CN1098883A - The production method of Gynostemma pentaphyllum honey and goods thereof - Google Patents
The production method of Gynostemma pentaphyllum honey and goods thereof Download PDFInfo
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- CN1098883A CN1098883A CN 93109949 CN93109949A CN1098883A CN 1098883 A CN1098883 A CN 1098883A CN 93109949 CN93109949 CN 93109949 CN 93109949 A CN93109949 A CN 93109949A CN 1098883 A CN1098883 A CN 1098883A
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- gynostemma pentaphyllum
- honey
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- gynostemma
- total saponin
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Abstract
The bee product that the present invention relates to a kind of drink producing method and produce by this method.It is raw material with the gynostemma pentaphyllum herb, extracts the gynosaponin concentrate.Be that main component is formulated with pure honey according to a certain ratio.Be characterized in adopting in the gynostemma pentaphyllum total saponin extraction process purifying process of low temperature diacolation, gradient elution and gelatin dehydrating agent Combined Processing, improved the yield of total saponin.Its technological process is simple, and raw material sources are wide, and constant product quality can be stored 18 months under the normal temperature, and this beverage has been concentrated the nutritive value of the effective-part of Gynostemma pentaphyllum and honey, is a kind of health natural beverage.
Description
The present invention relates to a kind of generation method of beverage and the goods of producing by this method.
Before the present invention makes, the honey preparation method who contains the gynostemma pentaphylla composition, can be referring to the clear 59-215376 patent application of Japanese publication, this patent application has proposed a kind of honey preparation method who contains the gynostemma pentaphylla composition, the herb that will belong to gynostemma pentaphylla (Curcurbitaceae) plant, contain saponin 30-50 gram, ratio adding decocting in 300ml is endured, again with granulated sugar and honey dissolving, make it compound, make the bait of honeybee, by the honeybee body of honeybee, can form the invertase of honey in the honeybee body, thereby generate the honey that contains the gynosaponin essence.
The design of this invention is the honey product that obtains to contain the gynosaponin composition by the bio-transformation expectation, its shortcoming is, producing this Gynostemma pentaphyllum honey, to influence the factor of bio-transformation many, transformation period is longer, can the Gynostemma pentaphyllum honey finished product that once transform needed by human body be difficult to prediction, simultaneously, prepares Gynostemma pentaphyllum honey according to this mode, the yield of its product and production cost thereof are all wayward, bring certain risk and difficulty to suitability for industrialized production.
Task of the present invention is directly to produce the Gynostemma pentaphyllum honey that contains the gynosaponin composition with artificial method, improve existing gynostemma pentaphyllum total saponin extraction process, determine the proportioning of this beverage, and produce honey and the honeybee product that contains the gynostemma pentaphyllum total saponin composition by this method.
The present invention realizes according to following technical scheme:
The blue drink producing method of a kind of strand glue, at first the herb with gynostemma pentaphylla (five leaves or seven leaf gynostemma pentaphyllums) plant cleans, oven dry, chopping, extract its total saponin mixed liquor with the chemical method of routine, it is characterized in that, described extraction process for total saponin is that gynostemma pentaphyllum herb (doing) is added 4-6 low-concentration ethanol doubly, extract the gynostemma pentaphyllum total saponin crude extract through insulation diacolation technology, add 3-5 then doubly (by weight, down with) ethanol of concentration from low to high, gynostemma pentaphyllum herb is carried out gradient elution, merging filtrate also concentrates, at this concentrate, middle adding edible gelatin and ethanol are regulated pH value and are carried out purifying, obtain the gynostemma pentaphyllum total saponin concentrate with this concentrate with 1: 40-60 ratio (by weight) be mixed through impurity elimination and the pure honey that concentrates, make a kind of Gynostemma pentaphyllum honey drink that contains the gynostemma pentaphyllum total saponin composition through the sterilization bottling.
More detailed invention details is by realizing in the following technical scheme:
In the gynostemma pentaphyllum total saponin extracting method, low temperature diacolation technology wherein comprises: the gynostemma pentaphyllum herb of chopping is added the doubly ethanol of (by weight) 65% of 4-6, be lower than 35 ℃ in temperature, in the PH7-9 scope, the certain flow of control extract, the gynostemma pentaphyllum herb insulation was soaked 8-12 hour, promptly obtain the gynostemma pentaphyllum total saponin refining liquid.
In the gynostemma pentaphyllum total saponin extracting method, gradient elution technology wherein comprises: doubly measure by above-mentioned gynostemma pentaphyllum herb and ethanol 1: 3-5 and add 70%, 80%, 90% and 95% ethanol respectively and handle 8-12 hour successively to gynostemma pentaphyllum herb or filter residue control flow, drip washing is for several times repeatedly to high concentration ethanol by low concentration, merging filtrate, be concentrated into 1: 1(V: V, strand bluegrass: gynosaponin concentrate concentrate).
In order further to remove gynostemma pentaphylla hardship, fishy smell and other impurity, need obtaining concentrate is carried out impurity elimination and purifying, this purifying process comprises: add 1 in this gynostemma pentaphylla concentrate: 18-22 (weight meter) 2% edible gelatin aqueous solution doubly, under PH3-6, left standstill 30 minutes, meanwhile, by 1: 3-5 95% ethanol doubly adds this concentrate rapidly, adjust PH3-6, stand at low temperature 8-12 hour, filter impurity elimination, through repeated treatments with this solution concentration to 1: 1 (gynostemma pentaphyllum herb: concentrate) gained filtrate is required gynostemma pentaphyllum total saponin concentrate by weight.
The half-finished preparation of honey selects natural honey to filter through 180-220 order filter cloth, concentrates 30 minutes in 65-75 ℃ of following vacuum, makes this honey be condensed into the honey of Baume 41-42 degree, is required pure honey.
With the gynostemma pentaphyllum total saponin concentrate for preparing in 1: 40-60 ratio (weight) be mixed with pure honey (vitamin C that also can add or not add 0.5-1 gram/Kg for the nutrition that improves this drink), looking canned condition can add maybe and needn't add the food preservative potassium sorbate, its addition is below the 0.2 gram/Kg of this Gynostemma pentaphyllum honey drink, through the Gynostemma pentaphyllum honey of packing steam sterilization method routinely, be finished product through check.
The beverage of making by the present invention, at least comprise gynosaponin composition through artificial extraction, this beverage contains the gynosaponin (panaxoside juice) of 8ppm at least, wherein the gynostemma pentaphyllum total saponin concentrate (with the ratio of gynostemma pentaphyllum herb volume be 1: 1) with the proportioning of the pure honey of Baume 41-42 degree be 1: 40-60, best proportioning is 1: 50, add or do not add Vc0.5-1 gram/Kg again, look canned condition, add or do not add food preservative sorbic acid acid potassium, its addition (by beverage weight) is below the 0.2g/Kg, produces Gynostemma pentaphyllum honey or other honeybee drink by this proportioning.
The Gynostemma pentaphyllum honey that the present invention produces detects through institute for drug control, Hubei Province and health and epidemic prevention department, and its total saponin content meets the standard that the Ministry of Public Health formulates.Health and physical and chemical index meet relative national standards.This Gynostemma pentaphyllum honey outward appearance is amber, and it is sweet slightly bitter to distinguish the flavor of, and has typical gynostemma pentaphylla local flavor and natural honey fragrant.This drink contains multiple saponin component, wherein content of ginsenoside is abundant, also contain nutritional labelings such as several amino acids, glucose, fructose, vitamin, selenium, calcium, iron, zinc, this drink combines the two advantage of gynostemma pentaphylla and honey, and finished product can be preserved 18 months at normal temperatures.Long-period drinking of said product is of value to health, does not have bad side effect, is a kind of desirable full-natural nutritive health beverages.
Compared with the prior art, advantage of the present invention is:
1, raw material sources are wide, be not subject to seasonal restrictions, and work simplification, with short production cycle;
2, Gynostemma pentaphyllum honey is nutritious, and wherein the stable content of important component gynostemma pentaphyllum total saponin can artificially be controlled, and product yield height is easy to use, thereby curative effect is reliable and stable by the product that the bio-transformation of bee variety body comes;
3, production cost than honeybee body transform low, and devoid of risk can be produced in the anniversary.
Introduce embodiments of the invention below:
Raw material and proportioning thereof are formed (unit: Kg)
By each embodiment first step of last table is that used five leaves or seven leaf gynostemma pentaphyllum raw materials and ratio thereof add doubly (weight) 65% ethanol of 4-6 with its hay, below 35 ℃, PH7-9, carry out the low temperature diacolation in the 8-12 scope, get crude extract, then with 70%, 80%, 90% and 95% concentration of alcohol carries out gradient elution in proper order, handled 8-12 hour, the ethanol addition is 3-5 a times of hay weight, merge each time filtrate, make 1: 1 gynostemma pentaphylla concentrate (gynostemma pentaphylla hay: concentrate, V: V), add 1 respectively at last: 18-22 (weight meter) 2% edible gelatin aqueous solution doubly, left standstill under PH3-6 30 minutes, meanwhile, by 1: 3-5 95% ethanol doubly adds this concentrate rapidly, adjust PH3-6, stand at low temperature 8-12 hour,, promptly obtain required gynostemma pentaphyllum total saponin concentrate with the smart filter of plate and frame type filter-press; Second step was that the honey with different cultivars filters respectively, be concentrated into the pure honey of proportion 41-42 Baume degrees, at last with above-mentioned gynostemma pentaphylla concentrate in 1: 40-60(weight), being mixed with pure honey, (making finished product finally contain gynostemma pentaphyllum total saponin, is 8ppm in panaxoside content; Add or do not add Vc0.5-1 to restrain/Kg), through bottling, steam sterilization.Check is finished product.
Claims (9)
1, the blue drink producing method of a kind of strand glue, the herb of gynostemma pentaphylla plant is cleaned, oven dry, chopping, extract its total saponin mixed liquor with the chemical method of routine, it is characterized in that, described extraction process for total saponin is that gynostemma pentaphyllum herb (doing) is added 4-6 low-concentration ethanol doubly, extract the gynostemma pentaphyllum total saponin crude extract through insulation diacolation technology, add then 3-5 doubly from low to high the ethanol of concentration gynostemma pentaphyllum herb is carried out gradient elution, merging filtrate also concentrates, adding edible gelatin and ethanol adjusting pH value carries out purifying in this concentrate, obtain the gynostemma pentaphyllum total saponin concentrate, with this concentrate with 1: 40-60 ratio (by weight) be mixed through impurity elimination and the pure honey that concentrates, make a kind of Gynostemma pentaphyllum honey that contains the gynostemma pentaphyllum total saponin composition through the sterilization bottling.
2, the method for claim 1, it is characterized in that described insulation diacolation technology comprises that the gynostemma pentaphyllum herb with chopping adds the doubly ethanol of (by weight) 65% of 4--6, be lower than 35 ℃ in temperature, in the PH7-9 scope, the certain flow of control extract, the gynostemma pentaphyllum herb insulation was soaked 8-12 hour, promptly obtain the gynostemma pentaphyllum total saponin crude extract.
3, method as claimed in claim 1 or 2, it is characterized in that, described gradient elution technology comprises: by above-mentioned gynostemma pentaphyllum herb and ethanol 1: 3-5 doubly (by weight) add 70%, 80%, 90% and 95% ethanol respectively and handle 8-12 hour successively gynostemma pentaphyllum herb or filter residue control flow, drip washing is for several times repeatedly to high concentration ethanol by low concentration, merging filtrate, be concentrated into 1: 1(V: V, strand bluegrass: gynosaponin concentrate concentrate).
4, as claim 1 or 3 described methods, it is characterized in that: described gynosaponin purifying process comprises: add 1 in this gynostemma pentaphylla concentrate: 18-22 (weight meter) 2% edible gelatin aqueous solution doubly, left standstill under PH3-6 30 minutes.
5, method as claimed in claim 4, it is characterized in that, also comprise at described gynosaponin liquid purifying process: add 1 in this gynostemma pentaphylla concentrate: 3-5 is 95% ethanol of (weight meter) doubly, at PH3-6, stand at low temperature 8-12 hour, filter impurity elimination, with this solution concentration to 1: 1(V: V, gynostemma pentaphyllum herb: concentrate) gained filtrate is required gynostemma pentaphyllum total saponin concentrate.
6, the method for claim 1 is characterized in that, adopts natural honey after filtration, concentrates 30 minutes in 65-75 ℃ of following vacuum, makes this honey be condensed into the honey of Baume 41-42 degree, is required pure honey.
7, as claim 1 or 6 described methods, it is characterized in that can adding in the described Gynostemma pentaphyllum honey (or not adding) vitamin C, its addition is the 0.5-1 gram/Kg of Gynostemma pentaphyllum honey (by weight).
8, as claim 1 or 6 described methods, it is characterized in that can adding (or not adding) food preservative potassium sorbate at Gynostemma pentaphyllum honey, its addition is below the 0.2g/Kg of Gynostemma pentaphyllum honey (weight).
9, a kind of production of natural drink, this beverage comprises the gynosaponin composition of artificial extraction at least, it is characterized in that this beverage contains the gynosaponin of 8ppm at least, wherein the gynostemma pentaphyllum total saponin concentrate (with the ratio of gynostemma pentaphyllum herb weight be 1: 1) with the proportioning of the pure honey of Baume 41-42 degree be 1: 40-60(weight meter), best proportioning is 1: 50, add or do not add Vc0.5-1 gram/Kg again, look canned condition, add or do not add the food preservative potassium sorbate, its addition (by beverage weight) is below the 0.2g/Kg, produces Gynostemma pentaphyllum honey or other honeybee drink by this proportioning.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 93109949 CN1098883A (en) | 1993-08-20 | 1993-08-20 | The production method of Gynostemma pentaphyllum honey and goods thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 93109949 CN1098883A (en) | 1993-08-20 | 1993-08-20 | The production method of Gynostemma pentaphyllum honey and goods thereof |
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| CN1098883A true CN1098883A (en) | 1995-02-22 |
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| CN 93109949 Pending CN1098883A (en) | 1993-08-20 | 1993-08-20 | The production method of Gynostemma pentaphyllum honey and goods thereof |
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Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102302110A (en) * | 2011-06-08 | 2012-01-04 | 蒋科罡 | Fiveleaf gynostemma herb health-care honey and preparation method |
| CN107048416A (en) * | 2017-03-30 | 2017-08-18 | 大连大学 | A kind of krill polypeptide compound preparation and preparation method with oxidation resistance |
| CN108618150A (en) * | 2018-06-12 | 2018-10-09 | 三明市园艺学会 | A kind of liver-protecting fat-dropping Capsules of health productions and its manufacture craft |
| CN111815202A (en) * | 2020-07-31 | 2020-10-23 | 四川生态诚品农业开发有限公司 | Prediction method and system for honey production |
-
1993
- 1993-08-20 CN CN 93109949 patent/CN1098883A/en active Pending
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102302110A (en) * | 2011-06-08 | 2012-01-04 | 蒋科罡 | Fiveleaf gynostemma herb health-care honey and preparation method |
| CN107048416A (en) * | 2017-03-30 | 2017-08-18 | 大连大学 | A kind of krill polypeptide compound preparation and preparation method with oxidation resistance |
| CN108618150A (en) * | 2018-06-12 | 2018-10-09 | 三明市园艺学会 | A kind of liver-protecting fat-dropping Capsules of health productions and its manufacture craft |
| CN111815202A (en) * | 2020-07-31 | 2020-10-23 | 四川生态诚品农业开发有限公司 | Prediction method and system for honey production |
| CN111815202B (en) * | 2020-07-31 | 2023-08-11 | 四川生态诚品农业开发有限公司 | Honey production prediction method and system |
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