CN110279622B

CN110279622B - Amino acid cleansing foam gel containing bionic petals and preparation method thereof

Info

Publication number: CN110279622B
Application number: CN201910594944.9A
Authority: CN
Inventors: 范国刚; 李雄山
Original assignee: Guangdong Basonnia Biotechnology Co ltd
Current assignee: Guangdong Basonnia Biotechnology Co ltd
Priority date: 2019-07-03
Filing date: 2019-07-03
Publication date: 2022-03-08
Anticipated expiration: 2039-07-03
Also published as: CN110279622A

Abstract

The invention relates to the technical field of skin care products, in particular to amino acid foam cleaning gel containing bionic petals and a preparation method thereof, wherein the amino acid foam cleaning gel containing the bionic petals comprises the following raw materials in parts by weight: 0.01-0.5 part of natural amino acid, 2-6 parts of cocamide MEA, 5-10 parts of auxiliary foaming agent, 10-20 parts of surfactant, 10-15 parts of bionic petals, 10-30 parts of deionized water A20-30 parts of thickening agent, 0.01-1 part of preservative, 4-8 parts of rose essence, 0.01-1 part of chelating agent, 4-8 parts of acrylate cross-linked polymer and 12-16 parts of cocamidopropyl betaine with the mass concentration of 20-30%. The foaming gel is mild and non-irritant, can effectively clean and whiten skin, improves the skin immunocompetence, and can quickly foam a large amount after being applied to the skin; the bionic petals contained in the flower petal imitation flower can quickly improve the moisture of skin when in use, increase the elasticity and luster of the skin, and particularly, various different nutrient petals made by adding different flower extracts to imitate the colors of the artificial flowers are added, so that the defect that the traditional dry petals are not easy to smear is avoided.

Description

Amino acid cleansing foam gel containing bionic petals and preparation method thereof

Technical Field

The invention relates to the technical field of skin care products, in particular to amino acid cleansing foam gel containing bionic petals and a preparation method thereof.

Background

Along with the development of economic life and the improvement of consumption level, people pay more and more attention to their appearance instruments in social life, and people pay more and more attention to skin care, the form of the traditional cosmetics is more and more single, wherein the gel skin care product is a skin care product for cleaning facial dirt and protecting skin, is one of indispensable daily necessities in daily life, and mainly plays a role in cleaning residual substances of skin grease, dirt, aged cuticle, skin care product cosmetics and the like, but the appearance of the traditional petal gel cosmetic is opaque and frosted, has too high viscosity, is jelly-shaped, influences use feeling and foam, has poor cleaning effect, poor foaming effect and single color, cannot meet the requirements of consumers on quality pursuit of appearance, can effectively clean skin, and is mild and not harsh. Therefore, the bionic petal type gel cosmetic obviously different from the traditional form is undoubtedly attractive to consumers.

Disclosure of Invention

In order to overcome the defects and shortcomings in the prior art, the invention aims to provide the amino acid foam cleaning gel containing the bionic petals, which uses alkaline materials, is mild, has no stimulation and side effects, can effectively clean and whiten the skin and improve the skin immunocompetence, and can quickly foam a large amount of skin after being applied to the skin.

The invention also aims to provide a preparation method of the amino acid foaming gel containing the bionic petals, the preparation method is easy to operate, convenient to control and low in production cost, and can be used for large-scale production, and the prepared foaming gel can effectively clean and whiten the skin, improves the skin immunocompetence, and can quickly foam a large amount of skin after being applied to the skin.

The purpose of the invention is realized by the following technical scheme: an amino acid cleansing foam gel containing bionic petals comprises the following raw materials in parts by weight:

the mass concentration of the cocamidopropyl betaine is 20-30%.

The foam cleaning gel is prepared by adopting the raw materials, and the prepared foam cleaning gel can quickly improve the moisture of skin and increase the elasticity and luster of the skin due to the fact that the gel contains the bionic petals, particularly, various different nutrient petals which are prepared by adding different flower extracts to simulate the color of a real flower are added to replace the traditional dry petals, the color is more bright, the defect that the traditional dry petals are not easy to smear is avoided, and the added flower extracts are easier to smear and absorb; the gel uses alkaline materials, is mild, has no stimulation, has no side effect, can effectively clean and whiten skin and improve the skin immunocompetence, and can quickly foam a large amount after being applied to the skin. The adopted natural amino acid is mild and non-irritant in the skin care product, is suitable for various skins, can be used for cleaning the skin more deeply in the cleansing gel, can remove aged cutin, enables skin grease to be balanced and secreted, and has triple effects of cleaning the skin, removing makeup and protecting the skin, and the cleansing gel can be used for cleaning the skin, eliminating the fatigue of the facial skin, supplementing moisture and nutrition to the skin, and enabling the skin to be clean, not tight, white and fine; the coconut oil amide MEA has excellent decontamination, emulsification, foaming, foam stabilization, dispersion and solubilization capacities, and the surfactant system is just assisted in the foaming gel to enhance the decontamination and cleaning effects of the foaming gel; the rose essence moisturizes and nourishes the skin, and is mild and nourishing due to the fact that the rose essence contains rich protein and vitamins, so that the rose essence is beneficial to improving the phenomena of skin darkness and roughness and improving the brightness of the skin; the acrylate cross-linked polymer can keep a dispersion state in a dispersion system to avoid coagulation, and the formed film can also provide water locking work for the foaming gel; the cocamidopropyl betaine belongs to an amphoteric surfactant, has good cleaning, foaming and conditioning effects, is low in irritation, mild in performance and fine and stable in foam when being added into the cleansing foam gel, and can enhance the softness of the skin.

Preferably, each part of the auxiliary foaming agent comprises the following raw materials in parts by weight:

the palmitic acid adopted by the auxiliary foaming agent in the raw materials can soften skin cutin, remove rough and aged surface layers and increase collagen and elastic fiber in dermis; the butane is used as a propellant of the foam cleaning gel due to low evaporation temperature, so that the effective components are smoothly sprayed out, and the butane is used as a coolant to keep the low temperature of cosmetics, but is not a gel drug effect component, is gaseous after the foam cleaning gel is sprayed out, is extremely easy to volatilize and has no damage to the skin; triethanolamine is used as emulsifier, humectant, moisturizer, thickener and pH balancing agent in the cleansing foam gel, and can be neutralized with fatty acid to form soap to enhance the cleansing ability of the gel.

Preferably, each part of the bionic petals comprises the following raw materials in parts by weight:

the conductivity of the deionized water B is less than 0.35 mu S/cm, and the pH value is 6-7; more preferably, the starch is corn starch.

The bionic petal is prepared by the following method:

a1 weighing agar according to weight parts, soaking in 30-50 deg.C warm water for 6-10min, wringing, mixing with fresh flower extract, heating to 90-110 deg.C, and dissolving to obtain mixture A;

a2, weighing starch, hydrogenated castor oil and diazolidinyl urea according to the parts by weight, and uniformly mixing and stirring to obtain a mixture B for later use;

a3, uniformly dispersing the mixture B obtained in the step A2 into the mixture A obtained in the step A1, homogenizing under the condition that the pressure is 1.5-2.0KPa, then continuously heating to 90-100 ℃ to obtain a mixture C, pouring the mixture C into a mold, pressing and cooling to obtain various bionic petals.

The starch adopted by the bionic petals in the raw materials can improve the skin feel of the product, relieve the greasy feel brought by oily cosmetics and provide various petal nutrient substances; and agar can be used as emulsifier, thickening, flavor additive and adhesive in the bionic petals; in addition, the fresh flower extract has the effects of beautifying, removing black spots on skin, enabling the skin to be tender, white and natural, preventing wrinkles, improving physique, enlarging breast and regulating menstruation; hydrogenated castor oil can further increase the solubility of agar and flower extract in deionized water B; the bi-imidazolidinyl urea is a preservative of the product, is mainly used for inhibiting the reproduction of microorganisms, and the branched low-molecular-weight ester can improve the spreadability of the bionic petals and has a smooth aftereffect feeling, so that the thick greasy feeling and the stickiness of the product caused by adding an ultraviolet absorbent and a pigment can be greatly reduced.

The bionic petals are prepared by the method, contain various nutritional ingredients and trace elements, and can quickly improve the moisture of the skin and increase the elasticity and luster of the skin. In the preparation step A1, the heating temperature is strictly controlled to be 90-110 ℃, if the temperature is too high, the flower extract is volatilized, and if the temperature is too low, the flower extract is not favorably and fully diffused into the agar; in the step a3, the homogenizing pressure is strictly controlled to be 1.5-2.0KPa, if the pressure is too high, the mixture B is partially crystallized and solidified, and if the temperature is too low, the effects of fully homogenizing the mixture a and the mixture B and discharging air bubbles cannot be achieved, so that the obtained bionic petals are poor in texture and poor in aesthetic feeling.

Preferably, the thickening agent is a mixture of coconut oil, carbomer 940 and guar gum in a weight ratio of 0.8-1.0:1.0: 1.0-1.2.

The coconut oil plays a role in moisturizing, meanwhile, the coconut oil also has a strong cleaning effect and can clean dirt in the skin, and the organic natural pure fresh coconut oil has no damage to the skin; carbomer 940 can be used as an efficient rheology modifier in the gel, can provide high viscosity under the condition of low dosage, has excellent thickening and suspending properties, and has the functions of moisturizing, refreshing and the like. The skin is more delicate and smooth. Guar gum can reduce the stimulation of washing to the skin, protect keratin from being damaged, smooth the skin, reduce the loss of natural lipid in the skin and increase the softness of the skin.

Preferably, the preservative is a mixture of phenoxyethanol, p-hydroxyben-mate and methylisothiazolinone in a weight ratio of 0.8:1.0: 1.0-1.2.

Preferably, the chelating agent is at least one of EDTA-2Na and citric acid; the surfactant is at least one of polyoxyethylene ether, alkyl alcohol polyether and lauramide.

In the invention, EDTA-2Na can adjust the pH value of the gel, namely the pH value of the gel can be automatically adjusted within a range which can be suitable for people, so as to protect the skin of people from strong stimulation; the citric acid can accelerate the renewal of cutin in the using process of the jelly, and the renewal of the cutin is beneficial to the shedding of melanin in the skin, the shrinking of pores, the dissolution of blackheads and the like. Benign surfactants are characterized by good detergency, milder, low toxicity and irritation to the skin and eyes, and good biodegradability. Several surfactants used in the invention can generate synergistic effect, and play the roles of softening, antistatic, emulsifying, dispersing and sterilizing in the cleansing foam gel.

A preparation method of amino acid cleansing foam gel containing bionic petals comprises the following steps:

1) weighing natural amino acid, rose essence, acrylate cross-linked polymer, cocamidopropyl betaine and deionized water A according to the weight parts, mixing at the speed of 1600-;

2) weighing and mixing the cocamide MEA, the auxiliary foaming agent, the surfactant and the thickening agent according to the weight parts, heating to 80-90 ℃, stirring and homogenizing to obtain a solution D for later use;

3) uniformly adding the solution C obtained in the step 1) into the solution D obtained in the step 2), slowly adding the thickening agent and the preservative, keeping the temperature at 80-90 ℃, and ultrasonically stirring for 10-20min at the frequency of 20000-25000Hz to obtain solution E for later use;

4) cooling the E liquid obtained in the step 3) to 30-50 ℃, adding the bionic petals into the E liquid, uniformly stirring, and keeping the temperature for 40-60h to obtain a gel primary product;

5) sterilizing the gel primary product obtained in the step 4) for 60-80min under the ultraviolet ray with the wavelength of 150-.

The preparation method of the amino acid foam cleaning gel containing the bionic petals is simple in operation steps, convenient to control and high in production efficiency, the synergistic effect among the raw materials can be fully utilized by strictly controlling the adding sequence of the raw materials during preparation, the natural amino acid, rose essence, the acrylate cross-linked polymer and the cocamidopropyl betaine are dissolved in the ionized water A to be fully dissolved with each other, the intersolubility of the four is improved, the activities of the cocamidopropyl betaine, the natural amino acid and the surfactant are activated on the premise that the cocamidopropyl MEA, the auxiliary foaming agent, the surfactant and the thickener are mixed, the bionic petals are added after the reaction of all the raw materials is finished, the integrity and the attractiveness of the bionic petals can be guaranteed, and the pH value of the clean foam gel is adjusted to be closer to the pH value of a human body, is mild and easy to absorb, and utilizes the original fragrance of the bionic petals and the rose essence to mutually promote to play a role in improving the fragrance, thereby improving the fragrance and the stability of the cleansing foam gel.

Wherein, the natural amino acid, the rose essence, the acrylate cross-linked polymer and the cocamidopropyl betaine can be effectively dissolved in the ionized water A for mutual diffusion and dissolution by strictly controlling the stirring speed in the step 1), the stirring speed is not too fast, if the stirring speed is too slow, the diffusion effect among the raw materials is insufficient, if the stirring speed is too slow, the mutual dissolution of the components is insufficient, the solubility is good at the stirring speed of 1600-; and in the step 4), the last addition of the bionic petals is strictly controlled, so that the damage to the structure of the bionic petals caused by high-speed stirring is avoided, meanwhile, the addition of the bionic petals is strictly controlled within the temperature range of 30-50 ℃, if the temperature is too high, the original structure of the bionic petals is partially dissolved and damaged, and if the temperature is too low, the bionic petals are not favorably dissolved in the E liquid to form homogeneous gel.

The invention has the beneficial effects that: the foaming gel disclosed by the invention uses alkaline materials, is mild, has no stimulation, has no side effect, can effectively clean and whiten skin and improve the skin immunocompetence, and can quickly foam a large amount after being applied to the skin. The adopted natural amino acid is mild and non-irritant in the skin care product, and is suitable for various skin types; in addition, the bionic petals can quickly improve the moisture of skin when in use, increase the elasticity and luster of the skin, particularly, various different nutritional petals made by adding different colors of flower extract simulation flowers replace the traditional dry petals, so that the color is more bright, and the defect that the traditional dry petals are not easy to smear is avoided.

The preparation method disclosed by the invention is simple to operate, convenient to control, high in production efficiency and low in production cost, can be used for large-scale production, and the prepared foaming gel is mild, non-irritant, free of side effects, capable of effectively cleaning and whitening skin and improving skin immunocompetence, and can quickly foam a large amount after being used for the skin.

Detailed Description

The present invention will be further described with reference to the following examples for facilitating understanding of those skilled in the art, and the description of the embodiments is not intended to limit the present invention.

Example 1

An amino acid cleansing foam gel containing bionic petals comprises the following raw materials in parts by weight:

the mass concentration of the cocamidopropyl betaine is 20%.

Each part of the auxiliary foaming agent comprises the following raw materials in parts by weight:

each part of the bionic petals comprises the following raw materials in parts by weight:

the conductivity of the deionized water B is less than 0.35 mu S/cm, and the pH value is 6.

The bionic petal is prepared by the following method:

a1 weighing agar according to weight parts, soaking in 30 deg.C warm water for 6min, wringing, mixing with fresh flower extract, heating to 90 deg.C, and dissolving to obtain mixture A;

a3, uniformly dispersing the mixture B obtained in the step A2 into the mixture A obtained in the step A1, homogenizing under the condition that the pressure is 1.5KPa, then continuously heating to 90 ℃ to obtain a mixture C, pouring the mixture C into a mold, and pressing and cooling to obtain various bionic petals.

The thickening agent is a mixture of coconut oil, carbomer 940 and guar gum according to a weight ratio of 0.8:1.0: 1.0.

The preservative is a mixture of phenoxyethanol, p-hydroxy benzoate and methylisothiazolinone in a weight ratio of 0.8:1.0: 1.0.

The chelating agent is EDTA-2 Na; the surfactant is polyoxyethylene ether.

1) weighing natural amino acid, rose essence, acrylate cross-linked polymer, cocamidopropyl betaine and deionized water A according to the weight parts, mixing at a speed of 1600r/min, and stirring for 20min to obtain solution C for later use;

2) weighing and mixing the coconut oil amide MEA, the auxiliary foaming agent, the surfactant and the thickening agent according to the weight parts, heating to 80 ℃, stirring and homogenizing to obtain a solution D for later use;

3) uniformly adding the solution C obtained in the step 1) into the solution D obtained in the step 2), slowly adding the thickening agent and the preservative, keeping the temperature at 80 ℃, and ultrasonically stirring at the frequency of 20000Hz for 10min to obtain a solution E for later use;

4) cooling the E liquid obtained in the step 3) to 30 ℃, adding the bionic petals into the E liquid, uniformly stirring, and preserving heat for 40 hours to obtain a gel primary product;

5) sterilizing the gel primary product obtained in the step 4) for 60min under the ultraviolet ray with the wavelength of 150nm to obtain a gel finished product.

Example 2

the mass concentration of the cocamidopropyl betaine is 23%.

the conductivity of the deionized water B is less than 0.35 mu S/cm, and the pH value is 6.3.

The bionic petal is prepared by the following method:

a1 weighing agar according to weight parts, soaking in 35 deg.C warm water for 7min, wringing, mixing with fresh flower extract, heating to 95 deg.C, and dissolving to obtain mixture A;

a3, uniformly dispersing the mixture B obtained in the step A2 into the mixture A obtained in the step A1, homogenizing under the condition that the pressure is 1.7KPa, then continuously heating to 93 ℃ to obtain a mixture C, pouring the mixture C into a mold, and pressing and cooling to obtain various bionic petals.

The thickening agent is a mixture of coconut oil, carbomer 940 and guar gum according to a weight ratio of 0.85:1.0: 1.05.

The preservative is a mixture of phenoxyethanol, p-hydroxy benzoate and methylisothiazolinone in a weight ratio of 0.8:1.0: 1.05.

The chelating agent is citric acid; the surfactant is alkyl alcohol polyether.

1) weighing natural amino acid, rose essence, acrylate cross-linked polymer, cocamidopropyl betaine and deionized water A according to the weight parts, mixing, and stirring at the speed of 1700r/min for 23min to obtain solution C for later use;

2) weighing and mixing the cocamide MEA, the auxiliary foaming agent, the surfactant and the thickening agent according to the weight parts, heating to 83 ℃, stirring and homogenizing to obtain a solution D for later use;

3) uniformly adding the solution C obtained in the step 1) into the solution D obtained in the step 2), slowly adding the thickening agent and the preservative, keeping the temperature at 83 ℃, and ultrasonically stirring at the frequency of 21750Hz for 13min to obtain a solution E for later use;

4) cooling the E liquid obtained in the step 3) to 35 ℃, adding the bionic petals into the E liquid, uniformly stirring, and keeping the temperature for 45 hours to obtain a gel primary product;

5) sterilizing the gel primary product obtained in the step 4) for 65min under the ultraviolet ray with the wavelength of 160nm to obtain a gel finished product.

Example 3

the mass concentration of the cocamidopropyl betaine is 25%.

the conductivity of the deionized water B is less than 0.35 mu S/cm, and the pH value is 6.5.

The bionic petal is prepared by the following method:

a1 weighing agar according to weight parts, soaking in 40 deg.C warm water for 8min, wringing, mixing with fresh flower extract, heating to 100 deg.C, and dissolving to obtain mixture A;

a3, uniformly dispersing the mixture B obtained in the step A2 into the mixture A obtained in the step A1, homogenizing under the condition that the pressure is 1.8KPa, then continuously heating to 95 ℃ to obtain a mixture C, pouring the mixture C into a mold, and pressing and cooling to obtain various bionic petals.

The thickening agent is a mixture of coconut oil, carbomer 940 and guar gum according to a weight ratio of 0.9:1.0: 1.1.

The preservative is a mixture of phenoxyethanol, p-hydroxy benzoate and methylisothiazolinone in a weight ratio of 0.8:1.0: 1.1.

The chelating agent is a mixture of EDTA-2Na and citric acid according to a mass ratio of 0.8: 1; the surfactant is a mixture of polyoxyethylene ether and alkyl alcohol polyether according to a mass ratio of 0.8:1.

1) weighing natural amino acid, rose essence, acrylate cross-linked polymer, cocamidopropyl betaine and deionized water A according to the weight parts, mixing at the speed of 1800r/min, and stirring for 25min to obtain solution C for later use;

2) weighing and mixing the coconut oil amide MEA, the auxiliary foaming agent, the surfactant and the thickening agent according to the weight parts, heating to 85 ℃, stirring and homogenizing to obtain a solution D for later use;

3) uniformly adding the solution C obtained in the step 1) into the solution D obtained in the step 2), slowly adding the thickening agent and the preservative, keeping the constant temperature at 85 ℃, and ultrasonically stirring at the frequency of 22500Hz for 15min to obtain a solution E for later use;

4) cooling the E liquid obtained in the step 3) to 40 ℃, adding the bionic petals into the E liquid, uniformly stirring, and keeping the temperature for 50h to obtain a gel primary product;

5) sterilizing the gel primary product obtained in the step 4) for 70min under the ultraviolet ray with the wavelength of 180nm to obtain a gel finished product.

Example 4

the mass concentration of the cocamidopropyl betaine is 28%.

the conductivity of the deionized water B is less than 0.35 mu S/cm, and the pH value is 6.8.

The bionic petal is prepared by the following method:

a1 weighing agar according to weight parts, soaking in 45 deg.C warm water for 9min, wringing, mixing with fresh flower extract, heating to 105 deg.C, and dissolving to obtain mixture A;

a3, uniformly dispersing the mixture B obtained in the step A2 into the mixture A obtained in the step A1, homogenizing under the condition that the pressure is 1.9KPa, then continuously heating to 98 ℃ to obtain a mixture C, pouring the mixture C into a mold, and pressing and cooling to obtain various bionic petals.

The thickening agent is a mixture of coconut oil, carbomer 940 and guar gum according to a weight ratio of 0.95:1.0: 1.15.

The preservative is a mixture of phenoxyethanol, p-hydroxy benzoate and methylisothiazolinone in a weight ratio of 0.8:1.0: 1.15.

The chelating agent is a mixture of EDTA-2Na and citric acid according to a mass ratio of 1: 1; the surfactant is a mixture of polyoxyethylene ether and lauramide according to the mass ratio of 0.8:1.

1) weighing natural amino acid, rose essence, acrylate cross-linked polymer, cocamidopropyl betaine and deionized water A according to the weight parts, mixing, and stirring at a speed of 1900r/min for 28min to obtain solution C for later use;

2) weighing and mixing the coconut oil amide MEA, the auxiliary foaming agent, the surfactant and the thickening agent according to the weight parts, heating to 88 ℃, stirring and homogenizing to obtain a solution D for later use;

3) uniformly adding the solution C obtained in the step 1) into the solution D obtained in the step 2), slowly adding the thickening agent and the preservative, keeping the temperature at 88 ℃, and ultrasonically stirring at the frequency of 24050Hz for 18min to obtain a solution E for later use;

4) cooling the E liquid obtained in the step 3) to 45 ℃, adding the bionic petals into the E liquid, uniformly stirring, and keeping the temperature for 55 hours to obtain a gel primary product;

5) sterilizing the gel primary product obtained in the step 4) for 75min under the ultraviolet ray with the wavelength of 190nm to obtain a gel finished product.

Example 5

the mass concentration of the cocamidopropyl betaine is 30%.

the conductivity of the deionized water B is less than 0.35 mu S/cm, and the pH value is 7.

The bionic petal is prepared by the following method:

a1 weighing agar according to weight parts, soaking in warm water at 50 deg.C for 10min, wringing, mixing with fresh flower extract, heating to 110 deg.C, and dissolving to obtain mixture A;

a3, uniformly dispersing the mixture B obtained in the step A2 into the mixture A obtained in the step A1, homogenizing under the condition that the pressure is 2.0KPa, then continuously heating to 100 ℃ to obtain a mixture C, pouring the mixture C into a mold, and pressing and cooling to obtain various bionic petals.

The thickening agent is a mixture of coconut oil, carbomer 940 and guar gum according to a weight ratio of 1.0:1.0: 1.2.

The preservative is a mixture of phenoxyethanol, p-hydroxy benzoate and methylisothiazolinone in a weight ratio of 0.8:1.0: 1.2.

The chelating agent is a mixture of EDTA-2Na and citric acid according to a mass ratio of 1: 1.2; the surfactant is a mixture of alkyl alcohol polyethers and lauramide according to the mass ratio of 0.8:1.

1) weighing natural amino acid, rose essence, acrylate cross-linked polymer, cocamidopropyl betaine and deionized water A according to the weight parts, mixing at the speed of 2000r/min, and stirring for 30min to obtain solution C for later use;

2) weighing and mixing the coconut oil amide MEA, the auxiliary foaming agent, the surfactant and the thickening agent according to the weight parts, heating to 90 ℃, stirring and homogenizing to obtain a solution D for later use;

3) uniformly adding the solution C obtained in the step 1) into the solution D obtained in the step 2), slowly adding the thickening agent and the preservative, keeping the constant temperature at 90 ℃, and ultrasonically stirring at the frequency of 25000Hz for 20min to obtain a solution E for later use;

4) cooling the E liquid obtained in the step 3) to 50 ℃, adding the bionic petals into the E liquid, uniformly stirring, and keeping the temperature for 60 hours to obtain a gel primary product;

5) sterilizing the gel primary product obtained in the step 4) for 80min under the ultraviolet ray with the wavelength of 200nm to obtain a gel finished product.

Comparative example 1

The bionic petal is prepared by the following method:

The chelating agent is EDTA-2 Na; the surfactant is polyoxyethylene ether.

1) weighing natural amino acid, rose essence, acrylate cross-linked polymer and deionized water A according to the weight parts, mixing at a speed of 1600r/min, and stirring for 20min to obtain solution C for later use;

Comparative example 2

the mass concentration of the cocamidopropyl betaine is 25%.

The bionic petal is prepared by the following method:

1) rose essence, acrylate cross-linked polymer, cocamidopropyl betaine and deionized water A are weighed according to the weight parts and mixed at the speed of 1800r/min and stirred for 25min to obtain solution C for later use;

Comparative example 3

the mass concentration of the cocamidopropyl betaine is 30%.

The bionic petal is prepared by the following method:

a1 weighing fresh flower extract according to weight parts, heating to 110 deg.C to dissolve to obtain hot melt A;

5) sterilizing the gel primary product obtained in the step 4) for 80min under the ultraviolet ray with the wavelength of 200nm to obtain a gel finished product

The gel containing the cleansing gels prepared in examples 1 to 5 and containing the cleansing gels prepared in comparative examples 1 to 4 were subjected to foaming time, foaming amount, cleansing effect, wrinkle removing effect and coating skin feel tests, respectively, and the results are shown in table 1 below.

TABLE 1

Item	Time to foam	Amount of foam	Cleaning effect	Wrinkle removing effect	Coating skin feel
						Example 1	Extrusion instant self-foaming	Is very rich	Superior food	Superior food	Superior food
Example 2	Extrusion instant self-foaming	Is very rich	Superior food	Superior food	Superior food
						Example 3	Extrusion instant self-foaming	Is very rich	Superior food	Superior food	Superior food
Example 4	Extrusion instant self-foaming	Is very rich	Superior food	Superior food	Superior food
						Example 5	Extrusion instant self-foaming	Is very rich	Superior food	Superior food	Superior food
Comparative example 1	No bubble after poking	In general	Difference (D)	Good wine	Difference (D)
						Comparative example 2	Extrusion instant self-foaming	In general	Difference (D)	Good wine	Difference (D)
Comparative example 3	Self-foaming retardation of extrusion	In general	Good wine	Difference (D)	Difference (D)

From the above results, it can be seen that the foaming gels of examples 1 to 5 of the present invention all have excellent foaming, cleansing, skin substantivity and wrinkle reducing effects, as well as excellent self-foaming, moisture absorption and moisture retention properties. Among them, the cleansing gel of example 3 is the most excellent in foaming effect, cleansing effect, skin-friendly property and wrinkle-removing effect.

Compared with the example 1, the raw materials of the foaming gel in the comparative example 1 are not added with the cocamidopropyl betaine, the foaming time, the foam quantity, the cleaning effect, the wrinkle removing effect and the coating skin feel test of the foaming gel prepared by using the raw materials are carried out, and the self-foaming effect, the cleaning effect, the skin affinity and the wrinkle removing effect of the foaming gel are relatively reduced through analysis, so that the foaming effect, the cleaning effect, the skin affinity and the wrinkle removing effect of the prepared foaming gel are poor; the coconut oil amido propyl betaine is added into the raw materials, so that the self-foaming effect, the cleaning effect, the skin affinity and the wrinkle removing effect of the prepared foaming gel can be improved, and the foaming gel also has the effects of brightening the skin and moisturizing the skin and brightening the skin color.

Compared with the example 3, the raw material of the foaming gel in the comparative example 2 is not added with natural amino acid, and tests on foaming time, foam quantity, cleaning effect, wrinkle removing effect and coating skin feel of the foaming gel prepared from the raw material of the foaming gel are carried out; the natural amino acid is added into the raw materials, so that the cleaning effect, the skin affinity and the wrinkle removing effect of the prepared foaming gel can be improved, and the foaming gel also has the effects of brightening the skin, moistening the skin and brightening the skin color.

Compared with the example 5, the raw material of the foaming gel in the comparative example 3 is not added with agar, and tests on foaming time, foam quantity, cleaning effect, wrinkle removing effect and coating skin feel of the foaming gel prepared from the raw material of the foaming gel are carried out; the agar is added into the raw materials, so that the skin affinity, the wrinkle removing effect, the self-foaming effect and the cleaning effect of the prepared foaming gel can be improved, and the foaming gel also has the effects of brightening the skin, moistening the skin and brightening the skin color.

The above-described embodiments are preferred implementations of the present invention, and the present invention may be implemented in other ways without departing from the spirit of the present invention.

Claims

1. An amino acid cleansing foam gel containing bionic petals, which is characterized in that: the feed comprises the following raw materials in parts by weight:

0.01-0.5 part of natural amino acid

2-6 parts of cocamide MEA

5-10 parts of auxiliary foaming agent

10-20 parts of surfactant

10-15 parts of bionic petals

20-30 parts of deionized water A

Rose essence 4-8 parts

0.01-1 part of thickening agent

0.01 to 0.5 portion of preservative

0.01-1 part of chelating agent

4-8 parts of acrylate cross-linked polymer

12-16 parts of cocamidopropyl betaine;

the mass concentration of the cocamidopropyl betaine is 20-30%;

1-5 parts of palmitic acid

1-5 parts of butane

4-8 parts of isovaleric acid

5-10 parts of triethanolamine;

5-10 parts of starch

15-20 parts of agar

Fresh flower extract 5-10 parts

10-20 parts of deionized water B

8-12 parts of hydrogenated castor oil

0.01-0.5 part of diazolidinyl urea;

the bionic petal is prepared by the following method:

a1 weighing agar according to weight parts, soaking in warm water, wringing, mixing with fresh flower extract, heating for dissolving to obtain mixture A;

a3, uniformly dispersing the mixture B obtained in the step A2 into the mixture A obtained in the step A1, homogenizing under high pressure, continuously heating to obtain a mixture C, pouring the mixture C into a mold, pressing and cooling to obtain various bionic petals;

the thickening agent is a mixture consisting of coconut oil, carbomer 940 and guar gum according to the weight ratio of 0.8-1.0:1.0: 1.0-1.2;

the surfactant is at least one of polyoxyethylene ether, alkyl alcohol polyether and lauramide;

the amino acid cleansing foam gel containing bionic petals is prepared by the following steps:

1) weighing natural amino acid, rose essence, acrylate cross-linked polymer, cocamidopropyl betaine and deionized water A according to the weight parts, mixing and stirring uniformly to obtain solution C for later use;

2) weighing and mixing the coconut oil amide MEA, the auxiliary foaming agent, the surfactant and the thickening agent according to the weight parts, heating, stirring and homogenizing to obtain a solution D for later use;

3) uniformly adding the solution C obtained in the step 1) into the solution D obtained in the step 2), slowly adding the thickening agent and the preservative, and ultrasonically stirring at constant temperature to obtain a solution E for later use;

4) cooling the E liquid obtained in the step 3), adding the bionic petals into the E liquid, uniformly stirring, and preserving heat to obtain a gel primary product;

5) sterilizing the gel primary product obtained in the step 4) under ultraviolet rays to obtain a gel finished product.

2. The amino acid cleansing foam gel containing bionic petals according to claim 1, which is characterized in that: the temperature of the warm water in the step A1 is 30-50 ℃, the soaking time is 6-10min, and the heating and dissolving temperature is 90-110 ℃; in the step A3, the homogenizing pressure is 1.5-2.0KPa, and the heating temperature is 90-100 ℃.

3. The amino acid cleansing foam gel containing bionic petals according to claim 1, which is characterized in that: the preservative is a mixture of phenoxyethanol, p-hydroxy benzoate and methylisothiazolinone in a weight ratio of 0.8:1.0: 1.0-1.2.

4. The amino acid cleansing foam gel containing bionic petals according to claim 1, which is characterized in that: the chelating agent is at least one of EDTA-2Na and citric acid.

5. The amino acid cleansing foam gel containing bionic petals according to claim 1, which is characterized in that: the stirring speed in the step 1) is 1600-2000r/min, and the stirring time is 20-30 min; heating to 80-90 ℃ in the step 2); in the step 3), the constant temperature is 80-90 ℃, the ultrasonic frequency is 20000-25000Hz, and the ultrasonic time is 10-20 min; cooling to 30-50 ℃ in the step 4), and keeping the temperature for 40-60 h; the wavelength of the ultraviolet rays in the step 5) is 150-200nm, and the sterilization time is 60-80 min.