CN109956780A - A kind of purification compound fertilizer and its preparation method and application - Google Patents

A kind of purification compound fertilizer and its preparation method and application Download PDF

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Publication number
CN109956780A
CN109956780A CN201711427160.4A CN201711427160A CN109956780A CN 109956780 A CN109956780 A CN 109956780A CN 201711427160 A CN201711427160 A CN 201711427160A CN 109956780 A CN109956780 A CN 109956780A
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China
Prior art keywords
compound fertilizer
purification compound
residue
parts
organic matter
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Withdrawn
Application number
CN201711427160.4A
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Chinese (zh)
Inventor
盛建平
张利军
欧阳琴华
李国恒
张燕梅
谭楚娟
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Chenzhou Tong Yuan Biotechnology Co Ltd
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Chenzhou Tong Yuan Biotechnology Co Ltd
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Priority to CN201711427160.4A priority Critical patent/CN109956780A/en
Publication of CN109956780A publication Critical patent/CN109956780A/en
Withdrawn legal-status Critical Current

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    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01CPLANTING; SOWING; FERTILISING
    • A01C21/00Methods of fertilising, sowing or planting
    • CCHEMISTRY; METALLURGY
    • C05FERTILISERS; MANUFACTURE THEREOF
    • C05BPHOSPHATIC FERTILISERS
    • C05B7/00Fertilisers based essentially on alkali or ammonium orthophosphates
    • CCHEMISTRY; METALLURGY
    • C05FERTILISERS; MANUFACTURE THEREOF
    • C05FORGANIC FERTILISERS NOT COVERED BY SUBCLASSES C05B, C05C, e.g. FERTILISERS FROM WASTE OR REFUSE
    • C05F17/00Preparation of fertilisers characterised by biological or biochemical treatment steps, e.g. composting or fermentation
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02WCLIMATE CHANGE MITIGATION TECHNOLOGIES RELATED TO WASTEWATER TREATMENT OR WASTE MANAGEMENT
    • Y02W30/00Technologies for solid waste management
    • Y02W30/40Bio-organic fraction processing; Production of fertilisers from the organic fraction of waste or refuse

Abstract

The invention discloses a kind of purification compound fertilizers and its preparation method and application.The purification compound fertilizer is formed by potassium sulfate, potassium nitrate, urea, phosphorus ammonium and material mixing containing organic matter, and the total content of the organic matter is 34 ~ 36%, and the total content of N, P, K are 24.5~26%;The substance containing organic matter is residue of monosodium glutamate, bacteria residue, rapeseed meal;After applying the purification compound fertilizer, the growth and development for avoiding chlorine fruits and vegetables is effectively facilitated, fruit tree is promoted to yield positive results, is improved to chlorine fruit-vegetable quality is avoided with major contribution.

Description

A kind of purification compound fertilizer and its preparation method and application
Technical field
The present invention relates to the technical fields of compound fertilizer, more particularly, to a kind of purification compound fertilizer and preparation method thereof And application.
Background technique
Chemical fertilizer is because cost is relatively low, efficiency is higher by universal use.But application chemical fertilizer not only can So that the physico chemical factor of soil is degenerated, and hinder the breeding of septic biology in soil, threatens their existence, disorder Soil ecosystem, consequence are that harmful parasitic organism is easy actively, to improve their population densities, then It is easy to multiple pest and disease damage, and earth is made to pull knot, soil fertility reduces.
Potassium chloride is commonly used in chemical fertilizer and supplements potassium element, but avoids chlorine during some crop growths, avoids chlorine work Object is very sensitive to chloride ion, when uptake reaches a certain level, yield and quality can be significantly influenced, when the chlorine in soil When ion is more, it is unfavorable for sugar and is converted into starch, for example, the reduction of the content of starch of root tuber and tuber crops can be made;Chloride ion energy Promote the hydrolysis of carbohydrate, watermelon, beet, grape can reduce sugar content;Chloride ion is more, will affect the flammability of tobacco, Cigarette is easily flame-out;When chloride ion is more, often cause damages to the seedling of sensitive crop.Tobacco, potato, sweet potato, sugarcane, watermelon, Grape, citrus, beet, watermelon, tealeaves, Chinese cabbage, capsicum, asparagus lettuce, three-coloured amaranth etc. are all fear-chlorion crops.Chlorine can produce solanaceous crops Raw adverse effect.Other crops, such as: soybean, kidney bean anti-chlorine performance are weaker.
Summary of the invention
The technical problem to be solved by the present invention is to overcome the technical deficiencies of existing compound fertilizer, provide a kind of purification compound fertilizer.
Another technical problems to be solved of the present invention are to provide the preparation method of the purification compound fertilizer.
The present invention also using technical problems to be solved be to provide it is described purification compound fertilizer as avoid chlorine fruits and vegetables fruits and vegetables plant Using.
Above-mentioned purpose of the present invention is achieved through the following technical solutions:
A kind of purification compound fertilizer is provided, by potassium sulfate, potassium nitrate, urea, phosphorus ammonium and material mixing containing organic matter and At the total content of the organic matter is 34~36%, and the total content of N, P, K are 24.5~26%;The substance containing organic matter For residue of monosodium glutamate, bacteria residue, rapeseed meal.
Preferably, the content of organic matter that the bacteria residue provides is 24.5~25.4%;The organic matter that the rapeseed meal provides contains Amount is 2.6~3.2%;The content of organic matter 6.3~7.3% that the residue of monosodium glutamate provides.
Preferably, the bacteria residue is that cotton seed hulls is cultivated remaining solid culture medium after bacterium.
Preferably, the residue of monosodium glutamate is to brew remaining solid material residue after monosodium glutamate.
Preferably, the content of organic matter that the bacteria residue provides is 25%;The content of organic matter that the rapeseed meal provides is 3%; The content of organic matter 7% that the residue of monosodium glutamate provides.
Preferably, in the purification compound fertilizer N total content total content >=6.9%, the N+P+K in the bacteria residue always contains Amount is 3.25%.
Preferably, according to mass fraction meter, the purification compound fertilizer is made of in proportion following each component:
Preferably, according to mass fraction meter, the purification compound fertilizer is made of in proportion following each component:
Present invention simultaneously provides the preparation methods of the purification compound fertilizer, comprising the following steps:
S1. it is fermented to obtain rapeseed meal fermentation material after bio-fermentation agent being added into rapeseed meal;By residue of monosodium glutamate, bacteria residue, each group Divide and pulverized and sieved, is mixed to get and is pulverized and mixed material;
S2. adjust pH value by rapeseed meal fermentation material and after being pulverized and mixed material mixing, then with potassium sulfate, urea, potassium nitrate, phosphorus ammonium It mixes, pack or is packed after being granulated in proportion to obtain the final product;
The bio-fermentation agent be aspergillus niger microbial inoculum, bacillus subtilis, lactobacillus plantarum, in EM microbial bacterial agent It is a kind of;The ratio between the bio-fermentation agent and rapeseed meal are 1:20~30.
Preferably, the bacteria residue was crushed to 10~20 meshes;The residue of monosodium glutamate was crushed to 10~30 meshes.
Preferably, the technological parameter of fermentation described in step S1 are as follows: fermentation temperature is 55~60 DEG C, fermentation time 10 ~14 days, every turning in 4~7 days was primary.
Preferably, described in step S2 tune pH value be adjusted to pH value be 5.5~8;Further, it is preferable to using quality hundred Divide the sulfuric acid or quick lime adjusting pH value that specific concentration is 5~10%.
The purification compound fertilizer is powdery or graininess.
The purification compound fertilizer can be advantageously applied to as the base manure or top dressing for avoiding chlorine fruits and vegetables.
Compared with prior art, the invention has the following advantages:
Contain organic matter in purification compound fertilizer prepared by the present invention, organic matter is the main source of plant nutrient, contains plant Nitrogen in various nutrients, especially soil required for growth and development is with organic state with the presence of 95% or more nitrogen In soil.In addition, organic matter is also the important sources of phosphorus in soil, Calcium Magnesium Sulphur and microelement.So organic matter More soil, nutrient content are also just more.Humic acid in organic matter, can be enhanced plant respiration, improve the infiltration of cell membrane Property, enhance absorption to nutriment, while vitamin in organic matter and some hormones can promote the growth and development of plant.
After applying the purification compound fertilizer, the growth and development for avoiding chlorine fruits and vegetables is effectively facilitated, fruit tree is promoted to yield positive results, to avoiding Chlorine fruit-vegetable quality, which improves, has major contribution.
Organic chemical fertilizer had both ensured that nutrient was comprehensive with inorganic fertilizer compound in the present invention, fertilizer efficiency mitigate and persistently, it is same When can ensure again early period can fast decoupled go out nutritional ingredient and keep soil nutrient full, and ingredient is simple, and dosage is less, behaviour Make that intensity is smaller, it is lighter to the pollution of water body, it is readily transported and stores.The present invention effectively facilitates growth and development of fruit tree, promotes Fruit tree yields positive results, and improving to fruit quality has major contribution.
Having used the watermelon of the fertilizer, single fresh fruit increases 36.4% again compared to the control group, realizes per mu yield growth rate Nearly 70%, soluble solid content increases about 20% compared to the control group, and effect is considerable.
Specific embodiment
The present invention is further illustrated below in conjunction with specific embodiment, but embodiment does not do any form to the present invention Restriction.Unless stated otherwise, the present invention uses reagent, method and apparatus for the art conventional reagent, method and are set It is standby.
Unless stated otherwise, following embodiment agents useful for same and material are commercially available.
The preparation of the purification compound fertilizer of embodiment 1
According to mass fraction meter, the purification compound fertilizer is made of in proportion following each component:
High purification compound fertilizer of the present invention the preparation method is as follows:
S1. it is fermented to obtain rapeseed meal fermentation material after EM microbial bacterial agent being added into rapeseed meal;By residue of monosodium glutamate, bacteria residue, each Component is pulverized and sieved, and is mixed to get and is pulverized and mixed material;
S2. adjust pH value by rapeseed meal fermentation material and after being pulverized and mixed material mixing, then with potassium sulfate, urea, potassium nitrate, phosphorus ammonium It mixes, is packed after granulation in proportion to obtain the final product;
Wherein, bacteria residue was crushed to 12 meshes;Residue of monosodium glutamate was crushed to 12 meshes;
The process conditions of fermentation described in step S1 are as follows: fermentation temperature is 55 DEG C, fermentation time is 14 days, every turning one in 7 days It is secondary;
Described in step S2 tune pH value be adjusted to pH value be 6;Further, it is preferable to use mass percent concentration for 5% Sulphur acid for adjusting pH value;
Through detecting, the N+P+K total content of the purification compound fertilizer in the present embodiment is 24.5% and N >=6.9%;Moisture contains Amount≤12%, total content >=35% of organic matter.
The preparation of the purification compound fertilizer of embodiment 2
According to mass fraction meter, the purification compound fertilizer is made of in proportion following each component:
High purification compound fertilizer of the present invention the preparation method is as follows:
S1. it is fermented to obtain rapeseed meal fermentation material after lactobacillus plantarum being added into rapeseed meal;By residue of monosodium glutamate, bacteria residue, each group Divide and pulverized and sieved, is mixed to get and is pulverized and mixed material;
S2. adjust pH value by rapeseed meal fermentation material and after being pulverized and mixed material mixing, then with potassium sulfate, urea, potassium nitrate, phosphorus ammonium It mixes, is packed after granulation in proportion to obtain the final product;
Wherein, bacteria residue was crushed to 12 meshes;Residue of monosodium glutamate was crushed to 12 meshes;
The process conditions of fermentation described in step S1 are as follows: fermentation temperature is 55 DEG C, fermentation time is 14 days, every turning one in 7 days It is secondary;
Described in step S2 tune pH value be adjusted to pH value be 6;Further, it is preferable to use mass percent concentration for 5% Sulphur acid for adjusting pH value;
Through detecting, the N+P+K total content of the purification compound fertilizer in the present embodiment is 25.1% and N >=6.9%;Moisture contains Amount≤12%, total content >=35% of organic matter.
The preparation of the purification compound fertilizer of embodiment 3
According to mass fraction meter, the purification compound fertilizer is made of in proportion following each component:
High purification compound fertilizer of the present invention the preparation method is as follows:
S1. it is fermented to obtain rapeseed meal fermentation material after EM microbial bacterial agent being added into rapeseed meal;By residue of monosodium glutamate, bacteria residue, each Component is pulverized and sieved, and is mixed to get and is pulverized and mixed material;
S2. adjust pH value by rapeseed meal fermentation material and after being pulverized and mixed material mixing, then with potassium sulfate, urea, potassium nitrate, phosphorus ammonium It mixes, is packed after granulation in proportion to obtain the final product;
Wherein, bacteria residue was crushed to 12 meshes;Residue of monosodium glutamate was crushed to 12 meshes;
The process conditions of fermentation described in step S1 are as follows: fermentation temperature is 55 DEG C, fermentation time is 14 days, every turning one in 7 days It is secondary;
Described in step S2 tune pH value be adjusted to pH value be 6;Further, it is preferable to use mass percent concentration for 5% Sulphur acid for adjusting pH value;
Through detecting, the N+P+K total content of the purification compound fertilizer in the present embodiment is 25.6% and N >=6.9%;Moisture contains Amount≤12%, total content >=35% of organic matter.
The preparation of the purification compound fertilizer of embodiment 4
According to mass fraction meter, the purification compound fertilizer is made of in proportion following each component:
High purification compound fertilizer of the present invention the preparation method is as follows:
S1. it is fermented to obtain rapeseed meal fermentation material after lactobacillus plantarum being added into rapeseed meal;By residue of monosodium glutamate, bacteria residue, each group Divide and pulverized and sieved, is mixed to get and is pulverized and mixed material;
S2. adjust pH value by rapeseed meal fermentation material and after being pulverized and mixed material mixing, then with potassium sulfate, urea, potassium nitrate, phosphorus ammonium It mixes, is packed after granulation in proportion to obtain the final product;
Wherein, bacteria residue was crushed to 12 meshes;Residue of monosodium glutamate was crushed to 12 meshes;
The process conditions of fermentation described in step S1 are as follows: fermentation temperature is 55 DEG C, fermentation time is 14 days, every turning one in 7 days It is secondary;
Described in step S2 tune pH value be adjusted to pH value be 6;Further, it is preferable to use mass percent concentration for 5% Sulphur acid for adjusting pH value;
Through detecting, the N+P+K total content of the purification compound fertilizer in the present embodiment is 26% and N >=6.9%;Moisture content ≤ 12%, total content >=35% of organic matter.
5 application test of embodiment
1. promoting the application effect appraisal of the fertilizer of fruits and vegetables growth:
Nutrient needed for fertilizer of the present invention can quickly supplement fruits and vegetables growth promotes fruits and vegetables growth.For verifying present invention preparation Fertilizer on fruits and vegetables large-scale demonstration apply actual effect, applicant selection experiment and demonstration has been carried out on watermelon.
1 materials and methods
1.1 are located in Zixing City watermelon base for examination place 1, and 10 mu of testing ground area, soil fertility level is more uniform.
1.2 for studying 1 watermelon of object, rattan line-spacing 0.6m*1m, the growing way golden mean of the Confucian school and consistent.
1.3 for examination fertilizer be made from Examples 1 to 4 purification organic and inorganic compound watermelon fertilizer product be powdery or Graininess.
1.4 carry out each 2 mu of each processing group of 5 test process for examination place:
1. example 1 group: soil is irrigated into bottom water, by embodiment 1 prepare for examination fertilizer with 80kg/ it is per mu it is even apply, Every month applies 5kg urea and 5kg potassium sulfate per acre after plantation seedling, applies to water leaching.
2. 2 groups of embodiment: soil is irrigated into bottom water, by embodiment 2 prepare for examination fertilizer with 80kg/ it is per mu it is even apply, Every month applies 5kg urea and 5kg potassium sulfate per acre after plantation seedling, applies to water leaching.
3. 3 groups of embodiment: soil is irrigated into bottom water, by embodiment 3 prepare for examination fertilizer with 80kg/ it is per mu it is even apply, Every month applies 5kg urea and 5kg potassium sulfate per acre after plantation seedling, applies to water leaching.
4. 4 groups of embodiment: soil is irrigated into bottom water, by embodiment 4 prepare for examination fertilizer with 80kg/ it is per mu it is even apply, Every month applies 5kg urea and 5kg potassium sulfate per acre after plantation seedling, applies to water leaching.
5. control group (CK): being replaced every time with the similar outer production fertilizer of same experimental group equivalent for trying fertilizer (Sichuan Lei Nanong per acre Crop composite chemical fertilizer) same time progress, the same processing of other measures of fertilizer is 1..
Embodiment group and control group are managed by local conventional cultivation technology.10 plants are determined in each processing at random The average value of melon vine investigation fruit size when the first fringe fruit is expanded and before harvesting, statistics per mu yield, each processing fruit product of detection Matter.2 results and analysis
The influence of 2.1 pairs of per mu yields
Statistics strain number per acre, random 10 points of samplings, counts total fruiting number, claims fresh fruit weight, calculates total fruiting number, single fresh The average value of fruit weight calculates theoretical per mu yield.
Through calculating, 1000 plants of watermelon vines, the average value of fruiting number, single fresh fruit weight and per mu yield such as table 1 are planted per acre. As shown in Table 1, having used the watermelon of the fertilizer, single fresh fruit increases 36.4% again compared to the control group, realizes that per mu yield increases Rate nearly 70%, effect is considerable.
Table 1
The influence of 2.2 pairs of soluble solid contents
It squeezes the juice after taking several fresh fruits to remove the peel at random, measures soluble fixture content, experimental group and control group respectively measure It 5 times, is averaged.Experimental result is as shown in table 2.
As shown in Table 2, which improves a lot to the fruit quality of watermelon, soluble solid content compared to pair About 20% is increased according to group.
Table 2
Processing Soluble solid content/%
Example 1 group 13.6
2 groups of embodiment 14.5
3 groups of embodiment 15.1
4 groups of embodiment 14.6
Control group 11.9
The above description is only a preferred embodiment of the present invention, is not intended to restrict the invention, for those skilled in the art For member, the invention may be variously modified and varied.All within the spirits and principles of the present invention, it is made it is any modification, Equivalent replacement, improvement etc. should be included within scope of the invention.

Claims (10)

1. a kind of purification compound fertilizer, which is characterized in that by potassium sulfate, potassium nitrate, urea, phosphorus ammonium and containing the material mixing of organic matter It forms, the total content of the organic matter is 34 ~ 36%, and the total content of N, P, K are 24.5~26%;The substance containing organic matter is Residue of monosodium glutamate, bacteria residue, rapeseed meal.
2. purification compound fertilizer according to claim 1, which is characterized in that the content of organic matter that the bacteria residue provides is 24.5 ~25.4%;The content of organic matter that the rapeseed meal provides is 2.6 ~ 3.2%;The content of organic matter 6.3 ~ 7.3% that the residue of monosodium glutamate provides.
3. purification compound fertilizer according to claim 1, which is characterized in that the content of organic matter that the bacteria residue provides is 25%; The content of organic matter that the rapeseed meal provides is 3%;The content of organic matter 7% that the residue of monosodium glutamate provides.
4. purification compound fertilizer according to claim 1, which is characterized in that the total content of N always contains in the purification compound fertilizer >=6.9% is measured, the N+P+K total content in the bacteria residue is 3.25%.
5. purification compound fertilizer according to claim 1, which is characterized in that according to mass fraction meter, the purification compound fertilizer It is made of in proportion following each component:
190 ~ 210 parts of potassium sulfate;
115 ~ 125 parts of urea;
45 ~ 55 parts of potassium nitrate;
65 ~ 75 parts of phosphorus ammonium;
95 ~ 105 parts of residue of monosodium glutamate;
490 ~ 510 parts of bacteria residue;
55 ~ 65 parts of rapeseed meal.
6. purification compound fertilizer according to claim 1, which is characterized in that according to mass fraction meter, the purification compound fertilizer It is made of in proportion following each component:
200 parts of potassium sulfate;
120 parts of urea;
50 parts of potassium nitrate;
70 parts of phosphorus ammonium;
100 parts of residue of monosodium glutamate;
500 parts of bacteria residue;
60 parts of rapeseed meal.
7. the preparation method of any one of claim 1 to the 6 purification compound fertilizer, which comprises the following steps:
S1. it is fermented to obtain rapeseed meal fermentation material after bio-fermentation agent being added into rapeseed meal;By residue of monosodium glutamate, bacteria residue, each component into Row pulverizes and sieves, and is mixed to get and is pulverized and mixed material;
S2. pH value is adjusted by rapeseed meal fermentation material and after being pulverized and mixed material mixing, then in proportion with potassium sulfate, urea, potassium nitrate, phosphorus ammonium Mixing, packs or packs after being granulated to obtain the final product;
The bio-fermentation agent is one of aspergillus niger microbial inoculum, bacillus subtilis, lactobacillus plantarum, EM microbial bacterial agent; The ratio between the bio-fermentation agent and rapeseed meal are 1:20 ~ 30.
8. purification compound fertilizer according to claim 7, which is characterized in that the bacteria residue was crushed to 10 ~ 20 meshes;It is described Residue of monosodium glutamate was crushed to 10 ~ 30 meshes.
9. purification compound fertilizer according to claim 7, which is characterized in that the technological parameter of fermentation described in step S1 are as follows: Fermentation temperature is 55~60 DEG C, fermentation time is 10 ~ 14 days, and every turning in 4~7 days is primary.
10. the application of any one of claim 1 to the 9 purification compound fertilizer, which is characterized in that applied to as avoiding chlorine fruits and vegetables kind The base manure of plant or top dressing.
CN201711427160.4A 2017-12-25 2017-12-25 A kind of purification compound fertilizer and its preparation method and application Withdrawn CN109956780A (en)

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Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101041807A (en) * 2007-03-06 2007-09-26 北京万泰新源生物科技有限公司 Fertilizer leaven and preparation method and application thereof
CN103288544A (en) * 2013-06-14 2013-09-11 河北新世纪周天生物科技有限公司 Production process of biological compound fertilizer
CN103588579A (en) * 2013-11-22 2014-02-19 宁夏共享集团有限责任公司 Organic-inorganic compound fertilizer special for watermelons and production method of organic-inorganic compound fertilizer
CN107011045A (en) * 2017-04-18 2017-08-04 高青山 A kind of wheat planting benefit nitrogen organic slow-release fertilizer

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101041807A (en) * 2007-03-06 2007-09-26 北京万泰新源生物科技有限公司 Fertilizer leaven and preparation method and application thereof
CN103288544A (en) * 2013-06-14 2013-09-11 河北新世纪周天生物科技有限公司 Production process of biological compound fertilizer
CN103588579A (en) * 2013-11-22 2014-02-19 宁夏共享集团有限责任公司 Organic-inorganic compound fertilizer special for watermelons and production method of organic-inorganic compound fertilizer
CN107011045A (en) * 2017-04-18 2017-08-04 高青山 A kind of wheat planting benefit nitrogen organic slow-release fertilizer

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