CN109172386A - A kind of compound moisturizing hydrogel - Google Patents
A kind of compound moisturizing hydrogel Download PDFInfo
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- CN109172386A CN109172386A CN201811183158.1A CN201811183158A CN109172386A CN 109172386 A CN109172386 A CN 109172386A CN 201811183158 A CN201811183158 A CN 201811183158A CN 109172386 A CN109172386 A CN 109172386A
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- compound moisturizing
- extract
- purslane
- skin
- moisturizing hydrogel
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/02—Cosmetics or similar toiletry preparations characterised by special physical form
- A61K8/04—Dispersions; Emulsions
- A61K8/042—Gels
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K47/00—Medicinal preparations characterised by the non-active ingredients used, e.g. carriers or inert additives; Targeting or modifying agents chemically bound to the active ingredient
- A61K47/46—Ingredients of undetermined constitution or reaction products thereof, e.g. skin, bone, milk, cotton fibre, eggshell, oxgall or plant extracts
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/49—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds
- A61K8/494—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with more than one nitrogen as the only hetero atom
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/64—Proteins; Peptides; Derivatives or degradation products thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/67—Vitamins
- A61K8/676—Ascorbic acid, i.e. vitamin C
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9789—Magnoliopsida [dicotyledons]
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K9/00—Medicinal preparations characterised by special physical form
- A61K9/06—Ointments; Bases therefor; Other semi-solid forms, e.g. creams, sticks, gels
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/02—Preparations for care of the skin for chemically bleaching or whitening the skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/08—Anti-ageing preparations
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/70—Biological properties of the composition as a whole
- A61K2800/72—Hypo-allergenic
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
- A61K2800/82—Preparation or application process involves sonication or ultrasonication
Abstract
The invention discloses a kind of compound moisturizing hydrogels, it includes the following components'mass percentage: widow's victory 100~500PPM of peptide, purslane extract 1~10%, camomile extract 1~5%, Essential Oil of Acorus tatarinowii 0.2~1%, glycerine polyacrylate 10~30%, propylene glycol 1~5%, glycerine 1~5%, parahydroxyacet-ophenone 0.1~0.5%, pungent glycol 0.1~0.5%, deionized water surplus.Skin sense while with strong moisture-keeping efficacy of the compound moisturizing hydrogel of the present invention also has the function of whitening, crease-resistant and anti-aging, active matter is helped to disperse and permeate, effectively promotion active function clearly without sticky.
Description
Technical field
The present invention relates to daily chemical product field more particularly to a kind of compound moisturizing hydrogels.
Background technique
With the improvement of living standards, the irradiation of operating pressure, ultraviolet light, irregular daily life system etc. cause aging to add
Speed, to use more extensive of cosmetics, while the requirement to cosmetics is also increasingly particular about, and pursues comfortable salubrious skin sense
It also wants both effectiveness simultaneously and realizes beauty, moisturizing moisturizing, the white exquisiteness of skin delays senescence, beautiful life.
Most hydrophilic traditional moisturizing raw materials currently on the market, including polyalcohol, polysaccharide, reed fragrant plant glue oil and macromolecule
Hyaluronic acid etc. is all more sticky.On the other hand, moistening effect is influenced by ambient humidity more easily, leads to the effect for retaining hydrone
Fruit decline, it is more difficult to reach the purpose of efficient moisture-retention, long-time moistening effect is also undesirable.Furthermore it was developed in cosmetic formulations
It is low with effective rate of utilization to be easy to appear effect failure for polypeptide, growth factor, Co-Q10, Polyphenols and other effects property raw material in journey
Situation causes product formula cost high effect undesirable.
Summary of the invention
To solve the above problems, the present invention provides a kind of compound moisturizing hydrogel, be it is a kind of have it is not sticky and can
The multi-functional glycerine polyacrylate cage type hydrogel of strong moistening effect is provided.Skin can be directly acted on, has one
Fixed light diffuses effect, is capable of providing pure and fresh smooth skin sense, and energy cutin-softening layer promotes skin fair and tender such as baby skin.Simultaneously
Also have the function of whitening, crease-resistant and anti-aging, active matter is helped to disperse and permeate, effectively promotion active function.
The present invention is achieved through the following technical solutions:
A kind of Multifunctional composite water gel, includes the following components'mass percentage: widow victory 100~500PPM of peptide, horse
Sativa extract 1~10%, camomile extract 1~5%, Essential Oil of Acorus tatarinowii 0.2~1%, glycerine polyacrylate 10~
30%, propylene glycol 1~5%, glycerine 1~5%, parahydroxyacet-ophenone 0.1~0.5%, pungent glycol 0.1~0.5%, deionization
Water surplus.
Further, the Multifunctional composite water gel further includes ascorbic acid glucoside 0.1~0.5%.
Further, the Multifunctional composite water gel, further include PCA zinc, Anjidew NL50, PCA magnesium 0.1~
0.5%, wherein PCA zinc, Anjidew NL50, PCA magnesium weight ratio be 1:3:2.
A kind of Multifunctional composite water gel, the purslane extract the preparation method comprises the following steps: (1) washes purslane cauline leaf
Decontamination is cleaned, and distilled water slightly soaking flushing 10-15min repetitive operation 2~3 times, dries；(2) it is placed in disinfection cabinet, uses
Pasteur's low temperature disinfection sterilizes 30~40min；(3) the purslane cauline leaf after disinfection is placed in juice extractor and is squeezed, obtain purslane
Crude extract；(4) purslane crude extract is used into ultrasonic cell disintegration instrument 10~15min of ultrasonic extraction, obtains purslane extract.
A kind of Multifunctional composite water gel, the camomile extract the preparation method comprises the following steps: (1) washes chamomile cauline leaf
Decontamination is cleaned, and distilled water slightly soaking flushing 10-15min repetitive operation 2~3 times, dries；(2) it is placed in disinfection cabinet, uses
Pasteur's low temperature disinfection sterilizes 30~40min；(3) the chamomile cauline leaf after disinfection is placed in juice extractor and is squeezed, obtain chamomile
Crude extract；(4) chamomile crude extract is used into ultrasonic cell disintegration instrument 10~15min of ultrasonic extraction, obtains camomile extract.
A kind of Multifunctional composite water gel, the Essential Oil of Acorus tatarinowii the preparation method comprises the following steps: (1) picks rhizoma acori graminei rhizome
Decontamination is cleaned, slightly impregnates, moisturize, and is sliced, dries；(2) be ground into powder with pulverizer, be added 1-4 times of parts by weight 70~
80% ethyl alcohol immersion 10~extracted after twenty minutes；(3) extraction conditions: 38~45 DEG C of constant temperature extractings, extracting pressure 30~
37MPa, CO22.5~3.2kg/h of flow velocity, 10~23MPa of separating pressure, 1.5~2h of extraction time；(4) separating-purifying obtains stone
Calamus volatile oil.
Hydrogel provided by the invention can be used for the preparation of cosmetics, wherein and the additive amount of hydrogel is 0.1~10%,
It can be used as preparation of the additive for facial mask.
The invention also discloses a kind of facial masks, further include the component of following mass percent: carbomer 0.1~0.3%, and three
Ethanol amine 0.1~0.3%, Chlorphenesin 0.1~0.3%, Phenoxyethanol 0.5~1.0%, deionized water surplus.
Conventional method generally realizes moisture-keeping efficacy using moisturizing, and the present invention uses Hydrogenbond and Van der Waals force shape
At lattice structure tightly lockked skin moisture, strong moistening effect is presented.
A kind of Multifunctional composite water gel of the present invention, has the following beneficial effects:
(1) moisture is tightly lockked by the lattice structure that Hydrogenbond and Van der Waals force are formed, there is strong moisturizing effect
Fruit is mainly used in medicine and personal care articles field, provides moisture-keeping efficacy for skin and hair, be strong skin-moisturizing, skin
Agent；
(2) also have the function of whitening, crease-resistant and anti-aging；
(3) have the function of dispersing and helping active matter infiltration, be the sustained release of other active matters, active matter is in hydrogel shape
At moisture film in can there is one uniformly to sprawl, have higher efficiency it, while the infiltration of the intraor extracellular interstitial of cutin
It is pressed in the help of hydrogel thoroughly and remains at the state of balance, to allow active matter is continual to seep into skin
Thoroughly；
(4) easy to use, it is conveniently used in the opaque products such as various personal care articles formula；
(5) mildly, it does not stimulate, antiallergy；
(6) in the products such as toner, facial mask, lotion, essence, cream and facial cleanser, can play well film forming moisturizing,
Skin sense conditioning, the effect for assisting both effectiveness raw material sustained release.
Specific embodiment
In order that those skilled in the art will better understand the technical solution of the present invention, below with reference to embodiment and to this
Invention product is described in further detail.Embodiments of the present invention are not limited thereto, and not specifically specified technique is joined
Several or condition can refer to routine techniques progress.
Each ingredient involved in composition of the present invention is described as follows:
Rhizoma acori graminei, slightly warm in nature, qi-regulating, promoting blood circulation.For the rhizome of day South section plant rhizoma acori graminei, rhizome and Ye Zhongjun are containing volatilization
Oily (0.11~0.42%), main component are beta-Asarones 63.2~81.2%, secondly asarone 8.8~13.7% is stone
Bamboo alkene, α-Humuleno, sekishone etc..Also contain amino acid, organic acid and carbohydrate.Beta-Asarone relative molecular mass is small, and liposoluble
Property it is preferable, with easy percutaneous absorbtion basic physicochemical property.
The flavones and saponin contained in purslane, which has, removes free radical and antioxidation, can be with delay skin aging.Horse
Biologically active amino acid has contraction to vascular smooth muscle in bitterroot, and such contraction has maincenter and tip concurrently
Property, it can soothe the skin, pruitus caused by inhibiting because of drying.Purslane extract has anti-drying aging, increasing in winter
Add skin comfort degree and remove free radical, improves the comprehensive performance of skin comfort etc..
Embodiment 1
A kind of Multifunctional composite water gel, includes the following components'mass percentage: widow victory peptide 245PPM, purslane mention
Take object 5.5%, camomile extract 3%, Essential Oil of Acorus tatarinowii 0.45%, glycerine polyacrylate 20%, propylene glycol 3%, third
Triol 3%, parahydroxyacet-ophenone 0.3%, pungent glycol 0.3%, ascorbic acid glucoside 0.3%, PCA zinc, Anjidew NL50, PCA magnesium
0.3%, deionized water surplus.The PCA zinc, Anjidew NL50, PCA magnesium weight ratio be 1:3:2.
Embodiment 2
A kind of Multifunctional composite water gel, includes the following components'mass percentage: widow victory peptide 100PPM, purslane mention
Take object 1%, camomile extract 1%, Essential Oil of Acorus tatarinowii 0.2%, glycerine polyacrylate 10~30%, propylene glycol 1%, third
Triol 1%, parahydroxyacet-ophenone 0.1%, pungent glycol 0.1%, ascorbic acid glucoside 0.1%, PCA zinc, Anjidew NL50, PCA magnesium
0.1%, deionized water surplus.The PCA zinc, Anjidew NL50, PCA magnesium weight ratio be 1:3:2.
Embodiment 3
A kind of Multifunctional composite water gel, includes the following components'mass percentage: widow victory peptide 500PPM, purslane mention
Take object 10%, camomile extract 5%, Essential Oil of Acorus tatarinowii 1%, glycerine polyacrylate 30%, propylene glycol 5%, glycerine
5%, parahydroxyacet-ophenone 0.5%, pungent glycol 0.5%, ascorbic acid glucoside 0.5%, PCA zinc, Anjidew NL50, PCA magnesium 0.5% are gone
Ion water surplus.The PCA zinc, Anjidew NL50, PCA magnesium weight ratio be 1:3:2.
Embodiment 4
A kind of Multifunctional composite water gel, includes the following components'mass percentage: widow victory peptide 160PPM, purslane mention
Take object 3%, camomile extract 2%, Essential Oil of Acorus tatarinowii 0.35%, glycerine polyacrylate 14%, propylene glycol 2.5%, third
Triol 2.5%, parahydroxyacet-ophenone 0.45%, pungent glycol 0.2%, ascorbic acid glucoside 0.2%, PCA zinc, Anjidew NL50, PCA magnesium
0.2%, deionized water surplus.The PCA zinc, Anjidew NL50, PCA magnesium weight ratio be 1:3:2.
Embodiment 5
A kind of compound moisturizing hydrogel, includes the following components'mass percentage: widow victory peptide 480PPM, purslane are extracted
Object 8.5%, camomile extract 4.5%, Essential Oil of Acorus tatarinowii 0.8%, glycerine polyacrylate 28%, propylene glycol 4.5%, third
Triol 4.5%, parahydroxyacet-ophenone 0.2%, pungent glycol 0.45%, ascorbic acid glucoside 0.14%, PCA zinc, Anjidew NL50, PCA magnesium
0.4%, deionized water surplus.The PCA zinc, Anjidew NL50, PCA magnesium weight ratio be 1:3:2.
Embodiment 6
A kind of facial mask, includes the following components'mass percentage: hydrogel 0.1% obtained by above-described embodiment 1, card wave
Nurse 0.1%, triethanolamine 0.1%, Chlorphenesin 0.1%, Phenoxyethanol 0.5%, deionized water surplus.
Embodiment 7
A kind of facial mask, includes the following components'mass percentage: hydrogel 10% obtained by above-described embodiment 1, card wave
Nurse 0.3%, triethanolamine 0.3%, Chlorphenesin 0.3%, Phenoxyethanol 1.0%, deionized water surplus.
Embodiment 8
A kind of facial mask, includes the following components'mass percentage: hydrogel 5%, carbomer obtained by above-described embodiment 1
0.2%, triethanolamine 0.2%, Chlorphenesin 0.2%, Phenoxyethanol 0.8%, deionized water surplus.
Embodiment 9
A kind of facial mask, includes the following components'mass percentage: hydrogel 1%, carbomer obtained by above-described embodiment 1
0.15%, triethanolamine 0.15%, Chlorphenesin 0.15%, Phenoxyethanol 0.85%, deionized water surplus.
Embodiment 10
A kind of facial mask, includes the following components'mass percentage: hydrogel 8.5% obtained by above-described embodiment 1, card wave
Nurse 0.25%, triethanolamine 0.25%, Chlorphenesin 0.25%, Phenoxyethanol 0.55%, deionized water surplus.
Comparative example 1
Difference with embodiment 6 is, purslane extract, camomile extract is not added in embodiment 1, and rhizoma acori graminei is waved
Hair oil.
Comparative example 2
It is with the difference for implementing 6, few victory peptide 90PPM is added in embodiment 1, purslane extract 11%, chamomile mentions
Take object 0.9%, Essential Oil of Acorus tatarinowii 1.1%.
Comparative example 3
Difference with embodiment 6 is, PCA zinc, Anjidew NL50, PCA magnesium is not added in embodiment 1.
Comparative example 4
Difference with embodiment 6 is, few victory peptide is not added in embodiment 1.
Comparative example 5
Difference with embodiment 6 is, few victory 501PPM, purslane extract 0.9%, chamomile are added in embodiment 1
Extract 5.1%, Essential Oil of Acorus tatarinowii 0.15%.
Control group
Certain commercially available moisture saver mask.
Human body patch test
Organize 50 volunteers according to the human skin patch of " cosmetics safety technical specification " (2015 editions) record,
The back of subject will be pasted on low sensitization adhesive tape added with the spot tester of tested material or forearm song is surveyed, gently pressed with palm and be allowed to equal
It is pasted on skin, continues for 24 hours evenly.Facial mask obtained by 6-10 of the embodiment of the present invention and comparative example 1-5 is tested to human body skin
The potential adverse reaction of skin, the results are shown in Table 1.
Table 1
Joined as can be seen from Table 1 facial mask made from the embodiment 6-10 of compound moisturizing hydrogel to human skin without
Irritation.
Moisture-keeping efficacy evaluation
Detection effect on probation is carried out to the embodiment 6-10 and comparative example 1-5 product prepared.Rear skin is used by detection
Percutaneous water loss amount verifies moisture-keeping efficacy.
Laboratory apparatus:
Moisture of skin scatters and disappears tester: TM300Courage+Khakaza Cologne Germany.
Test environment: 22 DEG C ± 1 DEG C of temperature, humidity is 50% ± 5%
Volunteer requires: effective volunteer at least 80 people；Age is between 18 years old~65 years old；Forearm test zone capacitance method
The basic value of moisture of skin analyzer is between 15 years old~45 without serious systemic disease, without immune deficiency or autoimmune disease
Person；No active anaphylactia person；Previously to skin-care cosmetics without severe allergy history person；Not using sharp in nearly 1 month
Plain class drug and immunosuppressor person；Other clinical test persons are not participated in；Use according to regulations tested material and all information；Before test
All volunteers should fill in informed consent form.
Prepare before test: any product (cosmetics or topical drug) cannot be used within 2 days~3 days before recipient site.Test
Before, subject, which needs to clean in both hands forearm, to survey, with dry face tissue wiped clean.After cleaning, in subject's both hands forearm
Measured zone label is carried out in survey.Before official testing, it should which sit quietly at least 30min in standard compliant room, cannot drink water, preceding
Arm exposure, places in test mode, keeps loosening.
Measurement through transepidermal water lost (TEWL)
Measure 80 subjects smear addition embodiment 6-10 and comparative example 1-5 facial mask before and smear 1h, 2h and 4h
Moisture of skin windage afterwards calculates TEWL mean value, the results are shown in Table 2.
Table 2: the facial mask water loss amount of different time measurement
| TEWL/% | 0h | 1h | 2h | 3h | 4h |
| Embodiment 6 | 13.9 | 13.6 | 12.8 | 11.2 | 10.6 |
| Embodiment 7 | 13.6 | 13.5 | 13.1 | 11.8 | 11.3 |
| Embodiment 8 | 13.9 | 13.8 | 13.5 | 12.9 | 11.4 |
| Embodiment 9 | 13.8 | 13.6 | 13.4 | 12.3 | 10.9 |
| Embodiment 10 | 13.8 | 13.4 | 12.9 | 11.9 | 11.1 |
| Comparative example 1 | 13.7 | 13.6 | 13.6 | 13.4 | 13.4 |
| Comparative example 2 | 14.1 | 13.9 | 13.5 | 13.1 | 12.8 |
| Comparative example 3 | 13.9 | 13.8 | 13.4 | 13.2 | 12.7 |
| Comparative example 4 | 13.8 | 13.7 | 13.4 | 13.3 | 12.9 |
| Comparative example 5 | 14.2 | 13.9 | 13.6 | 12.8 | 12.6 |
| Blank control | 13.8 | 13.5 | 13.8 | 13.4 | 13.2 |
As can be seen from Table 2, as time increases, smear embodiment 6-10 facial mask tested region water loss amount by
It gradually reduces, therefore adds subject hydrogel in face pack prescription, strong moistening effect can be played, and reduce the water of skin
Disperse vector.
Elastic efficacy validation
Detection effect on probation is carried out to the embodiment 6-10 and comparative example 1-5 product prepared.Rear skin is used by detection
Elasticity verifies moisture-keeping crease-shedding effect.
Test object: each experimental group is male 20 female 30 (25-50 year old)；Test zone: face；Test equipment: skin
Skin elastic apparatus (Cutometer MPA 580).It uses: applying 1 time, persistently use 4 weeks every other day；Test item: skin elasticity.
Method: the environment on the day of subject tests after face cleaning in 23~25 DEG C of room temperature, relative humidity 50%-60% is sat quietly
After 30min, looks steadily it and loosen facial muscle groups, gently close eyes.Its face is detected with skin elasticity instrument (Cutometer MPA 580)
Portion's skin elasticity, probe is averaged in same tested region duplicate measurements 3 times when measurement.Test environment phase is kept when measurement
To temperature, the influence of light, sound interference is avoided, is firmly wanted uniformly using when probe, the pressure of application should be constant.Subject
Use the elasticity number for measuring tested region after 1 week, 2 weeks, 3 weeks, 4 weeks again.Terminate measurement, saves data, finishing analysis data.
Test result and evaluation:
The tested region of subject is shown in Table 3 using before and after product, elastic test Value Data analysis is compared:
Tested elasticity of skin variation gradually shows a increasing trend with the product time is used in embodiment 6-10 seen from table 3.By
Embodiment 6-10 and comparative example 1-5 comparison can obtain each ingredient in compound moisturizing hydrogel of the invention and act synergistically, and realize brighter
Aobvious moistening effect, enhances skin wettability, and compact skin realizes anti-wrinkle effect.
Skin sense verifying
Skin sense detection effect is carried out to hydrogel made from embodiment 1 and tradition, selects 500 volunteers, every test group
Each 100 triers.Certain cream is separately added into using hydrogel made from embodiment 1, polyalcohol, polysaccharide, polymer hyaluronic acid
In liquid, participant respectively uses 1 time sooner or later daily, persistently uses 1 month.Other any skin cares must not be used to produce in experimentation
Product, and subject has been fully completed verification process, and experimental result is shown in Table 4, three states of effect point:
Upper hand skin sense: water profit is salubrious, score value are as follows: 7-10 points；More sticky, score value is 3-7 points；It is sticky, score value 1-3
Point.
Half-dried skin sense: sticky unobvious, score value are as follows: 8-10 points；More sticky, score value is 3-7 points；It is sticky obvious, score value
It is 1-3 points.
Table 4:
Absolutely dry skin sense: obvious silty sense, score value are as follows: 8.5-10 points；Silty sense is general, and score value is 3-7 points；Without silty sense,
Score value is 0 point.
As shown in Table 4, compound moisturizing hydrogel produced by the present invention can bring salubrious not sticky skin sense.
White-skinned face function verifying
Choose 880 volunteers, every each 80 triers of test group.The face prepared using embodiment 6-10, comparative example 1-5
The commercially available facial mask of film, control group, participant use 1 time daily, persistently use 1 month.Other any shields are not used in experimentation
Skin product, and subject has been fully completed verification process, and experimental result is shown in Table 1, and effect divides three grades:
Whitening effect is obvious: whitening effect is obvious, and spot significantly reduces；
Whitening effect is general: whitening effect is general, and spot fading effect is general；
Whitening effect is unobvious: the obscure no improvement of the colour of skin, the colour of skin and difference before are little, skin relaxation, without obvious after
Feel.
Table 5: each embodiment, comparative example, control group using effect
It can be seen that compound moisture retention water provided by the embodiment of the present invention from the result of the self-assessment of 5 trier of table
Gel has preferable skin white-skinned face function to most trier's skin, also has crease-resistant, compact skin effect, realizes that skin is grown
Profit, whitening, water is tender bright, smooth and high resilience.
The present invention is described by way of example above, but the present invention is not limited to above-mentioned specific embodiment, all to be based on
Any changes or modifications that the present invention is done are fallen within the scope of the claimed invention.
Claims (9)
1. a kind of compound moisturizing hydrogel, which is characterized in that include the following components'mass percentage: widow's victory peptide 100~
500PPM, purslane extract 1~10%, camomile extract 1~5%, Essential Oil of Acorus tatarinowii 0.2~1%, glycerol polypropylene
Acid esters 10~30%, propylene glycol 1~5%, glycerine 1~5%, parahydroxyacet-ophenone 0.1~0.5%, pungent glycol 0.1~
0.5%, deionized water surplus.
2. a kind of compound moisturizing hydrogel according to claim 1, which is characterized in that the system of the purslane extract
Preparation Method are as follows: (1) purslane cauline leaf is washed away into impurity, cleaned, distilled water slightly soaking flushing 10-15min, repetitive operation 2~3
It is secondary, it dries；(2) it is placed in disinfection cabinet, 30~40min is sterilized using Pasteur's low temperature disinfection；(3) by the purslane stem after disinfection
Leaf is placed in juice extractor and squeezes, and obtains purslane crude extract；(4) purslane crude extract is used into ultrasonic cell disintegration instrument ultrasonic extraction
10~15min obtains purslane extract.
3. a kind of compound moisturizing hydrogel according to claim 1, which is characterized in that the system of the camomile extract
Preparation Method are as follows: (1) chamomile cauline leaf is washed away into impurity, cleaned, distilled water slightly soaking flushing 10-15min, repetitive operation 2~3
It is secondary, it dries；(2) it is placed in disinfection cabinet, 30~40min is sterilized using Pasteur's low temperature disinfection；(3) by the chamomile stem after disinfection
Leaf is placed in juice extractor and squeezes, and obtains chamomile crude extract；(4) chamomile crude extract is used into ultrasonic cell disintegration instrument ultrasonic extraction
10~15min obtains camomile extract.
4. a kind of compound moisturizing hydrogel according to claim 1, which is characterized in that the system of the Essential Oil of Acorus tatarinowii
Preparation Method are as follows: (1) rhizoma acori graminei rhizome is picked into impurity, clean, slightly impregnate, moisturize, be sliced, dry；(2) it is ground into pulverizer
Powder, 70~80% ethyl alcohol that 1-4 times of parts by weight are added impregnate 10~it is extracted after twenty minutes；(3) extraction conditions: 38~45
DEG C constant temperature extracting, extracting pressure 30~37MPa, CO22.5~3.2kg/h of flow velocity, 10~23MPa of separating pressure, extraction time
1.5~2h；(4) separating-purifying obtains Essential Oil of Acorus tatarinowii.
5. a kind of compound moisturizing hydrogel according to claim 1, which is characterized in that the compound moisturizing hydrogel
It further include ascorbic acid glucoside 0.1~0.5%.
6. a kind of compound moisturizing hydrogel according to claim 1, which is characterized in that the compound moisturizing hydrogel
Further include PCA zinc, Anjidew NL50, PCA magnesium 0.1~0.5%, wherein PCA zinc, Anjidew NL50, PCA magnesium weight ratio be 1:3:2.
7. described in any item compound moisturizing hydrogels according to claim 1~6, which is characterized in that the compound moisturizing
Hydrogel can be used for the preparation of cosmetics, wherein additive amount is 0.1~10%.
8. compound moisturizing hydrogel as claimed in claim 7, which is characterized in that the compound moisturizing hydrogel can be used as
Additive is used for the preparation of facial mask.
9. a kind of facial mask, which is characterized in that further include the component of following mass percent: carbomer 0.1~0.3%, three ethyl alcohol
Amine 0.1~0.3%, Chlorphenesin 0.1~0.3%, Phenoxyethanol 0.5~1.0%, deionized water surplus.
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| CN201811183158.1A CN109172386A (en) | 2018-10-11 | 2018-10-11 | A kind of compound moisturizing hydrogel |
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| CN201811183158.1A CN109172386A (en) | 2018-10-11 | 2018-10-11 | A kind of compound moisturizing hydrogel |
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