CN106420368A - Preparation method of applying-type hydrogel-base facial mask - Google Patents
Preparation method of applying-type hydrogel-base facial mask Download PDFInfo
- Publication number
- CN106420368A CN106420368A CN201610939286.9A CN201610939286A CN106420368A CN 106420368 A CN106420368 A CN 106420368A CN 201610939286 A CN201610939286 A CN 201610939286A CN 106420368 A CN106420368 A CN 106420368A
- Authority
- CN
- China
- Prior art keywords
- facial mask
- pva
- preparation
- hydrogel
- solution
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
Classifications
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/02—Cosmetics or similar toiletry preparations characterised by special physical form
- A61K8/0212—Face masks
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/02—Cosmetics or similar toiletry preparations characterised by special physical form
- A61K8/04—Dispersions; Emulsions
- A61K8/042—Gels
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/81—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions involving only carbon-to-carbon unsaturated bonds
- A61K8/8129—Compositions of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by an alcohol, ether, aldehydo, ketonic, acetal or ketal radical; Compositions of hydrolysed polymers or esters of unsaturated alcohols with saturated carboxylic acids; Compositions of derivatives of such polymers, e.g. polyvinylmethylether
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
Landscapes
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Animal Behavior & Ethology (AREA)
- General Health & Medical Sciences (AREA)
- Public Health (AREA)
- Veterinary Medicine (AREA)
- Birds (AREA)
- Epidemiology (AREA)
- Chemical & Material Sciences (AREA)
- Dispersion Chemistry (AREA)
- Dermatology (AREA)
- Cosmetics (AREA)
Abstract
The invention discloses a preparation method of an applying-type hydrogel-base facial mask. The preparation method comprises the following steps: preparing a PVA (polyvinyl alcohol) water solution; adding corresponding skin care ingredients to the PVA solution which is uniformly stirred; and pouring a prepared mixed solution into a die, repeatedly conducting freeze-thawing, so that the hydrogel facial mask is prepared. The hydrogel facial mask prepared by the invention is high in moisture content, good in surface smooth elasticity and good in skin fitting property; and in addition, the preparation method of the hydrogel facial mask is simple, low in raw material cost and suitable for large-scale production.
Description
Technical field
The invention belongs to cosmetics exploitation preparation field, particularly to a kind of sticking type hydrogel substrate facial mask
Preparation method.
Background technology
Facial mask is that earliest beauty and make-up product, and face mask film is also the first step improved looks.With regard to face on market
The product of film makes the wide variety of facial mask because of the difference of facial mask interpolation composition, facial mask manufacture type and facial mask effect etc..Wherein
The manufacture type of facial mask is the significant consideration that consumer selects, and existing facial mask type mainly has paste mask, creams face
Film, jelly facial mask and SMD facial mask.Wherein paste mask, creams facial mask and jelly facial mask are that paste is applied directly to face
Portion, through after a period of time skin keratin being softened the absorption promoting skin to nutrient content and trace element, finally washes away face
Portion's paste composition.But the sealing of these cream packs is not it is impossible to fast lifting face temperature strengthens the suction of nutrient content ground
Receive and facial mask water loss quickly.Apply ointment or plaster chip facial mask because easy to use, face covers wide, and sealing preferably becomes facial mask
Developer researchs and develops the focus of new product.
Traditional sticking type facial mask adopts cotton paper or non-woven fabrics as the basilar memebrane absorbing beauty essence, and this facial mask is normal
It is commonly present the docile degree of facial mask not, the Essence of absorption is less, facial mask moisture evaporation is fast and the shortcomings of the waste of Essence.Water
The research and development of gel mask solve the shortcoming that traditional sticking type facial mask exists.Hydrogel is by polymer three-dimensional cross-linked network structure
The multicomponent system collectively constituting with filling solvent.Hydrogel have can absorb higher than after the moisture of sole mass hundreds of times keep
Gel state and be not dissolved in water, there is good water lock.In addition, can be good at after hydrogel water absorption and swelling simulating human body
Tissue, has certain flexibility and viscoplasticity, perfection can be attached to skin surface.Hydrogel be there are on market burn
Hinder dressing, the product such as percutaneous administration patch, and be applied to facial mask industry is not also a lot.
Polyvinyl alcohol (PVA) be by white obtained from Alcoholysis of Polyvinyl Acetate, hydrolysis or ammonolysis, powder or
Granular resin.It has the advantages that to synthesize convenience, safety and low toxicity, low price, is a kind of broad-spectrum water soluble polymer
Polymer.Any chemical reagent is not added with during plastic by the PVA hydrogel of physical crosslinking, remains material original
Biocompatibility.Meanwhile, PVA hydrogel moisture content is high, elastic good, excellent in mechanical performance, smooth surface.
With PVA for preparing hydrogel raw material, the Essence in traditional sticking type facial mask is prepared water-setting glue surface as solvent
Film, can prepare the hydrogel facial mask of corresponding function.Essence can all be received by this gel mask, it is to avoid Essence
Waste also avoid Essence to stick to your hands simultaneously.The water lock of gel is good, reduces the volatilization of the moisture in face mask film, perfect
Laminating degree softening skin cuticula lifted nutrient solution absorptivity.
Content of the invention
The technical problem to be solved is to provide a kind of preparation method of sticking type hydrogel substrate facial mask.
In order to solve the above problems, the invention provides a kind of preparation method of sticking type hydrogel substrate facial mask, it is special
Levy and be, comprise the following steps：
Step 1)：PVA powder is added in deionized water, stirs complete to PVA powder under the conditions of 95-100 DEG C of oil bath
CL, is subsequently cooled to room temperature.
Step 2)：Corresponding skin care ingredient is added according to product required function, after stirring, PVA mixed solution is toppled over
The mould entering then to will be equipped with PVA solution in facial mask mould is placed in ultra low temperature freezer freezing 8 hours, then is placed room temperature bar
Thaw under part；Freeze-thaw operation repeatedly can get smooth moistening PVA hydrogel facial mask.
Preferably, described step 1) mass percent of PVA is 2%-10% in the PVA solution that obtains.
Preferably, described step 2) in skin care ingredient adopt whitening class additive, anti-oxidant class additive or moisturizing class
Additive.
It is highly preferred that described whitening class additive be vitamin C and its derivative, ursin, Trenaxmine, niacinamide, really
The extract of plant sour or that there is whitening effect；Anti-oxidant class additive is lipoic acid, vitamin C, vitamin E, grape pip
Extract, glutathione GSH, lycopene or red clover；Moisturizing class additive is hyaluronic acid, glycerine, collagen, angle
MF59 or the sub- ester of snow.
Preferably, described step 2) in cryogenic temperature be set to -20 DEG C and less.
Preferably, described step 2) in freeze-thaw cycle-index be 2-4 time.
Good biocompatibility of the present invention, moisture content are high, viscoplasticity is good and smooth surface.In addition, this invention production process
Simply, reaction condition is gentle, the interpolation of unharmful substance and can be with mass production in course of reaction.
Compared with prior art, the beneficial effects of the present invention is：
(1) biocompatibility that the present invention has been had using raw material, reaction condition is gentle, is not added with any in course of reaction
Poisonous or sensitization organic solvent.
(2) present invention is simple to operate, and Setup Experiments are simple, suitable mass production.
(3) product of the present invention can reduce the waste of the skin care medicine of costliness, improves the utilization rate to nutrient solution for the user.Separately
Outer PVA hydrogel facial mask smooth surface, good with the laminating degree of skin, skin can be completely cut off and contact quick increase local skin with the external world
Temperature, be conducive to the expansion of skin pore to increase absorption to nutriment.
Brief description
Fig. 1 is the hydrogel facial mask of preparation in laboratory environment in embodiment 1.
Specific embodiment
For making the present invention become apparent, hereby with preferred embodiment, and accompanying drawing is coordinated to be described in detail below.
Embodiment 1
A kind of preparation method of sticking type hydrogel substrate facial mask：
(1) weigh 5g PVA powder and be added to that in 50ml deionized water, (in PVA solution, the mass percent of PVA is
10%), stir under the conditions of 95 DEG C of oil baths and be completely dissolved to PVA powder, be subsequently cooled to room temperature；
(2) PVA solution in step (1) is poured into then will be equipped with facial mask mould PVA solution mould be placed in-
80 DEG C of refrigerator freezings are after 8 hours, then placed defrosting under the conditions of room temperature；Freeze-thaw operates twice repeatedly, you can obtain table
Smooth moistening PVA hydrogel facial mask (as shown in Figure 1) in face.
Embodiment 2
A kind of preparation method of sticking type hydrogel substrate facial mask：
(1) weigh 2.5g PVA powder and be added to that in 50ml deionized water, (in PVA solution, the mass percent of PVA is
5%), stir under the conditions of 95 DEG C of oil baths and be completely dissolved to PVA powder, be subsequently cooled to room temperature；
(2) PVA solution in step (1) is poured into then will be equipped with facial mask mould PVA solution mould be placed in-
80 DEG C of refrigerator freezings are after 8 hours, then placed defrosting under the conditions of room temperature；Freeze-thaw operates three times repeatedly, you can obtain table
The smooth moistening PVA hydrogel facial mask in face.
Embodiment 3
A kind of preparation method of sticking type hydrogel substrate facial mask：
(1) weigh 1g PVA powder and be added in 50ml deionized water (in PVA solution, the mass percent of PVA is 2%),
Stir under the conditions of 95 DEG C of oil baths and be completely dissolved to PVA powder, be subsequently cooled to room temperature；
(2) PVA solution in step (1) is poured into then will be equipped with facial mask mould PVA solution mould be placed in-
80 DEG C of refrigerator freezings are after 8 hours, then placed defrosting under the conditions of room temperature；Freeze-thaw operates three times repeatedly, you can obtain table
The smooth moistening PVA hydrogel facial mask in face.
Claims (6)
1. a kind of preparation method of sticking type hydrogel substrate facial mask is it is characterised in that comprise the following steps：
Step 1)：PVA powder is added in deionized water, stirs completely molten to PVA powder under the conditions of 95-100 DEG C of oil bath
Solution, is subsequently cooled to room temperature.
Step 2)：Corresponding skin care ingredient is added according to product required function, after stirring, PVA mixed solution is poured into face
In film die, the mould that then will be equipped with PVA solution is placed in ultra low temperature freezer and freezes 8 hours, then under the conditions of being placed room temperature
Thaw；Freeze-thaw operation repeatedly can get smooth moistening PVA hydrogel facial mask.
2. the preparation method of hydrogel application formula facial mask as claimed in claim 1 is it is characterised in that described step 1) obtain
In PVA solution, the mass percent of PVA is 2%-10%.
3. the preparation method of hydrogel application formula facial mask as claimed in claim 1 is it is characterised in that described step 2) in shield
Skin composition adopts whitening class additive, anti-oxidant class additive or moisturizing class additive.
4. the preparation method of hydrogel application formula facial mask as claimed in claim 3 is it is characterised in that described whitening class additive
Extract for vitamin C and its derivative, ursin, Trenaxmine, niacinamide, tartaric acid or the plant with whitening effect；Anti-
Oxidation category additive is lipoic acid, vitamin C, vitamin E, grape seed extract, glutathione GSH, lycopene or redness
Clover；Moisturizing class additive is hyaluronic acid, glycerine, collagen, squalene or the sub- ester of snow.
5. the preparation method of hydrogel application formula facial mask as claimed in claim 1 is it is characterised in that described step 2) in freezing
Temperature is set to -20 DEG C and less.
6. the preparation method of hydrogel application formula facial mask as claimed in claim 1 is it is characterised in that described step 2) in cold
Jelly-thaw cycles number of times is 2-4 time.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610939286.9A CN106420368A (en) | 2016-11-01 | 2016-11-01 | Preparation method of applying-type hydrogel-base facial mask |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610939286.9A CN106420368A (en) | 2016-11-01 | 2016-11-01 | Preparation method of applying-type hydrogel-base facial mask |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN106420368A true CN106420368A (en) | 2017-02-22 |
Family
ID=58178872
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201610939286.9A Pending CN106420368A (en) | 2016-11-01 | 2016-11-01 | Preparation method of applying-type hydrogel-base facial mask |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN106420368A (en) |
Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107519030A (en) * | 2017-08-29 | 2017-12-29 | 苏州榭睿迦医疗科技发展有限公司 | A kind of skin-lightening cosmetic |
| CN110051691A (en) * | 2018-01-15 | 2019-07-26 | 张家港蓝智生物科技有限公司 | A kind of epoxy resin and cold compress patch having white-skinned face function |
| CN110167387A (en) * | 2017-09-25 | 2019-08-23 | 株式会社爱茉莉太平洋 | Utilize the beautifying skin film manufacturing device and its control method of hydrogel |
| CN110559275A (en) * | 2019-08-26 | 2019-12-13 | 西安博和医疗科技有限公司 | Application for skin anesthesia and preparation method thereof |
| WO2020218669A1 (en) * | 2019-04-25 | 2020-10-29 | 주식회사 씨앤피지 | Facial mask composition having improved moisturizing effect |
| WO2020218670A1 (en) * | 2019-04-25 | 2020-10-29 | 주식회사 씨앤피지 | Mask pack composition having improved wrinkle-reducing strength |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103054766A (en) * | 2011-10-21 | 2013-04-24 | 南通市通州区五接豆豆编织袋厂 | Strippable whitening and moisturizing mask |
| CN104257519A (en) * | 2014-10-10 | 2015-01-07 | 中国热带农业科学院农产品加工研究所 | Pineapple leaf nanocellulose moisturizing skin-whitening washing gel mask and preparation method thereof |
| CN104367533A (en) * | 2013-08-14 | 2015-02-25 | 金周垣 | Cream coated hydrogel mask |
| CN105726354A (en) * | 2016-02-22 | 2016-07-06 | 陕西科技大学 | Hydrogel mask matrix and preparing method thereof |
-
2016
- 2016-11-01 CN CN201610939286.9A patent/CN106420368A/en active Pending
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103054766A (en) * | 2011-10-21 | 2013-04-24 | 南通市通州区五接豆豆编织袋厂 | Strippable whitening and moisturizing mask |
| CN104367533A (en) * | 2013-08-14 | 2015-02-25 | 金周垣 | Cream coated hydrogel mask |
| CN104257519A (en) * | 2014-10-10 | 2015-01-07 | 中国热带农业科学院农产品加工研究所 | Pineapple leaf nanocellulose moisturizing skin-whitening washing gel mask and preparation method thereof |
| CN105726354A (en) * | 2016-02-22 | 2016-07-06 | 陕西科技大学 | Hydrogel mask matrix and preparing method thereof |
Cited By (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107519030A (en) * | 2017-08-29 | 2017-12-29 | 苏州榭睿迦医疗科技发展有限公司 | A kind of skin-lightening cosmetic |
| CN110167387A (en) * | 2017-09-25 | 2019-08-23 | 株式会社爱茉莉太平洋 | Utilize the beautifying skin film manufacturing device and its control method of hydrogel |
| CN110167387B (en) * | 2017-09-25 | 2022-05-03 | 株式会社爱茉莉太平洋 | Apparatus for manufacturing skin beauty mask using hydrogel and method for controlling the same |
| CN110051691A (en) * | 2018-01-15 | 2019-07-26 | 张家港蓝智生物科技有限公司 | A kind of epoxy resin and cold compress patch having white-skinned face function |
| WO2020218669A1 (en) * | 2019-04-25 | 2020-10-29 | 주식회사 씨앤피지 | Facial mask composition having improved moisturizing effect |
| WO2020218670A1 (en) * | 2019-04-25 | 2020-10-29 | 주식회사 씨앤피지 | Mask pack composition having improved wrinkle-reducing strength |
| CN110559275A (en) * | 2019-08-26 | 2019-12-13 | 西安博和医疗科技有限公司 | Application for skin anesthesia and preparation method thereof |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN106420368A (en) | Preparation method of applying-type hydrogel-base facial mask | |
| JP4959328B2 (en) | Temperature-sensitive state change hydrogel composition and method for producing the same | |
| CN102138870B (en) | Collagen facial mask and preparation method thereof | |
| KR101774342B1 (en) | Hydrogel maskpack composition, Hydrogel maskpack and the preparing method thereof | |
| WO2010143196A1 (en) | Novel synergistic transparent / translucent hydrogel composition; method of preparing it and a sheet / film made thereform | |
| CN103385820B (en) | Repair eye cream | |
| CN101513383A (en) | Face pack and preparation method thereof | |
| CN102920615A (en) | Gum composition for external use on skin | |
| KR20140040338A (en) | Maskpack compounds containing camucamu powder and making process of maskpack | |
| CN102988199B (en) | Skin-tendering and anti-allergic essence | |
| CN106074217B (en) | Body temperature is moulded into type skin caring material and skin nursing film and preparation method certainly | |
| CN101322677B (en) | Complexes of hydrolytic collagen protein and avenin and uses thereof | |
| CN103976887A (en) | Gel facial mask base material and preparation process thereof | |
| CN105193685A (en) | Traditional Chinese foot caring solution, preparation method of traditional Chinese foot caring solution and traditional Chinese foot caring mask | |
| CN106309332A (en) | Making process of edible honey lip-moistening lipstick | |
| CN104306165A (en) | Orange oil microcapsule as well as preparation method and application thereof | |
| CN103735426A (en) | Method for preparing gypsum facial mask | |
| WO2009124763A2 (en) | Dermal patch | |
| KR100851316B1 (en) | Gel type sheet for mask pack and menufacturing method thereof | |
| CN105617455A (en) | Preparation method of Chinese herbal woundplast ointment | |
| CN104306397A (en) | Antibacterial external use ointment and manufacturing method thereof | |
| CN106362203A (en) | Manufacturing method of smearing type band-aid | |
| CN206454028U (en) | Body temperature is moulded into type skin nursing film certainly | |
| CN108186444A (en) | A kind of tea oil mud cold cream and preparation method thereof | |
| CN108992387A (en) | White anti-acne MASQUE APAISANT HYDRATANT of Chinese medicine three and preparation method thereof |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| RJ01 | Rejection of invention patent application after publication |
Application publication date: 20170222 |
|
| RJ01 | Rejection of invention patent application after publication |