CN110037961B - Non-irritant oriental cherry sleeping mask - Google Patents
Non-irritant oriental cherry sleeping mask Download PDFInfo
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- CN110037961B CN110037961B CN201910409636.4A CN201910409636A CN110037961B CN 110037961 B CN110037961 B CN 110037961B CN 201910409636 A CN201910409636 A CN 201910409636A CN 110037961 B CN110037961 B CN 110037961B
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9789—Magnoliopsida [dicotyledons]
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/59—Mixtures
- A61K2800/592—Mixtures of compounds complementing their respective functions
- A61K2800/5922—At least two compounds being classified in the same subclass of A61K8/18
Abstract
The invention discloses a preparation method of a non-irritant cerasus grahami sleep mask, and belongs to the field of cosmetics. The non-irritant oriental cherry sleeping mask for light medical treatment consists of the following components in percentage by weight: alcohol humectant: 1.0-30.0%; thickening system: 0.1 to 10.0 percent; active extract: 0.1 to 17.5 percent; a bacteriostatic system: 0.1-2.5%; the remainder being water. The non-irritant light medical beauty cherry blossom sleeping mask disclosed by the invention has the effects of obvious moisturizing effect, refreshing, strong absorptivity, strong skin sticking property, strong air permeability and no-washing, and the skin is tender and tender after being applied, and can be used as a no-washing sleeping mask.
Description
Technical Field
The invention relates to the field of cosmetics, in particular to a non-irritant oriental cherry sleeping mask for light medicine.
Background
The oriental cherry is a plant of the genus oriental cherry of the family rosaceae, and is cultivated all over the world. Foreign research shows that the cherry blossom trees have various biological activities, such as anti-inflammatory activity, antioxidant activity, antibacterial activity and antitumor activity. Purslane is also called Changming grass, longevity vegetable, five-element grass, sour grass and nostoc commune, is the dry overground part of purslane of Portulacaceae, and is recorded in 2015 edition "Chinese pharmacopoeia". Experiments prove that the purslane has the effects of resisting convulsion, relieving cough and asthma, and has certain effects on resisting inflammation, reducing blood fat, reducing blood sugar, resisting oxidation and enhancing immunity. Chamomile is a plant of the genus Matricaria of the family Compositae, which is a perennial herb. Originates from Europe, has the effects of resisting inflammation, inhibiting bacteria, relieving pain and the like, and is widely applied to the fields of medicines, cosmetics and foods.
To date, there are many patents on the separate action of these three compositions, including a cherry blossom mask (application No. 201811290351.5) which teaches the efficacy of a cherry blossom mask; a purslane mask and a preparation method thereof (application number: 201811158217. X) relate to a purslane mask and a preparation method thereof; a facial mask (application No. 201710075643.6) containing flos Matricariae Chamomillae extract for removing red blood streak discloses a facial mask containing flos Matricariae Chamomillae extract for removing red blood streak. The three active substances are compounded to obtain the anti-inflammatory synergistic effect, so that the synergistic effect is not mentioned in the market when the synergistic effect is further used for preparing the nonirritating light medical and beauty sleeping mask.
Meanwhile, most common application type facial masks in the market at present can only be applied for 15 minutes, the mask liquid is almost completely dried after the application time is over, the longer the application time is, the higher the allergy rate is, the more sticky the mask liquid on the face is when the facial mask is used, and the skin is still rough after the mask liquid is dried. In addition, the common application type sleeping mask needs to be cleaned after use, otherwise, the phenomenon of pore blockage is easy to occur, stabbing pain, redness and stuffiness can also occur in use, the feeling of water dryness after cleaning is the same as that of nursing, and the conventional no-clean sleeping mask can only be used in a smearing mode. The research of the novel facial mask mainly solves the problem that the application type facial mask can not be used as a washing-free sleeping facial mask.
Disclosure of Invention
In order to solve the defects of the prior art, the invention provides the non-irritant light medical oriental cherry sleeping mask which has the effects of refreshing, strong absorptivity, strong skin adhesion and strong air permeability, has an excellent moisturizing effect, enables the skin to be tender and tender after being applied, and can be used as a wash-free sleeping mask.
The invention is realized by the following technical scheme:
a nonirritating mild medical oriental cherry sleeping mask comprises the following components in parts by weight:
alcohol humectant: 1.0-30.0%;
thickening system: 0.1 to 10.0 percent;
active extract: 0.1 to 17.5 percent;
a bacteriostatic system: 0.1-2.5%;
the remainder being water.
Further, the non-irritating mild medical cherry blossom sleeping mask comprises the following alcohol moisturizers: at least one or more of propylene glycol, glycerol and butanediol.
Further, the non-irritating mild medical cherry sleeping mask is characterized in that a thickening system is as follows: at least one or more of glycerol polyacrylate, xanthan gum and cellulose.
Further, the non-irritant oriental cherry sleeping mask comprises the following active extracts: a mixture of purslane extract, chamomile extract, and cherry extract.
Further, the bacteriostatic system is: p-hydroxyacetophenone and 1, 2-hexanediol.
The non-irritant light medical beauty cherry blossom sleeping mask has the effects of refreshing, strong absorption, strong skin sticking property, strong air permeability, no-washing and excellent moisturizing effect, and the skin is tender and tender after being applied, and can be used as a no-washing sleeping mask.
A preparation method of a non-irritant oriental cherry sleeping mask comprises the following steps:
step (1): dissolving alcohols and a thickening agent in deionized water, heating at 60-95 ℃, stirring and preserving heat for 30-60 minutes;
step (2): cooling the step (1) to 50-59 ℃, adding an antibacterial system, and stirring for 30-60 minutes;
and (3): cooling the step (2) to 25-49 ℃, adding the active extract, and stirring until the active extract is completely dissolved;
and (4): filling the obtained product in the step (3) into a silk mask cloth/tencel mask cloth mask, and packaging to obtain the product.
Compared with the prior art, the non-irritant cerasus grahami sleep mask uses the anti-allergy and anti-inflammation synergistic effects of the three compound active substances, and simultaneously solves the problem that the application type mask cannot be used as a wash-free sleep mask; the primrose flower sleep mask has long moisturizing time, fresh and cool skin feeling, tender feeling after use and no need of cleaning the facial skin after use; the preparation process is a low-cost, industrialized and recyclable process.
Detailed Description
Examples 1
A nonirritating mild medical oriental cherry sleeping mask comprises the following raw materials in parts by weight:
glycerol polyacrylate: 5.0 percent
Propylene glycol: 5.0 percent
Glycerol: 5.0 percent
Butanediol: 7.0 percent
P-hydroxyacetophenone: 0.5 percent
1, 2-hexanediol: 0.5 percent;
xanthan gum: 0.5 percent;
cellulose: 0.3 percent;
and (3) purslane extract: 1.5 percent;
chamomile extract: 1.5 percent;
cherry extract: 2.0 percent;
the remainder being water.
The preparation method comprises the following steps: step (1): dissolving alcohols and a thickening agent in deionized water, heating at 85 ℃, stirring and keeping the temperature for 45 minutes; step (2): cooling the temperature in the step (1) to 55 ℃, adding a bacteriostasis system, and stirring for 45 minutes; and (3): cooling the temperature in the step (2) to 30 ℃, adding the active extract, and stirring until the active extract is completely dissolved; and (4): filling the obtained product in the step (3) into a silk mask cloth/tencel mask cloth mask, and packaging to obtain the product.
Example 2 of embodiment
A nonirritating mild medical oriental cherry sleeping mask comprises the following raw materials in parts by weight:
glycerol polyacrylate: 5.0 percent
Propylene glycol: 5.0 percent
Glycerol: 5.0 percent
Butanediol: 7.0 percent
P-hydroxyacetophenone: 0.5 percent
1, 2-hexanediol: 0.5 percent;
xanthan gum: 0.5 percent;
cellulose: 0.3 percent;
and (3) purslane extract: 5.0 percent;
the remainder being water.
The preparation method comprises the following steps: step (1): dissolving alcohols and a thickening agent in deionized water, heating at 85 ℃, stirring and keeping the temperature for 45 minutes; step (2): cooling the temperature in the step (1) to 55 ℃, adding a bacteriostasis system, and stirring for 45 minutes; and (3): cooling the temperature in the step (2) to 30 ℃, adding the active extract, and stirring until the active extract is completely dissolved; and (4): filling the obtained product in the step (3) into a silk mask cloth/tencel mask cloth mask, and packaging to obtain the product.
EXAMPLE 3
A nonirritating mild medical oriental cherry sleeping mask comprises the following raw materials in parts by weight:
glycerol polyacrylate: 5.0 percent
Propylene glycol: 5.0 percent
Glycerol: 5.0 percent
Butanediol: 7.0 percent
P-hydroxyacetophenone: 0.5 percent
1, 2-hexanediol: 0.5 percent;
xanthan gum: 0.5 percent;
cellulose: 0.3 percent;
chamomile extract: 5.0 percent;
the remainder being water.
The preparation method comprises the following steps: step (1): dissolving alcohols and a thickening agent in deionized water, heating at 85 ℃, stirring and keeping the temperature for 45 minutes; step (2): cooling the temperature in the step (1) to 55 ℃, adding a bacteriostasis system, and stirring for 45 minutes; and (3): cooling the temperature in the step (2) to 30 ℃, adding the active extract, and stirring until the active extract is completely dissolved; and (4): filling the obtained product in the step (3) into a silk mask cloth/tencel mask cloth mask, and packaging to obtain the product.
Example 4:
a nonirritating mild medical oriental cherry sleeping mask comprises the following raw materials in parts by weight:
glycerol polyacrylate: 5.0 percent
Propylene glycol: 5.0 percent
Glycerol: 5.0 percent
Butanediol: 7.0 percent
P-hydroxyacetophenone: 0.5 percent
1, 2-hexanediol: 0.5 percent;
xanthan gum: 0.5 percent;
cellulose: 0.3 percent;
cherry extract: 5.0 percent;
the remainder being water.
The preparation method comprises the following steps: step (1): dissolving alcohols and a thickening agent in deionized water, heating at 85 ℃, stirring and keeping the temperature for 45 minutes; step (2): cooling the temperature in the step (1) to 55 ℃, adding a bacteriostasis system, and stirring for 45 minutes; and (3): cooling the temperature in the step (2) to 30 ℃, adding the active extract, and stirring until the active extract is completely dissolved; and (4): filling the obtained product in the step (3) into a silk mask cloth/tencel mask cloth mask, and packaging to obtain the product.
Example 5:
a common pasting type facial mask on the market is prepared from the following raw materials in percentage by weight:
carbomer: 0.2 percent of
Triethanolamine: 0.2 percent of
Glycerol: 3 percent of
Methyl paraben: 0.2 percent of
Propyl p-hydroxybenzoate: 0.15 percent
The remainder being water.
The preparation method comprises the following steps: step (1): dissolving alcohols and a thickening agent in deionized water, heating at 85 ℃, stirring and keeping the temperature for 45 minutes; step (2): cooling the temperature in the step (1) to 55 ℃, adding a bacteriostasis system, and stirring for 45 minutes; and (3): cooling the temperature in the step (2) to 30 ℃, adding the active extract, and stirring until the active extract is completely dissolved; and (4): filling the obtained product in the step (3) into a silk mask cloth/tencel mask cloth mask, and packaging to obtain the product.
Example 6:
a certain sleep mask (smearing type no-clean) on the market is prepared from the following raw materials in percentage by weight
Carbomer: 0.3 percent of
Triethanolamine: 0.3 percent of
Hydrophilic silicon powder: 2.0 percent
And (3) Geba gum: 15.0 percent
Hydrolyzing silk peptide: 3.0 percent
Hydrophilic silicone wax: 5.0 percent
Cyclopentasiloxane: 2.0 percent
Thickening auxiliary emulsifier: 1.0 percent
Phenoxyethanol: 0.5 percent
Ethyl hexyl glycerin: 0.5 percent
The remainder being water.
And (3) testing results:
1, moisturizing effect of the mask:
the tested person sits statically in a constant temperature and humidity room for 30 min, the skin (4 cm multiplied by 4 cm) at the inner side of the arm is taken, the Tewameter TM 300 skin water loss test probe is used for testing the water of the skin which is not coated with the tested sample and is recorded as T0(ii) a Soaking different facial mask liquids in the same facial mask cloth, applying for 30 min, taking off the facial mask cloth, waiting for 30 min, air drying the sample on skin, andthe skin moisture is tested every 1 hour, and after the skin moisture testing instrument is continuously used for 5 hours, the skin moisture change is tested and recorded, namely the skin moisture change is obtained. The calculation formula of the water loss rate is as follows: (T)n-T0)/T0。
Table 1 change table of skin moisture loss rate of different case masks
From the experimental results, table 1 shows that the facial masks of cases 1 to 6 all have certain moisture retention, wherein the moisture retention of the facial masks of cases 1 to 4 is obviously better than that of cases 5 and 6, which indicates that the moisture retention of the sleep facial mask is better than that of the common application facial mask on the market and the sleep facial mask existing on the market.
2 anti-inflammatory test of the mask:
TABLE 2 inhibition of Propionibacterium acnes by different cases of facial mask solutions
The bacteriostatic experiments were carried out using propionibacterium acnes, and deionized water as a blank group of bacteriostatic experiments, which were tested in cases 1-6, respectively. The lower the absorbance, the stronger the inhibitory effect on Propionibacterium acnes. From the analysis of the experimental results, the liquid of the blank group, case 5 and case 6 has no obvious inhibition effect on propionibacterium acnes, cases 1 to 4 have inhibition effects on propionibacterium acnes, and the facial mask liquid prepared in case 1 has the strongest inhibition effect on propionibacterium acnes, which shows that the compound of the purslane extract, the chamomile extract and the oriental cherry extract has a synergistic effect, and has certain innovative significance when being applied to a facial mask system.
The experimental result shows that the anti-inflammatory and bacteriostatic effects of case 1 to case 2 are more obvious than those of cases 3 and 4, and the three active extracts have synergistic effect and realize more effective non-irritant efficacy.
Active substance permeability test experiment of face mask:
24 SD male rats were anesthetized with 10% chloral hydrate (0.35 mL/100 g) and depilated on the back. Respectively adsorbing 30 μ L of nanosuspension, physical blending solution and common suspension sample to 1 cm2The method comprises the steps of (1) applying plastic adhesive tape filter paper on the filter paper, enabling the plastic adhesive tape filter paper to be tightly attached to the skin to ensure no gap, peeling the adhesive tape and the filter paper at l, 2, 3, 4 and 6 hours respectively, carrying out adhesive tape separation on residual medicines on the surface of the skin, repeating the steps for three times, cutting the adhesive tape and the filter paper into fragments, placing the fragments into 4mL of ethanol, carrying out ultrasonic treatment for 2 min, repeating the steps for two times, placing extract liquor obtained in the two times into a 10 mL volumetric flask, fixing the volume to a scale, filtering the extract liquor through a 0.22 mu m microporous filter membrane, measuring the content of three active substances by adopting a determined HPLC method, and calculating the skin permeation amount of the medicines according to the following experiment, wherein the experiment is repeated for 5 times. Drug skin penetration = dose-drug residual, which refers to the total amount of drug peeled off from the filter paper and tape at different time points.
Table 3 permeation effect of facial mask of different cases
As can be seen from the animal skin slices, the permeation effect of the facial mask prepared in case 1 is obviously higher than that of the samples of cases 5 and 6, the permeability of case 1 is obviously improved, the facial mask solution permeates the skin, the absorption of the facial mask solution by the skin is enhanced, and the skin is tender and fine.
Sensory test of the mask 4 test: volunteers (15-65 years old, 60 persons), 10 persons per group, were subjected to the application test using the masks prepared in cases 1-6, respectively. The experimental results are as follows:
Volunteer sensory test results surface: the novel nonirritating light medical and beauty sleeping mask simultaneously solves the problems that a pasting type mask cannot be used for a very long time and the sleeping mask can only be used in a smearing type, can be pasted and slept naturally, essence liquid used for more than 30 minutes is not dry, skin allergy phenomena such as redness and stabbing pain cannot occur for a very long time, a product is developed aiming at sensitive skin, the original liquid on a lightly-tapped face is fresh and cool in feeling and strong in air permeability when the product is used, and the skin looks tender after the essence liquid is dry, and can be used as a washing-free sleeping mask.
The present invention has been described above by way of example, but the present invention is not limited to the above-described specific embodiments, and any modification or variation made based on the present invention is within the scope of the present invention as claimed.
Claims (3)
1. The non-irritant oriental cherry sleeping mask is characterized by comprising the following components in percentage by weight:
glycerol polyacrylate: 5.0 percent
Propylene glycol: 5.0 percent
Glycerol: 5.0 percent
Butanediol: 7.0 percent
P-hydroxyacetophenone: 0.5 percent
1, 2-hexanediol: 0.5 percent;
xanthan gum: 0.5 percent;
cellulose: 0.3 percent;
and (3) purslane extract: 1.5 percent;
chamomile extract: 1.5 percent;
cherry extract: 2.0 percent;
the remainder being water.
2. The non-irritating cherry blossom sleep mask as claimed in claim 1, wherein the preparation method of the non-irritating cherry blossom sleep mask comprises the following steps:
step (1): dissolving alcohols and thickening agents of glycerol polyacrylate, xanthan gum and cellulose in deionized water, heating at 85 ℃, stirring and preserving heat for 45 minutes;
step (2): cooling the temperature in the step (1) to 55 ℃, adding p-hydroxyacetophenone and 1, 2-hexanediol serving as a bacteriostatic system, and stirring for 45 minutes;
and (3): cooling the temperature in the step (2) to 30 ℃, adding the active extract, and stirring until the active extract is completely dissolved;
and (4): and (3) filling the mixture into a silk mask cloth/tencel mask cloth mask, and packaging to obtain the product.
3. The non-irritating cherry blossom sleep mask as claimed in claim 1, is used in the cosmetic field.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201910409636.4A CN110037961B (en) | 2019-05-16 | 2019-05-16 | Non-irritant oriental cherry sleeping mask |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201910409636.4A CN110037961B (en) | 2019-05-16 | 2019-05-16 | Non-irritant oriental cherry sleeping mask |
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| Publication Number | Publication Date |
|---|---|
| CN110037961A CN110037961A (en) | 2019-07-23 |
| CN110037961B true CN110037961B (en) | 2022-03-11 |
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Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| KR20170027614A (en) * | 2015-09-02 | 2017-03-10 | 신혜경 | Natural cosmetic composition of mask pack and method for manufacturing natural cosmetic composition of mask pack |
| CN107735076A (en) * | 2016-02-22 | 2018-02-23 | (株)杰恩宝 | Cosmetic composition containing camellia, oriental cherry, Jasmine, Flos Chrysanthemi and lotus mixed extract |
| WO2018129659A1 (en) * | 2017-01-10 | 2018-07-19 | 孙丽霞 | Composite facial mask and preparation method therefor |
| CN109172386A (en) * | 2018-10-11 | 2019-01-11 | 广州华瑟科技有限公司 | A kind of compound moisturizing hydrogel |
-
2019
- 2019-05-16 CN CN201910409636.4A patent/CN110037961B/en active Active
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| KR20170027614A (en) * | 2015-09-02 | 2017-03-10 | 신혜경 | Natural cosmetic composition of mask pack and method for manufacturing natural cosmetic composition of mask pack |
| CN107735076A (en) * | 2016-02-22 | 2018-02-23 | (株)杰恩宝 | Cosmetic composition containing camellia, oriental cherry, Jasmine, Flos Chrysanthemi and lotus mixed extract |
| WO2018129659A1 (en) * | 2017-01-10 | 2018-07-19 | 孙丽霞 | Composite facial mask and preparation method therefor |
| CN109172386A (en) * | 2018-10-11 | 2019-01-11 | 广州华瑟科技有限公司 | A kind of compound moisturizing hydrogel |
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