CN104274357A - Scalp care composition containing plant tincture and preparation method of scalp care composition - Google Patents
Scalp care composition containing plant tincture and preparation method of scalp care composition Download PDFInfo
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- CN104274357A CN104274357A CN201410452088.0A CN201410452088A CN104274357A CN 104274357 A CN104274357 A CN 104274357A CN 201410452088 A CN201410452088 A CN 201410452088A CN 104274357 A CN104274357 A CN 104274357A
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Abstract
The invention relates to skin care compositions, and particularly relates to a composition for scalp care. The composition is prepared from a cosmetic acceptable vector, skin astringent in a tincture mode, skin cleanser, antioxidant and active ingredients with a scalp nourishing function, wherein the scalp nourishing active ingredients comprise the following components in percentage by weight based on the weight of the composition: (1) 0.005-0.5 percent of vitamin E, (2) 0.05-5 percent of vitamin B3, (3) 0.01-2 percent of provitamin B5 and (4) 0.01-2 percent of tetrahydropyrimidine. The scalp care composition belongs to an externally applied cosmetic, can be used for cleaning hair and scalp, has a good curative effect on the phenomenon of excessive seborrhea of scalp, and is capable of improving the integral appearance of hair.
Description
Technical field
The present invention relates to a kind of skin care compositions and methods, more specifically relate to a kind of compositions that may be used for skin of head nursing and the preparation method that contain plant tincture.
Background technology
Compare the skin protection market reached its maturity, hair care is just thought to have unlimited growth potential by more and more dealer.And for the manufacturer being intended to put expertise to good use in this field, " scalp care " is undoubtedly an important R&D direction.When scalp lacks water nourish, cell will become rapidly shrivelled, has no ability to work, and accretion rate becomes slow, does not have normal " growth " of enough power maintenance scalps, causes vicious cycle.Finally, the hair follicle on scalp becomes withered, and no longer carries out fat secretion, and nutrition unbalanced phenomena occurs, this just allows hair also lack power, and hair scale sheet is in the state of half-open semi-closure often, and water loss is faster, finally becomes extremely dry.In addition, do not think that season dry, scalp would not be greasy.Fat secretion is too much, and hair picture has been coated with a large amount of pomades, although glossy, has no level, and whole people also looks listless when water oil is unbalanced! Also have scalp " touch sensitive " phenomenon of a lot of people, as long as environment or the product that uses change, just cause various bad sensitivity response immediately.Such as, if you often scald dye, normal food is pungent, and scalp contacts a lot of chemicals and is subject to pessimal stimulation, and metabolic process will become slow and in disorder, and scalp also can become and compare " irritability " in whole process, and various sensitivity phenomenon is come without invitation.Tackle when spring in oiliness scalp, sixty-four dollar question is not control oil, but allows scalp reach water oil balance, and focuses on deep layer conditioning, nourishing, allows scalp while minimizing fat secretion, reaches best health status.Comprehensively above-mentioned, scalp can not bear various inside and outside bad burden and chemical stimulation, and scalp is done bad, crosses heavy wool more bad, only has the fat secretion of balance scalp to be only important solution.
The same with looks skin, scalp care also needs to improve moisturizing, barrier, anti-oxidation function etc., declare from effect and evaluate angle, scalp does not need crease-resistant and white-skinned face function, but need the evaluation about suppressing in dandruff and head pruritus, in addition, due to the covering of hair, namely be proved effective composition or product in skin care industry, also do not seem and can play one's part to the full on scalp.Therefore effective carrier technology is developed very important.Scalp also has a feature to be exactly that hair density on scalp is far above skin of face.Though the covering of hair can play certain protective effect to scalp, make scalp care operation more difficult than general skin protection, therefore, comprehensively above-mentioned, developing a kind of plant type scalp care product containing tincture will be emphasis of the present invention.
According to bibliographical information, during scalp health research center, " scalp care new development " HAPPI CHINA 2014.4.P28 Asia poplar is built, it is more that scalp and skin of face Main Differences point on physiology comprises the oils and fats that (1) scalp secretes, (2) the cuticular moisture of scalp is lower, (3) barrier function of scalp is lower, (4) the cuticular new city metabolism of scalp is faster, and various skin problem more easily occurs (5) scalp.In addition, the surface area of 100,000 hairs on hair is added up and will be exceeded the summation of human body skin area.It is dirty that so large surface area is easy to become oil, and need often to clean, the process of cleaning is improper, likely makes scalp impaired, and therefore scalp care need be based upon on gentle nursing basis.
According to " clinic skin section magazine " 03 phase in 2007, Xin Shujun; The power of Liu; The discussion of " research of China's normal human skin surface sebum and moisture ", the forehead of chronic pruritus dermatosis patient, forearm surface sebum level moisture are all starkly lower than skin sebum content and the moisture of Healthy subjects and catabasis pruritus dermatosis patient, therefore, forehead and skin of forearm surface sebum and moisture between pruritic condition patient and healthy population, there is significant difference.But scalp is too dry, water adipose membrane incomplete, also can cause the phenomenon of " itching ".This is due to dry weather, and scalp also can be dry, and scalp barrier is easy to be destroyed, therefore antibacterial and fungus invasion, and scalp is felt to itch.Further analysis is then that the moisture in scalp lacks owing to entering external environment condition change in winter, the loss of moist in health, aminoacid contained in scalp and trace element is made to reduce, scalp nutrient environment is unbalance, and the barrier function of scalp is disorderly, then occurs a lot of hair problem.The too much often damaged scalp of some sterilization anti-dandruff agent consumption, scalp is more itched, and dandruff is more, and therefore, scalp care is extremely important, scalp health, and hair just has brilliance.
Summary of the invention
The object of this invention is to provide a kind of scalp care compositions, the present invention contains plant tincture, is carried out the secretion of control head haze wax fat by the astriction of plant tincture, and the moisture of being nursed the scalp made by scalp tonic is strengthened and better nurses scalp.
The present invention also provides the preparation method of said composition.
The present invention is achieved through the following technical solutions:
A kind of scalp care compositions, except cosmetics acceptable carrier, its component is:
(1) the Peruvian bark tree tincture of composition weight percentage ratio 0.5% to 15% is accounted for,
(2) the Saponin tincture of composition weight percentage ratio 0.1% to 10% is accounted for,
(3) the Eucalyptus tincture of composition weight percentage ratio 0.1% to 5% is accounted for,
(4) extractive of flax seed of composition weight percentage ratio 0.05% to 5% is accounted for,
(5) ethanol of composition weight percentage ratio 50% to 95% is accounted for,
(6) the scalp tonic active component of composition weight percentage ratio 0.075% to 9.5% is accounted for;
Wherein said scalp tonic active component is:
A () accounts for the vitamin E of composition weight percentage ratio 0.005% to 0.5%,
B () accounts for the vitamin B of composition weight percentage ratio 0.05% to 5%
3,
C () accounts for the provitamin B of composition weight percentage ratio 0.01% to 2%
5
D () accounts for the tetrahydropyrimidine of composition weight percentage ratio 0.01% to 2%.
Scalp care compositions of the present invention, its component is optimized for further:
(1) account for composition weight percentage ratio 1% to 10% Peruvian bark tree tincture,
(2) the Saponin tincture of composition weight percentage ratio 0.5% to 5% is accounted for,
(3) the Eucalyptus tincture of composition weight percentage ratio 0.2% to 2% is accounted for,
(4) extractive of flax seed of composition weight percentage ratio 0.1% to 2% is accounted for,
(5) ethanol of composition weight percentage ratio 62% to 80% is accounted for,
(6) the scalp tonic active component of composition weight percentage ratio 0.21% to 3.3% is accounted for;
Scalp tonic active component is:
A () accounts for the vitamin E of composition weight percentage ratio 0.01% to 0.1%,
B () accounts for the vitamin B of composition weight percentage ratio 0.1% to 2%
3,
C () accounts for the provitamin B of composition weight percentage ratio 0.05% to 0.9%
5,
D () accounts for the tetrahydropyrimidine of composition weight percentage ratio 0.05% to 0.3%.
Scalp care compositions of the present invention, also containing 1,3 butanediols accounting for composition weight percentage ratio 10%.
Scalp care compositions of the present invention, its pH value range is 5-7, and preferable ph controls 6.
The present invention contains the scalp care compositions of plant tincture, and the component of its optimization formula and content are:
Account for the Peruvian bark tree tincture of composition weight percentage ratio 1% to 10%,
Account for the Saponin tincture of composition weight percentage ratio 0.5% to 5%,
Account for the Eucalyptus tincture of composition weight percentage ratio 0.2% to 2%,
Account for the extractive of flax seed of composition weight percentage ratio 0.1% to 2%,
Account for the ethanol of composition weight percentage ratio 72% to 90%,
Account for the vitamin E of composition weight percentage ratio 0.01% to 0.1%,
Account for the vitamin B of composition weight percentage ratio 0.1% to 2%
3,
Account for the provitamin B of composition weight percentage ratio 0.05% to 0.9%
5,
Account for the tetrahydropyrimidine of composition weight percentage ratio 0.05% to 0.3%,
Account for 1 of composition weight percentage ratio 10%, 3 butanediols,
Account for the carbomer 2020 of composition weight percentage ratio 0.1 to 0.6%,
Account for the disodiumedetate of composition weight percentage ratio 0.02% to 0.1%,
Appropriate coloring agent, essence, pH adjusting agent, and the deionized water of surplus.
Scalp care compositions of the present invention, wherein the preparation method of plant tincture is carried out according to the following steps:
A) preparation of Peruvian bark tree tincture: the ledger bark chopping grinds getting weight portion 25 parts, cross 200 mesh sieves, then the water of weight portion 45 parts is placed in, decocting in water 10 minutes, then cool and add the ethanol of weight portion 30 parts, soak 12 hours, add the dehydrated alcohol of residue dregs equivalent weight after then filtering, ageing obtained Peruvian bark tree tincture after 12 hours;
B) preparation of Quillaia saponaria tincture: china bark is shredded grinds, cross 200 mesh sieves, get soapbark powder weight portion 50 parts, the ethanol being then placed in weight portion 60 parts soaks, and is filtered and the ethanol adding weight portion 40 parts obtains Quillaia saponaria tincture after 12 hours by cotton-wool;
C) Eucalyptus tincture preparation: eucalyptus leaves is placed in weight portion 4 and doubly grinds to the glycerine water solution of eucalyptus leaves own wt, wherein the weight ratio of glycerol and water is 1:1, then the eucalyptus leaves lapping liquid of weight portion 25 parts is got, add the dehydrated alcohol of weight portion 75 parts, soak 12 hours, filtered by cotton-wool by mixture afterwards, finally add and the ethanol leaching dregs equivalent weight, Eucalyptus tincture is made in ageing for 12 hours;
D) Semen Lini tincture preparation: Semen Lini grinding is shattered, cross 200 mesh sieves, then the linseed meal of weight portion 50 parts and the ethanol of weight portion 50 parts is got, both weight ratio 1:1, soak 48 hours, then filtered by cotton-wool by mixture, finally add and the ethanol leaching dregs equivalent weight, ageing is for subsequent use after 12 hours.
Scalp care compositions of the present invention is a kind of technology being realized hair healthy by scalp care; the technology of the present invention controls the fat secretion of scalp by the skin contraction agent of plant tincture form; the skin cleaner of plant tincture form carrys out the excessive oils and fats in gentle removal scalp and hair; the skin antioxidant of plant tincture form prevents the peroxidization of sebum in scalp and hair; play the effect of protection scalp and hair, and with the active component with scalp tonic function to the barrier function of the water adipose membrane thus recovery scalp health of setting up scalp.In a word, the present invention improves scalp microecological environment by the cooperative effect of plant tincture and the scalp tonic factor, improves the health status of scalp, and then reaches the object improving hair healthy.
Beneficial effect of the present invention: scalp care dew of the present invention belongs to cosmetics for external use, can play clean effect, have good curative effect for scalp excessive seborrhea phenomenon to hair and scalp.Scalp care compositions of the present invention may be used for the anti-dandruff hair conditioner of hair, anti-dandruff shampoo, hair nursing liquid etc.
Detailed description of the invention
Below in conjunction with embodiment, the present invention is described in detail.
The supernatant liquid preparation that tincture in the present invention means the ethanol extraction of crude drug or medical material normal concentration or dissolving and makes, as Semen daturae tincture, Pericarpium Citri junoris tincture, iodine tincture etc., is called for short tincture, for for oral administration or external.The concentration of tincture is different with medical material character, and unless otherwise specified, the every 100ml of the tincture containing toxicity medicine is equivalent to crude drug 10g, the clear and definite person of effective ingredient, should be adjusted according to its half-finished content, makes to meet the regulation under corresponding kind item; Other tinctures, every 100ml is equivalent to crude drug 20g.Tincture preparation is simple, is easy to preserve.But containing more ethanol in solvent, therefore clinical practice has certain limitation, and tincture can use dissolution method, dilution method, infusion process or percolation to prepare.(1) dissolution method or dilution method get drug powder or fluid extract, add the appropriate amount of ethanol of normal concentration, dissolve or dilution, leave standstill, filter if desired, to obtain final product.(2) infusion process gets the medical material suitably pulverized, and is equipped with in lid container, and it is appropriate to add solvent, Mi Gai, stirs or jolting, floods 3 ~ 5 days or official hour, incline and get supernatant, add solvent more appropriate, flood in accordance with the law and fully leach to effective ingredient, merge leachate, after solubilizer to ormal weight, leave standstill 24 hours, filter, to obtain final product.(3) percolation is according to the method under fluid extract item, with the appropriate percolation of solvent, after reaching ormal weight to effluent, leaves standstill, filters, to obtain final product.If when tincture is long placed in and produces precipitation, when specifying under ethanol and active constituent content meet each kind item, removing precipitation can be filtered.Tincture should put sealed type storage in light-shielding container.
A kind of scalp care of the present invention dew for containing the organic Viability point of compositions formed of several natural origin, has the maintenance hair of excellence and the effect of scalp health.Said composition comprises (1) Peruvian bark tree tincture, (2) Saponin tincture, (3) Eucalyptus tincture, (4) Semen Lini tincture, (5) ethanol, (6) scalp tonic active component (7) distilled water.
Quinine tincture
Peruvian bark tree originates in South America, is found at first within the mountain valley of the east, Andes height above sea level 900 to 2700 meters.To mid-term in 19th century, Peruvian bark tree is transplanted is with cultivation to Southeast Asia one, and Indonesia is the country introduced a fine variety the earliest.China started to plant experimentally in Taiwan Province in 1906,1933, also start to introduce a fine variety in Chinese Guangdong, Yunnan and Taiwan, quinine can be refined for treatment malaria at that time by the bark of Peruvian bark tree, afterwards because quinine can by chemosynthesis, just gradually stop the relevant operation of Peruvian bark tree, and can find large quantities of quinine woods in fan level land district now, and can in the flat natural regeneration of fan.The dried bark of Peruvian bark tree, root bark, branch skin and seed, containing 26 kinds of alkaloids of having an appointment, be generically and collectively referred to as Cortex Cinchonae alkaloid.Wherein content at most and pharmaceutically the most important thing is quinine, is secondly cinchonine, cinchonidine, quinidine etc., all the other very low containing rate in bark.Their major parts are quinolines, also have only a few to be indole derivatives.In Cortex Cinchonae alkaloid, a lot of stereoisomer each other, as: quinine and quinidine, cinchonine and cinchonidine, cinchotine and hydrocinchonidine, epiquinine and epiquinidine, hydroqunine and quinotidine etc.In addition, cinchonicine is also had, quinotoxine, cupereine, quinamine, cinchonamine, Kui Buddhist nun ketone, aricine and paricine, succirubin, Methyl Succirubin, Kang Kuinaming, cusconidine, diconchinine etc.Except alkaloid, also containing cinchotannic acid, quininic acid, cinchona red etc.In bark, alkaloid is combined with cinchotannic acid, quininic acid.
The most important activity of Peruvian bark tree consists of cinchona alkaloid, is also quinine, and cinchona alkaloid to be present in ledger bark and to exist with the form of acylate.The preparation method of quinine extract is by the decocting in water 10 minutes of the cinchonae cortex pulveratus weight portion 40 parts of weight portion 25 parts, then cools, filters, be finally diluted with water to 100 parts again, as astringent lotion.
The preparation method of Peruvian bark tree tincture: the ledger bark chopping grinds getting weight portion 25 parts, about 200 orders, then the water of weight portion 45 parts is placed in, decocting in water 10 minutes, then cool and add the ethanol of weight portion 30 parts, soak 12 hours, add the dehydrated alcohol of residue dregs equivalent weight after then filtering, ageing obtained Peruvian bark tree tincture after 12 hours.
In the present invention, Peruvian bark tree tincture accounts for composition weight percentage ratio 0.5% to 15%, is optimized for 1% to 10% further.
Quillaia saponaria tincture
Quillaia saponaria (QUILLAJA SAPONARIA), china bark China Bark, family department Rosaceae rosaceae, gets the bark extract of Quillaia saponaria Quillaja Saponaria, and effective ingredient is saponin.The preparation method of Quillaia saponaria tincture: china bark is shredded grinds, about 200 orders, get soapbark powder weight portion 50 parts, then the ethanol being placed in weight portion 60 parts soaks, to filter after 12 hours and the ethanol adding weight portion 40 parts obtains Quillaia saponaria tincture, the material in Quillaia saponaria tincture with physiologically active comprises quillajic acid and sapotoxin, and commercially available saponin is the compositions of these two kinds of active component.In the present invention, Quillaia saponaria tincture is used for the emulsifying such as oils and fats and spot removal in scalp and hair, plays clean effect to scalp and hair.
In the present invention, Quillaia saponaria tincture accounts for composition weight percentage ratio 0.1% to 10%, is optimized for 0.5% to 5% further.
Eucalyptus tincture
Eucalyptus (Eucalyptus) has another name called eucalyptus globolus tree, be the general name of Myrtaceae, eucalyptus plant, originate in Australia, China mainly plants in Yunnan, Guangdong, the provinces and regions such as Guangxi and Chuan Xi.Varieties of plant has Eucalyptus globulus Labill, straight dry Eucalyptus globulus Labill, eucalyptus citriodora, Folium Eucalypti Robustae and sees blade profile copper coin eucalyptus globulus 5 kinds, and Eucalyptus is aithullium, has periodic Lao Ye obscission in 1 year, and large multi items is high megaphanerophyte, and minority is dungarunga, in seldom frutescent.Shape of tree-crown has steeple shape, racemosus shape and weeping branch shape etc.Dan Ye, Quan Yuan, keratin, is had the thin waxiness of one deck sometimes.Leaf can be divided into juvenile leaf, middle leaf and climax leaves three class, and Folium eucalypti globueli (Eucalyptus globulus Labill.) can extract Oleum Eucalypti (aromatic oil), and leaf and quintessence oil can be used as medicine, and has anti-inflammation and sterilization, stomach invigorating, eliminates the phlegm, the effect of wind dispelling.
Eucalyptus of the present invention (Eucalyptus robusta Smith) gets the kind of Chao-Shan Area, Guangdong plantation, and the another name of Eucalyptus in Chao-Shan Area is also cajeput oil tree, big tree, swamp mahogany etc.
Eucalyptus tincture preparation method of the present invention: eucalyptus leaves is placed in weight ratio 4 and doubly grinds to the glycerine water solution of eucalyptus leaves own wt, wherein the weight ratio of glycerol and water is 1:1, then the eucalyptus leaves lapping liquid of weight portion 25 parts is got, add the dehydrated alcohol of weight portion 75 parts, soak 12 hours, filtered by cotton-wool by mixture afterwards, finally add and the ethanol leaching dregs equivalent weight, Eucalyptus tincture is made in ageing for 12 hours.
Main active in eucalyptus leaves be polyphenols as tannin, catechols etc., therefore, in the present invention, the main application of eucalyptus leaves tincture is that it has certain astriction to skin (scalp).
In the present invention, Eucalyptus tincture accounts for composition weight percentage ratio 0.1% to 5%, is optimized for 0.2% to 2% further.
Semen Lini tincture
Extractive of flax seed Common Flax Seed P.E, it is the phytoestrogen extracted inside natural plants Semen Lini, Latin name: Linum usitatissmum L., source: Caulis et Folium Lini Linum usitatissmum L., extractive of flax seed derives from dry seed, Semen Lini grinding is shattered 200 orders, the ethanol (both weight ratio 1:1) of the linseed meal and weight portion 50 parts of then getting weight portion 50 parts soaks 48 hours, then mixture is filtered by cotton-wool, finally add and the ethanol leaching dregs equivalent weight, ageing is for subsequent use after 12 hours.
In the present invention, extractive of flax seed main active is secoisolariciresinol diglucoside Flax Lignans.Secoisolariciresinol diglucoside is SDG Secoisolariciresinol Diglycoside.This is the phytoestrogen quite similar with human body estrogen.Secoisolariciresinol diglucoside is mainly present in Semen Lini.Extractive of flax seed effect is in the present invention anti-sebum oxidation, and improves the lipid content of scalp.
In the present invention, Semen Lini tincture accounts for composition weight percentage ratio 0.05% to 5%, is optimized for 0.1% to 2% further.
Scalp tonic active component
According to the physiological characteristics of scalp and with the physiology similarities and differences of skin, to analyze the oils and fats that (1) scalp secretes more, (2) the cuticular moisture of scalp is lower, (3) barrier function of scalp is lower, (4) metabolism of scalp cuticular new city is faster, (5) more easily there are various skin problems etc. and can draw in scalp, the basis of scalp care is scalp horny layer, because the no matter number of scalp fat secretion, cuticular renewal speed, the number of horny layer moisture all be unable to do without the physiological function power of this protective barrier of scalp horny layer, therefore, safeguard the moisture of scalp, strengthening scalp barrier function is one of key of scalp and hair nursing.
Therefore, except containing except each kind of plant tincture in the present invention, also containing having the active component moistening and protect scalp.
Scalp tonic composition in the present invention, is selected from the solute component in vitamins and Natrinema altunense sp (halomonas elongate).Wherein, vitamin comprises a series of different organo-functional group as alcohol, acid, sterin, quinone.Fat dissolubility vitamin and water-soluble vitamin can be classified into.
The fat dissolubility vitamin used in daily chemical products compositions comprises: vitamin A, vitamin D
2, vitamin D
3, vitamin K
1and vitamin E; Water-soluble vitamin comprises: vitamin C, vitamin B
1, vitamin B
2, vitamin B
3, provitamin B
5, vitamin B
6, vitamin B
12deng; Solute in Natrinema altunense sp (halomonas elongate) is tetrahydropyrimidine and its derivant hydroxy tetrahydro pyrimidine.
In the present invention, scalp tonic composition accounts for composition weight percentage ratio 0.21% to 3.3%.Wherein, vitamin E accounts for composition weight percentage ratio 0.005% to 0.5%; Vitamin B
3account for composition weight percentage ratio 0.05% to 5%; Provitamin B
5account for composition weight percentage ratio 0.01% to 2%; Tetrahydropyrimidine accounts for composition weight percentage ratio 0.01% to 2%.
The vitamin E used in the present invention is selected from Vitamin E acetate, linoleic acid ester of vitamin e and vitamin e succinate, and preferred vitamin e acetate (BASF AG's production), the vitamin e acetate used in the present invention is fat dissolubility vitamin, there is good antioxygenic property, to hair growth promoting, hair care, there is clinical effect, contribute to the generation preventing scalp lipid peroxidation, produce helpful to anti-antidandruff; In the present invention, vitamin E accounts for composition weight percentage ratio 0.005% to 0.5%, is optimized for 0.01% to 0.1% further.
Provitamin B in the present invention
5having another name called pantothenylol, is water-soluble vitamin, is vitamin B
5hydrogenation products, provitamin B in skin and hair
5can vitamin B be changed into, be deep into root of hair, control moisture in hair, prevent trichoxerosis, come off, bifurcated, to be entangled with, give hair luster, accelerate hair growth; Provitamin B
5for Roche Holding Ag produces, the specific rotatory power of preferred pantothenylol is+29.0 ° ~+31.5 °, and index of refraction is 1.495 ~ 1.502.Provitamin B in the present invention
5account for composition weight percentage ratio 0.01% to 2%, be optimized for 0.05% to 0.9% further.
Vitamin B in the present invention
3also being vitamin PP, having another name called nicotiamide, niacin amide, is the one of vitamin B group.LONZA company of Switzerland produces, purity > 99%, PH6-7.5 (5% aqueous solution), and outward appearance is white crystalline powder, odorless, bitter in the mouth, in soluble in water, ethanol and glycerol, has faint hygroscopicity.Vitamin B
3there is inflammatory properties but not sterilization idiocratic, vitamin B
3scalp can be nourished, thus the realization contributing to anti-dandruff function can strengthen the effect of skin barrier function, Tanno O, Ota Y, Kitamura N, et al.Br J Dermatol.2000; 143:524-531. and J Cosmet Laser Ther.2006 Jun; 8 (2): 96-101. then report vitamin B respectively
3there is the function strengthening skin barrier and control skin fat secretion. in addition, provitamin B
5there is infiltration and moisture-keeping functions preferably, contribute to the balance safeguarding scalp moisture, thus prevent the generation of the abnormal obscission of scalp.Vitamin B in the present invention
3account for composition weight percentage ratio 0.05% to 5%, be optimized for 0.1% to 2% further.
Solute component in Natrinema altunense sp of the present invention (halomonas elongate) is the derivant hydroxy tetrahydro pyrimidine of tetrahydropyrimidine or tetrahydropyrimidine.The preferred tetrahydropyrimidine of the present invention, tetrahydropyrimidine chemical name is 5-hydroxyl-2 methyl isophthalic acid, 4,5,6-tetrahydropyrimidine 4 formic acid, molecular weight: 158.2g/mol, molecular formula: C
6h
10n
2o
3, white powder.In the present invention, tetrahydropyrimidine accounts for composition weight percentage ratio 0.01% to 2%, and one-step optimization of going forward side by side is 0.05% to 0.3%.
Cosmetics acceptable carrier
Polyhydric alcohol: in the present invention, polyhydric alcohol can be 1,3 butanediols, propylene glycol, glycerol (glycerol), 1,2-pentanediol etc., the present invention preferably 1,3 butanediols, use amount is for accounting for composition weight percentage ratio 15%, and one-step optimization of going forward side by side is for accounting for composition weight percentage ratio 10%.
Thickening agent: in the present invention, operable thickening agent comprises acrylate copolymer, carbomer, hydroxyethyl-cellulose, HANSHENGJIAO etc., the present invention preferentially uses carbomer, comprise carbopol 940, card ripple 934, card ripple 2020 etc., the present invention preferentially uses card ripple 2020,, use amount is for accounting for composition weight percentage ratio 0.05% to 1%, and one-step optimization of going forward side by side is for accounting for composition weight percentage ratio 0.1% to percent 0.6%.
Chelating agen: in the present invention, operable chelating agen comprises disodiumedetate and tetrasodium ethylenediamine tetraacetate, the present invention preferentially uses disodiumedetate, use amount is for accounting for composition weight percentage ratio 0.01% to 0.1%, and one-step optimization of going forward side by side is for accounting for composition weight percentage ratio 0.02% to percent 0.1%.
Antiseptic: in the present invention, operable antiseptic comprises parabens, diazonium alkyl ureas, phenoxyethanol etc., the present invention preferentially uses phenoxyethanol, use amount is for accounting for composition weight percentage ratio 0.1% to 1.0%, and one-step optimization of going forward side by side is for accounting for composition weight percentage ratio 0.5% to percent 0.8%.
Dehydrated alcohol: dehydrated alcohol uses in the present invention as solvent, use amount accounts for composition weight percentage ratio 50% to 95%, is optimized for 62% to 80% further.
PH adjusting agent (nertralizer): in the present invention, pH adjusting agent is triethanolamine conventional with aspect in formula technique, is mainly used in the neutralization of card wave number value.
Scalp care compositions of the present invention can by any known or other be effectively applicable to provide the technology of Haircare composition to prepare, the preparation method preparing scalp care compositions of the present invention comprises conventional preparation and hybrid technology, first carbomer 2020 is disperseed in ethanol, then by disodiumedetate in present component, vitamin B
3, provitamin B
5, vitamin E, tetrahydropyrimidine, 1,3 butanediols, add by respective percentage ratio and sequencing, and stirring and dissolving is until transparent, then quinine tincture is added, soapbark tincture, eucalyptus leaves tincture and Semen Lini tincture, add antiseptic, essence and remaining moisture, stir and dissolve, pH value is adjusted to 6 by the acceptable pH adjusting agent that finally applies some make up (nertralizer).
Using method
Scalp care compositions of the present invention uses after the clean hair of routine, mainly comprises following step:
(A) clean with appropriate shampoo cleans hair;
(B) get this compositions appropriate, be placed on scalp and massage 1 minute by finger belly, or wrap up 5-10 minute with hot towel;
(C) available clear water rinses, and also can rinse and then use other hair care ingredient.
These steps can repeatedly repeatedly, to reach sought nursing effect.
Embodiment
Here is the non-limiting example of scalp care compositions of the present invention.The providing of these embodiments is only used to the object illustrated, can not be interpreted as limitation of the invention, because without departing from the spirit and scope of the present invention, can carry out many changes to the present invention.In these embodiments, unless stated otherwise, all concentration is all percentage by weight.
Embodiment I-V
Embodiment VI-Ⅹ
Efficacy assessments
Efficacy assessments of the present invention is that the technological means adopted based on a kind of scalp care compositions containing plant tincture of the present invention and tincture preparation method is carried out.
Scalp care compositions of the present invention, a kind of compositions containing plant tincture and the scalp tonic factor, by the astriction of plant tincture to scalp, antioxidation and cleaning action realize the adjustment of scalp oils and fats, strengthened the water content of scalp by the scalp tonic factor, and improve scalp microenvironment by the cooperative effect of plant tincture and the scalp tonic factor, therefore, scalp care compositions of the present invention can improve the health status of scalp, and then reaches the object improving hair healthy.Therefore, the present invention passes through to measure scalp moisture levels in efficacy test, and the numerical value of test scalp percutaneous moisture loss TEWL, and the mensuration of scalp oils and fats judges the effect of the present invention to scalp care.
In the present invention, scalp moisture levels and scalp fat content adopt the MPA9 multifunctional testing platform of German CK company, main frame self, containing the connecting hole of an oils and fats test probe and eight skin tests probe, can connect maximum eight identical or different skin test probes.Often kind of probe all has different analysis software and display window.The probe connected comprises: Corneometer CM825 (moisture content test probe), Sebumeter SM815 (oil content test probe), Skin-pH-Meter PH905 (acid-base value test probe), Mexameter MX18 (melanin and haemachrome test probe)--refer to mottle content and scytitis reaction, Tewameter TM300 (water loss test probe TEWL), Reviscometer RVM600 (elastic fibrous tissue's test probe) and Temperature & Rel.Air humidity (environment temperature and humidity test probe).
In the present invention, the percentage ratio that after adopting moisture content test probe Corneometer CM825 test to use the embodiment of the present invention, scalp moisture increases, adopt change and the percentage ratio of oil content test probe Sebumeter SM815 scalp oils and fats, and adopt (water loss test probe Tewameter TM300 test scalp percutaneous water loss value.
Test scalp percutaneous water loss (TEWL) numerical value: TEWL value is larger, the water loss of scalp fast, illustrate that the barrier action of scalp is poorer, otherwise, the TEWL value of test is less, illustrate that scalp keeps the ability of moisture strong, then illustrate that scalp barrier function is strengthened, the present invention tests position: position, the crown; Scalp moisture test position of the present invention: position, the crown; Scalp oils and fats test position of the present invention: overhead.
The present invention's difference testing example the 7th day, the scalp TEWL value of the 28th day; Scalp moisture value added, tests the 7th day and the 28th day scalp moisture value (the 28th day scalp moisture value-7 days scalp moisture value)/the 7th day scalp moisture value * 100%); And the scalp oils and fats reduced value of the 28th day, test scalp oils and fats value and reduced value (the 7th top margin of a page haze wax fat value-28 top margin of a page haze wax fat value)/the 7th day scalp moisture value * 100% of the 7th day and the 28th day).
Choosing has dandruff or head pruritus personage (man, female does not limit), 22 examples, age between 20-40 year, be divided into two groups, often organize efficiently individual quantity 10 people, in use embodiment of the present invention sample, its living habit, the shampoo brand in the past used all does not change.
First group, in 10 people, wherein 5 people use comfort 1, and all the other 5 people use comfort 2, and the using method that using method is drafted with the present invention is as the criterion, and the 7th day respectively, measure the TEWL value (averaging) of scalp when the 28th day
Second group, in 10 people, use the embodiment of the present invention I to Ⅹ respectively, the using method that using method is drafted with the present invention is as the criterion, and the 7th day respectively, measure the TEWL value of scalp when the 28th day, the moisture value of scalp and the fat content of scalp;
Efficacy assessments table 1
TEWL reduces percentage ratio %, moisture increases percentage ratio %, grease reduces percentage ratio %
Show from above result: use the present invention to contrast comfort 1 measurement on request and use the percutaneous water loss numerical value of rear 7th day scalp and use rear 28th day scalp percutaneous water loss numerical value, within the 28th day as a result, scalp percutaneous water loss numerical value reduces 1.9%, illustrate that after using comfort 1, the numerical value of the percutaneous water loss of scalp does not change substantially; The present invention contrasts comfort 2 measurement and uses the percutaneous water loss numerical value of rear 7th day scalp and use rear 28th day scalp percutaneous water loss numerical value, within the 28th day as a result, scalp percutaneous water loss numerical value reduces 2.3%, illustrate that the numerical value of the percutaneous water loss of scalp changes little, be equal to and do not change.
And edition with parallel text inventive embodiments I to Ⅹ, the percutaneous water loss numerical value the 28th day of the scalp recorded all had compared with the 7th day minimizing in various degree (minimum as embodiment 1 have 6.4% minimizing, at most as embodiment VIII has the increase of 34.1%) the use embodiment of the present invention is described after scalp barrier function obtain enhancing.
In the test of moisture value added, placebo 1 and its moisture value added of placebo 2 are respectively 1.2% and 0.8%, compared in the embodiment of the present invention I to Ⅹ as minimum in embodiment 1 6.5% and the numerical value of the highest reduced value 12.8% of embodiment Ⅹ have very large gap, illustrate that the embodiment of the present invention has good scalp moisturization effect.
In the test of scalp oils and fats reduction, placebo 1 and its moisture value added of placebo 2 are respectively 0.2% and-2%, there is very large gap compared to the value added of reduced value 5.4% as minimum in embodiment 1 in the embodiment of the present invention I to Ⅹ and embodiment VII the highest 17.5%, illustrate that the embodiment of the present invention has the regulating action of scalp astriction and scalp oils and fats.
Claims (7)
1. a scalp care compositions, except cosmetics acceptable carrier, its component is:
(1) the Peruvian bark tree tincture of composition weight percentage ratio 0.5% to 15% is accounted for,
(2) the Saponin tincture of composition weight percentage ratio 0.1% to 10% is accounted for,
(3) the Eucalyptus tincture of composition weight percentage ratio 0.1% to 5% is accounted for,
(4) extractive of flax seed of composition weight percentage ratio 0.05% to 5% is accounted for,
(5) ethanol of composition weight percentage ratio 50% to 95% is accounted for,
(6) the scalp tonic active component of composition weight percentage ratio 0.075% to 9.5% is accounted for;
Wherein said scalp tonic active component is:
A () accounts for the vitamin E of composition weight percentage ratio 0.005% to 0.5%,
B () accounts for the vitamin B of composition weight percentage ratio 0.05% to 5%
3,
C () accounts for the provitamin B of composition weight percentage ratio 0.01% to 2%
5
D () accounts for the tetrahydropyrimidine of composition weight percentage ratio 0.01% to 2%.
2. scalp care compositions according to claim 1, its component is:
(1) account for composition weight percentage ratio 1% to 10% Peruvian bark tree tincture,
(2) the Saponin tincture of composition weight percentage ratio 0.5% to 5% is accounted for,
(3) the Eucalyptus tincture of composition weight percentage ratio 0.2% to 2% is accounted for,
(4) extractive of flax seed of composition weight percentage ratio 0.1% to 2% is accounted for,
(5) ethanol of composition weight percentage ratio 62% to 80% is accounted for,
(6) the scalp tonic active component of composition weight percentage ratio 0.21% to 3.3% is accounted for;
Scalp tonic active component is:
A () accounts for the vitamin E of composition weight percentage ratio 0.01% to 0.1%,
B () accounts for the vitamin B of composition weight percentage ratio 0.1% to 2%
3,
C () accounts for the provitamin B of composition weight percentage ratio 0.05% to 0.9%
5,
D () accounts for the tetrahydropyrimidine of composition weight percentage ratio 0.05% to 0.3%.
3. scalp care compositions according to claim 1, also containing 1,3 butanediols accounting for composition weight percentage ratio 10%.
4. scalp care compositions according to claim 1, its pH value range is 5-7.
5. scalp care compositions according to claim 4, its pH value controls 6.
6. the scalp care compositions containing plant tincture, its component and content are:
Account for the Peruvian bark tree tincture of composition weight percentage ratio 1% to 10%,
Account for the Saponin tincture of composition weight percentage ratio 0.5% to 5%,
Account for the Eucalyptus tincture of composition weight percentage ratio 0.2% to 2%,
Account for the extractive of flax seed of composition weight percentage ratio 0.1% to 2%,
Account for the ethanol of composition weight percentage ratio 72% to 90%,
Account for the vitamin E of composition weight percentage ratio 0.01% to 0.1%,
Account for the vitamin B of composition weight percentage ratio 0.1% to 2%
3,
Account for the provitamin B of composition weight percentage ratio 0.05% to 0.9%
5,
Account for the tetrahydropyrimidine of composition weight percentage ratio 0.05% to 0.3%,
Account for 1 of composition weight percentage ratio 10%, 3 butanediols,
Account for the carbomer 2020 of composition weight percentage ratio 0.1 to 0.6%,
Account for the disodiumedetate of composition weight percentage ratio 0.02% to 0.1%,
Appropriate coloring agent, essence, pH adjusting agent, and the deionized water of surplus.
7. scalp care compositions according to claim 1, wherein the preparation method of plant tincture is carried out according to the following steps:
A) preparation of Peruvian bark tree tincture: the ledger bark chopping grinds getting weight portion 25 parts, cross 200 mesh sieves, then the water of weight portion 45 parts is placed in, decocting in water 10 minutes, then cool and add the ethanol of weight portion 30 parts, soak 12 hours, add the dehydrated alcohol of residue dregs equivalent weight after then filtering, ageing obtained Peruvian bark tree tincture after 12 hours;
B) preparation of Quillaia saponaria tincture: china bark is shredded grinds, cross 200 mesh sieves, get soapbark powder weight portion 50 parts, the ethanol being then placed in weight portion 60 parts soaks, and is filtered and the ethanol adding weight portion 40 parts obtains Quillaia saponaria tincture after 12 hours by cotton-wool;
C) Eucalyptus tincture preparation: eucalyptus leaves is placed in weight portion 4 and doubly grinds to the glycerine water solution of eucalyptus leaves own wt, wherein the weight ratio of glycerol and water is 1:1, then the eucalyptus leaves lapping liquid of weight portion 25 parts is got, add the dehydrated alcohol of weight portion 75 parts, soak 12 hours, filtered by cotton-wool by mixture afterwards, finally add and the ethanol leaching dregs equivalent weight, Eucalyptus tincture is made in ageing for 12 hours;
D) Semen Lini tincture preparation: Semen Lini grinding is shattered, cross 200 mesh sieves, then the linseed meal of weight portion 50 parts and the ethanol of weight portion 50 parts is got, both weight ratio 1:1, soak 48 hours, then filtered by cotton-wool by mixture, finally add and the ethanol leaching dregs equivalent weight, ageing is for subsequent use after 12 hours.
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| US10874700B2 (en) | 2016-03-31 | 2020-12-29 | Gojo Industries, Inc. | Sanitizer composition with probiotic/prebiotic active ingredient |
| US11633451B2 (en) | 2016-03-31 | 2023-04-25 | Gojo Industries, Inc. | Antimicrobial peptide stimulating cleansing composition |
| WO2018098143A1 (en) * | 2016-11-23 | 2018-05-31 | Gojo Industries, Inc. | Antimicrobial peptide stimulating sanitizing composition |
| US11564879B2 (en) | 2016-11-23 | 2023-01-31 | Gojo Industries, Inc. | Sanitizer composition with probiotic/prebiotic active ingredient |
| CN108159192A (en) * | 2018-03-06 | 2018-06-15 | 四川农业大学 | Giant panda epidermis expelling parasite spray and preparation method thereof |
| CN108159192B (en) * | 2018-03-06 | 2020-10-27 | 四川农业大学 | Giant panda epidermis insect expelling spray and preparation method thereof |
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