CN110200877A - A kind of Chinese medicine shampoo and preparation method thereof - Google Patents
A kind of Chinese medicine shampoo and preparation method thereof Download PDFInfo
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9789—Magnoliopsida [dicotyledons]
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/002—Preparations for repairing the hair, e.g. hair cure
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/02—Preparations for cleaning the hair
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/12—Preparations containing hair conditioners
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/70—Biological properties of the composition as a whole
- A61K2800/72—Hypo-allergenic
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Abstract
The present invention relates to daily cosmetics technical field, a kind of Chinese medicine shampoo and preparation method thereof is disclosed.Should be the preparation method comprises the following steps: (1) mix folium artemisiae argyi, Chinese prickly ash with water, distillating extracting oil obtains the extraction raffinate and the dregs of a decoction that volatile oil is spare, after collection is distilled respectively until volatile oil is not further added by；(2) it by leaf of elm tree, Fructus Liquidambaris, tribulus terrestris, Radix Astragali, Caulis Spatholobi and the above dregs of a decoction, is filtered after being decocted with water, obtains filtrate；(3) raffinate will be extracted and filtrate merges, and be condensed into clear cream；(4) sodium sulfate of polyethenoxy ether of fatty alcohol and coconut oil diethanol amide heating melted, stirred evenly, after volatile oil and clear cream is added, heating stirring adds essence, glycerol, softening agent, glycine betaine, pearlite slurry and ethylparaben, stirs evenly up to the Chinese medicine shampoo.Shampoo of the invention can effectively black hair, hair care, hair care, strengthen the hair, while there is sterilizing and itch-relieving, relieving mental strain and helping sleep, tonifying Qi and blood and other effects.
Description
Technical field
The present invention relates to daily cosmetics technical fields, and in particular to a kind of Chinese medicine shampoo and preparation method thereof.
Background technique
The a part of hair as body, plays an important role in our daily life.Hair has directly scalp
Protective effect is connect, external force to scalp can work as a buffer, and protect head.Chinese medicine thinks hair is the sign of blood condition, kidney storing essence, China
It is sending out, the growth of hair relies on the full of essence and blood, and dense glossy hair represents health.With people's rhythm of life accelerate,
The problems such as life stress increases, it is irregular to work and rest, insomnia takes place frequently and city environmental pollution is serious, leads to various hair diseases
Or damage, such as hair easily dirty, scalp pruritus, dandruff, alopecia, this can bring puzzlement, therefore select correctly hair washing
Water nurse to hair particularly important.
The anti-dandruff and itching-relieving ingredient in most of shampoos is mostly artificial compound currently on the market, has toxicity and there is peace
Full hidden danger, long-time service is larger to the damage of scalp, and certain pollution is caused to environment.With people's consumption concept and health
The raising of consciousness, the hair washing product containing natural plants or traditional Chinese medicine ingredients are concerned by people.
Summary of the invention
In view of the deficiencies of the prior art, the present invention intends to provide a kind of Chinese medicine shampoo and its preparation side
Method, can effectively hair care hair care, sterilizing and itch-relieving, and can calm the nerves, invigorating the spleen, tonifying Qi, promoting blood circulation.
To achieve the goals above, first aspect present invention provides a kind of Chinese medicine shampoo, including following raw material components, with
Mass parts are calculated as: 10-100 parts of leaf of elm tree, 10-50 parts of Chinese prickly ash, 10-100 parts of Fructus Liquidambaris, 5-100 parts of folium artemisiae argyi, tribulus terrestris 10-100
Part, 10-100 parts of Radix Astragali, 10-100 parts of Caulis Spatholobi, 1-10 parts of essence, 2-10 parts of glycerol, coconut oil diethanol amide 20-200
Part, 3-50 parts of softening agent, 3-100 parts of glycine betaine, 0.1-10 parts of pearlite slurry, 1-20 parts of sodium sulfate of polyethenoxy ether of fatty alcohol, Buddhist nun
Moor golden 0.1-5 parts of ethyl ester.
Preferably, the Chinese medicine shampoo includes following raw material components, is calculated as with mass parts: 10-30 parts of leaf of elm tree, Chinese prickly ash
10-20 parts, 10-20 parts of Fructus Liquidambaris, 5-15 parts of folium artemisiae argyi, 10-20 parts of tribulus terrestris, 10-20 parts of Radix Astragali, 10-20 parts of Caulis Spatholobi, essence
1.5-3 parts, 2.5-5 parts of glycerol, 35-70 parts of coconut oil diethanol amide, 4-12 parts of softening agent, 5-10 parts of glycine betaine, pearlite slurry
0.8-3 parts, 2.5-5 parts of sodium sulfate of polyethenoxy ether of fatty alcohol, 0.1-0.3 parts of ethylparaben.
Preferably, the essence is jasmine flower essence, carnation essence, orchid compound, Mint Essence, flavoring rose essence, smokes
One of clothing hay-scented essence, violet compound, milk flavour, fruity essence, sweet basil essence and green tea essence are a variety of, described
Softening agent is one of dimethyl silicone polymer, silicone emulsion, diethanol distearyl acid and triethanolamine or a variety of.
Second aspect of the present invention provides a kind of preparation method of Chinese medicine shampoo, comprising the following steps:
(1) folium artemisiae argyi, Chinese prickly ash are mixed with water, distillating extracting oil is volatilized until volatile oil is not further added by
Oil is spare, collects extraction raffinate and the dregs of a decoction after distillation respectively；
(2) dregs of a decoction for obtaining leaf of elm tree, Fructus Liquidambaris, tribulus terrestris, Radix Astragali and Caulis Spatholobi and step (1), after being decocted with water
Filtering, obtains filtrate；
(3) the extraction raffinate that step (1) obtains and the filtrate that step (2) obtains are merged, is condensed into clear cream；
(4) sodium sulfate of polyethenoxy ether of fatty alcohol and coconut oil diethanol amide heating melted, stirred evenly, step is added
Suddenly after the clear cream that the volatile oil and step (3) that (1) obtains obtain, heating stirring adds essence, glycerol, softening agent, beet
Alkali, pearlite slurry and ethylparaben stir evenly up to the Chinese medicine shampoo；
Wherein, the dosage of the above raw material is calculated as with mass parts: 10-100 parts of leaf of elm tree, 10-50 parts of Chinese prickly ash, Fructus Liquidambaris 10-
100 parts, 5-100 parts of folium artemisiae argyi, 10-100 parts of tribulus terrestris, 10-100 parts of Radix Astragali, 10-100 parts of Caulis Spatholobi, 1-10 parts of essence, glycerol
2-10 parts, 20-200 parts of coconut oil diethanol amide, 3-50 parts of softening agent, 3-100 parts of glycine betaine, 0.1-10 parts of pearlite slurry, rouge
1-20 parts of fat alcohol polyethenoxy ether sodium sulfate, 0.1-5 parts of ethylparaben.
Preferably, the essence is jasmine flower essence, carnation essence, orchid compound, Mint Essence, flavoring rose essence, smokes
One of clothing hay-scented essence, violet compound, milk flavour, fruity essence, sweet basil essence and green tea essence are a variety of, described
Softening agent is one of dimethyl silicone polymer, silicone emulsion, diethanol distearyl acid and triethanolamine or a variety of.
Preferably, the mass ratio of the gross mass and water of folium artemisiae argyi and Chinese prickly ash is 1:5-10 in step (1).
Preferably, in step (2), the process decocted with water includes being decocted 2-3 times with water, is carried out after decocting every time
Filter, merging filtrate；Wherein, in each decoction process, the gross mass of each raw material and the mass ratio of water be 1:5-10, time 1-
2h。
Preferably, the density at 50 DEG C of clear cream described in step (3) is 1.1-1.4g/cm3。
Preferably, step (4) further includes molten in sodium sulfate of polyethenoxy ether of fatty alcohol and coconut oil diethanol amide heating
Change, after mixing evenly, be cooled to room temperature, pH adjusting agent is added, adjusts pH to 5-6；It is obtained in step (4) in addition step (1)
Volatile oil and the obtained clear cream of step (3) after, the temperature of heating stirring is 50-70 DEG C, time 0.5-2h.
Third aspect present invention provides Chinese medicine shampoo prepared by the above method.
Through the above technical solutions, the invention has the benefit that
1, the present invention has effects that tranquilizing the mind, invigorating the spleen, also contains antibacterial and whitening composition using leaf of elm tree as primary raw material,
And it is nonirritant.Chinese prickly ash, Fructus Liquidambaris, folium artemisiae argyi, tribulus terrestris sterilizing and itch-relieving, Radix Astragali invigorating qi for strengthening superficies, Caulis Spatholobi blood circulation promoting and enriching, Quan Fangwu
Hair, hair care, hair care, strengthen the hair, and there is sterilizing and itch-relieving, relieving mental strain and helping sleep, tonifying Qi and blood and other effects.
2, Chinese medicine shampoo safety and environmental protection of the invention, mild nonirritant, will not generate damage to hair or scalp, no
Pollute environment.
Specific embodiment
The endpoint of disclosed range and any value are not limited to the accurate range or value herein, these ranges or
Value should be understood as comprising the value close to these ranges or value.For numberical range, between the endpoint value of each range, respectively
It can be combined with each other between the endpoint value of a range and individual point value, and individually between point value and obtain one or more
New numberical range, these numberical ranges should be considered as specific open herein.
In a first aspect, the present invention provides a kind of Chinese medicine shampoo, including following raw material components, it is calculated as with mass parts: elm
10-100 parts of leaf, 10-50 parts of Chinese prickly ash, 10-100 parts of Fructus Liquidambaris, 5-100 parts of folium artemisiae argyi, 10-100 parts of tribulus terrestris, Radix Astragali 10-100
Part, 10-100 parts of Caulis Spatholobi, 1-10 parts of essence, 2-10 parts of glycerol, 20-200 parts of coconut oil diethanol amide, softening agent 3-50
Part, 3-100 parts of glycine betaine, 0.1-10 parts of pearlite slurry, 1-20 parts of sodium sulfate of polyethenoxy ether of fatty alcohol, ethylparaben 0.1-5
Part.
The effect of Chinese medicine shampoo each component of the invention, is as follows:
Leaf of elm tree: elm leaf extract has antibacterial and whitening function, and property is mild, nonirritant.
Chinese prickly ash: warm in pain, desinsection is antipruritic, increases microcirculation.
Fructus Liquidambaris: dispelling wind and removing obstruction in the meridians.
Folium artemisiae argyi: removing dampness to stop itchin, it is anti-dandruff.
Tribulus terrestris: high concentration activation is all had to the activity of external melanocyte and tyrosinase, low concentration inhibits
Dual regulation can activate tyrosinase activity by activation melanocyte, to promote the generation of hair melanin, from
And the effect of reaching black hair.
Radix Astragali: invigorating qi for strengthening superficies, containing there are many saponin(e, polysaccharide, flavones, amino acid, glycine betaine, folic acid, alkaloid and human bodies
Required microelement, nutrition, the prevention and treatment alopecia, trichogenous effect that there is expansion blood vessel, improve skin.
Caulis Spatholobi: blood circulation promoting and enriching, relaxing tendons and activating collaterals, nutrition hair, prevention and treatment alopecia.
Preferably, the Chinese medicine shampoo includes following raw material components, is calculated as with mass parts: 10-30 parts of leaf of elm tree, Chinese prickly ash
10-20 parts, 10-20 parts of Fructus Liquidambaris, 5-15 parts of folium artemisiae argyi, 10-20 parts of tribulus terrestris, 10-20 parts of Radix Astragali, 10-20 parts of Caulis Spatholobi, essence
1.5-3 parts, 2.5-5 parts of glycerol, 35-70 parts of coconut oil diethanol amide, 4-12 parts of softening agent, 5-10 parts of glycine betaine, pearlite slurry
0.8-3 parts, 2.5-5 parts of sodium sulfate of polyethenoxy ether of fatty alcohol, 0.1-0.3 parts of ethylparaben.
Preferably, the essence is jasmine flower essence, carnation essence, orchid compound, Mint Essence, flavoring rose essence, smokes
One of clothing hay-scented essence, violet compound, milk flavour, fruity essence, sweet basil essence and green tea essence are a variety of, described
Softening agent is one of dimethyl silicone polymer, silicone emulsion, diethanol distearyl acid and triethanolamine or a variety of.
Second aspect, the present invention provide a kind of preparation method of Chinese medicine shampoo, comprising the following steps:
(1) folium artemisiae argyi, Chinese prickly ash are mixed with water, distillating extracting oil is volatilized until volatile oil is not further added by
Oil is spare, collects extraction raffinate and the dregs of a decoction after distillation respectively；
(2) dregs of a decoction for obtaining leaf of elm tree, Fructus Liquidambaris, tribulus terrestris, Radix Astragali and Caulis Spatholobi and step (1), after being decocted with water
Filtering, obtains filtrate；
(3) the extraction raffinate that step (1) obtains and the filtrate that step (2) obtains are merged, is condensed into clear cream；
(4) sodium sulfate of polyethenoxy ether of fatty alcohol and coconut oil diethanol amide heating melted, stirred evenly, step is added
Suddenly after the clear cream that the volatile oil and step (3) that (1) obtains obtain, heating stirring adds essence, glycerol, softening agent, beet
Alkali, pearlite slurry and ethylparaben stir evenly up to the Chinese medicine shampoo；
Wherein, the dosage of the above raw material is calculated as with mass parts: 10-100 parts of leaf of elm tree, 10-50 parts of Chinese prickly ash, Fructus Liquidambaris 10-
100 parts, 5-100 parts of folium artemisiae argyi, 10-100 parts of tribulus terrestris, 10-100 parts of Radix Astragali, 10-100 parts of Caulis Spatholobi, 1-10 parts of essence, glycerol
2-10 parts, 20-200 parts of coconut oil diethanol amide, 3-50 parts of softening agent, 3-100 parts of glycine betaine, 0.1-10 parts of pearlite slurry, rouge
1-20 parts of fat alcohol polyethenoxy ether sodium sulfate, 0.1-5 parts of ethylparaben.
Preferably, the essence is jasmine flower essence, carnation essence, orchid compound, Mint Essence, flavoring rose essence, smokes
One of clothing hay-scented essence, violet compound, milk flavour, fruity essence, sweet basil essence and green tea essence are a variety of, described
Softening agent is one of dimethyl silicone polymer, silicone emulsion, diethanol distearyl acid and triethanolamine or a variety of.
Preferably, the mass ratio of the gross mass and water of folium artemisiae argyi and Chinese prickly ash is 1:5-10 in step (1).
Preferably, in step (2), the process decocted with water includes being decocted 2-3 times with water, is carried out after decocting every time
Filter, merging filtrate；Wherein, in each decoction process, the gross mass of each raw material and the mass ratio of water be 1:5-10, time 1-
2h。
In the present invention, the concentration of step (3) can be carried out using concentration tank or a kind of equipment of any other concentration.It is excellent
Selection of land, the density at 50 DEG C of clear cream described in step (3) is 1.1-1.4g/cm3。
Preferably, step (4) further includes molten in sodium sulfate of polyethenoxy ether of fatty alcohol and coconut oil diethanol amide heating
Change, after mixing evenly, be cooled to room temperature, pH adjusting agent is added, adjusts pH to 5-6；It is obtained in step (4) in addition step (1)
Volatile oil and the obtained clear cream of step (3) after, the temperature of heating stirring is 50-70 DEG C, time 0.5-2h.PH in the present invention
Regulator can select any one to adjust the reagent of pH, it is preferable that pH adjusting agent is citric acid.The temperature of heating stirring is specific
Can arbitrary value between 50 DEG C, 55 DEG C, 60 DEG C, 65 DEG C, 70 DEG C or above-mentioned two value, the time can for 0.5h, 1h,
Arbitrary value between 1.5h, 2h or above-mentioned two value.
The third aspect, the present invention provide Chinese medicine shampoo prepared by the above method.
The present invention will be described in detail by way of examples below.In following embodiment, Kunming system (KM) mouse is purchased from
Hunan SJA Laboratory Animal Co. , Ltd, leaf of elm tree are purchased from Hui nationality's medicinal material market, remaining raw material is obtained by commercially available
The conventional products obtained.
Embodiment 1
(1) 1kg folium artemisiae argyi, 1.5kg Chinese prickly ash are mixed with 20kg water, distillating extracting oil, until volatile oil is not further added by
Until, obtain the extraction raffinate and the dregs of a decoction that volatile oil is spare, after collection is distilled respectively；
(2) by 2kg leaf of elm tree, 1.5kg Fructus Liquidambaris, 1.5kg tribulus terrestris, 1.5kg Radix Astragali and 1.5kg Caulis Spatholobi and step
(1) dregs of a decoction obtained are decocted 2 times with water, and the mass ratio of the gross mass of each raw material and water is 1:8, decocting time when decocting every time
For 1.5h, it is filtered after decocting every time, merging filtrate；
(3) the extraction raffinate that step (1) obtains and the filtrate that step (2) obtains are merged, is condensed into density with concentration tank
About 1.25g/cm3The clear cream of (50 DEG C)；
(4) by 0.35kg sodium sulfate of polyethenoxy ether of fatty alcohol and 5.5kg coconut oil diethanol amide heating fusing, stirring
Uniformly, lemon acid for adjusting pH is added after being cooled to room temperature to 5-6, the volatile oil and step (3) that then addition step (1) obtains obtain
The clear cream arrived is heated to 60 DEG C and stirs 1h, adds 0.2kg jasmine flower essence, 0.4kg glycerol, 0.8kg polydimethylsiloxanes
Alkane, 0.8kg glycine betaine, 0.2kg pearlite slurry and 20g ethylparaben stir evenly up to the Chinese medicine shampoo.
Embodiment 2
(1) 0.5kg folium artemisiae argyi, 1kg Chinese prickly ash are mixed with 15kg water, distillating extracting oil, until volatile oil is not further added by
Until, obtain the extraction raffinate and the dregs of a decoction that volatile oil is spare, after collection is distilled respectively；
(2) 1kg leaf of elm tree, 1kg Fructus Liquidambaris, 1kg tribulus terrestris, 1kg Radix Astragali and 1kg Caulis Spatholobi and step (1) are obtained
The dregs of a decoction are decocted 2 times with water, when decocting every time the gross mass of each raw material and the mass ratio of water be 1:10, decocting time 2h, every time
It is filtered after decoction, merging filtrate；
(3) the extraction raffinate that step (1) obtains and the filtrate that step (2) obtains are merged, is condensed into density with concentration tank
About 1.4g/cm3The clear cream of (50 DEG C)；
(4) by 0.25kg sodium sulfate of polyethenoxy ether of fatty alcohol and 3.5kg coconut oil diethanol amide heating fusing, stirring
Uniformly, lemon acid for adjusting pH is added after being cooled to room temperature to 5-6, the volatile oil and step (3) that then addition step (1) obtains obtain
The clear cream arrived is heated to 50 DEG C and stirs 2h, add 0.15kg carnation essence, 0.25kg glycerol, 0.4kg silicone emulsion,
0.5kg glycine betaine, 80g pearlite slurry and 10g ethylparaben stir evenly up to the Chinese medicine shampoo.
Embodiment 3
(1) 1.5kg folium artemisiae argyi, 2kg Chinese prickly ash are mixed with 17.5kg water, distillating extracting oil, until volatile oil no longer increases
It adds as stopping, obtains the extraction raffinate and the dregs of a decoction that volatile oil is spare, after collection is distilled respectively；
(2) 3kg leaf of elm tree, 2kg Fructus Liquidambaris, 2kg tribulus terrestris, 2kg Radix Astragali and 2kg Caulis Spatholobi and step (1) are obtained
The dregs of a decoction are decocted 3 times with water, when decocting every time the gross mass of each raw material and the mass ratio of water be 1:5, decocting time 1h, every time
It is filtered after decoction, merging filtrate；
(3) the extraction raffinate that step (1) obtains and the filtrate that step (2) obtains are merged, is condensed into density with concentration tank
About 1.1g/cm3The clear cream of (50 DEG C)；
(4) by 0.5kg sodium sulfate of polyethenoxy ether of fatty alcohol and 7kg coconut oil diethanol amide heating fusing, stirring
It is even, lemon acid for adjusting pH is added after being cooled to room temperature to 5-6, the volatile oil and step (3) that then addition step (1) obtains obtain
Clear cream, be heated to 70 DEG C and stir 0.5h, add 0.2kg orchid compound, 0.1kg green tea essence, 0.5kg glycerol, 0.6kg
Triethanolamine, 0.6kg diethanol distearyl acid, 1kg glycine betaine, 0.3kg pearlite slurry and 30g ethylparaben, after mixing evenly
Up to the Chinese medicine shampoo.
Embodiment 4
(1) 0.5kg folium artemisiae argyi, 1kg Chinese prickly ash are mixed with 12kg water, distillating extracting oil, until volatile oil is not further added by
Until, obtain the extraction raffinate and the dregs of a decoction that volatile oil is spare, after collection is distilled respectively；
(2) 1kg leaf of elm tree, 1kg Fructus Liquidambaris, 1kg tribulus terrestris, 1kg Radix Astragali and 1kg Caulis Spatholobi and step (1) are obtained
The dregs of a decoction are decocted 2 times with water, when decocting every time the gross mass of each raw material and the mass ratio of water be 1:3, decocting time 1h, every time
It is filtered after decoction, merging filtrate；
(3) the extraction raffinate that step (1) obtains and the filtrate that step (2) obtains are merged, is condensed into density with concentration tank
About 1.05g/cm3The clear cream of (50 DEG C)；
(4) by 0.1kg sodium sulfate of polyethenoxy ether of fatty alcohol and 2kg coconut oil diethanol amide heating fusing, stirring
It is even, lemon acid for adjusting pH is added after being cooled to room temperature to 5-6, the volatile oil and step (3) that then addition step (1) obtains obtain
Clear cream, be heated to 60 DEG C and stir 1h, add 0.1kg Mint Essence, 0.2kg glycerol, 0.3kg dimethyl silicone polymer,
0.3kg glycine betaine, 10g pearlite slurry and 10g ethylparaben stir evenly up to the Chinese medicine shampoo.
Embodiment 5
(1) 10kg folium artemisiae argyi, 5kg Chinese prickly ash are mixed with 120kg water, distillating extracting oil, until volatile oil is not further added by
Until, obtain the extraction raffinate and the dregs of a decoction that volatile oil is spare, after collection is distilled respectively；
(2) 10kg leaf of elm tree, 10kg Fructus Liquidambaris, 10kg tribulus terrestris, 10kg Radix Astragali and 10kg Caulis Spatholobi and step (1) are obtained
The dregs of a decoction arrived are decocted 2 times with water, when decocting every time the gross mass of each raw material and the mass ratio of water be 1:8, decocting time 2h,
It is filtered after decocting every time, merging filtrate；
(3) the extraction raffinate that step (1) obtains and the filtrate that step (2) obtains are merged, is condensed into density with concentration tank
About 1.05g/cm3The clear cream of (50 DEG C)；
(4) by 2kg sodium sulfate of polyethenoxy ether of fatty alcohol and 20kg coconut oil diethanol amide heating fusing, stirring
It is even, the volatile oil that step (1) obtains and the clear cream that step (3) obtains then is added, is heated to 50 DEG C and stirs 2h, add
0.5kg flavoring rose essence, 0.5kg sweet basil essence, 1kg glycerol, 5kg silicone emulsion, 10kg glycine betaine, 1kg pearlite slurry and 0.5kg Buddhist nun
Golden ethyl ester is moored, is stirred evenly up to the Chinese medicine shampoo.
Evaluation of 1 shampoo of test case to Pityrosporum oval bacteriostasis
The preparation of test sample: embodiment 1 to 5 test sample of embodiment (is made into the molten of different volumes score with sterile distilled water
Liquid is spare -12.5mg/L, 25mg/L, 50mg/L, 100mg/L, 200mg/L), while using the shampoo of certain commercially available brand as
Control group.
Spawn incubation: having squarrose normal head part's materials using scrapings method, be inoculated in Leeming-Notman
In culture medium flat plate, at 32 DEG C, cultivates 10 days, the bacteria suspension (10 of Pityrosporum oval is configured to sterile water6-107cfu/
mL)。
Antibacterial ring size experiment: take that qualitative filter paper breaks into diameter 5mm circular filter paper piece with punch and sterilization treatment obtains sample
Piece dips test sample to be checked with tweezers in coupons respectively, as far as possible smears coupons uniform；Take bacteria suspension (106-
107Cfu/mL) 0.3mL is applied on Leeming-Notman culture medium flat plate, and sterile wind is utilized in aseptic superclean bench
Dry up plate；5 test prints (embodiment 1- embodiment 5 is each a piece of), 1 control group are placed in each plate, totally 6, are made
It is close to planar surface；Plate is covered, sets and is inverted culture 7 days in 32 DEG C of constant incubators, recorded with vernier caliper measurement antibacterial
The diameter of circle.
The results are shown in Table 1 for influence of the test sample in vitro culture bacterial strain, and data indicate inhibition zone diameter (mm) in table.
Evaluation of 1 Chinese medicine shampoo of table to Pityrosporum oval bacteriostasis
| Number | 12.5mg/L | 25mg/L | 50mg/L | 100mg/L | 200mg/L |
| Embodiment 1 | 0 | 0 | 20 | 27 | 32 |
| Embodiment 2 | 0 | 0 | 16 | 20 | 26 |
| Embodiment 3 | 0 | 0 | 15 | 22 | 24 |
| Embodiment 4 | 0 | 0 | 12 | 16 | 21 |
| Embodiment 5 | 0 | 0 | 11 | 14 | 19 |
| Control group | 0 | 0 | 0 | 0 | 0 |
It can be seen that by the result of table 1 real using the embodiment 1- of Chinese medicine shampoo formula of the present invention and preparation method
Applying example 5 has good inhibiting effect to Pityrosporum oval, and minimal inhibitory concentration is 50mg/L.
The hair washing antipruritic test of liquid extract of test case 2
Kunming mouse is randomly divided into 5 groups of example 1 group-embodiment, control group (is made with the shampoo of certain commercially available brand
For control group) and model blank group, totally 7 groups, every group 10；2d before testing, by back of mice shaving, shaving area area is 3cm
Corresponding shampoo is uniformly applied to shaving for every group of mouse by × 3cm, the experiment same day, 5 groups of example 1 group-embodiment and control group
On the skin of hair-fields, deionized water is uniformly applied on the shaving area skin of mouse by model blank group, and the applying amount of every mouse is
1mL；4-aminopyridine 1mg/kg is subcutaneously injected in 30min at shaving after smearing, and record groups of animals is in injection 4-aminopyridine
Afterwards in 10min Licking response number.The shampoo of embodiment 1- embodiment 5 and control group licks 4-aminopyridine induced mice
The influence of precursor reactant number, the results are shown in Table 2, reaction times using SPSS23.0 carry out statistical analysis, experimental data with
Means standard deviation (x ± s) indicates.
The evaluation of 2 Chinese medicine shampoo antipruritic effect of table
| Number | Number of cases (only) | Reaction times |
| Embodiment 1 | 10 | 16±4** |
| Embodiment 2 | 10 | 18±5** |
| Embodiment 3 | 10 | 19±3** |
| Embodiment 4 | 10 | 28±3* |
| Embodiment 5 | 10 | 29±4 |
| Control group | 10 | 35±5 |
| Model blank group | 10 | 45±5 |
Note: P < 0.01 * P < 0.05, * *
It can be seen that by the result of table 2 real using the embodiment 1- of Chinese medicine shampoo formula of the present invention and preparation method
Example 5 is applied, compared with model blank group, can inhibit Licking response number caused by 4-aminopyridine in various degree, with control group phase
Than effect becomes apparent from.
The trial effect of 3 shampoo of test case
Research object: itching of the scalp, dandruff be more, dry hair crowd, is divided into five experimental groups (embodiment 1- embodiment
5 each one group) and Normal group, every group of each 20 people.
Trial scheme: five experimental groups respectively correspondingly use Chinese medicine made from 1- of embodiment of the present invention embodiment 5 to have one's hair wash
Head is washed, is used continuously 1 month；Control group is washed hair using the shampoo of certain commercially available brand, is used continuously 1 month, experimental result
As shown in table 3.
It can be seen that by the result of table 3 real using the embodiment 1- of Chinese medicine shampoo formula of the present invention and preparation method
Example 5 is applied, compared with the control group, for itching of the scalp, dandruff is more, crowd of dry hair, has obvious effects on after long-time service.
Table 3
| Number | Improve completely | It is obviously improved | Slightly improve | In vain | Deteriorate |
| Embodiment 1 | 16 | 3 | 1 | 0 | 0 |
| Embodiment 2 | 15 | 5 | 3 | 0 | 0 |
| Embodiment 3 | 14 | 4 | 2 | 0 | 0 |
| Embodiment 4 | 12 | 4 | 4 | 0 | 0 |
| Embodiment 5 | 10 | 6 | 4 | 0 | 0 |
| Control group | 0 | 0 | 6 | 14 | 0 |
The preferred embodiment of the present invention has been described above in detail, and still, the present invention is not limited thereto.In skill of the invention
In art conception range, can with various simple variants of the technical solution of the present invention are made, including each technical characteristic with it is any its
Its suitable method is combined, and it should also be regarded as the disclosure of the present invention for these simple variants and combination, is belonged to
Protection scope of the present invention.
Claims (10)
1. a kind of Chinese medicine shampoo, which is characterized in that including following raw material components, be calculated as with mass parts: 10-100 parts of leaf of elm tree,
10-50 parts of Chinese prickly ash, 10-100 parts of Fructus Liquidambaris, 5-100 parts of folium artemisiae argyi, 10-100 parts of tribulus terrestris, 10-100 parts of Radix Astragali, Caulis Spatholobi 10-
100 parts, 1-10 parts of essence, 2-10 parts of glycerol, 20-200 parts of coconut oil diethanol amide, 3-50 parts of softening agent, glycine betaine 3-100
Part, 0.1-10 parts of pearlite slurry, 1-20 parts of sodium sulfate of polyethenoxy ether of fatty alcohol, 0.1-5 parts of ethylparaben.
2. Chinese medicine shampoo according to claim 1, which is characterized in that including following raw material components, be calculated as with mass parts:
10-30 parts of leaf of elm tree, 10-20 parts of Chinese prickly ash, 10-20 parts of Fructus Liquidambaris, 5-15 parts of folium artemisiae argyi, 10-20 parts of tribulus terrestris, 10-20 parts of Radix Astragali,
10-20 parts of Caulis Spatholobi, 1.5-3 parts of essence, 2.5-5 parts of glycerol, 35-70 parts of coconut oil diethanol amide, 4-12 parts of softening agent, sweet tea
5-10 parts of dish alkali, 0.8-3 parts of pearlite slurry, 2.5-5 parts of sodium sulfate of polyethenoxy ether of fatty alcohol, 0.1-0.3 parts of ethylparaben.
3. Chinese medicine shampoo according to claim 1 or 2, which is characterized in that the essence is jasmine flower essence, carnation
Essence, orchid compound, Mint Essence, flavoring rose essence, lavender oil, violet compound, milk flavour, fruity essence, sieve
One of essence and green tea essence or a variety of are strangled, the softening agent is dimethyl silicone polymer, silicone emulsion, diethanol two are hard
One of resin acid and triethanolamine are a variety of.
4. a kind of preparation method of Chinese medicine shampoo, which comprises the following steps:
(1) folium artemisiae argyi, Chinese prickly ash are mixed with water, it is standby to obtain volatile oil until volatile oil is not further added by for distillating extracting oil
With extraction raffinate and the dregs of a decoction after collection is distilled respectively；
(2) dregs of a decoction for obtaining leaf of elm tree, Fructus Liquidambaris, tribulus terrestris, Radix Astragali and Caulis Spatholobi and step (1), are filtered after being decocted with water,
Obtain filtrate；
(3) the extraction raffinate that step (1) obtains and the filtrate that step (2) obtains are merged, is condensed into clear cream；
(4) sodium sulfate of polyethenoxy ether of fatty alcohol and coconut oil diethanol amide heating melted, stirred evenly, step is added
(1) after the clear cream that the volatile oil and step (3) obtained obtains, heating stirring, add essence, glycerol, softening agent, glycine betaine,
Pearlite slurry and ethylparaben stir evenly up to the Chinese medicine shampoo；
Wherein, the dosage of the above raw material is calculated as with mass parts: 10-100 parts of leaf of elm tree, 10-50 parts of Chinese prickly ash, Fructus Liquidambaris 10-100
Part, 5-100 parts of folium artemisiae argyi, 10-100 parts of tribulus terrestris, 10-100 parts of Radix Astragali, 10-100 parts of Caulis Spatholobi, 1-10 parts of essence, glycerol 2-10
Part, 20-200 parts of coconut oil diethanol amide, 3-50 parts of softening agent, 3-100 parts of glycine betaine, 0.1-10 parts of pearlite slurry, fatty alcohol
1-20 parts of polyethenoxy ether sodium sulfate, 0.1-5 parts of ethylparaben.
5. the preparation method according to claim 4, which is characterized in that the essence be jasmine flower essence, carnation essence,
Orchid compound, Mint Essence, flavoring rose essence, lavender oil, violet compound, milk flavour, fruity essence, sweet basil essence
With one of green tea essence or a variety of, the softening agent be dimethyl silicone polymer, silicone emulsion, diethanol distearyl acid and
One of triethanolamine is a variety of.
6. the preparation method according to claim 4, which is characterized in that the gross mass and water of folium artemisiae argyi and Chinese prickly ash in step (1)
Mass ratio be 1:5-10.
7. the preparation method according to claim 4, which is characterized in that in step (2), the process decocted with water includes
It is decocted 2-3 times, is filtered after decocting every time, merging filtrate with water；
Wherein, in each decoction process, the gross mass of each raw material and the mass ratio of water be 1:5-10, time 1-2h.
8. the preparation method according to claim 4, which is characterized in that the density at 50 DEG C of clear cream described in step (3) is
1.1-1.4g/cm3。
9. the preparation method according to claim 4, which is characterized in that step (4) further includes in fatty alcohol polyoxyethylene ether
Sodium sulphate and coconut oil diethanol amide heating fusing, after mixing evenly, be cooled to room temperature, be added pH adjusting agent, adjust pH to
5-6；In step (4) after the volatile oil that step (1) obtains and the clear cream that step (3) obtains is added, the temperature of heating stirring is
50-70 DEG C, time 0.5-2h.
10. the Chinese medicine shampoo being prepared according to claim 4-9 any one the method.
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