CN107582460A - A kind of amino acid cleansing breast and preparation method thereof - Google Patents
A kind of amino acid cleansing breast and preparation method thereof Download PDFInfo
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- CN107582460A CN107582460A CN201710952994.0A CN201710952994A CN107582460A CN 107582460 A CN107582460 A CN 107582460A CN 201710952994 A CN201710952994 A CN 201710952994A CN 107582460 A CN107582460 A CN 107582460A
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Abstract
The present invention relates to a kind of amino acid cleansing breast comprising astringent and preparation method thereof, and preparing the raw material of the astringent includes hazel extract, indigo naturalis, sulphur, radix rehmanniae recen and Radix Angelicae Sinensis.The amino acid cleansing breast of the present invention is suitable for daily morning and evening face cleaning and used, it is gentle non-stimulated, suitable for sensitive skin, the effect reduced pore, improve cutaneous roughness can be played from antibacterial, convergence, cleaning, anti-inflammatory, antiallergy, the various aspects such as stimulate circulation collaboration, and to no skin irritation, resilience is not easy after deactivation, health diet and rule can be coordinated to move, reaches the long-term purpose for improving skin condition, beautifying skin.
Description
Technical field
The invention belongs to aesthetic care products technical field, and in particular to a kind of to have convergence, the ammonia of pore refining effect
Base acid mildy wash and preparation method thereof.
Background technology
The follicular orifice that pore refers to, it is the Common openings of hair follicle and sebaceous glands, has specific physiological function, such as drain
The secretion of sebaceous glands.When sebum excessive secretion fails to clear up in time again, it is thick to easily cause pore, and it is skin that pore is thick
The main reason for skin is coarse, and nurse other skin problems such as improper very easy initiation acne, small pox, blackhead, outward appearance pole
Unsightly.Pore is thick to be often as hormone in vivo parasecretion, and pressure is excessive and environmental pollution, cleaning are not carried out
Caused by reason.In addition, with advancing age, skin gradually follows the string, perifollicolar lacks support structure, is also easy to
Pore is set to seem bigger；The skin environment done in outer oil, also can make pore become thick.
The thick method of reply pore mainly has interior tune, external application and cosmetic means at present, and interior tune refers to take with regulation
Fat secretion, enriching yin, the product for the qi-blood-body fluid and other effects that stimulates circulation, supplies, nutrition is supplied from body interior to skin
Material, make hair pore shrinkage, skin fine and smooth white clean and bear elasticity.However, interior adjust works relatively slowly, it is necessary to the conditioning ability of long period
It can take effect, easily consumer is lost confidence, and formula for oral administration is according to personal skin quality, constitution and physiological status（Such as pass through,
The different physiology courses such as pregnant, production, breast）, it is difficult to accomplish unified allocation of resources, extensive use.Can also promptly it be tackled by cosmetic means
Pore is thick, such as has the color make-up products such as the foundation emulsion for hiding the flaw and acting on, muffin by film, however, this means can only lead to
Cross physics mode and cover thick pore, visually give the fine and smooth sensation of skin, it is impossible to it is thick fundamentally to solve pore
Greatly, the problem of pachylosis.On the other hand, city environmental pollution is serious, and skin physiological status is posed a big pressure, therefore,
Cleaning and nursing are only that reply pore is thick, important means of pachylosis.
Amino acid cleansing breast is the face cleaning product for adding amino acid surfactant, wherein amino acid surfactant example
Such as come from glutamic acid, glycine, alanine or arginic surfactant.Relative to the common soap base mildy wash of meta-alkalescence,
Amino acid cleansing breast face cleaning is gentleer, nonirritant.But current face cleaning product more focuses on cleaning dynamics, to skin cleannes
Persistence concern deficiency.
The content of the invention
It can effectively restrain in order to obtain, reduce pore, make the face cleaning milk product that skin is moist, the present inventor's research and development
Go out a kind of new astringent, be added into amino acid cleansing breast, do not influence mildy wash cleaning force in itself and gentle antiallergy
Characteristic, so as to complete the present invention.
Therefore, in one aspect, the invention provides a kind of amino acid cleansing breast, the amino acid cleansing breast is comprising molten
Agent, amino acid surfactant, emulsifying agent, astringent, pH adjusting agent and preservative, wherein, prepare the raw material of the astringent
Including hazel extract, indigo naturalis, sulphur, radix rehmanniae recen and Radix Angelicae Sinensis.
Witch hazel（Hamamelis mollis Oliver）, fragrant, ox steps on fruit in alias wood, in its petal containing Quercetin,
A variety of active principles rich in high activity hydroxyl such as Kaempferol, astragalin, tannin, sebum secretion can be adjusted, promote lymph
Blood circulation, have releive, calmness, convergence, anti-inflammatory, antibacterial, the effect of anti-aging, have particularly with cracking, sunburn, acne etc.
Good improvement result, is widely used in aesthetic care products at present.The hazel extract is by the following method
Prepare, witch hazel petal is cleaned and uses saline sook 30min, after filtering, the ethyl acetate backflow for adding 5 times of weight carries
3h is taken, is filtered, filtrate is distilled to solvent-free at reduced pressure conditions to be steamed, and the distilled water diluting of 20 times of weight is added after weighing, is obtained
Obtain hazel extract.
Indigo naturalis is that justicia reward section plant acanthaceous indigo, polygonaceae plant indigo plant, the leaf of cruciferae isatis or cauline leaf are processed
Obtained dried powder, agglomerate or particle, have the effect such as clearing heat and detoxicating, blood cooling and ecchymoses removing, purging intense heat arresting convulsion, be also commonly used for printing in ancient times
Dye cloth, thrush etc..Research is found to clay into power a small amount of indigo naturalis external application, can adsorb skin surface metabolite, and cleaning is received
Contracting pore, stimulate circulation, active cell in life, contribute to skin repair, make whitening skin.
Sulphur has Controlling oil effect, can suppress sebum secretion, kill bacterium, fungi, mould, acarid, parasite etc., and
Suppression colonizes in the bacterial growth of skin surface, is especially suitable for the disease of skin such as acne, acne.
Radix rehmanniae recen is the fresh or dried root of scrophulariaceae rehmannia glutinosa plant.Containing a variety of glycosides, carbohydrate and amino acid, β-paddy steroid
Alcohol, rehmanin, mannitol, glucose, alkaloid, irony, vitamin A and various trace elements.With certain anti-mistake of anti-inflammatory
Quick effect, the growth to a variety of fungies have inhibitory action.Radix rehmanniae recen can be made into that rehmannia root wine is for oral administration or external application, with except acne work(
Effect.But splenasthenic diarrhea, stomach void deficiency of food, the more phlegm persons of chest diaphragm should not take orally.
Radix Angelicae Sinensis is a kind of Chinese medicine commonly used in prescription, and usual levigation uses, and has beauty functions and medical functions, property
Temperature, acrid-sweet flavor, nontoxic, external application, which is applied face and can played, to stimulate circulation, and makes the delicate glossiness effect of skin, especially to yellowish-brown
Spot, freckle have unique curative effect.
Preferably, the hazel extract of the raw material including 10-12 parts by weight of the astringent, 5-8 parts by weight are prepared
Indigo naturalis, the sulphur of 8-10 parts by weight, the radix rehmanniae recen of 5-8 parts by weight and 15-20 parts by weight Radix Angelicae Sinensis, more preferably 12 parts by weight gold
Thread plum extract solution, the indigo naturalis of 7 parts by weight, the sulphur of 8 parts by weight, the Radix Angelicae Sinensis of the radix rehmanniae recen of 8 parts by weight and 18 parts by weight.
The astringent is prepared by the following method, and the radix rehmanniae recen of withdrawal and Radix Angelicae Sinensis are done in drying oven respectively
Dry, then fragmentation is blocking, grind into powder after being mixed with indigo naturalis and sulphur, crosses 16 mesh sieves, obtains mixed-powder, adds 3 times of weights
Amount（Relative to the mixed-powder）0.5% ethanol water, refluxing extraction 6-8h, filtering, by filter residue repeat extract two again
It is secondary, merging filtrate, lower distillation is depressurized to the residue of residue about 1/10th and without alcohol taste, witch hazel is added after being down to room temperature
Extract solution mixes, and obtains the astringent.
Preferably, the amino acid cleansing breast includes solvent, the amino acid surface of 10-20 parts by weight of 60-70 parts by weight
Activating agent, the emulsifying agent of 5-8 parts by weight, the astringent of 8-10 parts by weight, the pH adjusting agent of 0.2-0.5 parts by weight and 0.1-0.3
The preservative of parts by weight.
Wherein, the solvent is water, glycerine, the mixture of propane diols.
The amino acid surfactant is selected from sodium cocoyl glutamate, sodium lauroyl glutamate, stearoyl-glutamic acid
Sodium, palmityl sodium glutamate, sodium cocoyl glycinate, cocounut oil acyl Sodium L-alaninate.
The emulsifying agent is preferably chosen from EGDS, cetostearyl alcohol, tristerin.
The pH adjusting agent is citric acid.
The preservative is preferably chosen from methyl benzoate, Phenoxyethanol, dimethyloldimethylhydantoin.
In addition, the amino acid cleansing breast of the present invention can also add the conventional functional additive of other cosmetic fields,
Such as NMF, spices, whitening agent, sedative, pigment etc..
In another aspect, present invention also offers the preparation method of above-mentioned amino acid cleansing breast, methods described includes will
Emulsifying agent, pH adjusting agent are added in solvent, are heated to 75-85 DEG C, homogeneous 10min, are cooled to 45-55 DEG C, add amino acid table
Face activating agent, astringent, preservative, stir, and are down to room temperature, filling after the assay was approved.
The amino acid cleansing breast of the present invention is suitable for daily morning and evening face cleaning and used, gentle non-stimulated, suitable for sensitive skin.
The present invention amino acid cleansing breast contain made of kinds of traditional Chinese medicines material astringent, can from it is antibacterial, convergence, cleaning,
Anti-inflammatory, antiallergy, the various aspects such as stimulate circulation collaboration play the effect reduced pore, improve cutaneous roughness, and
To no skin irritation, resilience is not easy after deactivation, health diet and rule can be coordinated to move, reach it is long-term improve skin condition,
Beautify the purpose of skin.
Embodiment
Technical scheme is further described with reference to specific embodiment.
Prepare embodiment 1
The witch hazel petal of fresh harvesting is cleaned, with saline sook 30min, after filtering, the ethyl acetate for adding 5 times of weight returns
Stream extraction 3h, filtering, filtrate is distilled to solvent-free at reduced pressure conditions to be steamed, and the distilled water that 20 times of weight are added after weighing is dilute
Release, obtain hazel extract.
The radix rehmanniae recen of withdrawal and Radix Angelicae Sinensis are dried in drying oven respectively, then fragmentation is blocking, weighs the 80kg dried rhizome of rehmannia respectively
Yellow, 180kg Radix Angelicae Sinensis, after mix with 70kg indigo naturalis and 80kg sulphur in grinder grind into powder, 16 mesh sieves of mistake, mixed
Powder, add the 0.5% of about 1200L（Volume ratio）Ethanol water, refluxing extraction 8h, filtering, filter residue is repeated to extract two again
It is secondary, merging filtrate, lower distillation is depressurized to remaining about 360mL residues and without alcohol taste, 120L witch hazels are added after being down to room temperature
Extract solution mixes, and obtains the astringent.
Embodiment 1
It is using 50kg water, 10kg glycerine and 2kg mixed with propylene glycol as mixed solvent, 3kg cetostearyl alcohols, 3kg stearic acid is sweet
Grease, 0.2kg citric acids add in the mixed solvent, are heated to 80 DEG C, the homogeneous 10min in homogenizer, are cooled to 50 DEG C, add
10kg sodium cocoyl glycinates, 5kg sodium lauroyl glutamates, 8kg prepare astringent, the 0.2kg Phenoxyethanols that embodiment 1 obtains
Stir, be down to room temperature, it is filling after the assay was approved, obtain the amino acid cleansing breast of the present invention.
Embodiment 2
Using 40kg water, 20kg glycerine and 5kg mixed with propylene glycol as mixed solvent, by 5kg EGDSs, 0.3kg
Citric acid adds in the mixed solvent, is heated to 85 DEG C, the homogeneous 10min in homogenizer, is cooled to 45 DEG C, adds 10kg cocounut oil acyls
Sodium glutamate, 10kg cocounut oil acyls Sodium L-alaninate, 10kg prepare astringent, the 0.3kg methyl benzoates that embodiment 1 obtains and stirred
It is even, room temperature is down to, it is filling after the assay was approved, obtain the amino acid cleansing breast of the present invention.
Embodiment 3
It is using 50kg water, 5kg glycerine and 5kg mixed with propylene glycol as mixed solvent, 3kg cetostearyl alcohols, 5kg ethylene glycol is double hard
Resin acid ester, 0.5kg citric acids add in the mixed solvent, are heated to 70 DEG C, the homogeneous 10min in homogenizer, are cooled to 55 DEG C, add
Enter 8kg sodium cocoyl glycinates, 8kg palmityls sodium glutamate, 4kg stearoyl-glutamic acids sodium, 9kg and prepare what embodiment 1 obtained
Astringent, 0.1kg dimethyloldimethylhydantoins stir, and are down to room temperature, filling after the assay was approved, obtain the present invention
Amino acid cleansing breast.
Embodiment 4
Using 60kg water, 8kg glycerine and 2kg mixed with propylene glycol as mixed solvent, by 4kg cetostearyl alcohols, 4kg glycerol stearates
Ester, 0.4kg citric acids add in the mixed solvent, are heated to 75 DEG C, the homogeneous 10min in homogenizer, are cooled to 50 DEG C, add
8kg sodium cocoyl glycinates, 2kg sodium lauroyl glutamates, 8kg prepare astringent, the 0.1kg Phenoxyethanols that embodiment 1 obtains
Stir, be down to room temperature, it is filling after the assay was approved, obtain the amino acid cleansing breast of the present invention.
The amino acid cleansing breast that 1-4 of the embodiment of the present invention is obtained visual observations, outward appearance under room temperature and non-direct sunlight is equal
Even consistent, no obvious irritation peculiar smell, foaming is abundant after mixing water.
Three sensitive skin volunteers are selected, hypersensitive test, the embodiment 1-4 equal nothing of amino acid cleansing breast are carried out after ear
Allergic phenomena.Appropriate amino acid mildy wash is squeezed in hand, adds a small amount of water rubbing foaming, then cleaning face, massages 2min, uses
Clear water cleans the foam of residual.Volunteer is conducted interviews, feels salubrious after and moistens, nonirritant pain, to facial skin
Skin is observed, and visually pore has the sensation of diminution, and skin is delicate, and the fuel-displaced phenomenon unobvious of m seq, presses down well
Fuel-displaced phenomenon has been made, has persistently reduced pore.
Add the astringent of multi-flavor medicinal material combination so that amino acid cleansing breast of the invention has obvious convergence, contracting
It the effect of small pore, can from many aspects start with, nurse one's health sebum secretion emphatically, effectively inhibit the resilience of the thick problem of pore.
Above only describes the better embodiment of the present invention, but the present invention is not limited to above-described embodiment.This area skill
Art personnel all should fall into the present invention it is understood that any same or similar means of the technology of the present invention effect can be realized
Protection domain in.
Claims (7)
1. a kind of amino acid cleansing breast, the amino acid cleansing breast includes solvent, amino acid surfactant, emulsifying agent, convergence
Agent, pH adjusting agent and preservative, wherein, preparing the raw material of the astringent includes hazel extract, indigo naturalis, sulphur, the dried rhizome of rehmannia
Yellow and Radix Angelicae Sinensis.
2. amino acid cleansing breast according to claim 1, it is characterised in that the hazel extract is by with lower section
What method prepared, witch hazel petal is cleaned and uses saline sook 30min, after filtering, adds the ethyl acetate backflow of 5 times of weight
3h is extracted, filtering, filtrate is distilled to solvent-free at reduced pressure conditions to be steamed, and the distilled water diluting of 20 times of weight is added after weighing,
Obtain hazel extract.
3. amino acid cleansing breast according to claim 1, it is characterised in that preparing the raw material of the astringent includes 10-
The hazel extract of 12 parts by weight, the indigo naturalis of 5-8 parts by weight, the sulphur of 8-10 parts by weight, 5-8 parts by weight radix rehmanniae recen and
The Radix Angelicae Sinensis of 15-20 parts by weight, the preferably hazel extract of 12 parts by weight, the indigo naturalis of 7 parts by weight, the sulphur of 8 parts by weight, 8 weights
Measure the radix rehmanniae recen of part and the Radix Angelicae Sinensis of 18 parts by weight.
4. amino acid cleansing breast according to claim 1, it is characterised in that the amino acid cleansing breast includes 60-70 weights
Measure the solvent of part, the amino acid surfactant of 10-20 parts by weight, 5-8 parts by weight emulsifying agent, 8-10 parts by weight convergence
The preservative of agent, the pH adjusting agent of 0.2-0.5 parts by weight and 0.1-0.3 parts by weight.
5. amino acid cleansing breast according to claim 1, it is characterised in that the amino acid surfactant is selected from coconut palm
Oleoyl sodium glutamate, sodium lauroyl glutamate, stearoyl-glutamic acid sodium, palmityl sodium glutamate, sodium cocoyl glycinate, cocounut oil
Acyl Sodium L-alaninate.
6. amino acid cleansing breast according to claim 1, it is characterised in that the amino acid cleansing breast also includes moisturizing
At least one of agent, spices, whitening agent, sedative, pigment.
7. the preparation method of the amino acid cleansing breast any one of claim 4-6, methods described are included emulsifying agent, pH
Conditioning agent is added in solvent, is heated to 75-85 DEG C, homogeneous 10min, is cooled to 45-55 DEG C, add amino acid surfactant,
Astringent, preservative, stir, and are down to room temperature, filling after the assay was approved.
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| CN201710952994.0A CN107582460A (en) | 2017-10-13 | 2017-10-13 | A kind of amino acid cleansing breast and preparation method thereof |
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| CN201710952994.0A CN107582460A (en) | 2017-10-13 | 2017-10-13 | A kind of amino acid cleansing breast and preparation method thereof |
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Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108904390A (en) * | 2018-09-07 | 2018-11-30 | 广州壹嘉生物科技有限公司 | The preparation method of hamamelis extract and its application in acne-eliminating cosmetic |
| CN108992364A (en) * | 2018-07-25 | 2018-12-14 | 广州依露美化妆品有限公司 | A kind of moisturizing mildy wash containing sodium lauroyl glutamate |
| CN109223700A (en) * | 2018-11-23 | 2019-01-18 | 谢树群 | A kind of facial cleanser formula with bactericidal effect |
| CN109512715A (en) * | 2019-01-15 | 2019-03-26 | 宁夏艾伊生物工程研发有限公司 | A kind of foster skin washing cream and preparation method thereof |
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| CN102397223A (en) * | 2011-11-18 | 2012-04-04 | 大连得达科技发展有限公司 | Natural anti-wrinkle facial cleanser |
| CN105147532A (en) * | 2015-08-19 | 2015-12-16 | 广州科玛生物科技有限公司 | Amino acid facial cleanser and preparation method thereof |
| CN105616226A (en) * | 2014-10-31 | 2016-06-01 | 郁丁丁 | Moisture preserving facial cleanser with nourishing efficacy |
| CN105997739A (en) * | 2016-07-12 | 2016-10-12 | 广州丹奇日用化工厂有限公司 | Skin tendering facial cleanser |
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Patent Citations (4)
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| CN102397223A (en) * | 2011-11-18 | 2012-04-04 | 大连得达科技发展有限公司 | Natural anti-wrinkle facial cleanser |
| CN105616226A (en) * | 2014-10-31 | 2016-06-01 | 郁丁丁 | Moisture preserving facial cleanser with nourishing efficacy |
| CN105147532A (en) * | 2015-08-19 | 2015-12-16 | 广州科玛生物科技有限公司 | Amino acid facial cleanser and preparation method thereof |
| CN105997739A (en) * | 2016-07-12 | 2016-10-12 | 广州丹奇日用化工厂有限公司 | Skin tendering facial cleanser |
Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108992364A (en) * | 2018-07-25 | 2018-12-14 | 广州依露美化妆品有限公司 | A kind of moisturizing mildy wash containing sodium lauroyl glutamate |
| CN108992364B (en) * | 2018-07-25 | 2021-12-28 | 广州依露美化妆品有限公司 | Moisturizing facial cleanser containing sodium lauroyl glutamate |
| CN108904390A (en) * | 2018-09-07 | 2018-11-30 | 广州壹嘉生物科技有限公司 | The preparation method of hamamelis extract and its application in acne-eliminating cosmetic |
| CN108904390B (en) * | 2018-09-07 | 2021-07-16 | 广州壹嘉生物科技有限公司 | Preparation method of Hamamelis virginiana extract and application of Hamamelis virginiana extract in acne-removing cosmetics |
| CN109223700A (en) * | 2018-11-23 | 2019-01-18 | 谢树群 | A kind of facial cleanser formula with bactericidal effect |
| CN109512715A (en) * | 2019-01-15 | 2019-03-26 | 宁夏艾伊生物工程研发有限公司 | A kind of foster skin washing cream and preparation method thereof |
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