CN109620751A - A kind of micro- peptide freeze-drying wadding and preparation method thereof - Google Patents
A kind of micro- peptide freeze-drying wadding and preparation method thereof Download PDFInfo
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- CN109620751A CN109620751A CN201910110906.1A CN201910110906A CN109620751A CN 109620751 A CN109620751 A CN 109620751A CN 201910110906 A CN201910110906 A CN 201910110906A CN 109620751 A CN109620751 A CN 109620751A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/02—Cosmetics or similar toiletry preparations characterised by special physical form
- A61K8/0204—Specific forms not provided for by any of groups A61K8/0208 - A61K8/14
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
- A61K8/44—Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof
- A61K8/442—Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof substituted by amido group(s)
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/64—Proteins; Peptides; Derivatives or degradation products thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/67—Vitamins
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/20—Chemical, physico-chemical or functional or structural properties of the composition as a whole
- A61K2800/30—Characterized by the absence of a particular group of ingredients
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
- A61K2800/84—Products or compounds obtained by lyophilisation, freeze-drying
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- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Animal Behavior & Ethology (AREA)
- General Health & Medical Sciences (AREA)
- Public Health (AREA)
- Veterinary Medicine (AREA)
- Birds (AREA)
- Epidemiology (AREA)
- Dermatology (AREA)
- Cosmetics (AREA)
- Coloring Foods And Improving Nutritive Qualities (AREA)
- Peptides Or Proteins (AREA)
Abstract
The present invention relates to cosmetic fields, specifically a kind of micro- peptide freeze-drying wadding, Essence containing micro- peptide components is poured into be freeze-dried in vial and is made at after flocculent substance, wherein Essence includes following raw material by weight: micro- peptide mixer 5-35 parts, 70-110 parts of aseptic deionized water；Micro- peptide mixer is the mixture of oligopeptides -1, oligopeptides -2, oligopeptides -3, hexapeptide -11, glutamine and vitamin synthesis.Raw material is easy to generate denaturation or be decomposed in the case where the effect of water and heat changes in the present invention, and the moisture content of 95-99% in substance can be removed by vacuum freeze drying, so that the micro- peptide freeze-drying wadding stability produced is good, is easy to long-term preservation effective component；Using no corrosion-resistant system, irritation is small.
Description
Technical field
The present invention relates to cosmetic field, specifically a kind of micro- peptide freeze-drying wadding and preparation method thereof.
Background technique
With the rapid growth of China's economic, improvement of living standard, people start to pay attention to the image problem of oneself, makeup
The demand of product skin care products increasingly increases, and the product type of existing cosmetics is generally the states such as water and milk frost, and formula composition is generally
Solvent, moisturizer, emollient, active matter, surfactant and preservative composition,
The general cosmetics addition preservative pot-life is 2 years, and active matter can inactivate increase with time and gradually, and consumer makes
Used time is unable to reach expected effect；The general irritation of formula for adding preservative is biggish, can be to the sensitive skin of consumer
It is easy to cause certain adverse reaction.
Therefore it provides a kind of micro- peptide freeze-drying wadding and preparation method thereof, to solve the above problems.
Summary of the invention
The purpose of the present invention is to provide a kind of micro- peptide freeze-drying waddings and preparation method thereof, to solve to mention in above-mentioned background technique
Out the problem of.
To achieve the above object, the invention provides the following technical scheme:
Essence containing micro- peptide components is poured into vial freeze-drying at making after flocculent substance by a kind of micro- peptide freeze-drying wadding
, wherein Essence includes following raw material by weight: micro- peptide mixer 5-35 parts, 70-110 parts of aseptic deionized water；Institute
State the mixture that micro- peptide mixer is oligopeptides -1, oligopeptides -2, oligopeptides -3, hexapeptide -11, glutamine and vitamin synthesis.
As a further solution of the present invention: the Essence containing micro- peptide components is poured into glass by micro- peptide freeze-drying wadding
Freeze-drying is made at after flocculent substance in bottle, and wherein Essence includes following raw material by weight: micro- peptide mixer 7-20
Part, 80-100 parts of aseptic deionized water；Micro- peptide mixer is oligopeptides -1, oligopeptides -2, oligopeptides -3, hexapeptide -11, glutamine
With the mixture of vitamin synthesis.
As further scheme of the invention: the Essence containing micro- peptide components is poured into glass by micro- peptide freeze-drying wadding
Freeze-drying is made at after flocculent substance in glass bottle, and wherein Essence includes following raw material by weight: micro- peptide mixer 10
Part, 90 parts of aseptic deionized water；Micro- peptide mixer is oligopeptides -1, oligopeptides -2, oligopeptides -3, hexapeptide -11, glutamine and dimension
The mixture of raw element synthesis.
As it is a further object to provide a kind of preparation methods of micro- peptide freeze-drying wadding, comprising the following steps:
1), cleaning and sterilizing container, pleura mold and blender；
2), aseptic deionized water is added in blender, is warming up to 45 DEG C, is then stirred the addition of micro- peptide mixer；
3), after stirring, stop blender, heat preservation stands 20-80min under 45 DEG C of environment, then defoams, and obtains clear
Clear transparent micro- peptide Essence；
4) micro- peptide Essence, is subjected to 35-45 DEG C of constant temperature processing, micro- peptide Essence 5ml is into vial ware；
5), the vial ware equipped with micro- peptide Essence is put into freeze drier, pre-freeze control temperature is set as -45 DEG C, holds
Continuous temperature control 160min；
6), freeze drier carries out seven primary drying stages and six parsing-desiccation stages to micro- peptide Essence；
7), freeze drier runs 36.3h, after carrying out freeze-drying molding to Essence, shuts down, and wadding is lyophilized in micro- peptide and is taken out,
Sealing packaging.
As further scheme of the invention: it is 40-60min that the heat preservation in the step 3), which is stood,.
As further scheme of the invention: the temperature that constant temperature is handled in the step 4) is 42 DEG C.
As further scheme of the invention: seven primary dryings that the freeze drier carries out micro- peptide Essence
Stage are as follows:
First stage temperature is set as -35 DEG C, and the duration sets 30min；
Second stage temperature is set as -25 DEG C, and the duration sets 30min；
Phase III temperature is set as -20 DEG C, and the duration sets 30min；
Fourth stage temperature is set as -15 DEG C, and the duration sets 30min；
5th phase temperature is set as -10 DEG C, and the duration sets 120min；
6th phase temperature is set as -5 DEG C, and the duration sets 30min；
7th phase temperature is set as 0 DEG C, and the duration sets 60min.
As further scheme of the invention: six parsing-desiccations that the freeze drier carries out micro- peptide Essence
Stage are as follows:
First stage temperature is set as 10 DEG C, and the duration sets 120min；
Second stage temperature is set as 20 DEG C, and the duration sets 30min；
Phase III temperature is set as 35 DEG C, and the duration sets 60min；
Fourth stage temperature is set as 40 DEG C, and the duration sets 360min；
5th phase temperature is set as 35 DEG C, and the duration sets 120min；
6th phase temperature is set as 30 DEG C, and the duration sets 60min.
Compared with prior art, the beneficial effects of the present invention are:
1, the entire drying process of the present invention carries out at a lower temperature, and easy to operate, gnotobasis is convenient for control；
2, raw material is easy to generate denaturation or be decomposed in the case where the effect of water and heat changes in the present invention, can be removed by vacuum freeze drying
The moisture content of 95-99% in substance is removed, so that the micro- peptide freeze-drying wadding stability produced is good, is easy to long-term preservation effective component；
3, for the present invention using no corrosion-resistant system, irritation is small.
Specific embodiment
Below in conjunction with the embodiment of the present invention, technical scheme in the embodiment of the invention is clearly and completely described,
Obviously, described embodiments are only a part of the embodiments of the present invention, instead of all the embodiments.Based in the present invention
Embodiment, every other embodiment obtained by those of ordinary skill in the art without making creative efforts, all
Belong to the scope of protection of the invention.
Embodiment 1
In the embodiment of the present invention, the Essence containing micro- peptide components is poured into vial and is freeze-dried by a kind of micro- peptide freeze-drying wadding
It is made at after flocculent substance, wherein Essence includes following raw material by weight: 5 parts of micro- peptide mixer, aseptic deionized water
70 parts；Micro- peptide mixer is the mixing of oligopeptides -1, oligopeptides -2, oligopeptides -3, hexapeptide -11, glutamine and vitamin synthesis
Object.
Embodiment 2
In the embodiment of the present invention, the Essence containing micro- peptide components is poured into vial and is freeze-dried by a kind of micro- peptide freeze-drying wadding
It is made at after flocculent substance, wherein Essence includes following raw material by weight: 35 parts of micro- peptide mixer, aseptic deionized water
110 parts；Micro- peptide mixer is the mixing of oligopeptides -1, oligopeptides -2, oligopeptides -3, hexapeptide -11, glutamine and vitamin synthesis
Object.
Embodiment 3
In the embodiment of the present invention, the Essence containing micro- peptide components is poured into vial and is freeze-dried by a kind of micro- peptide freeze-drying wadding
It is made at after flocculent substance, wherein Essence includes following raw material by weight: 7 parts of micro- peptide mixer, aseptic deionized water
80 parts；Micro- peptide mixer is the mixing of oligopeptides -1, oligopeptides -2, oligopeptides -3, hexapeptide -11, glutamine and vitamin synthesis
Object.
Embodiment 4
In the embodiment of the present invention, the Essence containing micro- peptide components is poured into vial and is freeze-dried by a kind of micro- peptide freeze-drying wadding
It is made at after flocculent substance, wherein Essence includes following raw material by weight: 20 parts of micro- peptide mixer, aseptic deionized water
100 parts；Micro- peptide mixer is the mixing of oligopeptides -1, oligopeptides -2, oligopeptides -3, hexapeptide -11, glutamine and vitamin synthesis
Object.
Embodiment 5
In the embodiment of the present invention, the Essence containing micro- peptide components is poured into vial and is freeze-dried by a kind of micro- peptide freeze-drying wadding
It is made at after flocculent substance, wherein Essence includes following raw material by weight: 10 parts of micro- peptide mixer, aseptic deionized water
90 parts；Micro- peptide mixer is the mixing of oligopeptides -1, oligopeptides -2, oligopeptides -3, hexapeptide -11, glutamine and vitamin synthesis
Object.
A kind of preparation method of micro- peptide freeze-drying wadding, comprising the following steps:
1), cleaning and sterilizing container, pleura mold and blender；
2), aseptic deionized water is added in blender, is warming up to 45 DEG C, is then stirred the addition of micro- peptide mixer；
3), after stirring, stop blender, heat preservation stands 20-80min under 45 DEG C of environment, then defoams, and obtains clear
Clear transparent micro- peptide Essence；
4) micro- peptide Essence, is subjected to 35-45 DEG C of constant temperature processing, micro- peptide Essence 5ml is into vial ware；
5), the vial ware equipped with micro- peptide Essence is put into freeze drier, pre-freeze control temperature is set as -45 DEG C, holds
Continuous temperature control 160min；
6), freeze drier carries out seven primary drying stages and six parsing-desiccation stages to micro- peptide Essence；
7), freeze drier runs 36.3h, after carrying out freeze-drying molding to Essence, shuts down, and wadding is lyophilized in micro- peptide and is taken out,
Sealing packaging.
Wherein, it is 40-60min that the heat preservation in the step 3), which is stood,；The temperature that constant temperature is handled in the step 4) is 42
℃。
Seven primary drying stages that the freeze drier carries out micro- peptide Essence are as follows:
First stage temperature is set as -35 DEG C, and the duration sets 30min；
Second stage temperature is set as -25 DEG C, and the duration sets 30min；
Phase III temperature is set as -20 DEG C, and the duration sets 30min；
Fourth stage temperature is set as -15 DEG C, and the duration sets 30min；
5th phase temperature is set as -10 DEG C, and the duration sets 120min；
6th phase temperature is set as -5 DEG C, and the duration sets 30min；
7th phase temperature is set as 0 DEG C, and the duration sets 60min.
Six parsing-desiccation stages that the freeze drier carries out micro- peptide Essence are as follows:
First stage temperature is set as 10 DEG C, and the duration sets 120min；
Second stage temperature is set as 20 DEG C, and the duration sets 30min；
Phase III temperature is set as 35 DEG C, and the duration sets 60min；
Fourth stage temperature is set as 40 DEG C, and the duration sets 360min；
5th phase temperature is set as 35 DEG C, and the duration sets 120min；
6th phase temperature is set as 30 DEG C, and the duration sets 60min.
It is obvious to a person skilled in the art that invention is not limited to the details of the above exemplary embodiments, Er Qie
In the case where without departing substantially from spirit or essential attributes of the invention, the present invention can be realized in other specific forms.Therefore, no matter
From the point of view of which point, the present embodiments are to be considered as illustrative and not restrictive, and the scope of the present invention is by appended power
Benefit requires rather than above description limits, it is intended that all by what is fallen within the meaning and scope of the equivalent elements of the claims
Variation is included within the present invention.
In addition, it should be understood that although this specification is described in terms of embodiments, but not each embodiment is only wrapped
Containing an independent technical solution, this description of the specification is merely for the sake of clarity, and those skilled in the art should
It considers the specification as a whole, the technical solutions in the various embodiments may also be suitably combined, forms those skilled in the art
The other embodiments being understood that.
Claims (8)
1. a kind of micro- peptide freeze-drying wadding, which is characterized in that by the Essence containing micro- peptide components pour into vial freeze-drying at
It is made after flocculent substance, wherein Essence includes following raw material by weight: micro- peptide mixer 5-35 parts, aseptic deionized water
70-110 parts；Micro- peptide mixer is oligopeptides -1, oligopeptides -2, oligopeptides -3, hexapeptide -11, glutamine and vitamin synthesis
Mixture.
2. a kind of micro- peptide freeze-drying wadding according to claim 1, which is characterized in that micro- peptide freeze-drying wadding will contain micro- peptide
The Essence of ingredient pours into vial freeze-drying and is made at after flocculent substance, wherein Essence include it is following by weight
Raw material: micro- peptide mixer 7-20 parts, 80-100 parts of aseptic deionized water；Micro- peptide mixer is oligopeptides -1, oligopeptides -2, widow
The mixture that peptide -3, hexapeptide -11, glutamine and vitamin synthesize.
3. a kind of micro- peptide freeze-drying wadding according to claim 1, which is characterized in that micro- peptide freeze-drying wadding will contain micro- peptide
The Essence of ingredient pours into vial freeze-drying and is made at after flocculent substance, wherein Essence include it is following by weight
Raw material: 10 parts of micro- peptide mixer, 90 parts of aseptic deionized water；Micro- peptide mixer is oligopeptides -1, oligopeptides -2, oligopeptides -3, six
The mixture of peptide -11, glutamine and vitamin synthesis.
4. a kind of preparation method of micro- peptide freeze-drying wadding according to claim 1 to 3, which is characterized in that including following step
It is rapid:
1), cleaning and sterilizing container, pleura mold and blender；
2), aseptic deionized water is added in blender, is warming up to 45 DEG C, is then stirred the addition of micro- peptide mixer；
3), after stirring, stop blender, heat preservation stands 20-80min under 45 DEG C of environment, then defoams, and obtains clear
Clear transparent micro- peptide Essence；
4) micro- peptide Essence, is subjected to 35-45 DEG C of constant temperature processing, micro- peptide Essence 5ml is into vial ware；
5), the vial ware equipped with micro- peptide Essence is put into freeze drier, pre-freeze control temperature is set as -45 DEG C, holds
Continuous temperature control 160min；
6), freeze drier carries out seven primary drying stages and six parsing-desiccation stages to micro- peptide Essence；
7), freeze drier runs 36.3h, after carrying out freeze-drying molding to Essence, shuts down, and wadding is lyophilized in micro- peptide and is taken out,
Sealing packaging.
5. a kind of micro- peptide freeze-drying wadding according to claim 4 and preparation method thereof, which is characterized in that in the step 3)
It is 40-60min that heat preservation, which is stood,.
6. a kind of micro- peptide freeze-drying wadding according to claim 4 and preparation method thereof, which is characterized in that permanent in the step 4)
The temperature of temperature processing is 42 DEG C.
7. a kind of micro- peptide freeze-drying wadding according to claim 4 and preparation method thereof, which is characterized in that the freeze drier
Seven primary drying stages that micro- peptide Essence is carried out are as follows:
First stage temperature is set as -35 DEG C, and the duration sets 30min；
Second stage temperature is set as -25 DEG C, and the duration sets 30min；
Phase III temperature is set as -20 DEG C, and the duration sets 30min；
Fourth stage temperature is set as -15 DEG C, and the duration sets 30min；
5th phase temperature is set as -10 DEG C, and the duration sets 120min；
6th phase temperature is set as -5 DEG C, and the duration sets 30min；
7th phase temperature is set as 0 DEG C, and the duration sets 60min.
8. a kind of micro- peptide freeze-drying wadding according to claim 4 and preparation method thereof, which is characterized in that the freeze drier
Six parsing-desiccation stages that micro- peptide Essence is carried out are as follows:
First stage temperature is set as 10 DEG C, and the duration sets 120min；
Second stage temperature is set as 20 DEG C, and the duration sets 30min；
Phase III temperature is set as 35 DEG C, and the duration sets 60min；
Fourth stage temperature is set as 40 DEG C, and the duration sets 360min；
5th phase temperature is set as 35 DEG C, and the duration sets 120min；
6th phase temperature is set as 30 DEG C, and the duration sets 60min.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
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| CN201910110906.1A CN109620751A (en) | 2019-02-12 | 2019-02-12 | A kind of micro- peptide freeze-drying wadding and preparation method thereof |
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| Application Number | Priority Date | Filing Date | Title |
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| CN201910110906.1A CN109620751A (en) | 2019-02-12 | 2019-02-12 | A kind of micro- peptide freeze-drying wadding and preparation method thereof |
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| CN109620751A true CN109620751A (en) | 2019-04-16 |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN114983836A (en) * | 2022-06-15 | 2022-09-02 | 广州陶妆生物科技有限公司 | Repairing type freeze-dried wadding and preparation method thereof |
| CN115006280A (en) * | 2022-06-28 | 2022-09-06 | 广州暨创医美生物科技有限公司 | Collagen freeze-dried floc essence with flocculent structure and preparation method thereof |
-
2019
- 2019-02-12 CN CN201910110906.1A patent/CN109620751A/en not_active Withdrawn
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN114983836A (en) * | 2022-06-15 | 2022-09-02 | 广州陶妆生物科技有限公司 | Repairing type freeze-dried wadding and preparation method thereof |
| CN115006280A (en) * | 2022-06-28 | 2022-09-06 | 广州暨创医美生物科技有限公司 | Collagen freeze-dried floc essence with flocculent structure and preparation method thereof |
| CN115006280B (en) * | 2022-06-28 | 2023-12-19 | 广州暨创医美生物科技有限公司 | Collagen freeze-dried flocculation essence with flocculent structure and preparation method thereof |
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