CN110279622A - A kind of clean bubble gel of the amino acid containing bionical petal and preparation method thereof - Google Patents
A kind of clean bubble gel of the amino acid containing bionical petal and preparation method thereof Download PDFInfo
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
- A61K8/41—Amines
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
- A61K8/42—Amides
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
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- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
- A61K8/44—Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof
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- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/81—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions involving only carbon-to-carbon unsaturated bonds
- A61K8/8141—Compositions of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides or nitriles thereof; Compositions of derivatives of such polymers
- A61K8/8152—Homopolymers or copolymers of esters, e.g. (meth)acrylic acid esters; Compositions of derivatives of such polymers
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9789—Magnoliopsida [dicotyledons]
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/02—Preparations for care of the skin for chemically bleaching or whitening the skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
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- A61Q19/10—Washing or bathing preparations
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Abstract
The present invention relates to skin-protection product technical fields, more particularly to clean bubble gel of a kind of amino acid containing bionical petal and preparation method thereof, the clean bubble gel of amino acid containing bionical petal includes the raw material of following parts by weight: 0.01-0.5 parts of natural amino acid, MEA2-6 parts of coconut oleoyl amine, 5-10 parts of auxiliary blowing agent, 10-20 parts of surfactant, bionical petal 10-15 parts, A20-30 parts of deionized water, 0.01-1 parts of thickener, 0.01-0.5 parts of preservative, 4-8 parts of rose essence, 0.01-1 parts of chelating agent, 4-8 parts of acrylate crosspolymers and mass concentration are 12-16 parts of Cocoamidopropyl betaine of 20%-30%.Clean bubble gel of the invention is mildly non-stimulated, can effectively clean, skin whitening, improve cutaneous immunisation ability, for after skin can rapid, high volume spume；Its bionical petal contained can quickly improve the moisture of musculus cutaneus skin when in use, increase the elasticity and gloss of skin, especially add various Different Nutrition petals made of the color of different fresh flower extract mould artificial flowers, avoid traditional dry petal and be not easy the shortcomings that smearing.
Description
Technical field
The present invention relates to skin-protection product technical fields, and in particular to a kind of clean bubble gel of the amino acid containing bionical petal and
Preparation method.
Background technique
With the development of economic life and the raising of the level of consumption, people increasingly focus on oneself in social life
Appearance instrument, people also increasingly pay attention to the maintenance of skin, and traditional cosmetics form seems more and more single, wherein gel
Class skin care item are a kind of skin care item for cleaning face's dirt, protecting skin, are indispensable daily necessities in our daily lifes
One of, the effect of the residuals of cleaning skin grease, dirt, aging cutin layer, skin care item cosmetics etc. is primarily served, however
Traditional petal class gel cosmetic appearance is in zone of opacity frosted shape, and viscosity is excessively high, will affect use feeling again in g., jelly-like
And foam, in addition cleaning effect, foaming effect are poor, color is single, are unable to satisfy the same of quality pursuit of the consumer for appearance
When can effective cleaning skin, mild inirritative demand.Thus invent a kind of bionical petal class for being clearly distinguishable from traditional form
Gel cosmetics undoubtedly can have great attraction to consumer.
Summary of the invention
In order to overcome shortcoming and defect existing in the prior art, the purpose of the present invention is to provide one kind to contain bionic flower
The clean bubble gel of the amino acid of valve, which uses the material of meta-alkalescence, mild non-stimulated, without side-effects, while can be effectively clean
Skin, whitening, improve cutaneous immunisation ability, and for after skin, can rapid, high volume spume.
Another object of the present invention is to provide a kind of preparation methods of the clean bubble gel of amino acid containing bionical petal, should
Preparation method is easily operated, easy to control, and production cost is low, can be used for being mass produced, and clean bubble gel obtained can be effectively clean
Net skin, whitening, improve cutaneous immunisation ability, and for after skin, can rapid, high volume spume.
The purpose of the invention is achieved by the following technical solution: a kind of clean bubble gel of the amino acid containing bionical petal, packet
Include the raw material of following parts by weight:
The mass concentration of the Cocoamidopropyl betaine is 20%-30%.
Clean bubble gel of the invention is made by using above-mentioned raw materials, and clean bubble gel obtained containing bionical petal due to existing
The moisture that musculus cutaneus skin can be quickly improved when use, increases the elasticity and gloss of skin, especially adds different fresh flower extract moulds
Various Different Nutrition petals made of the color of artificial flowers substitute traditional dry petal, and color is more bright-coloured, while avoiding tradition
Dry petal disadvantage not easy to apply, and added fresh flower extract is easier to smear and absorb；The gel uses meta-alkalescence
Material, it is mild non-stimulated, it is without side-effects, at the same can effectively clean skin, whitening, improve cutaneous immunisation ability, and be used for skin
After skin, can rapid, high volume spume.And wherein the natural amino acid used used does not stimulate mildly in skin care item, is suitble to each
Kind skin quality can remove the cutin of aging in this clean bubble gel with the cleaning skin of deeper, make skin oil and fat balance point
It secretes, also there is cleaning skin, the triple function of skin is protected in makeup removing, is gone back while wash clean skin using this clean bubble gel
The fatigue that skin of face can be eliminated, keeps the skin wet and nutrition to skin, keeps skin completely not tight, pale exquisiteness；Cocounut oil acyl
Amine MEA has excellent decontamination, emulsification, foaming, foam stabilizing, dispersion, solubilising power, and just auxiliary surface is living in this clean bubble gel
Property agent system enhancing this it is clean bubble gel decontamination cleaning effect；Rose essence moisturizing and nourishing skin, because it contains protein abundant
And vitamin, it is mild to nourish, help to improve that skin is dim mute and coarse phenomenon, promotes skin brilliant white degree；It is acrylate cross linked poly-
Closing object can keep dispersing morphology to avoid condensing in dispersion, and the film of formation can also provide water lock function to clean bubble gel；Coconut palm
Oleamide propyl betaine belongs to amphoteric surfactant, has good cleaning, blistering, opsonic action, this clean bubble Gel is added
Curry irritation is small, performance is mild, and foam is fine and smooth and stablizes, and can enhance the flexibility to skin.
Preferably, every part of auxiliary blowing agent includes the raw material of following parts by weight:
The palmitinic acid that auxiliary blowing agent described in raw material of the present invention uses can be with softening skin cutin, removal coarse aging
Surface layer increases the collagen and elastomer of intradermal；And promotion of the butane since evaporating temperature is low, for this clean bubble gel
Agent sprays effective component smoothly, while doing coolant, keeps cosmetics low temperature, but it is not gel effective component, and at this
Clean bubble gel is all gaseous after gushing out, and highly volatile is to skin zero damage；Triethanolamine is in this clean bubble gel
As emulsifier, moisturizer, humidizer, thickener, pH poising agent, soap can be neutralized into fatty acid enhances the cleaning energy of this gel
Power.
Preferably, every part of bionical petal includes the raw material of following parts by weight:
The conductivity of the deionized water B is less than 0.35 μ S/cm, pH value 6-7；The more preferably described starch is corn
Starch.
The bionical petal comprises the following steps:
It is to impregnate 6-10min in 30-50 DEG C of warm water that A1 weighs agar to place it in temperature according to parts by weight, after wringing out with
It is 90-110 DEG C of dissolution that fresh flower extract, which is mixed and heated to temperature, obtains mixture A, spare；
A2 weighs starch, rilanit special and bi-imidazolidinyl urea according to parts by weight and is mixed evenly, and obtains mixture
B, it is spare；
A3 evenly spreads to mixture B obtained in step A2 in the mixture A that step A1 is obtained, and is 1.5- in pressure
Homogeneous under conditions of 2.0KPa continues to be heated to 90-100 DEG C later, obtains mixture C, and mixture C is poured into pressing mold in mold
Diversiform bionical petal is obtained after cooling.
The starch that bionical petal uses described in raw material of the present invention can improve product skin sense, mitigate oil-based cosmetic preparation and bring
Greasy feeling, and provide various petal nutriments；And agar can be used as emulsifier, thickening, perfume (or spice) in the bionical petal
Feed additives and adhesive；In addition fresh flower extract has effects that skin maintenance and cosmetic benefits, applies the blackspot that can remove on skin, enables skin
Tender white nature, anti-wrinkle, while there are also improve constitution, chest enlarge menstruation regulating；Rilanit special can further increase agar, fresh flower
Dissolubility of the extract in deionized water B；Bi-imidazolidinyl urea is the preservative of this product, is mainly used for inhibiting microorganism
Breeding, this branched chain low molecular weight ester can be improved the coatability of bionical petal and have a kind of smooth aftereffect to feel, can be with
Greatly reduce product because of thick and heavy greasy feeling and viscosity caused by adding ultraviolet absorbing agent and pigment.
Bionical petal of the present invention by using the above method be made, obtained bionical petal contain a variety of nutrition at
Point and microelement, can quickly improve the moisture of skin, increase elasticity of skin and gloss.And it strictly to be controlled in preparation step A1
Heating temperature processed is 90-110 DEG C, causes fresh flower extract to volatilize if temperature is excessively high, if the too low fresh flower that is unfavorable for of temperature mentions
Object is taken sufficiently to be diffused into agar；It is 1.5-2.0KPa that strict control homogenization pressure is wanted in step A3, can if hypertonia
Lead to mixture part B crystallisation solidification, being unable to reach if temperature is too low makes mixture A and the abundant homogeneous of mixture B and discharge
The effect of bubble, and then bionical petal quality difference obtained is caused to lack aesthetic feeling.
Preferably, the thickener be by coconut oil, card wave 940 and guar gum according to weight ratio be 0.8-1.0:1.0:
1.0-1.2 the mixture of composition.
Heretofore described coconut oil plays the role of moisturizing, while coconut oil also has the cleaning effect of relatively strength, can
Dirt in cleaning skin, and organic natural pure fresh coconut oil, it is not damaged to skin；Card wave 940 can be used as high in this gel
The rheology modifier of effect is capable of providing high viscosity in low dosage, has excellent thickening and suspendability, in addition also
There are the functions such as moisturizing, moisturizing, skin toner.Make the finer and smoother lubrication of skin.And guar gum can reduce the stimulation washed to skin, protection
Keratin is injury-free, keeps skin smooth, reduces the loss of natural lipid in skin, increases the pliability of skin.
Preferably, the preservative be by phenoxetol, to this formic acid esters of hydroxyl and methylisothiazolinone according to weight
Amount is than the mixture for 0.8:1.0:1.0-1.2 composition.
Preferably, the chelating agent is at least one of EDTA-2Na and citric acid；The surfactant is polyoxy second
At least one of alkene ethers, alkylol polyethers and lauramide.
EDTA-2Na is adjustable the pH value in gel in the present invention, that is, can automatically adjust the acid-base property of gel at me
In the range that can be suitble to, to protect our skin not by strong stimulation；And citric acid can add in this gel use process
Fast cutin updates, and the update of cutin facilitates falling off for the middle melanin of skin, and the receipts of pore are thin, the dissolution etc. of blackhead.It is benign
The characteristics of surfactant is that have good scourability, and compare mild, hypotoxicity and the low stimulation to skin, eyes
Property and good biological degradability.Several surfactants used in the present invention can generate synergy and answer, in this clean bubble
Play soft, antistatic, emulsification, dispersion and sterilization in gel.
A kind of preparation method of the clean bubble gel of the amino acid containing bionical petal, includes the following steps:
1) natural amino acid, rose essence, acrylate crosspolymers, cocamidopropyl propyl amide sweet tea are weighed according to parts by weight
Dish alkali and deionized water A mixing obtain C liquid with the 1600-2000r/min rate equal 20-30min of stirring, spare；
2) coconut oleoyl amine MEA, auxiliary blowing agent, surfactant, thickener are weighed according to parts by weight to mix, is warming up to
80-90 DEG C of stirring homogeneous, obtains D liquid, spare；
3) C liquid obtained in step 1) is uniformly added into step 2) in gained D liquid, then by the thickener and anti-corrosion
Agent is slowly added to, and constant temperature is kept for 80-90 DEG C, is stirred 10-20min with the frequency ultrasound of 20000-25000Hz, is obtained E liquid, standby
With；
4) it is cooled to 30-50 DEG C to E liquid obtained in step 3), E liquid is added in the bionical petal and is stirred evenly, and is protected
Warm 40-60h obtains gel first product；
5) the gel first product that step 4) obtains is subjected to sterilization 60-80min in the case where wavelength is the ultraviolet light of 150-200nm,
Obtain gel finished product.
A kind of preparation step of the clean bubble gel of amino acid containing bionical petal of the present invention is grasped as described above, adopting this with method
It is simple to make step, easy to control, high production efficiency, the sequence that when preparation is added by strict control raw material can make full use of original
Synergistic effect between material, first by natural amino acid, rose essence, acrylate crosspolymers, cocamidopropyl propyl amide beet
Alkali is dissolved in ionized water A, makes four to be sufficiently mutually dissolved, the intersolubility of raising, and further by coconut oleoyl amine MEA,
Cocamidopropyl propyl amide beet, natural amino acid, surface are activated under the premise of auxiliary blowing agent, surfactant, thickener mixing
The activity of activating agent three, all raw materials add after reaction bionical petal can guarantee bionical petal integrality and
Aesthetics finally adjusts the pH value of clean bubble gel closer to human body acid-base, mild easily absorption, and utilizes bionical petal and rose
The original fragrance of essence combines, and mutually promotes and plays the role of Titian, improves the fragrance and stability of clean bubble gel.
Wherein, step 1), can be effectively by natural amino acid, rose essence, acrylate by strict control stirring rate
Cross-linked polymer, Cocoamidopropyl betaine, which are dissolved in be diffused in ionized water A, to dissolve each other, and stirring rate be not easy it is too fast,
The diffusion that will lead between each raw material if crossing is insufficient, if dissolving each other for the excessively slow each ingredient of stirring rate is insufficient,
Solubility under the stirring rate of 1600-2000r/min is good, can promote and the mutual solubility of unclassified stores；And it is tight in step 4)
Lattice control biomimetics petal is eventually adding the structure for avoiding due to high-speed stirred and destroying bionical petal, while wanting strict control imitative
Raw petal will be added in 30-50 DEG C of temperature range, and it is original to will lead to the bionical broken meeting of petal sections dissolution if temperature is excessively high
Structure is unfavorable for bionical petal if temperature is too low and is dissolved in formation homogeneous gel in E liquid.
The beneficial effects of the present invention are: clean bubble gel of the invention uses the material of meta-alkalescence, mild non-stimulated, no pair
Effect, at the same can effectively clean skin, whitening, improve cutaneous immunisation ability, and for after skin, can rapid, high volume blistering
Foam.And wherein the natural amino acid used used does not stimulate mildly in skin care item, is suitble to various skin quality；Additionally, due to containing
Bionical petal can quickly improve the moisture of musculus cutaneus skin when in use, increase the elasticity and gloss of skin, and especially addition is different fresh
Various Different Nutrition petals made of the color of flower extract mould artificial flowers substitute traditional dry petal, and color is more bright-coloured, simultaneously
It avoids traditional dry petal and is not easy the shortcomings that smearing.
Preparation method of the invention is easy to operate, easy to control, and high production efficiency, production cost is low, can be used for extensive
Production, clean bubble gel obtained is mildly non-stimulated, without side-effects, at the same can effectively clean skin, whitening, raising cutaneous immunisation energy
Power, and for after skin, can rapid, high volume spume.
Specific embodiment
For the ease of the understanding of those skilled in the art, below with reference to embodiment, the present invention is further illustrated, real
The content that the mode of applying refers to not is limitation of the invention.
Embodiment 1
A kind of clean bubble gel of the amino acid containing bionical petal, the raw material including following parts by weight:
The mass concentration of the Cocoamidopropyl betaine is 20%.
Every part of auxiliary blowing agent includes the raw material of following parts by weight:
Every part of bionical petal includes the raw material of following parts by weight:
The conductivity of the deionized water B is less than 0.35 μ S/cm, pH value 6.
The bionical petal comprises the following steps:
A1 weighs agar and place it in the warm water that temperature is 30 DEG C according to parts by weight impregnates 6min, mentions after wringing out with fresh flower
Taking object to be mixed and heated to temperature is 90 DEG C of dissolutions, obtains mixture A, spare；
A2 weighs starch, rilanit special and bi-imidazolidinyl urea according to parts by weight and is mixed evenly, and obtains mixture
B, it is spare；
A3 evenly spreads to mixture B obtained in step A2 in the mixture A that step A1 is obtained, and is in pressure
Homogeneous under conditions of 1.5KPa continues to be heated to 90 DEG C later, obtains mixture C, and it is cooling that mixture C is poured into pressing mold in mold
After obtain diversiform bionical petal.
The mixing that the thickener is made of coconut oil, card wave 940 and guar gum according to weight ratio for 0.8:1.0:1.0
Object.
The preservative is to be according to weight ratio by phenoxetol, to this formic acid esters of hydroxyl and methylisothiazolinone
The mixture of 0.8:1.0:1.0 composition.
The chelating agent is EDTA-2Na；The surfactant is polyethenoxy ether class.
A kind of preparation method of the clean bubble gel of the amino acid containing bionical petal, includes the following steps:
1) natural amino acid, rose essence, acrylate crosspolymers, cocamidopropyl propyl amide sweet tea are weighed according to parts by weight
Dish alkali and deionized water A mixing obtain C liquid with the 1600r/min rate equal 20min of stirring, spare；
2) coconut oleoyl amine MEA, auxiliary blowing agent, surfactant, thickener are weighed according to parts by weight to mix, is warming up to 80
DEG C stirring homogeneous, obtain D liquid, it is spare；
3) C liquid obtained in step 1) is uniformly added into step 2) in gained D liquid, then by the thickener and anti-corrosion
Agent is slowly added to, and constant temperature is kept for 80 DEG C, is stirred 10min with the frequency ultrasound of 20000Hz, is obtained E liquid, spare；
4) 30 DEG C are cooled to E liquid obtained in step 3), E liquid is added in the bionical petal and is stirred evenly, and is kept the temperature
40h obtains gel first product；
5) the gel first product that step 4) obtains is subjected to sterilization 60min in the case where wavelength is the ultraviolet light of 150nm, obtains gel
Finished product.
Embodiment 2
A kind of clean bubble gel of the amino acid containing bionical petal, the raw material including following parts by weight:
The mass concentration of the Cocoamidopropyl betaine is 23%.
Every part of auxiliary blowing agent includes the raw material of following parts by weight:
Every part of bionical petal includes the raw material of following parts by weight:
The conductivity of the deionized water B is less than 0.35 μ S/cm, pH value 6.3.
The bionical petal comprises the following steps:
A1 weighs agar and place it in the warm water that temperature is 35 DEG C according to parts by weight impregnates 7min, mentions after wringing out with fresh flower
Taking object to be mixed and heated to temperature is 95 DEG C of dissolutions, obtains mixture A, spare；
A2 weighs starch, rilanit special and bi-imidazolidinyl urea according to parts by weight and is mixed evenly, and obtains mixture
B, it is spare；
A3 evenly spreads to mixture B obtained in step A2 in the mixture A that step A1 is obtained, and is in pressure
Homogeneous under conditions of 1.7KPa continues to be heated to 93 DEG C later, obtains mixture C, and it is cooling that mixture C is poured into pressing mold in mold
After obtain diversiform bionical petal.
The thickener is made of coconut oil, card wave 940 and guar gum according to weight ratio for 0.85:1.0:1.05 mixed
Close object.
The preservative is to be according to weight ratio by phenoxetol, to this formic acid esters of hydroxyl and methylisothiazolinone
The mixture of 0.8:1.0:1.05 composition.
The chelating agent is citric acid；The surfactant is alkylol polyethers.
A kind of preparation method of the clean bubble gel of the amino acid containing bionical petal, includes the following steps:
1) natural amino acid, rose essence, acrylate crosspolymers, cocamidopropyl propyl amide sweet tea are weighed according to parts by weight
Dish alkali and deionized water A mixing obtain C liquid with the 1700r/min rate equal 23min of stirring, spare；
2) coconut oleoyl amine MEA, auxiliary blowing agent, surfactant, thickener are weighed according to parts by weight to mix, is warming up to 83
DEG C stirring homogeneous, obtain D liquid, it is spare；
3) C liquid obtained in step 1) is uniformly added into step 2) in gained D liquid, then by the thickener and anti-corrosion
Agent is slowly added to, and constant temperature is kept for 83 DEG C, is stirred 13min with the frequency ultrasound of 21750Hz, is obtained E liquid, spare；
4) 35 DEG C are cooled to E liquid obtained in step 3), E liquid is added in the bionical petal and is stirred evenly, and is kept the temperature
45h obtains gel first product；
5) the gel first product that step 4) obtains is subjected to sterilization 65min in the case where wavelength is the ultraviolet light of 160nm, obtains gel
Finished product.
Embodiment 3
A kind of clean bubble gel of the amino acid containing bionical petal, the raw material including following parts by weight:
The mass concentration of the Cocoamidopropyl betaine is 25%.
Every part of auxiliary blowing agent includes the raw material of following parts by weight:
Every part of bionical petal includes the raw material of following parts by weight:
The conductivity of the deionized water B is less than 0.35 μ S/cm, pH value 6.5.
The bionical petal comprises the following steps:
A1 weighs agar and place it in the warm water that temperature is 40 DEG C according to parts by weight impregnates 8min, mentions after wringing out with fresh flower
Taking object to be mixed and heated to temperature is 100 DEG C of dissolutions, obtains mixture A, spare；
A2 weighs starch, rilanit special and bi-imidazolidinyl urea according to parts by weight and is mixed evenly, and obtains mixture
B, it is spare；
A3 evenly spreads to mixture B obtained in step A2 in the mixture A that step A1 is obtained, and is in pressure
Homogeneous under conditions of 1.8KPa continues to be heated to 95 DEG C later, obtains mixture C, and it is cooling that mixture C is poured into pressing mold in mold
After obtain diversiform bionical petal.
The mixing that the thickener is made of coconut oil, card wave 940 and guar gum according to weight ratio for 0.9:1.0:1.1
Object.
The preservative is to be according to weight ratio by phenoxetol, to this formic acid esters of hydroxyl and methylisothiazolinone
The mixture of 0.8:1.0:1.1 composition.
The chelating agent is EDTA-2Na and citric acid is according to the mixture that mass ratio is that 0.8:1 is formed；The surface is living
Property agent to be polyethenoxy ether class and alkylol polyethers according to mass ratio be 0.8:1 composition mixture.
A kind of preparation method of the clean bubble gel of the amino acid containing bionical petal, includes the following steps:
1) natural amino acid, rose essence, acrylate crosspolymers, cocamidopropyl propyl amide sweet tea are weighed according to parts by weight
Dish alkali and deionized water A mixing obtain C liquid with the 1800r/min rate equal 25min of stirring, spare；
2) coconut oleoyl amine MEA, auxiliary blowing agent, surfactant, thickener are weighed according to parts by weight to mix, is warming up to 85
DEG C stirring homogeneous, obtain D liquid, it is spare；
3) C liquid obtained in step 1) is uniformly added into step 2) in gained D liquid, then by the thickener and anti-corrosion
Agent is slowly added to, and constant temperature is kept for 85 DEG C, is stirred 15min with the frequency ultrasound of 22500Hz, is obtained E liquid, spare；
4) 40 DEG C are cooled to E liquid obtained in step 3), E liquid is added in the bionical petal and is stirred evenly, and is kept the temperature
50h obtains gel first product；
5) the gel first product that step 4) obtains is subjected to sterilization 70min in the case where wavelength is the ultraviolet light of 180nm, obtains gel
Finished product.
Embodiment 4
A kind of clean bubble gel of the amino acid containing bionical petal, the raw material including following parts by weight:
The mass concentration of the Cocoamidopropyl betaine is 28%.
Every part of auxiliary blowing agent includes the raw material of following parts by weight:
Every part of bionical petal includes the raw material of following parts by weight:
The conductivity of the deionized water B is less than 0.35 μ S/cm, pH value 6.8.
The bionical petal comprises the following steps:
A1 weighs agar and place it in the warm water that temperature is 45 DEG C according to parts by weight impregnates 9min, mentions after wringing out with fresh flower
Taking object to be mixed and heated to temperature is 105 DEG C of dissolutions, obtains mixture A, spare；
A2 weighs starch, rilanit special and bi-imidazolidinyl urea according to parts by weight and is mixed evenly, and obtains mixture
B, it is spare；
A3 evenly spreads to mixture B obtained in step A2 in the mixture A that step A1 is obtained, and is in pressure
Homogeneous under conditions of 1.9KPa continues to be heated to 98 DEG C later, obtains mixture C, and it is cooling that mixture C is poured into pressing mold in mold
After obtain diversiform bionical petal.
The thickener is made of coconut oil, card wave 940 and guar gum according to weight ratio for 0.95:1.0:1.15 mixed
Close object.
The preservative is to be according to weight ratio by phenoxetol, to this formic acid esters of hydroxyl and methylisothiazolinone
The mixture of 0.8:1.0:1.15 composition.
The chelating agent is EDTA-2Na and citric acid is according to the mixture that mass ratio is that 1:1 is formed；The surface-active
Agent is polyethenoxy ether class and lauramide according to the mixture that mass ratio is that 0.8:1 is formed.
A kind of preparation method of the clean bubble gel of the amino acid containing bionical petal, includes the following steps:
1) natural amino acid, rose essence, acrylate crosspolymers, cocamidopropyl propyl amide sweet tea are weighed according to parts by weight
Dish alkali and deionized water A mixing obtain C liquid with the 1900r/min rate equal 28min of stirring, spare；
2) coconut oleoyl amine MEA, auxiliary blowing agent, surfactant, thickener are weighed according to parts by weight to mix, is warming up to 88
DEG C stirring homogeneous, obtain D liquid, it is spare；
3) C liquid obtained in step 1) is uniformly added into step 2) in gained D liquid, then by the thickener and anti-corrosion
Agent is slowly added to, and constant temperature is kept for 88 DEG C, is stirred 18min with the frequency ultrasound of 24050Hz, is obtained E liquid, spare；
4) 45 DEG C are cooled to E liquid obtained in step 3), E liquid is added in the bionical petal and is stirred evenly, and is kept the temperature
55h obtains gel first product；
5) the gel first product that step 4) obtains is subjected to sterilization 75min in the case where wavelength is the ultraviolet light of 190nm, obtains gel
Finished product.
Embodiment 5
A kind of clean bubble gel of the amino acid containing bionical petal, the raw material including following parts by weight:
The mass concentration of the Cocoamidopropyl betaine is 30%.
Every part of auxiliary blowing agent includes the raw material of following parts by weight:
Every part of bionical petal includes the raw material of following parts by weight:
The conductivity of the deionized water B is less than 0.35 μ S/cm, pH value 7.
The bionical petal comprises the following steps:
A1 weighs agar and place it in the warm water that temperature is 50 DEG C according to parts by weight impregnates 10min, wrings out rear and fresh flower
It is 110 DEG C of dissolutions that extract, which is mixed and heated to temperature, obtains mixture A, spare；
A2 weighs starch, rilanit special and bi-imidazolidinyl urea according to parts by weight and is mixed evenly, and obtains mixture
B, it is spare；
A3 evenly spreads to mixture B obtained in step A2 in the mixture A that step A1 is obtained, and is in pressure
Homogeneous under conditions of 2.0KPa continues to be heated to 100 DEG C later, obtains mixture C, and it is cold that mixture C is poured into pressing mold in mold
But diversiform bionical petal is obtained afterwards.
The mixing that the thickener is made of coconut oil, card wave 940 and guar gum according to weight ratio for 1.0:1.0:1.2
Object.
The preservative is to be according to weight ratio by phenoxetol, to this formic acid esters of hydroxyl and methylisothiazolinone
The mixture of 0.8:1.0:1.2 composition.
The chelating agent is EDTA-2Na and citric acid is according to the mixture that mass ratio is that 1:1.2 is formed；The surface is living
Property agent to be alkylol polyethers and lauramide according to mass ratio be 0.8:1 composition mixture.
A kind of preparation method of the clean bubble gel of the amino acid containing bionical petal, includes the following steps:
1) natural amino acid, rose essence, acrylate crosspolymers, cocamidopropyl propyl amide sweet tea are weighed according to parts by weight
Dish alkali and deionized water A mixing obtain C liquid with the 2000r/min rate equal 30min of stirring, spare；
2) coconut oleoyl amine MEA, auxiliary blowing agent, surfactant, thickener are weighed according to parts by weight to mix, is warming up to 90
DEG C stirring homogeneous, obtain D liquid, it is spare；
3) C liquid obtained in step 1) is uniformly added into step 2) in gained D liquid, then by the thickener and anti-corrosion
Agent is slowly added to, and constant temperature is kept for 90 DEG C, is stirred 20min with the frequency ultrasound of 25000Hz, is obtained E liquid, spare；
4) 50 DEG C are cooled to E liquid obtained in step 3), E liquid is added in the bionical petal and is stirred evenly, and is kept the temperature
60h obtains gel first product；
5) the gel first product that step 4) obtains is subjected to sterilization 80min in the case where wavelength is the ultraviolet light of 200nm, obtains gel
Finished product.
Comparative example 1
A kind of clean bubble gel of the amino acid containing bionical petal, the raw material including following parts by weight:
Every part of auxiliary blowing agent includes the raw material of following parts by weight:
Every part of bionical petal includes the raw material of following parts by weight:
The conductivity of the deionized water B is less than 0.35 μ S/cm, pH value 6.
The bionical petal comprises the following steps:
A1 weighs agar and place it in the warm water that temperature is 30 DEG C according to parts by weight impregnates 6min, mentions after wringing out with fresh flower
Taking object to be mixed and heated to temperature is 90 DEG C of dissolutions, obtains mixture A, spare；
A2 weighs starch, rilanit special and bi-imidazolidinyl urea according to parts by weight and is mixed evenly, and obtains mixture
B, it is spare；
A3 evenly spreads to mixture B obtained in step A2 in the mixture A that step A1 is obtained, and is in pressure
Homogeneous under conditions of 1.5KPa continues to be heated to 90 DEG C later, obtains mixture C, and it is cooling that mixture C is poured into pressing mold in mold
After obtain diversiform bionical petal.
The mixing that the thickener is made of coconut oil, card wave 940 and guar gum according to weight ratio for 0.8:1.0:1.0
Object.
The preservative is to be according to weight ratio by phenoxetol, to this formic acid esters of hydroxyl and methylisothiazolinone
The mixture of 0.8:1.0:1.0 composition.
The chelating agent is EDTA-2Na；The surfactant is polyethenoxy ether class.
A kind of preparation method of the clean bubble gel of the amino acid containing bionical petal, includes the following steps:
1) natural amino acid, rose essence, acrylate crosspolymers and deionized water A is weighed according to parts by weight to mix
It closes and equal 20min is stirred with 1600r/min rate, obtain C liquid, it is spare；
2) coconut oleoyl amine MEA, auxiliary blowing agent, surfactant, thickener are weighed according to parts by weight to mix, is warming up to 80
DEG C stirring homogeneous, obtain D liquid, it is spare；
3) C liquid obtained in step 1) is uniformly added into step 2) in gained D liquid, then by the thickener and anti-corrosion
Agent is slowly added to, and constant temperature is kept for 80 DEG C, is stirred 10min with the frequency ultrasound of 20000Hz, is obtained E liquid, spare；
4) 30 DEG C are cooled to E liquid obtained in step 3), E liquid is added in the bionical petal and is stirred evenly, and is kept the temperature
40h obtains gel first product；
5) the gel first product that step 4) obtains is subjected to sterilization 60min in the case where wavelength is the ultraviolet light of 150nm, obtains gel
Finished product.
Comparative example 2
A kind of clean bubble gel of the amino acid containing bionical petal, the raw material including following parts by weight:
The mass concentration of the Cocoamidopropyl betaine is 25%.
Every part of auxiliary blowing agent includes the raw material of following parts by weight:
Every part of bionical petal includes the raw material of following parts by weight:
The conductivity of the deionized water B is less than 0.35 μ S/cm, pH value 6.5.
The bionical petal comprises the following steps:
A1 weighs agar and place it in the warm water that temperature is 40 DEG C according to parts by weight impregnates 8min, mentions after wringing out with fresh flower
Taking object to be mixed and heated to temperature is 100 DEG C of dissolutions, obtains mixture A, spare；
A2 weighs starch, rilanit special and bi-imidazolidinyl urea according to parts by weight and is mixed evenly, and obtains mixture
B, it is spare；
A3 evenly spreads to mixture B obtained in step A2 in the mixture A that step A1 is obtained, and is in pressure
Homogeneous under conditions of 1.8KPa continues to be heated to 95 DEG C later, obtains mixture C, and it is cooling that mixture C is poured into pressing mold in mold
After obtain diversiform bionical petal.
The mixing that the thickener is made of coconut oil, card wave 940 and guar gum according to weight ratio for 0.9:1.0:1.1
Object.
The preservative is to be according to weight ratio by phenoxetol, to this formic acid esters of hydroxyl and methylisothiazolinone
The mixture of 0.8:1.0:1.1 composition.
The chelating agent is EDTA-2Na and citric acid is according to the mixture that mass ratio is that 0.8:1 is formed；The surface is living
Property agent to be polyethenoxy ether class and alkylol polyethers according to mass ratio be 0.8:1 composition mixture.
A kind of preparation method of the clean bubble gel of the amino acid containing bionical petal, includes the following steps:
1) according to parts by weight weigh rose essence, acrylate crosspolymers, Cocoamidopropyl betaine and go from
Sub- water A mixing stirs equal 25min with 1800r/min rate, obtains C liquid, spare；
2) coconut oleoyl amine MEA, auxiliary blowing agent, surfactant, thickener are weighed according to parts by weight to mix, is warming up to 85
DEG C stirring homogeneous, obtain D liquid, it is spare；
3) C liquid obtained in step 1) is uniformly added into step 2) in gained D liquid, then by the thickener and anti-corrosion
Agent is slowly added to, and constant temperature is kept for 85 DEG C, is stirred 15min with the frequency ultrasound of 22500Hz, is obtained E liquid, spare；
4) 40 DEG C are cooled to E liquid obtained in step 3), E liquid is added in the bionical petal and is stirred evenly, and is kept the temperature
50h obtains gel first product；
5) the gel first product that step 4) obtains is subjected to sterilization 70min in the case where wavelength is the ultraviolet light of 180nm, obtains gel
Finished product.
Comparative example 3
A kind of clean bubble gel of the amino acid containing bionical petal, the raw material including following parts by weight:
The mass concentration of the Cocoamidopropyl betaine is 30%.
Every part of auxiliary blowing agent includes the raw material of following parts by weight:
Every part of bionical petal includes the raw material of following parts by weight:
The conductivity of the deionized water B is less than 0.35 μ S/cm, pH value 7.
The bionical petal comprises the following steps:
It is 110 DEG C of dissolutions that A1 weighs fresh flower extract to be heated to temperature according to parts by weight, obtains hot melt liquid A, spare；
A2 weighs starch, rilanit special and bi-imidazolidinyl urea according to parts by weight and is mixed evenly, and obtains mixture
B, it is spare；
A3 evenly spreads to mixture B obtained in step A2 in the mixture A that step A1 is obtained, and is in pressure
Homogeneous under conditions of 2.0KPa continues to be heated to 100 DEG C later, obtains mixture C, and it is cold that mixture C is poured into pressing mold in mold
But diversiform bionical petal is obtained afterwards.
The mixing that the thickener is made of coconut oil, card wave 940 and guar gum according to weight ratio for 1.0:1.0:1.2
Object.
The preservative is to be according to weight ratio by phenoxetol, to this formic acid esters of hydroxyl and methylisothiazolinone
The mixture of 0.8:1.0:1.2 composition.
The chelating agent is EDTA-2Na and citric acid is according to the mixture that mass ratio is that 1:1.2 is formed；The surface is living
Property agent to be alkylol polyethers and lauramide according to mass ratio be 0.8:1 composition mixture.
A kind of preparation method of the clean bubble gel of the amino acid containing bionical petal, includes the following steps:
1) natural amino acid, rose essence, acrylate crosspolymers, cocamidopropyl propyl amide sweet tea are weighed according to parts by weight
Dish alkali and deionized water A mixing obtain C liquid with the 2000r/min rate equal 30min of stirring, spare；
2) coconut oleoyl amine MEA, auxiliary blowing agent, surfactant, thickener are weighed according to parts by weight to mix, is warming up to 90
DEG C stirring homogeneous, obtain D liquid, it is spare；
3) C liquid obtained in step 1) is uniformly added into step 2) in gained D liquid, then by the thickener and anti-corrosion
Agent is slowly added to, and constant temperature is kept for 90 DEG C, is stirred 20min with the frequency ultrasound of 25000Hz, is obtained E liquid, spare；
4) 50 DEG C are cooled to E liquid obtained in step 3), E liquid is added in the bionical petal and is stirred evenly, and is kept the temperature
60h obtains gel first product；
5) the gel first product that step 4) obtains is subjected to sterilization 80min in the case where wavelength is the ultraviolet light of 200nm, obtains gel
Finished product
When respectively will be obtained containing specific embodiment 1-5 and being blistered containing clean bubble gel made from comparative example 1-4
Between, foam volume, cleaning effect, go wrinkle effect and be coated with skin sensing examination, as a result as shown in table 1 below.
Table 1
| Project | Cream time | Foam volume | Cleaning effect | Go wrinkle effect | It is coated with skin sense |
| Embodiment 1 | Moment is squeezed out from foaming | It is very rich | It is excellent | It is excellent | It is excellent |
| Embodiment 2 | Moment is squeezed out from foaming | It is very rich | It is excellent | It is excellent | It is excellent |
| Embodiment 3 | Moment is squeezed out from foaming | It is very rich | It is excellent | It is excellent | It is excellent |
| Embodiment 4 | Moment is squeezed out from foaming | It is very rich | It is excellent | It is excellent | It is excellent |
| Embodiment 5 | Moment is squeezed out from foaming | It is very rich | It is excellent | It is excellent | It is excellent |
| Comparative example 1 | It is not blistering not rub stamp | Generally | Difference | It is good | Difference |
| Comparative example 2 | Moment is squeezed out from foaming | Generally | Difference | It is good | Difference |
| Comparative example 3 | It is slow from foaming to squeeze out | Generally | It is good | Difference | Difference |
From the above results, the clean bubble gel in 1-5 of the embodiment of the present invention all has good foaming effect, cleaning effect
Fruit, skin compatibility and wrinkle effect is gone, while had well from foaming effect, hygroscopicity and moisture retention.Wherein, embodiment 3
In the bubble effect of clean bubble gel, cleaning effect, skin compatibility and go wrinkle effect best.
Compared with Example 1, without addition Cocoamidopropyl betaine in the raw material of the clean bubble gel of comparative example 1, to benefit
With its raw material be made clean bubble gel carry out cream time, foam volume, cleaning effect, go wrinkle effect and be coated with skin sensing examination, analysis
It was found that this clean bubble gel from foaming effect, cleaning effect, skin compatibility and remove wrinkle effect relative reduction, make clean bubble obtained
The foaming effect of gel, cleaning effect, skin compatibility and go wrinkle effect poor；Illustrate that coconut oleoyl amine is added in raw material in the present invention
Propyl betaine can improve be made it is clean bubble gel from foaming effect, cleaning effect, skin compatibility and go wrinkle effect, simultaneously also
With moistening skin lightening water, the effect of bright color.
Compared with Example 3, natural amino acid is not added in the raw material of the clean bubble gel of comparative example 2, to its raw material of utilization
Clean bubble gel is made to carry out cream time, foam volume, cleaning effect, go wrinkle effect and be coated with skin sensing examination, analysis finds that this is clean
The cleaning effect and skin compatibility for steeping gel reduce significantly, remove wrinkle effect relative drop, make the cleaning of clean bubble gel obtained
Effect, skin compatibility and go wrinkle effect it is poor；Illustrate that the present invention can be improved in raw material addition natural amino acid and clean bubble Gel is made
The cleaning effect of curry, skin compatibility and wrinkle effect is gone, while also having moistens skin lightening water, the effect of bright color.
Compared with Example 5, it is made clean to using its raw material without addition agar in the raw material of the clean bubble gel of comparative example 3
Bubble gel carries out cream time, foam volume, cleaning effect, goes wrinkle effect and be coated with skin sensing examination, and analysis finds this clean bubble gel
Skin compatibility, go wrinkle effect to reduce significant, cleaning effect relative drop, make the foaming effect, clear of clean bubble gel obtained
Clean effect, skin compatibility and go wrinkle effect it is poor；Illustrate that the present invention can be improved in raw material addition agar and clean bubble gel is made
Skin compatibility goes wrinkle effect, from foaming effect and cleaning effect, while also having moistens skin lightening water, bright color
Effect.
Above-described embodiment is the preferable implementation of the present invention, and in addition to this, the present invention can be realized with other way,
Do not depart under the premise of present inventive concept it is any obviously replace it is within the scope of the present invention.
Claims (10)
1. a kind of clean bubble gel of the amino acid containing bionical petal, it is characterised in that: the raw material including following parts by weight:
The mass concentration of the Cocoamidopropyl betaine is 20%-30%.
2. the clean bubble gel of a kind of amino acid containing bionical petal according to claim 1, it is characterised in that: described in every part
Auxiliary blowing agent includes the raw material of following parts by weight:
3. the clean bubble gel of a kind of amino acid containing bionical petal according to claim 1, it is characterised in that: described in every part
Bionical petal includes the raw material of following parts by weight:
4. the clean bubble gel of a kind of amino acid containing bionical petal according to claim 3, it is characterised in that: described bionical
Petal comprises the following steps:
A1 weighs agar and place it in warm water according to parts by weight to be impregnated, and is dissolved, is obtained with fresh flower extract Hybrid Heating after wringing out
It is spare to mixture A；
A2 weighs starch, rilanit special and bi-imidazolidinyl urea according to parts by weight and is mixed evenly, and obtains mixture B, standby
With；
A3 evenly spreads to mixture B obtained in step A2 in the mixture A that step A1 is obtained, under the conditions of high pressure
Matter continues to heat later, obtains mixture C, and mixture C is poured into mold after pressing mold is cooling and obtains diversiform bionic flower
Valve.
5. the clean bubble gel of a kind of amino acid containing bionical petal according to claim 4, it is characterised in that: in step A1
The temperature of the warm water is 30-50 DEG C, soaking time 6-10min, and dissolving by heating temperature is 90-110 DEG C；Described in step A3
Homogenization pressure is 1.5-2.0KPa, and heating temperature is 90-100 DEG C.
6. the clean bubble gel of a kind of amino acid containing bionical petal according to claim 1, it is characterised in that: the thickening
The mixture that agent is made of coconut oil, card wave 940 and guar gum according to weight ratio for 0.8-1.0:1.0:1.0-1.2.
7. the clean bubble gel of a kind of amino acid containing bionical petal according to claim 1, it is characterised in that: the anti-corrosion
Agent is by phenoxetol, according to weight ratio is 0.8:1.0:1.0-1.2 group to this formic acid esters of hydroxyl and methylisothiazolinone
At mixture.
8. the clean bubble gel of a kind of amino acid containing bionical petal according to claim 1, it is characterised in that: the chelating
Agent is at least one of EDTA-2Na and citric acid；The surfactant be polyethenoxy ether class, alkylol polyethers and
At least one of lauramide.
9. a kind of preparation method of the clean bubble gel of the amino acid containing bionical petal as described in claim 1, it is characterised in that:
Include the following steps:
1) natural amino acid, rose essence, acrylate crosspolymers, Cocoamidopropyl betaine are weighed according to parts by weight
It is mixed with deionized water A, obtains C liquid, it is spare；
2) it weighs coconut oleoyl amine MEA, auxiliary blowing agent, surfactant, thickener according to parts by weight to mix, heating stirring is equal
Matter obtains D liquid, spare；
3) C liquid obtained in step 1) is uniformly added into step 2) in gained D liquid, then the thickener and preservative is delayed
Slow to be added, thermostatic ultrasonic stirring obtains E liquid, spare；
4) cooling of E liquid obtained in step 3) is given, E liquid is added in the bionical petal and is stirred evenly, and is kept the temperature, at the beginning of obtaining gel
Product；
5) the gel first product that step 4) obtains is sterilized under ultraviolet light, obtains gel finished product.
10. a kind of preparation method of the clean bubble gel of amino acid containing bionical petal according to claim 9, feature exist
In: the stirring rate in the step 1) is 1600-2000r/min, mixing time 20-30min；It is warming up in step 2)
80-90℃；In step 3), the thermostat temperature is 80-90 DEG C, supersonic frequency 20000-25000Hz, ultrasonic time 10-
20min；30-50 DEG C is cooled in step 4), soaking time 40-60h；The wavelength of ultraviolet light described in step 5) is 150-
200nm, sterilizing time 60-80min.
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| US20060014662A1 (en) * | 2004-07-14 | 2006-01-19 | Beiersdorf Ag | Cleansing gel |
| KR100659512B1 (en) * | 2005-12-06 | 2006-12-20 | (주)테라이엔씨 | Cosmetic composition for face washing |
| CN101411679A (en) * | 2007-09-20 | 2009-04-22 | 吴志刚 | Chemical article containing petal composition and preparation method thereof |
| KR20090126030A (en) * | 2008-06-03 | 2009-12-08 | 주식회사 엘지생활건강 | High viscosity transparent gel-type cleansing foam cosmetic composition |
| CN106361596A (en) * | 2016-08-31 | 2017-02-01 | 广州欧慕生物科技有限公司 | Amino acid foaming cleansing gel and preparation method thereof |
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2019
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| US20060014662A1 (en) * | 2004-07-14 | 2006-01-19 | Beiersdorf Ag | Cleansing gel |
| KR100659512B1 (en) * | 2005-12-06 | 2006-12-20 | (주)테라이엔씨 | Cosmetic composition for face washing |
| CN101411679A (en) * | 2007-09-20 | 2009-04-22 | 吴志刚 | Chemical article containing petal composition and preparation method thereof |
| KR20090126030A (en) * | 2008-06-03 | 2009-12-08 | 주식회사 엘지생활건강 | High viscosity transparent gel-type cleansing foam cosmetic composition |
| CN106361596A (en) * | 2016-08-31 | 2017-02-01 | 广州欧慕生物科技有限公司 | Amino acid foaming cleansing gel and preparation method thereof |
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| CN114392204A (en) * | 2021-12-24 | 2022-04-26 | 广州那比昂生物科技有限公司 | Skin cleaning composition and preparation method and application thereof |
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