitening effect reduce obvious, while SIMMONDSIA CHINENSIS SEED OIL has and promotes the skin to absorb Effect, therefore moisture retention and elasticity have reduction;By comparative example 2 it is found that not using constant temperature phase inversion emulsification, lead to Essence Micron order even nanoscale is not arrived, and skin is poor to the absorption of Essence, therefore moisturizing degree, elasticity, calmness, whitening effect all drop Low, sensibility improves;By comparative example 3 it is found that being not added with triethanolamine, so that the pH value of system is unbalance, whole moisturizing degree, bullet Property, anti-inflammatory is sedative all substantially reduces, and cutaneous sensibility improves.
Specific embodiment described herein is only an example for the spirit of the invention.The neck of technology belonging to the present invention The technical staff in domain can make various modifications or additions to the described embodiments or replace by a similar method In generation, however, it does not deviate from the spirit of the invention or beyond the scope of the appended claims.

Claims (10)

1. a kind of preparation process of whitening antioxidation white tea facial mask, including facial mask essence, which is characterized in that the facial mask essence Liquid the preparation method is as follows:
Step 1: taking white tea to be crushed, and filters after extraction, collects filtrate;
Step 2: the filtrate of collection is crossed into column, concentration, obtains white tea extracting solution;
Step 3: obtained white tea extracting solution is mixed with emulsifier A, SIMMONDSIA CHINENSIS SEED OIL and/or borage oil and/or evening primrose oil Water is added in stirring, mixing while, obtains emulsion I;
Step 4: thickener, moisturizer, emulsifier B, pH adjusting agent, additive are mixed, mixture is obtained;
Step 5: being added the emulsion I in obtained mixture, after mixing evenly, obtains the facial mask essence.
2. a kind of preparation process of the anti-ageing white tea facial mask of whitening according to claim 1, which is characterized in that the step 3 Specifically: (1) by obtained white tea extracting solution and SIMMONDSIA CHINENSIS SEED OIL and/or borage oil and/or evening primrose oil, emulsifier A to turn 6000 ~ 6500r/min of speed stirs 8 ~ 12min, and it is 220 ~ 300r/min that (2), which reduce mixing speed, by water with 45 ~ 50 drops/min Speed is added dropwise in mixture, and the 58% ~ 64% of the emulsion quality that the amount of ultimately joining of water is, obtain emulsion I.
3. a kind of preparation process of the anti-ageing white tea facial mask of whitening according to claim 1, which is characterized in that the emulsifier A is spans emulsifier.
4. a kind of preparation process of the anti-ageing white tea facial mask of whitening according to claim 1, which is characterized in that the emulsifier B is N- amide groups and its salt compounds and/or betaines zwitterionic compound and/or tween emulsifier type.
5. a kind of preparation process of the anti-ageing white tea facial mask of whitening according to claim 1, which is characterized in that the thickener Including carbomer and/or xanthan gum and/or algaroba glue.
6. a kind of preparation process of the anti-ageing white tea facial mask of whitening according to claim 1, which is characterized in that the additive Including beta glucan and/or transdermal peptide EFG and/or trehalose and/or niacinamide.
7. a kind of preparation process of the anti-ageing white tea facial mask of whitening according to claim 1, which is characterized in that the pH is adjusted Agent includes triethanolamine.
8. according to a kind of preparation process of any anti-ageing white tea facial mask of whitening of claim 2 ~ 7, which is characterized in that described Step 4 specifically: (1) carbomer is added to the water stirring and dissolving, Sodium Hyaluronate, trehalose, coconut oleoyl amine third is then added Base hydroxy sulfo lycine, polyoxyethylene sorbitan fatty acid ester, 85 ~ 95 DEG C, 500 ~ 520r/min be mixed 8 ~ 12min obtains mixture II;(2) it is added triethanolamine, propylene glycol, butanediol in mixture II, 58 ~ 62 DEG C, 500 ~ 8 ~ 12min is mixed in 520r/min, obtains mixture III;(3) xanthan gum is added in obtained mixture III, β-Portugal gathers Sugar, 35 ~ 40 DEG C, 500 ~ 520r/min, 12 ~ 18min of mixing, obtains mixture IV;(4) add in obtained mixture IV Enter transdermal peptide EFG, 28 ~ 32 DEG C, after 500 ~ 520r/min is stirred 8 ~ 12min, obtain mixture VI.
9. a kind of preparation process of the anti-ageing white tea facial mask of whitening according to claim 8, which is characterized in that the step 5 Specifically: the emulsion I is added in obtained mixture VI, maintains 28 ~ 32 DEG C, is stirred with the speed of 780 ~ 850r/min 20 ~ 25min is mixed, the facial mask essence is obtained.
10. a kind of white tea mask product that whitening is anti-ageing, which is characterized in that according to claim 1,9 any method institutes It is made.
CN201910664720.0A 2019-07-23 2019-07-23 A kind of preparation process and its mask product of whitening antioxidation white tea facial mask Pending CN110302110A (en)

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CN116236427A (en) * 2022-12-29 2023-06-09 肇庆学院 White tea whitening and moisturizing facial mask essence and preparation method and application thereof

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