CN110184121A - Cigarette quick-fried pearl essential oil and the preparation method and application thereof - Google Patents
Cigarette quick-fried pearl essential oil and the preparation method and application thereof Download PDFInfo
- Publication number
- CN110184121A CN110184121A CN201910354573.7A CN201910354573A CN110184121A CN 110184121 A CN110184121 A CN 110184121A CN 201910354573 A CN201910354573 A CN 201910354573A CN 110184121 A CN110184121 A CN 110184121A
- Authority
- CN
- China
- Prior art keywords
- quick
- fried pearl
- cigarette
- emblic
- essential oil
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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Classifications
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/24—Treatment of tobacco products or tobacco substitutes by extraction; Tobacco extracts
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24D—CIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
- A24D3/00—Tobacco smoke filters, e.g. filter-tips, filtering inserts; Filters specially adapted for simulated smoking devices; Mouthpieces for cigars or cigarettes
- A24D3/04—Tobacco smoke filters characterised by their shape or structure
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
Abstract
The present invention relates to technical field of tobacco, provide a kind of cigarette quick-fried pearl essential oil and the preparation method and application thereof.A kind of cigarette preparation method of quick-fried pearl essential oil, is formed by the material allocation of following weight percent: the quick-fried pearl extract 0.5~6% of emblic, Span80 surfactant 0.08~0.15%, Glycerin, mixed triester with caprylic acid capric acid surplus；The quick-fried pearl extract of emblic is to extract to obtain by supercritical extraction with emblic raw material.The present invention, as raw material, has the breath of apparent emblic faint scent using the quick-fried pearl extract of emblic, and whole odor characteristic is fresh and clean.And it is extracted using supercritical extraction, the high odor characteristic at low cost and that emblic itself can be effectively maintained of extraction efficiency.The present invention also provides a kind of cigarette quick-fried pearl essential oils and its application.
Description
Technical field
The present invention relates to technical field of tobacco more particularly to a kind of cigarette quick-fried pearl essential oils and the preparation method and application thereof.
Background technique
Quick-fried pearl refers to a small glue bead of liquid in filter tip, it has wrapped up the liquid of different type fragrance, smoker
It can be pinched in sucking process quick-fried, flow out liquid, realize the artificial controllable characteristic fragrance release in aspiration procedure, subtract
Few external environment loses the influence and essence of inhaling taste, abundant to suck taste.
With the continuous improvement of " quick-fried pearl addition " market cognition degree, more and more home brands are released using the technology
Recent specifications product adds quick-fried pearl propulsion brand upgrading to old product on the basis of original specification.It glides in conventional cigarette sales volume
Background under, be stepped up using the product sales volume specific gravity of " quick-fried pearl add " technology, if currently quick-fried pearl cigarette disappears according to the U.S.
Take specific gravity balance 3% to calculate, China " quick-fried pearl " cigarette market capacity is more than 1,500,000 casees.Therefore, the development space of quick-fried pearl flavoring
It is huge.In recent years, domestic tobacco enterprise has carried out a large amount of work in terms of quick-fried pearl research and development, wherein trying to explore that quick-fried pearl is suitble to add
Fragrant new raw material is one of current most important work.
Summary of the invention
It is an object of the invention to overcome the above-mentioned prior art, a kind of cigarette quick-fried pearl essential oil and its preparation side are provided
Method and application.
In order to solve the above technical problems, invention uses technical solution as described below.A kind of preparation of the quick-fried pearl essential oil of cigarette
Method is formed by the material allocation of following weight percent:
The quick-fried pearl extract 0.5~6% of emblic
Span80 surfactant 0.08~0.15%
Glycerin, mixed triester with caprylic acid capric acid surplus；
The quick-fried pearl extract of emblic is to extract to obtain by supercritical extraction with emblic raw material.
Preferably, the extraction of the quick-fried pearl extract of the emblic includes: to go to obstruct by fresh emblic, is rubbed after cleaning, so
Supercritical extract is carried out using the CO 2 fluid under supercriticality as extractant afterwards.
Preferably, the temperature of the supercritical extract is 30-60 DEG C.
Preferably, the pressure of the supercritical extract is 35-45MPa.
Preferably, the when a length of 2-4h of the supercritical extract.
Preferably, the cigarette further includes being stirred after mixing all raw materials with the preparation method of quick-fried pearl essential oil.
Preferably, the revolving speed of the stirring is 200-300r/min, the when a length of 1-2h of stirring.
A kind of quick-fried pearl essential oil of cigarette is prepared using above-mentioned cigarette with the preparation method of quick-fried pearl essential oil.
Cigarette is made with quick-fried pearl, in cigarette with quick-fried pearl essential oil in above-mentioned cigarette by a kind of application of the quick-fried pearl essential oil of cigarette.
The beneficial effects of the present invention are:
For the present invention using the quick-fried pearl extract of emblic as raw material, the breath with apparent emblic faint scent is whole fragrant
Gas feature is fresh and clean.And extracted using supercritical extraction, extraction efficiency is high at low cost and can be effectively maintained emblic sheet
The odor characteristic of body.
Specific embodiment
To make those skilled in the art that the purposes, technical schemes and advantages of invention be more clearly understood, below
Invention is further elaborated in conjunction with the embodiments.
Emblic also known as Yunnan olive, Phyllanthus embical fruit, Phyllanthus embical fruit etc., be mainly distributed on Yunnan, Guangxi, Guangdong, Fujian, Guizhou,
The provinces and regions such as Taiwan, Hainan.It is recorded according to Compendium of Material Medica, emblic " sweet in flavor cold, nontoxic " has " gas is strengthened in help ", " Xie Jinshi
Poison ", " main wind abnormal heat gas ", various health-care effects such as " long term usage is made light of one's life by commiting suicide, and macrobiosis is long-living ".Modern scientific research shows
Emblic has anti-inflammatory, antitumor, anti-rich in the various actives substance such as superoxide dismutase (SOD), Vc, polyphenol and polysaccharide
Mutation, lowering blood pressure and blood fat, hypoglycemic, liver protection and other effects.
Currently, yet there are no emblic in correlative study and application of the cigarette in terms of quick-fried pearl.And mentioning for emblic
It takes, generallys use traditional solvent extraction.Conventional solvent extraction are as follows: it is rubbed after fresh emblic is gone stalk, cleaning, by 1:
Petroleum ether is added in the solid-liquid ratio of 5-1:10, and heat reflux extraction 1-3h, cooled and filtered, filter vacuum are concentrated at 50-70 DEG C
Until petroleum ether all volatilizes.This conventional solvent extraction has the disadvantage that:
(1) petroleum ether is inflammable and explosive, there is very big security risk in production process.
(2) petroleum ether has certain toxicity, easily there is dissolvent residual in product, therefore hidden with certain edible safety
Suffer from.
(3) solvent usage amount is big, and a large amount of loss is easily caused in production process, so as to cause cost raising.
(4) in concentration process, fragrance component is be easy to cause to lose.
(5) petroleum ether poor selectivity, there are some ingredients to be not completely soluble in Glycerin, mixed triester with caprylic acid capric acid in extract.
Embodiment one
A kind of cigarette preparation method of quick-fried pearl essential oil, is formed by the material allocation of following weight percent:
The quick-fried pearl extract 0.5~6% of emblic
Span80 surfactant 0.08~0.15%
Glycerin, mixed triester with caprylic acid capric acid surplus；
The quick-fried pearl extract of emblic is to extract to obtain by supercritical extraction with emblic raw material.
For the present invention using the quick-fried pearl extract of emblic as raw material, the breath with apparent emblic faint scent is whole fragrant
Gas feature is fresh and clean.And extracted using supercritical extraction, extraction efficiency is high at low cost and can be effectively maintained emblic sheet
The odor characteristic of body.In some preferably embodiments, the emblic derives from Shanwei Lufeng City overseas Chinese farm.
Preferably, the extraction of the quick-fried pearl extract of the emblic includes: to go to obstruct by fresh emblic, is rubbed after cleaning, so
Supercritical extract is carried out using the CO 2 fluid under supercriticality as extractant afterwards.With the dioxy under supercriticality
Change carbon flow body as extractant, nontoxic, environmentally protective, there is no safety problems in production process, and solvent is not present
Residual, edible safety.In some specific embodiments, the extraction of the quick-fried pearl extract of emblic is the following steps are included: new
Fresh emblic --- goes to obstruct --- cleaning --- rubbing --- extraction --- separation.That is, rubbed after fresh emblic is gone stalk, cleaning,
Be then placed in extraction kettle, will carbon dioxide gas import extraction kettle in, make carbon dioxide gas in the supercritical state with day
Right material contact, is dissolved in the oil-soluble ingredients in emblic in supercritical fluid, collects extract from the outlet of separating still.
In some preferred embodiments, further determine that the process conditions of supercritical extract, including temperature, pressure and when
It is long.Preferably, the temperature of the supercritical extract is 30-60 DEG C；The pressure of the supercritical extract is 35-45MPa；It is described super
The when a length of 2-4h of critical extraction.By setting these process conditions, the property of can choose extract be dissolved in Glycerin, mixed triester with caprylic acid capric acid at
Point.The recovery rate of emblic extract is 1% under optimum process condition.
Preferably, the cigarette further includes being stirred after mixing all raw materials with the preparation method of quick-fried pearl essential oil.?
Preparing raw material according to above-mentioned weight percent, and above-mentioned material is successively put into the container with agitating device and is carried out
Stirring.Preferably, the revolving speed of the stirring is 200-300r/min, the when a length of 1-2h of stirring.In some specific embodiments
In, for stirring 1-2h under room temperature under conditions of revolving speed is 200--300r/min to solution clear, the as quick-fried pearl of emblic
Extract.
The cigarette is had the advantage that with the preparation method of quick-fried pearl essential oil
(1) present invention is nontoxic, environmentally protective using the CO 2 fluid under supercriticality as extractant,
Safety problem is not present in production process, and dissolvent residual, edible safety is not present.
(2) solvent is recycled in the same system, and solvent consumption is small and price is cheap, therefore extracts at low cost.
(3) extraction temperature is low, and extraction cycle is short, can be effectively retained the odor characteristic of emblic itself.
(4) can according to the characteristic of raw material itself, set extraction conditions, selective extraction be dissolved in Glycerin, mixed triester with caprylic acid capric acid at
Point.
Embodiment two
A kind of quick-fried pearl essential oil of cigarette is prepared into using cigarette provided in embodiment one with the preparation method of quick-fried pearl essential oil
It arrives.
Embodiment three
Cigarette is made with quick-fried pearl with quick-fried pearl essential oil in cigarette provided in embodiment two by a kind of application of the quick-fried pearl essential oil of cigarette,
For in cigarette.Quick-fried pearl essential oil is used to prepare cigarette quick-fried pearl as oil-soluble content the cigarette, with quick-fried pearl wall material compatibility
Good, quick-fried pearl molding qualification rate is high.By the quick-fried pearl in cigarette filter pinch it is quick-fried after, the faint scent of emblic pulp is obvious, with this perfume of tobacco
In conjunction with coordination, the soft exquisiteness of flue gas promotes the production of body fluid back sweet obvious, significantly improves cigarette in the comfort of sucking process.
It is in certain embodiments, by the cigarette with quick-fried pearl essential oil after Fruit storage 10-20min,
With the dripping pill lapping being placed in pill dripping machine rubber cement tank and be placed in contain ball device in curing agent according to dripping pill manufacture craft
Cigarette is made with quick-fried pearl, and the positioning of quick-fried pearl is applied in filter stick in filter tow forming process.The advantage is that:
(1) raw material selected by the present invention is fresh emblic, and fragrance is more pure and fresh, naturally, oral cavity comfort is good.
(2) compared with traditional solvent extraction technology, the invention has the characteristics that: with the titanium dioxide under supercriticality
Carbon flow body is recycled in the same system as extractant, the solvent, and solvent consumption is small and price is cheap, thus extract at
This is low；Extraction temperature is low, and extraction cycle is short, can be effectively retained the odor characteristic of emblic itself.
(3) main function of Glycerin, mixed triester with caprylic acid capric acid is dispersing and dissolving emblic extract in the present invention, has cost of material
The advantages that low, colorless and odorless, viscosity is low, not oxidizable, stable system.
(4) the quick-fried pearl extract of emblic modulated of the present invention can be used as core material and directly apply in the quick-fried pearl of cigarette, and quick-fried
Pearl wall material has good compatibility, and quick-fried pearl online production ratio of briquetting is high, and the abnormal phenomenon such as permeability, bias, rupture are less.
(5) after pinching brokenly quick-fried pearl in cigarette filter rod, the distinctive faint scent of emblic is obvious, and personalized note is prominent, with cigarette
Draft perfume (or spice) is coordinated, and the soft exquisiteness of flue gas, pleasant impression is comfortable, improves the sense organ comfort level of cigarette.
Some specific embodiments are provided below
Embodiment 1
(1) it rubs, is then placed in extraction kettle after fresh emblic being gone stalk, cleaning, carbon dioxide gas is imported and is extracted
It takes in kettle, contacts carbon dioxide gas with natural material in the supercritical state；Extraction temperature is 50 DEG C, pressure 40MPa,
Extraction time is 3h, is dissolved in the oil-soluble ingredients in emblic in supercritical fluid, collects and extracts from the outlet of separating still
Object.
(2) prepare raw material according to following weight percent: the quick-fried pearl extract of the emblic prepared in step (1) 0.5~
6%, Span80 surfactant 0.08~0.15%, surplus are Glycerin, mixed triester with caprylic acid capric acid；And above-mentioned material is successively put into band
Have in the container of agitating device, under conditions of revolving speed is 200-300r/min under room temperature stirring 1-2h to solution clear,
The as quick-fried pearl essential oil of cigarette.
Embodiment 2
(1) it is rubbed after fresh emblic first being gone stalk, cleaning, is then placed in extraction kettle, carbon dioxide gas is imported
In extraction kettle, contact carbon dioxide gas with natural material in the supercritical state: 55 DEG C of extraction temperature, pressure is
35MPa, extraction time 3h are dissolved in the oil-soluble ingredients in emblic in supercritical fluid, receive from the outlet of separating still
Collect extract.
(2) prepare raw material according to following weight percent: the quick-fried pearl extract of the emblic prepared in step (1) 0.5~
6%, Span80 surfactant 0.08~0.15%, surplus are Glycerin, mixed triester with caprylic acid capric acid；And above-mentioned material is successively put into band
Have in the container of agitating device, under conditions of revolving speed is 200-300r/min under room temperature stirring 1-2h to solution clear,
The as quick-fried pearl essential oil of cigarette.
Embodiment 3
(1) it rubs, is then placed in extraction kettle after fresh emblic being gone stalk, cleaning, carbon dioxide gas is imported and is extracted
It takes in kettle, contacts carbon dioxide gas with natural material in the supercritical state: 40 DEG C of extraction temperature, pressure 45MPa,
Extraction time is 4h, is dissolved in the oil-soluble ingredients in emblic in supercritical fluid, collects and extracts from the outlet of separating still
Object.
(2) prepare raw material according to following weight percent: the quick-fried pearl extract of the emblic prepared in step (1) 0.5~
6%, Span80 surfactant 0.08~0.15%, surplus are Glycerin, mixed triester with caprylic acid capric acid；And above-mentioned material is successively put into band
Have in the container of agitating device, under conditions of revolving speed is 200-300r/min under room temperature stirring 1-2h to solution clear,
The as quick-fried pearl essential oil of cigarette.
Embodiment 4
By the quick-fried pearl essential oil of the cigarette prepared in embodiment 1, after Fruit storage 10-20min, referring to the quick-fried pearl of cigarette
Conventional production process, with the dripping pill lapping being placed in pill dripping machine rubber cement tank and be placed in contain ball device in curing agent according to
Cigarette is made with quick-fried pearl in the manufacture craft of dripping pill, and detects the performance for preparing quick-fried pearl, and testing result shows: cigarette is made with quick-fried pearl essential oil
For oil-soluble content, there is good compatibility with quick-fried pearl wall material, the quick-fried online molding effect of pearl is stablized, and product qualification rate reaches
98% or more, the abnormal phenomenon such as solid pearl, permeability, bias, rupture are few.
Embodiment 5
By the quick-fried pearl essential oil of the cigarette prepared in embodiment 1-3, respectively after Fruit storage 10-20min, referring to volume
The conventional production process of the quick-fried pearl of cigarette, with the dripping pill lapping being placed in pill dripping machine rubber cement tank and as the solidification contained in ball device
Cigarette is made with quick-fried pearl according to the manufacture craft of dripping pill in agent, and the positioning of quick-fried pearl is applied to filter stick in filter tow forming process
In, three kinds of cigarette are made, and evaluated referring to State Bureau's evaluation standard, quick-fried pearl is pinched in aspiration procedure.The group of smokeing panel test has
10 cigarette sensory evaluation experts composition using secretly commenting mode to carry out sensory evaluation and give a mark, and is compared with blank cigarette,
Its Analyses Methods for Sensory Evaluation Results is as shown in table 1.
The quick-fried pearl cigarette sensory effects evaluation result of table 1
| Sample | Blank 1 | Blank 2 | Embodiment 1 | Embodiment 2 | Embodiment 3 |
| Mean scores | 81.3 | 81.6 | 87.5 | 88.2 | 87.9 |
It can be seen that the quick-fried pearl prepared using emblic extract by above-mentioned smoking result, during the smoking process
Pinch it is quick-fried after, sensory effects evaluation score significantly improve, effect is more significant.The distinctive faint scent of emblic is obvious, personalized note
It is prominent, coordinate with this perfume of tobacco, the soft exquisiteness of flue gas, pleasant impression is comfortable, improves the sense organ comfort level of cigarette.
Specific embodiments of the present invention are described above.It is to be appreciated that the invention is not limited to above-mentioned
Particular implementation, those skilled in the art can make various deformations or amendments within the scope of the claims, this not shadow
Ring substantive content of the invention.
Claims (9)
1. a kind of cigarette preparation method of quick-fried pearl essential oil, it is characterised in that:
It is formed by the material allocation of following weight percent:
The quick-fried pearl extract 0.5~6% of emblic
Span80 surfactant 0.08~0.15%
Glycerin, mixed triester with caprylic acid capric acid surplus；
The quick-fried pearl extract of emblic is to extract to obtain by supercritical extraction with emblic raw material.
2. the cigarette as described in claim 1 preparation method of quick-fried pearl essential oil, it is characterised in that: the quick-fried pearl extract of emblic
Extraction include: to go to obstruct by fresh emblic, rubbed after cleaning, then using the CO 2 fluid under supercriticality as extraction
Solvent is taken to carry out supercritical extract.
3. the cigarette as claimed in claim 2 preparation method of quick-fried pearl essential oil, it is characterised in that: the temperature of the supercritical extract
It is 30-60 DEG C.
4. the cigarette as claimed in claim 2 preparation method of quick-fried pearl essential oil, it is characterised in that: the pressure of the supercritical extract
For 35-45MPa.
5. the cigarette as claimed in claim 2 preparation method of quick-fried pearl essential oil, it is characterised in that: the duration of the supercritical extract
For 2-4h.
6. the cigarette as described in claim 1 preparation method of quick-fried pearl essential oil, it is characterised in that: further include mixing all raw materials
After be stirred.
7. the cigarette as claimed in claim 6 preparation method of quick-fried pearl essential oil, it is characterised in that: the revolving speed of the stirring is 200-
300r/min, the when a length of 1-2h of stirring.
8. a kind of quick-fried pearl essential oil of cigarette, it is characterised in that: using the system of quick-fried pearl essential oil of cigarette described in claim any one of 1-7
Preparation Method is prepared.
9. a kind of application of quick-fried pearl essential oil of cigarette, it is characterised in that: with quick-fried pearl essential oil cigarette will be made by cigarette as claimed in claim 8
With quick-fried pearl, it is used in cigarette.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201910354573.7A CN110184121A (en) | 2019-04-29 | 2019-04-29 | Cigarette quick-fried pearl essential oil and the preparation method and application thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201910354573.7A CN110184121A (en) | 2019-04-29 | 2019-04-29 | Cigarette quick-fried pearl essential oil and the preparation method and application thereof |
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| Publication Number | Publication Date |
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| CN110184121A true CN110184121A (en) | 2019-08-30 |
Family
ID=67715295
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| CN201910354573.7A Pending CN110184121A (en) | 2019-04-29 | 2019-04-29 | Cigarette quick-fried pearl essential oil and the preparation method and application thereof |
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Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4490398A (en) * | 1979-08-02 | 1984-12-25 | Henkel Kommanditgesellschaft Auf Aktien | Process for the preparation of spice extracts |
| EP0338831A2 (en) * | 1988-04-21 | 1989-10-25 | R.J. Reynolds Tobacco Company | Process for providing tobacco extracts |
| CN1568841A (en) * | 2004-04-28 | 2005-01-26 | 李聪 | Application of emblic leafflower fruit extract as free radical scavenger of tobacco products and relevant tobacco products thereof |
| CN106668117A (en) * | 2016-12-27 | 2017-05-17 | 云南中烟工业有限责任公司 | Supercritical extraction method capable of improving taste ability of fructus phyllanthi polyphenol |
| CN108004024A (en) * | 2018-01-16 | 2018-05-08 | 武汉黄鹤楼香精香料有限公司 | A kind of ginkgo leaf cigarette is applied with quick-fried pearl essential oil and preparation method thereof and in cigarette |
-
2019
- 2019-04-29 CN CN201910354573.7A patent/CN110184121A/en active Pending
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4490398A (en) * | 1979-08-02 | 1984-12-25 | Henkel Kommanditgesellschaft Auf Aktien | Process for the preparation of spice extracts |
| EP0338831A2 (en) * | 1988-04-21 | 1989-10-25 | R.J. Reynolds Tobacco Company | Process for providing tobacco extracts |
| CN1568841A (en) * | 2004-04-28 | 2005-01-26 | 李聪 | Application of emblic leafflower fruit extract as free radical scavenger of tobacco products and relevant tobacco products thereof |
| CN106668117A (en) * | 2016-12-27 | 2017-05-17 | 云南中烟工业有限责任公司 | Supercritical extraction method capable of improving taste ability of fructus phyllanthi polyphenol |
| CN108004024A (en) * | 2018-01-16 | 2018-05-08 | 武汉黄鹤楼香精香料有限公司 | A kind of ginkgo leaf cigarette is applied with quick-fried pearl essential oil and preparation method thereof and in cigarette |
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Application publication date: 20190830 |