CN110151652A - There is the lotion and preparation method thereof of anti-aging containing Flos Nelumbinis extract - Google Patents

There is the lotion and preparation method thereof of anti-aging containing Flos Nelumbinis extract Download PDF

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Publication number
CN110151652A
CN110151652A CN201910489463.1A CN201910489463A CN110151652A CN 110151652 A CN110151652 A CN 110151652A CN 201910489463 A CN201910489463 A CN 201910489463A CN 110151652 A CN110151652 A CN 110151652A
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phase
group
flos nelumbinis
grouped
parts
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CN110151652B (en
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廖文贵
杨述义
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Guangzhou Micro Peptide Biological Science And Technology Co Ltd
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Guangzhou Micro Peptide Biological Science And Technology Co Ltd
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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/33Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
    • A61K8/34Alcohols
    • A61K8/342Alcohols having more than seven atoms in an unbroken chain
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/40Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
    • A61K8/41Amines
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/55Phosphorus compounds
    • A61K8/553Phospholipids, e.g. lecithin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/67Vitamins
    • A61K8/678Tocopherol, i.e. vitamin E
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/73Polysaccharides
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/73Polysaccharides
    • A61K8/735Mucopolysaccharides, e.g. hyaluronic acid; Derivatives thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/81Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions involving only carbon-to-carbon unsaturated bonds
    • A61K8/8141Compositions of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides or nitriles thereof; Compositions of derivatives of such polymers
    • A61K8/8147Homopolymers or copolymers of acids; Metal or ammonium salts thereof, e.g. crotonic acid, (meth)acrylic acid; Compositions of derivatives of such polymers
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • A61K8/9706Algae
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • A61K8/9783Angiosperms [Magnoliophyta]
    • A61K8/9789Magnoliopsida [dicotyledons]
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • A61K8/9783Angiosperms [Magnoliophyta]
    • A61K8/9794Liliopsida [monocotyledons]
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • A61Q19/08Anti-ageing preparations
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/40Chemical, physico-chemical or functional or structural properties of particular ingredients
    • A61K2800/59Mixtures
    • A61K2800/592Mixtures of compounds complementing their respective functions

Abstract

The invention belongs to cosmetic technical fields, propose a kind of lotion and preparation method thereof containing Flos Nelumbinis extract with anti-aging, including A phase, B phase, C phase and D phase, wherein, A phase is composed of the following components: saualane, jojoba seed oil, shea butter, cetostearyl alcohol, tocopherol acetate;B phase is composed of the following components: glycerol, butanediol, plant lactic fermentation rice, hydrolecithin, carbomer, xanthan gum, Sodium Hyaluronate, algae extract, fragrant fresh ketone, 1,2- hexylene glycol;C phase is composed of the following components: triethanolamine;D phase is composed of the following components: Flos Nelumbinis extract, essence.Through the above technical solutions, solving the problems, such as that the skin care item with anti-oxidation efficacy can not fundamentally prevent the generation of natural aging in the prior art.

Description

There is the lotion and preparation method thereof of anti-aging containing Flos Nelumbinis extract
Technical field
The invention belongs to cosmetic technical field, be related to it is a kind of containing Flos Nelumbinis extract have anti-aging lotion and its Preparation method.
Background technique
Aging, it may be said that be that the worried most of women of the common maximum of global women is deep is aggravated by because the age increases The puzzlement of the skin problem such as color spot, wrinkle, relaxation, has survey report to point out, in the women of 30~59 years old now age bracket, nearly 85% At concern " anti-aging ".
The aging of skin can be divided into light aging and natural aging two major classes.Light aging refers to the work generated after ultraviolet light irradiation Property oxygen cell DNA is caused to damage, cause skin to generate color spot, wrinkle, the symptoms such as relaxation.During this, ultraviolet light is to flesh The influence of skin aging is huge, therefore some sunscreen products are necessary the protection of ultraviolet light;But even if carry out ultraviolet light Protection can not also prevent natural aging, and along with the growth at age, life entity function falls into a decline, therefore natural aging also produces It is raw.Wherein active oxygen is currently to think the main reason for causing natural aging.So more on the market with anti-oxidation efficacy Skin care item can play partial action for natural aging, but still can not fundamentally prevent the generation of natural aging.
Summary of the invention
The present invention proposes a kind of lotion and preparation method thereof containing Flos Nelumbinis extract with anti-aging, solves existing Leading to the problem of for natural aging can not fundamentally be prevented by having the skin care item of anti-oxidation efficacy in technology.
The technical scheme of the present invention is realized as follows:
A kind of lotion containing Flos Nelumbinis extract with anti-aging, including A phase, B phase, C phase and D phase,
The A phase is composed of the following components:
Saualane, jojoba seed oil, shea butter, cetostearyl alcohol, tocopherol acetate;
The B phase is composed of the following components:
Glycerol, butanediol, plant lactic fermentation rice, hydrolecithin, carbomer, xanthan gum, Sodium Hyaluronate, algae are extracted Object, fragrant fresh ketone, 1,2- hexylene glycol;
The C phase is composed of the following components:
Triethanolamine;
The D phase is composed of the following components:
Flos Nelumbinis extract, essence.
As further technical solution, the A phase is grouped as by the group of following parts by weight:
1~5 part of saualane, 1~5 part of jojoba seed oil, 1~3 part of shea butter, 1~5 part of cetostearyl alcohol, tocopherol 0.1~1 part of acetic acid esters;
The B phase is grouped as by the group of following parts by weight:
1~8 part of glycerol, 1~10 part of butanediol, 0.5~3 part of plant lactic fermentation rice, 0.1~1 part of hydrolecithin, card It is 0.01~0.5 part of wave nurse, 0.01~0.5 part of xanthan gum, 0.01~0.1 part of Sodium Hyaluronate, 0.1~5 part of algae extract, fragrant fresh 0.1~1 part of ketone, 1,2- 0.1~1 part of hexylene glycol;
The C phase is grouped as by the group of following parts by weight:
0.01~0.5 part of triethanolamine;
The D phase is grouped as by the group of following parts by weight:
0.1~3 part of Flos Nelumbinis extract, 0.01~0.2 part of essence.
As further technical solution, the A phase is grouped as by the group of following parts by weight:
1~3 part of saualane, 1~3 part of jojoba seed oil, 1~2 part of shea butter, 1~3 part of cetostearyl alcohol, tocopherol 0.1~0.5 part of acetic acid esters;
The B phase is grouped as by the group of following parts by weight:
1~5 part of glycerol, 1~5 part of butanediol, 1~2 part of plant lactic fermentation rice, 0.3~1 part of hydrolecithin, card wave 0.05~0.3 part of nurse, 0.05~0.3 part of xanthan gum, 0.05~0.1 part of Sodium Hyaluronate, 0.1~3 part of algae extract, fragrant fresh ketone 0.5~1 part, 1,2- 0.5~1 part of hexylene glycol;
The C phase is grouped as by the group of following parts by weight:
0.05~0.3 part of triethanolamine;
The D phase is grouped as by the group of following parts by weight:
0.5~3 part of Flos Nelumbinis extract, 0.05~0.2 part of essence.
As further technical solution, the A phase is grouped as by the group of following parts by weight:
2 parts of saualane, 1.5 parts of jojoba seed oil, 1 part of shea butter, 2.5 parts of cetostearyl alcohol, tocopherol acetate 0.2 Part;
The B phase is grouped as by the group of following parts by weight:
4 parts of glycerol, 2 parts of butanediol, 1.5 parts of plant lactic fermentation rice, 0.3 part of hydrolecithin, 0.1 part of carbomer, the Chinese 0.1 part of raw rubber, 0.05 part of Sodium Hyaluronate, 23 parts of algae extract, fragrant 0.5 part of fresh ketone, 1,2- 0.5 part of hexylene glycol;
The C phase is grouped as by the group of following parts by weight:
0.1 part of triethanolamine;
The D phase is grouped as by the group of following parts by weight:
2 parts of Flos Nelumbinis extract, 0.1 part of essence.
It is including following the invention also provides a kind of preparation method of lotion containing Flos Nelumbinis extract with anti-aging Step:
S1. according to a kind of formula of above-mentioned lotion containing Flos Nelumbinis extract with anti-aging, each phase raw material is weighed It is spare;
S2. each raw material of B phase is mixed, is heated with stirring to 82 DEG C, homogeneous 5 minutes, the B phase raw material after obtaining homogeneous;
S3. each raw material of A phase is mixed, is heated with stirring to 82 DEG C, keep the temperature 10 minutes, the A phase raw material after being heated;
S4. the A phase raw material after step S3 being heated filters in the B phase raw material after obtaining homogeneous to step S2, homogeneous 5 Minute, insulated and stirred 20 minutes, obtain just mixing;
S5. first mixing step S4 obtained cools to 50 DEG C, and C phase is added, and stirs 15 minutes, obtains mixed material;
S6. the obtained mixed material of step S5 is cooled to 40 DEG C, D phase is added, stirred 10 minutes, discharging obtains one kind There is the lotion of anti-aging containing Flos Nelumbinis extract.
As further technical solution, homogeneous is specially the homogeneous under the speed of 1500~2500r/min in step S2.
As further technical solution, mixing speed is 600~800r/min in step S2.
As further technical solution, mixing speed is 600~800r/min in step S3.
As further technical solution, homogeneous is specially the homogeneous under the speed of 1500~2500r/min in step S4.
As further technical solution, step S5, the mixing speed in step S6 is 500~600r/min.
It the working principle of the invention and has the beneficial effect that
1, in the present invention, lotion is prepared by A phase, B phase, C phase and D phase raw material, in formula between each phase raw material mutually Cooperation, so that the lotion of preparation is safe and reliable, stability is good, not only has good moisture-keeping efficacy after use, improves skin Wettability, and there is good anti-aging, the wrinkle condition of skin can be improved after use, while making skin-tightening light It is sliding, improve skin brightness, the skin care item with anti-oxidation efficacy can not fundamentally prevent very good solution in the prior art Natural aging is led to the problem of.
2, it the study found that natural aging has its source in abnormal mitochondria accumulation, accumulates with age and constantly Abnormal mitochondria results in the aging of skin.Mitochondria is that our intracellular maximum active oxygens generate organ, since the age increases Long, mitochondria is damaged, and causes to operate not normal, loses normal function, ultimately becomes abnormal mitochondria.Contain in Flos Nelumbinis extract There is the active constituent by extracting in lotus flower, start with from the root of natural aging, enhances the autophagy function of mitochondria, effectively reduce The accumulation of abnormal mitochondria, Scavenger of ROS, autophagy isolation digest abnormal mitochondria, and inhibition causes the different of skin self deterioration The generation of normal mitochondria, is different from anti-aging product conventional on the market, and not simple going is anti-oxidant, attacks aging root directly This reason provides new solution for anti-aging, after Flos Nelumbinis extract plays a role, skin can be allowed to distribute from inside to outside Youth, is effectively improved wrinkle, improves that skin is coarse, the skin agings problem such as obscure.Applicant has found during the test, individually Flos Nelumbinis extract is added in lotion, the effect of Flos Nelumbinis extract can not bring into play well, the anti-aging effects of lotion It is not that very significantly, in the present invention, by compounding Flos Nelumbinis extract with tocopherol acetate, algae extract, can sufficiently send out The effect of waving Flos Nelumbinis extract, enhancing improve the anti-aging effects of lotion.
3, in the present invention, Sodium Hyaluronate and triethanolamine, algae extract cooperate, and protect well so that lotion has Wet effect, is obviously improved the wettability of skin, the addition of tocopherol acetate and algae extract, and auxiliary enhances Flos Nelumbinis extract Anti-aging effects, cetostearyl alcohol and Sodium Hyaluronate, plant lactic fermentation rice, tocopherol acetate act synergistically so that The lotion of preparation keeps skin more compact smooth after being used for skin, and hydrolecithin and plant lactic fermentation rice, carbomer, the Chinese are raw The mutual compatibility of glue, triethanolamine, significantly improves emulsion intercalation method, and lotion is made to place three in 40 DEG C of electro-heating standing-temperature cultivators Phenomena such as after restoring after a month to room temperature without permeability, bleed, demulsification, standing time length, long service life.
Specific embodiment
Below in conjunction with the embodiment of the present invention, technical scheme in the embodiment of the invention is clearly and completely described, Obviously, described embodiments are only a part of the embodiments of the present invention, instead of all the embodiments.Based in the present invention Embodiment, every other embodiment obtained by those of ordinary skill in the art without making creative efforts, all Belong to the scope of protection of the invention.
Embodiment 1
A kind of lotion containing Flos Nelumbinis extract with anti-aging, including A phase, B phase, C phase and D phase, wherein
A phase is grouped as by the group of following parts by weight:
1~5 part of saualane, 1~5 part of jojoba seed oil, 1~3 part of shea butter, 1~5 part of cetostearyl alcohol, tocopherol 0.1~1 part of acetic acid esters;
B phase is grouped as by the group of following parts by weight:
1~8 part of glycerol, 1~10 part of butanediol, 0.5~3 part of plant lactic fermentation rice, 0.1~1 part of hydrolecithin, card It is 0.01~0.5 part of wave nurse, 0.01~0.5 part of xanthan gum, 0.01~0.1 part of Sodium Hyaluronate, 0.1~5 part of algae extract, fragrant fresh 0.1~1 part of ketone, 1,2- 0.1~1 part of hexylene glycol;
C phase is grouped as by the group of following parts by weight:
0.01~0.5 part of triethanolamine;
D phase is grouped as by the group of following parts by weight:
0.1~3 part of Flos Nelumbinis extract, 0.01~0.2 part of essence;
Preparation method includes the following steps:
S1. according to above-mentioned formula, each phase raw material for standby is weighed;
S2. each raw material of B phase is added in emulsion pot, is stirred under the speed of 600~800r/min, is heated to 82 DEG C Homogeneous 5 minutes under the speed of 1500~2500r/min afterwards, the B phase raw material after obtaining homogeneous, heat preservation for standby use;
S3. each raw material of A phase is added in oily phase pot and is mixed, be stirred, be heated under the speed of 600~800r/min 82 DEG C, 10 minutes are kept the temperature, the A phase raw material after being heated;
S4. the A phase raw material after heating that step S3 is obtained slowly is filtered in emulsion pot, in 1500~2500r/min Speed under homogeneous 5 minutes, insulated and stirred 20 minutes under the speed of 500~600r/min, obtain just mixing;
S5. first mixing step S4 obtained cools to 50 DEG C, and C phase raw material is added, and stirs 15 minutes, obtains mixture Material;
S6. the obtained mixed material of step S5 is cooled to 40 DEG C, D phase raw material is added, stirred 10 minutes, discharging obtains A kind of lotion containing Flos Nelumbinis extract with anti-aging.
Embodiment 2
A kind of lotion containing Flos Nelumbinis extract with anti-aging, including A phase, B phase, C phase and D phase, wherein
A phase is grouped as by the group of following parts by weight:
1~5 part of saualane, 1~5 part of jojoba seed oil, 1~3 part of shea butter, 1~5 part of cetostearyl alcohol, tocopherol 0.1~1 part of acetic acid esters;
B phase is grouped as by the group of following parts by weight:
1~8 part of glycerol, 1~10 part of butanediol, 0.5~3 part of plant lactic fermentation rice, 0.1~1 part of hydrolecithin, card It is 0.01~0.5 part of wave nurse, 0.01~0.5 part of xanthan gum, 0.01~0.1 part of Sodium Hyaluronate, 0.1~5 part of algae extract, fragrant fresh 0.1~1 part of ketone, 1,2- 0.1~1 part of hexylene glycol;
C phase is grouped as by the group of following parts by weight:
0.01~0.5 part of triethanolamine;
D phase is grouped as by the group of following parts by weight:
0.1~3 part of Flos Nelumbinis extract, 0.01~0.2 part of essence;
Preparation method is the same as embodiment 1.
Embodiment 3
A kind of lotion containing Flos Nelumbinis extract with anti-aging, including A phase, B phase, C phase and D phase, wherein
A phase is grouped as by the group of following parts by weight:
1~3 part of saualane, 1~3 part of jojoba seed oil, 1~2 part of shea butter, 1~3 part of cetostearyl alcohol, tocopherol 0.1~0.5 part of acetic acid esters;
B phase is grouped as by the group of following parts by weight:
1~5 part of glycerol, 1~5 part of butanediol, 1~2 part of plant lactic fermentation rice, 0.3~1 part of hydrolecithin, card wave 0.05~0.3 part of nurse, 0.05~0.3 part of xanthan gum, 0.05~0.1 part of Sodium Hyaluronate, 0.1~3 part of algae extract, fragrant fresh ketone 0.5~1 part, 1,2- 0.5~1 part of hexylene glycol;
C phase is grouped as by the group of following parts by weight:
0.05~0.3 part of triethanolamine;
D phase is grouped as by the group of following parts by weight:
0.5~3 part of Flos Nelumbinis extract, 0.05~0.2 part of essence;
Preparation method is the same as embodiment 1.
Embodiment 4
A kind of lotion containing Flos Nelumbinis extract with anti-aging, including A phase, B phase, C phase and D phase, wherein
A phase is grouped as by the group of following parts by weight:
1~3 part of saualane, 1~3 part of jojoba seed oil, 1~2 part of shea butter, 1~3 part of cetostearyl alcohol, tocopherol 0.1~0.5 part of acetic acid esters;
B phase is grouped as by the group of following parts by weight:
1~5 part of glycerol, 1~5 part of butanediol, 1~2 part of plant lactic fermentation rice, 0.3~1 part of hydrolecithin, card wave 0.05~0.3 part of nurse, 0.05~0.3 part of xanthan gum, 0.05~0.1 part of Sodium Hyaluronate, 0.1~3 part of algae extract, fragrant fresh ketone 0.5~1 part, 1,2- 0.5~1 part of hexylene glycol;
C phase is grouped as by the group of following parts by weight:
0.05~0.3 part of triethanolamine;
D phase is grouped as by the group of following parts by weight:
0.5~3 part of Flos Nelumbinis extract, 0.05~0.2 part of essence;
Preparation method is the same as embodiment 1.
Embodiment 5
A kind of lotion containing Flos Nelumbinis extract with anti-aging, including A phase, B phase, C phase and D phase, wherein
A phase is grouped as by the group of following parts by weight:
2 parts of saualane, 1.5 parts of jojoba seed oil, 1 part of shea butter, 2.5 parts of cetostearyl alcohol, tocopherol acetate 0.2 Part;
B phase is grouped as by the group of following parts by weight:
4 parts of glycerol, 2 parts of butanediol, 1.5 parts of plant lactic fermentation rice, 0.3 part of hydrolecithin, 0.1 part of carbomer, the Chinese 0.1 part of raw rubber, 0.05 part of Sodium Hyaluronate, 23 parts of algae extract, fragrant 0.5 part of fresh ketone, 1,2- 0.5 part of hexylene glycol;
C phase is grouped as by the group of following parts by weight:
0.1 part of triethanolamine;
D phase is grouped as by the group of following parts by weight:
2 parts of Flos Nelumbinis extract, 0.1 part of essence;
Preparation method is the same as embodiment 1.
Comparative example 1
A kind of lotion, including A phase, B phase, C phase and D phase, wherein
A phase is grouped as by the group of following parts by weight:
2 parts of saualane, 1.5 parts of jojoba seed oil, 1 part of shea butter, 2.5 parts of cetostearyl alcohol, tocopherol acetate 0.2 Part;
B phase is grouped as by the group of following parts by weight:
4 parts of glycerol, 2 parts of butanediol, 1.5 parts of plant lactic fermentation rice, 0.3 part of hydrolecithin, 0.1 part of carbomer, the Chinese 0.1 part of raw rubber, 0.05 part of Sodium Hyaluronate, 23 parts of algae extract, fragrant 0.5 part of fresh ketone, 1,2- 0.5 part of hexylene glycol;
C phase is grouped as by the group of following parts by weight:
0.1 part of triethanolamine;
D phase is grouped as by the group of following parts by weight:
0.1 part of essence;
Flos Nelumbinis extract is deleted in the corresponding D phase raw material by step S6 of preparation method, remaining step is the same as embodiment 1.
Comparative example 2
A kind of lotion containing Flos Nelumbinis extract with anti-aging, including A phase, B phase and D phase, wherein
A phase is grouped as by the group of following parts by weight:
2 parts of saualane, 1.5 parts of jojoba seed oil, 1 part of shea butter, 2.5 parts of cetostearyl alcohol, tocopherol acetate 0.2 Part;
B phase is grouped as by the group of following parts by weight:
4 parts of glycerol, 2 parts of butanediol, 1.5 parts of plant lactic fermentation rice, 0.3 part of hydrolecithin, 0.1 part of carbomer, card 0.1 part of wave nurse, fragrant 0.5 part of fresh ketone, 1,2- 0.5 part of hexylene glycol;
D phase is grouped as by the group of following parts by weight:
2 parts of Flos Nelumbinis extract, 0.1 part of essence;
Sodium Hyaluronate, algae extract are deleted in the corresponding B phase raw material by step S2 of preparation method, and step S5 is deleted It removes, remaining step is the same as embodiment 1.
Comparative example 3
A phase is grouped as by the group of following parts by weight:
2 parts of saualane, 1.5 parts of jojoba seed oil, 1 part of shea butter, 2.5 parts of cetostearyl alcohol;
B phase is grouped as by the group of following parts by weight:
4 parts of glycerol, 2 parts of butanediol, 1.5 parts of plant lactic fermentation rice, 0.3 part of hydrolecithin, 0.1 part of carbomer, the Chinese 0.1 part of raw rubber, 0.05 part of Sodium Hyaluronate, 23 parts of algae extract, fragrant 0.5 part of fresh ketone, 1,2- 0.5 part of hexylene glycol;
C phase is grouped as by the group of following parts by weight:
0.1 part of triethanolamine;
D phase is grouped as by the group of following parts by weight:
2 parts of Flos Nelumbinis extract, 0.1 part of essence;
Tocopherol acetate is deleted in the corresponding B phase raw material by step S2 of preparation method, the same embodiment of remaining step 1。
Comparative example 4
A phase is grouped as by the group of following parts by weight:
2 parts of saualane, 1.5 parts of jojoba seed oil, 1 part of shea butter, 2.5 parts of cetostearyl alcohol, tocopherol acetate 0.2 Part;
B phase is grouped as by the group of following parts by weight:
4 parts of glycerol, 2 parts of butanediol, 1.5 parts of plant lactic fermentation rice, 0.3 part of hydrolecithin, 0.1 part of carbomer, the Chinese 0.1 part of raw rubber, 0.05 part of Sodium Hyaluronate, 23 parts of algae extract, fragrant 0.5 part of fresh ketone, 1,2- 0.5 part of hexylene glycol;
C phase is grouped as by the group of following parts by weight:
0.1 part of triethanolamine;
D phase is grouped as by the group of following parts by weight:
2 parts of Flos Nelumbinis extract, 0.1 part of essence;
Plant lactic fermentation rice, carbomer, xanthan gum are deleted in the corresponding B phase raw material by step S2 of preparation method, Remaining step is the same as embodiment 1.
The lotion prepared to above-described embodiment 1~5 and comparative example 1~4 performs the following performance tests:
1, Micro biological Tests: according in method testing product specified in " cosmetics safety technical specification (version in 2015) " The projects such as total number of bacteria, mould/saccharomycete sum, heat-resisting coliform, staphylococcus aureus, pseudomonas aeruginosa;
2, stability: restore after product to be detected is placed three months in 40 DEG C of electro-heating standing-temperature cultivators to room temperature, see Examine product whether there is or not permeability, bleed, demulsification phenomena such as;
The Micro biological Tests result of lotion prepared by 1 Examples 1 to 5 of table and comparative example 1~4
Note: in upper table, *, which must not indicate, to be detected, -- expression is not detected.
It can be seen from the data in Table 1 that total number of bacteria < 10/ in the product emulsion of Examples 1 to 5 and comparative example 1~4 ML, mould/saccharomycete sum < 10/mL, heat-resisting coliform, staphylococcus aureus, pseudomonas aeruginosa are not detected, micro- Bioassay meets the requirement of " cosmetics safety technical specification (version in 2015) " as the result is shown, illustrates lotion prepared by the present invention Securely and reliably.
Emulsion intercalation method measurement result prepared by 2 Examples 1 to 5 of table and comparative example 1~4
Group Stability
Embodiment 1 Phenomena such as no permeability, bleed, demulsification
Embodiment 2 Phenomena such as no permeability, bleed, demulsification
Embodiment 3 Phenomena such as no permeability, bleed, demulsification
Embodiment 4 Phenomena such as no permeability, bleed, demulsification
Embodiment 5 Phenomena such as no permeability, bleed, demulsification
Comparative example 1 Phenomena such as no permeability, bleed, demulsification
Comparative example 2 There are demulsification, bleed phenomenon
Comparative example 3 Phenomena such as no permeability, bleed, demulsification
Comparative example 4 There is demulsifying phenomenon
It can be seen from the data in Table 2 that lotion prepared by Examples 1 to 5 and comparative example 1~4 is trained in 40 DEG C of electric heating constant temperatures It supports and restores after being placed three months in case to room temperature, the product emulsion of Examples 1 to 5 preparation is existing without permeability, bleed, demulsification etc. As illustrating that lotion prepared by the present invention is with good stability, standing time length, long service life.
Using effect evaluation: tested 180 people of crowd between 30~55 years old age, is divided into 9 groups, every group of 20 people, skin Meet subject enrollment standard.Given the test agent is the lotion prepared in Examples 1 to 5 and comparative example 1~4.9 groups use respectively Given the test agent is stated, wherein the lotion that 1 group 1 is prepared with embodiment 1, the lotion made from embodiment 2 of group 2, the implementation of group 3 Lotion made from example 3, the lotion made from embodiment 4 of group 4, the lotion made from embodiment 5 of group 5, group 6 use comparative example Lotion made from 1, the lotion made from embodiment 2 of group 7, the lotion made from embodiment 3 of group 3, the embodiment 3 of group 3 Application method: lotion obtained, the lotion made from embodiment 3 of group 3 use the lotion sooner or later daily, are massaged into absorption, hold It is continuous to use 45 days, it then collects as a result, summarize data, see the table below:
The using effect evaluation result of lotion prepared by 3 Examples 1 to 5 of table and comparative example 1~4
Group Slickness Wettability Compact sense Wrinkled appearance Skin brightness
Group 1 +++ +++ ++++ ++++ +++
Group 2 +++ +++ ++++ ++++ +++
Group 3 +++ ++++ ++++ ++++ +++
Group 4 +++ ++++ ++++ ++++ +++
Group 5 ++++ ++++ ++++ ++++ +++
Group 6 + +++ + It is unchanged +
Group 7 + + ++ ++ ++
Group 8 ++ ++ + + ++
Group 9 + + It is unchanged + +
Note :+indicate slight change, ++ expression changes, +++ indicate significant change, ++++indicate pole significant change.
From table 3 it is observed that being prepared compared with lotion prepared by comparative example 1~4 using the embodiment of the present invention 1~5 Slickness, wettability, compact sense, wrinkled appearance and the skin brightness of subject's cheek skin of lotion have obvious and and obvious Variation illustrate lotion prepared by the present invention not only there is good moistening effect, but also play good anti-aging effects, The wettability of skin can not only be improved after use, but also improve the wrinkle condition of skin, so that the skin of user more steps up Cause smooth, skin brightness is more preferable.
Compared with the lotion of Examples 1 to 5, after the lotion of comparative example 1 does not have anti-aging effects, subject to use 45 days Cheek wrinkle of skin appearance is unchanged, and skin-tightening sense, slickness and skin brightness change unobvious, the lotion of comparative example 1 It is not added with Flos Nelumbinis extract in formula, illustrates that Flos Nelumbinis extract is added in lotion in the present invention, lotion can be significantly improved Anti-aging, subject using after the lotion of addition Flos Nelumbinis extract skin smoothness, compactness, outside skin brightness and wrinkle Sight has significant change.
Compared with the lotion of comparative example 1~5, the stability of emulsion of comparative example 2 is poor, moisture retention is poor, and subject uses 45 days The slickness of cheek skin only has slight change and wettability afterwards, and the variation of compact sense, skin brightness and wrinkled appearance is also opposite It is smaller, it is not added with Sodium Hyaluronate, triethanolamine, algae extract in the raw material of comparative example 2, illustrates Sodium Hyaluronate and three second The mutual compatibility of hydramine, algae extract, effectively increases emulsion intercalation method and moisture retention, meanwhile, algae extract is to its in formula Its component plays synergistic effect, improves the anti-aging effects of lotion.
Compared with the lotion of comparative example 1~5, the stability of emulsion of comparative example 3 is poor, anti-aging is poor, and subject uses 45 Compact sense of cheek skin and wrinkled appearance only have minor change, skin smoothness, wettability and skin brightness variation after it It is relatively smaller, it is not added with tocopherol acetate in the formula of comparative example 3, illustrates for tocopherol acetate to be added in lotion, with Flos Nelumbinis extract in lotion cooperates, and can significantly improve the anti-aging effects of lotion, and tocopherol acetate is only added It is added without Flos Nelumbinis extract, lotion also without anti-aging effects, illustrates tocopherol acetate and Flos Nelumbinis extract of the invention Play the role of synergy in lotion, tocopherol acetate also with the Sodium Hyaluronate in formula, triethanolamine, algae extract phase Mutually cooperation, improves the moistening effect of lotion.
Compared with the lotion of comparative example 1~5, the stability of emulsion of comparative example 4, anti-aging and moisture retention are poor, The compact sense of cheek skin is unchanged after subject uses 45 days, and slickness, wettability, wrinkled appearance, skin brightness only have micro- Small variation is not added with plant lactic fermentation rice, carbomer, xanthan gum in the formula of comparative example 4, illustrate plant lactic fermentation rice with The mutual compatibility of carbomer, xanthan gum, enhances emulsion intercalation method, to improve the moisture retention and anti-aging effects of lotion.
The above is merely preferred embodiments of the present invention, be not intended to limit the invention, it is all in spirit of the invention and Within principle, any modification, equivalent replacement, improvement and so on be should all be included in the protection scope of the present invention.

Claims (10)

1. a kind of lotion containing Flos Nelumbinis extract with anti-aging, which is characterized in that including A phase, B phase, C phase and D phase,
The A phase is composed of the following components:
Saualane, jojoba seed oil, shea butter, cetostearyl alcohol, tocopherol acetate;
The B phase is composed of the following components:
Glycerol, butanediol, plant lactic fermentation rice, hydrolecithin, carbomer, xanthan gum, Sodium Hyaluronate, algae extract, Fragrant fresh ketone, 1,2- hexylene glycol;
The C phase is composed of the following components:
Triethanolamine;
The D phase is composed of the following components:
Flos Nelumbinis extract, essence.
2. a kind of lotion containing Flos Nelumbinis extract with anti-aging according to claim 1, which is characterized in that described A phase is grouped as by the group of following parts by weight:
1~5 part of saualane, 1~5 part of jojoba seed oil, 1~3 part of shea butter, 1~5 part of cetostearyl alcohol, tocopheryl acetate 0.1~1 part of ester;
The B phase is grouped as by the group of following parts by weight:
1~8 part of glycerol, 1~10 part of butanediol, 0.5~3 part of plant lactic fermentation rice, 0.1~1 part of hydrolecithin, carbomer 0.01~0.5 part, 0.01~0.5 part of xanthan gum, 0.01~0.1 part of Sodium Hyaluronate, 0.1~5 part of algae extract, fragrant fresh ketone 0.1~1 part, 1,2- 0.1~1 part of hexylene glycol;
The C phase is grouped as by the group of following parts by weight:
0.01~0.5 part of triethanolamine;
The D phase is grouped as by the group of following parts by weight:
0.1~3 part of Flos Nelumbinis extract, 0.01~0.2 part of essence.
3. a kind of lotion containing Flos Nelumbinis extract with anti-aging according to claim 1, which is characterized in that described A phase is grouped as by the group of following parts by weight:
1~3 part of saualane, 1~3 part of jojoba seed oil, 1~2 part of shea butter, 1~3 part of cetostearyl alcohol, tocopheryl acetate 0.1~0.5 part of ester;
The B phase is grouped as by the group of following parts by weight:
1~5 part of glycerol, 1~5 part of butanediol, 1~2 part of plant lactic fermentation rice, 0.3~1 part of hydrolecithin, carbomer 0.05~0.3 part, 0.05~0.3 part of xanthan gum, 0.05~0.1 part of Sodium Hyaluronate, 0.1~3 part of algae extract, fragrant fresh ketone 0.5~1 part, 1,2- 0.5~1 part of hexylene glycol;
The C phase is grouped as by the group of following parts by weight:
0.05~0.3 part of triethanolamine;
The D phase is grouped as by the group of following parts by weight:
0.5~3 part of Flos Nelumbinis extract, 0.05~0.2 part of essence.
4. a kind of lotion containing Flos Nelumbinis extract with anti-aging according to claim 1, which is characterized in that described A phase is grouped as by the group of following parts by weight:
2 parts of saualane, 1.5 parts of jojoba seed oil, 1 part of shea butter, 2.5 parts of cetostearyl alcohol, 0.2 part of tocopherol acetate;
The B phase is grouped as by the group of following parts by weight:
4 parts of glycerol, 2 parts of butanediol, 1.5 parts of plant lactic fermentation rice, 0.3 part of hydrolecithin, 0.1 part of carbomer, xanthan gum 0.1 part, 0.05 part of Sodium Hyaluronate, 23 parts of algae extract, fragrant 0.5 part of fresh ketone, 1,2- 0.5 part of hexylene glycol;
The C phase is grouped as by the group of following parts by weight:
0.1 part of triethanolamine;
The D phase is grouped as by the group of following parts by weight:
2 parts of Flos Nelumbinis extract, 0.1 part of essence.
5. a kind of preparation method of the lotion containing Flos Nelumbinis extract with anti-aging, which comprises the following steps:
S1. matching according to a kind of lotion containing Flos Nelumbinis extract with anti-aging described in Claims 1 to 4 any one Side, weighs each phase raw material for standby;
S2. each raw material of B phase is mixed, is heated with stirring to 82 DEG C, homogeneous 5 minutes, the B phase raw material after obtaining homogeneous;
S3. each raw material of A phase is mixed, is heated with stirring to 82 DEG C, keep the temperature 10 minutes, the A phase raw material after being heated;
S4. the A phase raw material after step S3 being heated filters in the B phase raw material after obtaining homogeneous to step S2, and homogeneous 5 divides Clock insulated and stirred 20 minutes, obtains just mixing;
S5. first mixing step S4 obtained cools to 50 DEG C, and C phase is added, and stirs 15 minutes, obtains mixed material;
S6. the obtained mixed material of step S5 is cooled to 40 DEG C, D phase is added, stirred 10 minutes, discharging obtains one kind and contains Flos Nelumbinis extract has the lotion of anti-aging.
6. a kind of preparation method of lotion containing Flos Nelumbinis extract with anti-aging according to claim 5, special Sign is that homogeneous is specially the homogeneous under the speed of 1500~2500r/min in step S2.
7. a kind of preparation method of lotion containing Flos Nelumbinis extract with anti-aging according to claim 5, special Sign is that mixing speed is 600~800r/min in step S2.
8. a kind of preparation method of lotion containing Flos Nelumbinis extract with anti-aging according to claim 5, special Sign is that mixing speed is 600~800r/min in step S3.
9. a kind of preparation method of lotion containing Flos Nelumbinis extract with anti-aging according to claim 5, special Sign is that homogeneous is specially the homogeneous under the speed of 1500~2500r/min in step S4.
10. a kind of preparation method of lotion containing Flos Nelumbinis extract with anti-aging according to claim 5, special Sign is that step S5, the mixing speed in step S6 is 500~600r/min.
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