CN1097184A - Leaf-spraying growth promotor for crop - Google Patents
Leaf-spraying growth promotor for crop Download PDFInfo
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- CN1097184A CN1097184A CN93107778A CN93107778A CN1097184A CN 1097184 A CN1097184 A CN 1097184A CN 93107778 A CN93107778 A CN 93107778A CN 93107778 A CN93107778 A CN 93107778A CN 1097184 A CN1097184 A CN 1097184A
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- leaf
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- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05G—MIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
- C05G5/00—Fertilisers characterised by their form
- C05G5/20—Liquid fertilisers
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- Life Sciences & Earth Sciences (AREA)
- Pest Control & Pesticides (AREA)
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Fertilizers (AREA)
Abstract
The present invention relates to a kind of preparation method of plant leaf surface spraying growth promotor for crop and the product for preparing by this method thereof, it is characterized in that adopting animal/vegetable protein is raw material, make the multiple amino acids hydrolyzed solution through low-concentration sulfuric acid hydrolysis neutralization, being furnished with four kinds of trace elements and synergistic agent again forms through mixing stirring reaction again, this method is easy, product has wide accommodation, fertilizer efficiency height, it is fast to absorb, consumption is few, cost is low, comprehensive nutrition, isostatic advantage, be suitable for various plant leaf surfaces and spray, its effect of increasing income is remarkable.
Description
The present invention relates to a kind of plant leaf surface and spray fertile preparation method and products thereof, particularly is the preparation method of the leaf-spraying growth promotor for crop formed of the multiple amino acids of raw material and trace element and synergistic agent and by the product of this method preparation with the animal/vegetable protein.
At present by amino acid and the micro-fertilizer for spraying on leaf surface of forming, a kind of preparation method is arranged, it is with the hair that contains keratoprotein of people or fowl, skin, hoof, the angle, blood is raw material, through the reaction that is hydrolyzed of the hydrochloric acid of excessive concentrations, not only the raw material limitation is big, and the employed hydrochloric acid of hydrolysis has been brought too much chlorine root into to amino acid fertilizer, too much chlorine root can make carbohydrate inversion, it is unfavorable that starch in the plant materials is formed, some plant such as tobacco, very sensitive to chlorine, the chlorine of hyperabsorption can make the tobacco weak flavor, easily flame-out, some is not that all plants are all essential for the trace element that this fertilizer adds, and as cobalt element, only is the needed nutritive element of part plant, and cobalt salt costs an arm and a leg, and therefore causes the waste of raw material and increasing of cost; Also having a kind of is that the plant leaf surface of feedstock production sprays fertilizer with fish, this method is that the sulfuric acid with 50% concentration is hydrolyzed, same raw material sources difficulty, and the sulfuric acid consumption is also high, also will remove too much sulfate radical in process of production, consume a large amount of neutralization reagents, the preparation method is complicated, and the same micro-kind that adds is many, some price comparison costliness, and be not that all plant institutes are essential, make cost up equally.
The objective of the invention is to overcome the shortcoming of above-mentioned prior art with not enough, and provide a kind of preparation method of leaf-spraying growth promotor for crop and by the product of this method preparation, it adopts, and the source is wide, many, the low-cost animal/vegetable proteins of kind are raw material, with rational nutritive ingredient prescription and synergistic agent, make leaf-spraying growth promotor for crop have the concentrated fertilizer of comprehensive nutrition effect balancing.
The objective of the invention is to realize: this leaf-spraying growth promotor for crop by following technical proposal, be out of proportion according to N, P in China's long-term application chemical fertilizer process, K, the trace element general lacking is developed, it contains organotrophy composition and inorganic nutrients composition and a large amount of nutritive elements and trace element, under the effect of synergistic agent, not only comprehensive nutrition is supplied balanced, and can reach higher fertilizer efficiency, thereby reach the high yield good harvest.
The organotrophy composition be with vegetable-protein or animal proteinum or animal/vegetable protein with the low concentration sulphuric acid hydrolysis with in ammoniacal liquor or the volatile salt and gained, it contains 20 kinds or be less than 20 seed amino acids, and the inorganic nutrients composition is the present situations of the four big trace elements that generally lack according to civitas terrena and scientific and reasonable formulated.
Contain the plant nutrition synergistic agent in the leaf-spraying growth promotor for crop of the present invention, as ammonium power pyrimidine (by the development and production of contributing Wuchuan service department of Beijing Ke Sheng technology company), it can make plant pass through the easier performance sorption in blade face, the metabolic process that simultaneously can regulate plant, help cell proliferation, improve photosynthesis of plant, promote the synergism of macroelement and fertilizer effect of microelement, improve the utilization ratio of various nutritive elements comprehensively and fully.
The raw materials used vegetable-protein of the present invention can adopt soya-bean cake, cottonseed cake, peanut cake, rapeseed cake, animal proteinum can adopt scleroproein (comprising collagen protein), the sphaeroprotein of people, animal, fowl, as hair, skin, cheese, fish meal, powdered egg.
The preparation method of leaf-spraying growth promotor for crop of the present invention, be made up of the following step:
A) select for use vegetable-protein or animal proteinum or animals and plants mixed protein be raw material in reactor with 20～30% concentration sulfuric acid hydrolysis reaction of heating, 100～120 ℃ of controlled temperature;
B) the said hydrolyzed reaction product is carried out filter cleaner, its filtrate makes its PH=3～7 with ammoniacal liquor or volatile salt neutralization; Perhaps directly neutralize with ammoniacal liquor or volatile salt after hydrolysis reaction, filter cleaner obtains the multiple amino acids hydrolyzed solution then;
C) in the hydrolyzed solution of (b) gained, add inorganic salt or the compound and the synergistic agent ammonium power pyrimidine of boracic, zinc, manganese, molybdenum element, in reactor, mix stirring reaction, promptly obtain leaf-spraying growth promotor for crop product of the present invention.
Used vegetable-protein, animal proteinum, the animals and plants mixed protein of preparation method of the present invention can be the mixing of wherein any one or two kinds of arbitrary proportions, its raw material consumption and sulfuric acid amount ratio are 1: 1.5～2.0, the inorganic salt of the trace element that adds or compound can be any one or two or more combinations, therefore can prepare series product as required.
Product compositions content (by weight) by the leaf-spraying growth promotor for crop of preparation method of the present invention preparation is:
Multiple amino acids hydrolyzed solution 800-1200 part;
Boric acid or borax 40-60 part;
Manganous nitrate or manganous sulfate or manganese monoxide 80-120 part;
Zinc nitrate or zinc sulfate or zinc oxide 80-120 part;
Ammonium molybdate or Sodium orthomolybdate 4-8 part;
Synergistic agent ammonium power pyrimidine 150-200 part.
Each component optimum content (by weight) is:
Multiple amino acids hydrolyzed solution 900-1000 part;
Boric acid or borax 50-60 part;
Manganous nitrate or manganous sulfate or manganese monoxide 90-100 part;
Zinc nitrate or zinc sulfate or zinc oxide 90-100 part;
Ammonium molybdate or Sodium orthomolybdate 5-6 part;
Synergistic agent ammonium power pyrimidine 160-180 part.
Leaf-spraying growth promotor for crop technical target of the product of the present invention is:
The brown brown liquid of outward appearance (can contain throw out)
Proportion 〉=1.05
PH value 3～7
Organotrophy composition 〉=1g/l
Inorganic nutrients composition 〉=1g/l
Dilute with water during use≤2000 times
Compared with the prior art the technology of the present invention has following advantage and effect:
A) because prescription of the present invention is the defective that exists according to China's long-term fertilization, and the rational formula of taking, the comprehensive and effect balancing of its nutritive ingredient;
B) raw material sources are extensive, be easy to get, and low price, cost is low;
C) fertilizer efficiency height absorbs soon, sprays in 20 hours and can absorb fully, and consumption is few, and every mu only needs 0.5～1.0 kilogram, and amount of increase in production is big, and yield-increasing efficiency reaches 10～100%;
D) applied widely, but to all increasing both production and income of crop of each department;
C) the inorganic nutrients composition adopts nitrate, and not only trace element is the desired nutritional of plant, and nitrate radical also is effective nutritive ingredient of crop as nitric nitrogen simultaneously.
Test of products result of the present invention: (seeing Table 1)
Table 1
The crop title sprays stimulation ratio % as a result in period
The jowar corn growing season, the growth vigorous sturdy
Filling stage lodging-prevention, full grains 15-30
Connect table 1
Shift to an earlier date 5 days maturations
Rice and wheat children in tillering phase fringe divides increases the lodging-prevention of tillering
The heading of filling stage change phase is neat,
Full seed, precocious 3 days 15-28
When cotton grew three leaves, aphid was few, thick shape, and the shedding of cotton bolls is few
When growing ten leaves, spray output height, results are 15-28 early
Once, when first the flowers are in blossom,
Before cotton boll splits
Melon to stretch the per 15 days melons in climing back big, and body is big, evenly,
It is good to spray a melon matter, increases sugar, 10-60
Improve output
Each spray once increases setting percentage, the good 10-30 of growing way before and after the peanut beans florescence
Leaf of spray in every month is tender, green after the vegetables final singling, the prosperous 20-100 of growing way
Contain the output height
Quality better of spray in tobacco 10-15 days, volume increase 15-40
Embodiment 1:
Get 250 kilograms of soya-bean cakes, 550 kilograms in 20% concentration sulfuric acid adds the hydrolysis of heating in the reactor simultaneously, controlled temperature 100-120 ℃, reaction finishes, and adds in the ammoniacal liquor and said hydrolyzed liquid, make PH=3, filter then, slagging-off, obtain the multiple amino acids hydrolyzed solution, add 40 kilograms of boric acid again, 80 kilograms of manganous nitrates, 80 kilograms of zinc nitrates, 4 kilograms of ammonium molybdates, 150 kilograms of ammonium power pyrimidines, mix stirring reaction in reactor, promptly having prepared by vegetable-protein is the leaf-spraying growth promotor for crop of raw material.
Embodiment 2:
Get 150 kilograms in pig hair, 150 kilograms of soya-bean cakes (cottonseed cake), 700 kilograms of 25% concentration sulphuric acid solns, add the hydrolysis reaction of heating in the reactor simultaneously, controlled temperature 100-120 ℃, reaction finishes, filter, slagging-off adds ammoniacal liquor and neutralizes in its filtrate, make its PH=5, obtain the multiple amino acids hydrolyzed solution, add 50 kilograms of boraxs again, 100 kilograms of manganous sulfates, 100 kilograms in zinc sulfate, 6 kilograms of Sodium orthomolybdates, 180 kilograms of ammonium power pyrimidines mix stirring reaction in reactor, promptly having prepared by animal/vegetable protein is the leaf-spraying growth promotor for crop of raw material.
Embodiment 3:
Get 400 kilograms in pig hair, 800 kilograms of 30% concentration sulphuric acid solns add the hydrolysis of heating in the reactor simultaneously, controlled temperature 100-120 ℃, reaction finishes the after-filtration slagging-off, and its filtrate neutralizes with volatile salt, make PH=7, add 60 kilograms of boraxs then, manganese monoxide 120 kg, zinc oxide 120 kg, 8 kilograms of Sodium orthomolybdates, 200 kilograms of ammonium power pyrimidines mix stirring reaction in reactor, promptly having prepared by animal proteinum is the leaf-spraying growth promotor for crop of raw material.
Claims (6)
1, a kind of preparation method of leaf-spraying growth promotor for crop is characterized in that being made up of the following step:
A) select for use vegetable-protein or animal proteinum or animals and plants mixed protein be raw material in reactor with 20～30% concentration sulfuric acid hydrolysis reaction of heating, 100～120 ℃ of controlled temperature;
B) the said hydrolyzed reaction product is carried out filter cleaner, its filtrate makes its PH=3～7 with ammoniacal liquor or volatile salt neutralization; Perhaps directly neutralize with ammoniacal liquor or volatile salt after hydrolysis reaction, filter cleaner obtains the multiple amino acids hydrolyzed solution then;
C) in the hydrolyzed solution of (b) gained, add inorganic salt or the compound and the synergistic agent ammonium power pyrimidine of boracic, zinc, manganese, molybdenum element, in reactor, mix stirring reaction, promptly obtain leaf-spraying growth promotor for crop product of the present invention.
2, according to the leaf-spraying growth promotor for crop of the described preparation method's preparation of claim 1, comprise the inorganic salt or the compound of multiple amino acids hydrolyzed solution, trace element, it is characterized in that also adding synergistic agent ammonium power pyrimidine, each component concentration (by weight) is:
Multiple amino acids hydrolyzed solution 800-1200 part;
Boric acid or borax 40-60 part;
Manganous nitrate or manganous sulfate or manganese monoxide 80-120 part;
Zinc nitrate or zinc sulfate or zinc oxide 80-120 part;
Ammonium molybdate or Sodium orthomolybdate 4-8 part;
Synergistic agent ammonium power pyrimidine 150-200 part.
3, leaf-spraying growth promotor for crop according to claim 2 is characterized in that described each component optimum content (by weight) is:
Multiple amino acids hydrolyzed solution 900-1000 part;
Boric acid or borax 50-60 part;
Manganous nitrate or manganous sulfate or manganese monoxide 90-100 part;
Zinc nitrate or zinc sulfate or zinc oxide 90-100 part;
Ammonium molybdate or Sodium orthomolybdate 5-6 part;
Synergistic agent ammonium power pyrimidine 160-180 part.
4, the preparation method of leaf-spraying growth promotor for crop according to claim 1, the raw material that it is characterized in that described vegetable-protein or animal proteinum or animals and plants mixed protein can be wherein the mixing of any one or two kinds of arbitrary proportions.
5, the preparation method of leaf-spraying growth promotor for crop according to claim 1 is characterized in that described raw material consumption and sulfuric acid amount ratio are 1: 1.5～2.0.
6, the preparation method of leaf-spraying growth promotor for crop according to claim 1 is characterized in that the inorganic salt of the trace element that adds or compound can be any one or two or more combinations.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN93107778A CN1097184A (en) | 1993-07-03 | 1993-07-03 | Leaf-spraying growth promotor for crop |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN93107778A CN1097184A (en) | 1993-07-03 | 1993-07-03 | Leaf-spraying growth promotor for crop |
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| Publication Number | Publication Date |
|---|---|
| CN1097184A true CN1097184A (en) | 1995-01-11 |
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| Application Number | Title | Priority Date | Filing Date |
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| CN93107778A Pending CN1097184A (en) | 1993-07-03 | 1993-07-03 | Leaf-spraying growth promotor for crop |
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Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101696133B (en) * | 2009-10-26 | 2011-09-14 | 广东省生态环境与土壤研究所 | Fruit and vegetable nutrition regulator, preparation method thereof and usage method thereof |
| CN103804032A (en) * | 2014-01-28 | 2014-05-21 | 南京农业大学 | Liquid amino acid compound produced by dead porcine proteins and application thereof |
| CN104211480A (en) * | 2014-09-11 | 2014-12-17 | 桂林市和胤祥新型材料有限公司 | Water-soluble nutritional liquid fertilizer containing amino acids and preparation method of water-soluble nutritional liquid fertilizer |
| CN113880641A (en) * | 2021-11-02 | 2022-01-04 | 台沃科技集团股份有限公司 | Preparation method of core-shell type multi-effect foliar fertilizer based on collagen polypeptide nanospheres |
-
1993
- 1993-07-03 CN CN93107778A patent/CN1097184A/en active Pending
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101696133B (en) * | 2009-10-26 | 2011-09-14 | 广东省生态环境与土壤研究所 | Fruit and vegetable nutrition regulator, preparation method thereof and usage method thereof |
| CN103804032A (en) * | 2014-01-28 | 2014-05-21 | 南京农业大学 | Liquid amino acid compound produced by dead porcine proteins and application thereof |
| CN103804032B (en) * | 2014-01-28 | 2015-05-27 | 南京农业大学 | Liquid amino acid compound produced by dead porcine proteins and application thereof |
| CN104211480A (en) * | 2014-09-11 | 2014-12-17 | 桂林市和胤祥新型材料有限公司 | Water-soluble nutritional liquid fertilizer containing amino acids and preparation method of water-soluble nutritional liquid fertilizer |
| CN113880641A (en) * | 2021-11-02 | 2022-01-04 | 台沃科技集团股份有限公司 | Preparation method of core-shell type multi-effect foliar fertilizer based on collagen polypeptide nanospheres |
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