CN1083379A - Cassia occidentalis extraction process and preparation method of cassia occidentalis crystal cassia occidentalis beverage - Google Patents
Cassia occidentalis extraction process and preparation method of cassia occidentalis crystal cassia occidentalis beverage Download PDFInfo
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- CN1083379A CN1083379A CN 93108879 CN93108879A CN1083379A CN 1083379 A CN1083379 A CN 1083379A CN 93108879 CN93108879 CN 93108879 CN 93108879 A CN93108879 A CN 93108879A CN 1083379 A CN1083379 A CN 1083379A
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- semen cassiae
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- clear paste
- cassia occidentalis
- beverage
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- 235000013361 beverage Nutrition 0.000 title claims abstract description 14
- 239000013078 crystal Substances 0.000 title claims abstract description 8
- 238000000605 extraction Methods 0.000 title claims description 8
- 244000062995 Cassia occidentalis Species 0.000 title abstract 5
- 235000001948 Cassia occidentalis Nutrition 0.000 title abstract 5
- 238000002360 preparation method Methods 0.000 title description 2
- 238000000034 method Methods 0.000 claims abstract description 13
- 244000037364 Cinnamomum aromaticum Species 0.000 claims abstract description 8
- 235000014489 Cinnamomum aromaticum Nutrition 0.000 claims abstract description 8
- 239000000284 extract Substances 0.000 claims abstract description 4
- 210000000582 semen Anatomy 0.000 claims description 29
- 238000004519 manufacturing process Methods 0.000 claims description 11
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 10
- 239000003814 drug Substances 0.000 claims description 8
- WVDDGKGOMKODPV-UHFFFAOYSA-N Benzyl alcohol Chemical compound OCC1=CC=CC=C1 WVDDGKGOMKODPV-UHFFFAOYSA-N 0.000 claims description 6
- 238000001035 drying Methods 0.000 claims description 6
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 5
- 229930006000 Sucrose Natural products 0.000 claims description 5
- CZMRCDWAGMRECN-UGDNZRGBSA-N Sucrose Chemical compound O[C@H]1[C@H](O)[C@@H](CO)O[C@@]1(CO)O[C@@H]1[C@H](O)[C@@H](O)[C@H](O)[C@@H](CO)O1 CZMRCDWAGMRECN-UGDNZRGBSA-N 0.000 claims description 5
- 239000000654 additive Substances 0.000 claims description 5
- 230000000996 additive effect Effects 0.000 claims description 5
- 229940079593 drug Drugs 0.000 claims description 5
- 238000012856 packing Methods 0.000 claims description 5
- KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid Chemical compound OC(=O)CC(O)(C(O)=O)CC(O)=O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 claims description 4
- 238000001914 filtration Methods 0.000 claims description 4
- 239000008187 granular material Substances 0.000 claims description 4
- 239000000203 mixture Substances 0.000 claims description 4
- 239000000706 filtrate Substances 0.000 claims description 3
- 238000003756 stirring Methods 0.000 claims description 3
- 239000004677 Nylon Substances 0.000 claims description 2
- 229910000831 Steel Inorganic materials 0.000 claims description 2
- 235000019445 benzyl alcohol Nutrition 0.000 claims description 2
- 238000004140 cleaning Methods 0.000 claims description 2
- 238000001816 cooling Methods 0.000 claims description 2
- 239000003651 drinking water Substances 0.000 claims description 2
- 235000020188 drinking water Nutrition 0.000 claims description 2
- 238000011049 filling Methods 0.000 claims description 2
- 230000008676 import Effects 0.000 claims description 2
- 239000012535 impurity Substances 0.000 claims description 2
- 229920001778 nylon Polymers 0.000 claims description 2
- 239000002244 precipitate Substances 0.000 claims description 2
- 239000010959 steel Substances 0.000 claims description 2
- 230000001954 sterilising effect Effects 0.000 claims description 2
- 238000004659 sterilization and disinfection Methods 0.000 claims description 2
- 238000009472 formulation Methods 0.000 claims 1
- 239000013521 mastic Substances 0.000 claims 1
- 230000008569 process Effects 0.000 abstract description 3
- 150000001413 amino acids Chemical class 0.000 abstract description 2
- 239000011573 trace mineral Substances 0.000 abstract description 2
- 235000013619 trace mineral Nutrition 0.000 abstract description 2
- CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 description 4
- LQGUBLBATBMXHT-UHFFFAOYSA-N chrysophanol Chemical compound C1=CC=C2C(=O)C3=CC(C)=CC(O)=C3C(=O)C2=C1O LQGUBLBATBMXHT-UHFFFAOYSA-N 0.000 description 4
- 206010010774 Constipation Diseases 0.000 description 3
- 239000000047 product Substances 0.000 description 3
- CFLNHFUPWNRWJA-UHFFFAOYSA-N Obtusin Chemical compound O=C1C2=CC(C)=C(O)C(OC)=C2C(=O)C2=C1C=C(OC)C(OC)=C2O CFLNHFUPWNRWJA-UHFFFAOYSA-N 0.000 description 2
- OBBJQZSMXOJMCN-UHFFFAOYSA-N Obtusin Natural products COc1cc2C=CC(=O)Oc2c3OCC(Oc13)C(=C)C OBBJQZSMXOJMCN-UHFFFAOYSA-N 0.000 description 2
- 230000008901 benefit Effects 0.000 description 2
- HVYWMOMLDIMFJA-DPAQBDIFSA-N cholesterol Chemical compound C1C=C2C[C@@H](O)CC[C@]2(C)[C@@H]2[C@@H]1[C@@H]1CC[C@H]([C@H](C)CCCC(C)C)[C@@]1(C)CC2 HVYWMOMLDIMFJA-DPAQBDIFSA-N 0.000 description 2
- 239000006071 cream Substances 0.000 description 2
- 238000005516 engineering process Methods 0.000 description 2
- 239000003205 fragrance Substances 0.000 description 2
- 239000000049 pigment Substances 0.000 description 2
- 239000006228 supernatant Substances 0.000 description 2
- FPIPGXGPPPQFEQ-UHFFFAOYSA-N 13-cis retinol Natural products OCC=C(C)C=CC=C(C)C=CC1=C(C)CCCC1(C)C FPIPGXGPPPQFEQ-UHFFFAOYSA-N 0.000 description 1
- FFRBMBIXVSCUFS-UHFFFAOYSA-N 2,4-dinitro-1-naphthol Chemical group C1=CC=C2C(O)=C([N+]([O-])=O)C=C([N+]([O-])=O)C2=C1 FFRBMBIXVSCUFS-UHFFFAOYSA-N 0.000 description 1
- 208000002177 Cataract Diseases 0.000 description 1
- 235000005979 Citrus limon Nutrition 0.000 description 1
- 244000131522 Citrus pyriformis Species 0.000 description 1
- 206010010144 Completed suicide Diseases 0.000 description 1
- 206010010741 Conjunctivitis Diseases 0.000 description 1
- 241000196324 Embryophyta Species 0.000 description 1
- 208000010412 Glaucoma Diseases 0.000 description 1
- 206010019233 Headaches Diseases 0.000 description 1
- 206010022998 Irritability Diseases 0.000 description 1
- 244000269722 Thea sinensis Species 0.000 description 1
- FPIPGXGPPPQFEQ-BOOMUCAASA-N Vitamin A Natural products OC/C=C(/C)\C=C\C=C(\C)/C=C/C1=C(C)CCCC1(C)C FPIPGXGPPPQFEQ-BOOMUCAASA-N 0.000 description 1
- -1 adding and stirring Chemical compound 0.000 description 1
- FPIPGXGPPPQFEQ-OVSJKPMPSA-N all-trans-retinol Chemical compound OC\C=C(/C)\C=C\C=C(/C)\C=C\C1=C(C)CCCC1(C)C FPIPGXGPPPQFEQ-OVSJKPMPSA-N 0.000 description 1
- 235000001014 amino acid Nutrition 0.000 description 1
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- 239000008280 blood Substances 0.000 description 1
- 230000036772 blood pressure Effects 0.000 description 1
- 230000008859 change Effects 0.000 description 1
- NZPQWZZXRKZCDU-UHFFFAOYSA-N chrysophanol Natural products Cc1cc(O)c2C(=O)c3c(O)cccc3Oc2c1 NZPQWZZXRKZCDU-UHFFFAOYSA-N 0.000 description 1
- 239000008294 cold cream Substances 0.000 description 1
- 239000012141 concentrate Substances 0.000 description 1
- 235000009508 confectionery Nutrition 0.000 description 1
- 201000010099 disease Diseases 0.000 description 1
- 208000037265 diseases, disorders, signs and symptoms Diseases 0.000 description 1
- 235000013399 edible fruits Nutrition 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 208000001780 epistaxis Diseases 0.000 description 1
- 239000010685 fatty oil Substances 0.000 description 1
- 235000013305 food Nutrition 0.000 description 1
- 235000011389 fruit/vegetable juice Nutrition 0.000 description 1
- 210000000232 gallbladder Anatomy 0.000 description 1
- 210000004907 gland Anatomy 0.000 description 1
- 231100000869 headache Toxicity 0.000 description 1
- 235000013402 health food Nutrition 0.000 description 1
- 210000000936 intestine Anatomy 0.000 description 1
- 210000004185 liver Anatomy 0.000 description 1
- 239000002398 materia medica Substances 0.000 description 1
- 231100000957 no side effect Toxicity 0.000 description 1
- 235000008935 nutritious Nutrition 0.000 description 1
- 210000001328 optic nerve Anatomy 0.000 description 1
- 230000000144 pharmacologic effect Effects 0.000 description 1
- 230000001737 promoting effect Effects 0.000 description 1
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- 235000018102 proteins Nutrition 0.000 description 1
- 102000004169 proteins and genes Human genes 0.000 description 1
- 108090000623 proteins and genes Proteins 0.000 description 1
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- 230000009467 reduction Effects 0.000 description 1
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- 235000019155 vitamin A Nutrition 0.000 description 1
- 239000011719 vitamin A Substances 0.000 description 1
- 229940045997 vitamin a Drugs 0.000 description 1
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Abstract
A process for extracting the cassia seed extract used to prepare beverage, the preparing process of cassia seed crystal and the preparing method of serial beverages are disclosed. Contains various trace elements and amino acids essential to human body. The development of the cassia occidentalis is concerned by the whole society, and the cassia occidentalis has a popularization prospect in China and a wide prospect of entering the international market.
Description
The present invention relates to a kind of manufacture method of body-care beverage, it comprises the extraction process of Semen Cassiae clear paste, the manufacture method of the processing technology of cassia seed crystal and Semen Cassiae beverage.
Semen Cassiae derives from the mature seed of leguminous plant Semen Cassiae, and it is paid attention to by the successive dynasties physician, and Shennong's Herbal is classified it as top grade, and says and can control all ophthalmics, for a long time the clothes benefit with nothing left, make light of one's life by commiting suicide." Japan hanako materia medica " says it: side of body irritability, beneficial smart water is controlled headache, " " the general side of group " " also carried to end epistaxis: " Semen Cassiae can be made cakes and sweetmeats, controls all diseases in the order, side of body liver benefit essence ".Modern pharmacological research proves: the main chemical compositions of Semen Cassiae is U.S. obtusin, obtusin, chrysophanic acid, chrysophanol, protein, fatty oil, natural pigment, vitamin A etc.Has clearing away heat to improve acuity of vision; loosening bowel to relieve constipation; function of gallbladder promoting, strong, the anti-ageing effect of waiting for a long time; optic nerve there is protective effect, is applicable to treatment cataract, glaucoma, conjunctivitis, constipation with heat retention, dryness of the intestine constipation etc., and has the reduction serum cholesterol; the effect of blood fat reducing, blood pressure; according to clinical report: Semen Cassiae reduces serum cholesterol, descends 85% in two weeks, reduces to normal level in all around.Total effective rate is 98%.Semen Cassiae is one band and Japan in China Jiangsu and Zhejiang Provinces, South Korea all has fries the custom of back decocting for tea, it is Ministry of Public Health, State Administration of Traditional Chinese Medicine (87) defend 33 kinds of No. 57 plaintext document regulation of anti-word be food be again one of kind of medicine, have no side effect, nutritious, contain necessary trace element of multiple human body and aminoacid, it is golden yellow that this product is, dense as succinum, the fragrance people that oozes, and the fragrance of similar coffee arranged, look good, smell good and taste good, need not add pigment, fragrant and sweet good to eat, be developed as series beverage, health food, will be subjected to the deepest concern of the whole society, the prospect of popularization is not only arranged at home, and have the bright prospects that squeeze into the international market.
The objective of the invention is in the Semen Cassiae fruit, to extract clear paste, prepare a kind of series beverage that is suitable for body-care.
Extraction process of the present invention is as follows:
Fig. 1 is Semen Cassiae extraction process and beverage production process flow chart.
With the Semen Cassiae after cleaning, put and decoct with water twice in the multi-function extractor, add 10 times of weight of water for the first time and decocted 2 hours, take out and filter.Add for the second time 8 times of weight of water and decocted 2 hours, emit medicine juice, after the filtration filtrate was left standstill 24 hours, extract supernatant, put in the worn-out mouthful concentration pan and concentrate, survey to proportion d=1.04(heat) receive cream.(every 1ml is equivalent to crude drug 2g).
Get cold cream and put in the hermetic container, after times weight 95% ethanol such as adding and stirring, precipitate 12 hours, get supernatant, put recovered alcohol in the concentrating under reduced pressure jar.Being concentrated into proportion is that d=1.04(heat is surveyed), receive cream and place stand-by.(every 1ml is equivalent to crude drug 4g)
The processing technology of cassia seed crystal
Fig. 2 is cassia seed crystal technological process of production figure.
With the clear paste that extracts be concentrated into the crude drug ratio be 1: 10(g/g), get powdered sugar 10kg, add Semen Cassiae clear paste 1kg, (being equivalent to Semen Cassiae 10kg) fully makes granule behind mix homogeneously, and (14 order nylon wire) sieves; To moisture content＜2%, make granule in drying room inner drying (thick 1-2cm, temperature 70-80 ℃), (12 orders do not lure steel mesh) packing, packing, finished product, check, warehouse-in sieve.
The manufacture method of Semen Cassiae beverage:
Prescription (additive): Semen Cassiae clear paste 250ml
White sugar 1250g
Folium Stevlae Rebaudianae 2g
Citric acid 37.5g
Benzyl alcohol 3.125g
Drinking water adds to 25000ml
Method for making: shown in Fig. 1 Semen Cassiae extraction process and beverage production process flow chart: Semen Cassiae clear paste, white sugar are added water mix back adding jacketed pan, send vapour to boil, put charging basket into, add above additive simultaneously, cooling to 120 ℃ of filtrations.Be filtered into batch can then, import 101 ultraviolet sterilizations by pipeline, 102 impurity are handled, and enter mixer again and pour CO
2, H
2O enters filling machine packing, check, gland, finished product, check, packing, warehouse-in.
The preparation of Semen Cassiae series beverage can change the kind and the prescription of additive, just can prepare: Semen Cassiae magnetic water soda pop, Fructus Ananadis comosi type soda pop, Fructus Citri tangerinae type soda pop, lemon type soda pop.
Claims (5)
1, a kind of extraction process of Chinese medicine Semen Cassiae: it is characterized in that this extraction process step is:
A gets the Semen Cassiae after cleaning, and puts in the multi-function extractor, adds 10 times of weight water, decocts 2 hours, and take out and filter,
B gets above-mentioned filtrate and adds 8 times of weight of water once more, puts in the multi-function extractor to decoct 2 hours, and taking-up is left standstill filtrate 24 hours after filtering,
C with the above-mentioned upper clear supernate that leaves standstill, puts and is condensed into proportion in the uncovered concentration pan and is 1.04 the water of (heat is surveyed) is carried clear paste,
D in above-mentioned mastic hermetic container, after 95% ethanol that adds equivalent weight stirs, precipitate 12 hours, gets upper clear supernate, puts that to reclaim wine in the concentrating under reduced pressure pot clear, and being condensed into proportion is the clear paste of 1.04 (heat surveys).
2, a kind of manufacture method of cassia seed crystal, it is characterized in that the clear paste that will extract be concentrated into the crude drug ratio be 1: 10(g/g), getting white sugar 10kg adds Semen Cassiae clear paste 1kg(and is equivalent to Semen Cassiae 10kg) the back system granule (14 order nylon wire) that stirs sieves, in the drying room inner drying to moisture content＜2%, granulate (12 order stainless (steel) wire) sieves.
3, the manufacture method of cassia seed crystal according to claim 2 is characterized in that drying room inner drying temperature is 70-80 ℃.
4, a kind of manufacture method of Semen Cassiae beverage, it is characterized in that the Semen Cassiae clear paste, white sugar, water adds jacketed pan, send vapour to boil to 120 ℃ of filtrations, put charging basket into, add additive simultaneously, cooling, be filtered into jar then, import 101 ultraviolet sterilizations by pipeline, 102 impurity are handled, and enter mixer again and pour CO
2, H
2O enters the filling machine packing.
5, the manufacture method of Semen Cassiae beverage according to claim 4, its additive formulations is:
Semen Cassiae clear paste 250ml
White sugar 1250g
Folium Stevlae Rebaudianae 2g
Acidum Citricum 37.5g
Benzyl alcohol 3.125g
Drinking water adds to 25000ml
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 93108879 CN1083379A (en) | 1993-07-28 | 1993-07-28 | Cassia occidentalis extraction process and preparation method of cassia occidentalis crystal cassia occidentalis beverage |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 93108879 CN1083379A (en) | 1993-07-28 | 1993-07-28 | Cassia occidentalis extraction process and preparation method of cassia occidentalis crystal cassia occidentalis beverage |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN1083379A true CN1083379A (en) | 1994-03-09 |
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN 93108879 Pending CN1083379A (en) | 1993-07-28 | 1993-07-28 | Cassia occidentalis extraction process and preparation method of cassia occidentalis crystal cassia occidentalis beverage |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN1083379A (en) |
Cited By (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2004077967A1 (en) * | 2003-03-03 | 2004-09-16 | Yingbin Quan | Herbal blood-pressure lowering and blood-lipid lower food |
| CN100376177C (en) * | 2005-11-16 | 2008-03-26 | 于兴洲 | Method for preparing beverage of Doushi cassia seed |
| CN104287035A (en) * | 2014-09-30 | 2015-01-21 | 江苏奇力康皮肤药业有限公司 | Method for preparing semen cassiae carbonated beverage |
| CN105533738A (en) * | 2015-12-21 | 2016-05-04 | 株洲千金药业股份有限公司 | Cassia seed extract and preparation method and application thereof |
| CN105594915A (en) * | 2015-12-21 | 2016-05-25 | 株洲千金药业股份有限公司 | Semen cassiae instant tea and preparation method therefor |
| CN105594944A (en) * | 2015-12-21 | 2016-05-25 | 株洲千金药业股份有限公司 | Semen cassiae instant coffee and preparation method thereof |
| CN108739636A (en) * | 2018-05-03 | 2018-11-06 | 山东胜伟旅游发展有限公司 | Utilize the method for salt sward Cassia feed feeding cow |
| CN108887229A (en) * | 2018-05-03 | 2018-11-27 | 山东胜伟旅游发展有限公司 | In the method for the raw rye grass feeding cow of salt |
-
1993
- 1993-07-28 CN CN 93108879 patent/CN1083379A/en active Pending
Cited By (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2004077967A1 (en) * | 2003-03-03 | 2004-09-16 | Yingbin Quan | Herbal blood-pressure lowering and blood-lipid lower food |
| CN100376177C (en) * | 2005-11-16 | 2008-03-26 | 于兴洲 | Method for preparing beverage of Doushi cassia seed |
| CN104287035A (en) * | 2014-09-30 | 2015-01-21 | 江苏奇力康皮肤药业有限公司 | Method for preparing semen cassiae carbonated beverage |
| CN105533738A (en) * | 2015-12-21 | 2016-05-04 | 株洲千金药业股份有限公司 | Cassia seed extract and preparation method and application thereof |
| CN105594915A (en) * | 2015-12-21 | 2016-05-25 | 株洲千金药业股份有限公司 | Semen cassiae instant tea and preparation method therefor |
| CN105594944A (en) * | 2015-12-21 | 2016-05-25 | 株洲千金药业股份有限公司 | Semen cassiae instant coffee and preparation method thereof |
| CN105533738B (en) * | 2015-12-21 | 2018-07-03 | 株洲千金药业股份有限公司 | A kind of cassia seed extract and preparation method and application |
| CN108739636A (en) * | 2018-05-03 | 2018-11-06 | 山东胜伟旅游发展有限公司 | Utilize the method for salt sward Cassia feed feeding cow |
| CN108887229A (en) * | 2018-05-03 | 2018-11-27 | 山东胜伟旅游发展有限公司 | In the method for the raw rye grass feeding cow of salt |
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| C01 | Deemed withdrawal of patent application (patent law 1993) | ||
| WD01 | Invention patent application deemed withdrawn after publication |